DE1267772B - Verfahren zum Anfahren der hydrierenden Spaltung von Kohlenwasserstoffdestillaten - Google Patents
Verfahren zum Anfahren der hydrierenden Spaltung von KohlenwasserstoffdestillatenInfo
- Publication number
- DE1267772B DE1267772B DEP1267A DE1267772A DE1267772B DE 1267772 B DE1267772 B DE 1267772B DE P1267 A DEP1267 A DE P1267A DE 1267772 A DE1267772 A DE 1267772A DE 1267772 B DE1267772 B DE 1267772B
- Authority
- DE
- Germany
- Prior art keywords
- catalyst
- sulfur
- conversion
- percent
- hydrogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 60
- 229930195733 hydrocarbon Natural products 0.000 title claims description 26
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 25
- 238000003776 cleavage reaction Methods 0.000 title claims description 22
- 230000007017 scission Effects 0.000 title claims description 22
- 239000004215 Carbon black (E152) Substances 0.000 title claims description 20
- 230000008569 process Effects 0.000 title description 36
- 239000003054 catalyst Substances 0.000 claims description 106
- 229910052717 sulfur Inorganic materials 0.000 claims description 73
- 239000011593 sulfur Substances 0.000 claims description 73
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 70
- 238000006243 chemical reaction Methods 0.000 claims description 54
- 229910052739 hydrogen Inorganic materials 0.000 claims description 42
- 239000001257 hydrogen Substances 0.000 claims description 42
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 38
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 34
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 24
- 239000007788 liquid Substances 0.000 claims description 21
- 229910052759 nickel Inorganic materials 0.000 claims description 19
- 229910052736 halogen Inorganic materials 0.000 claims description 17
- 150000002367 halogens Chemical class 0.000 claims description 16
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 16
- 229910052721 tungsten Inorganic materials 0.000 claims description 15
- 239000010937 tungsten Substances 0.000 claims description 15
- 230000000694 effects Effects 0.000 claims description 14
- 229910052757 nitrogen Inorganic materials 0.000 claims description 13
- 238000009835 boiling Methods 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 7
- 229910017464 nitrogen compound Inorganic materials 0.000 claims description 6
- 150000002830 nitrogen compounds Chemical class 0.000 claims description 6
- -1 nitrogen containing hydrocarbon Chemical class 0.000 claims description 5
- 235000012239 silicon dioxide Nutrition 0.000 claims description 5
- 238000005336 cracking Methods 0.000 claims description 4
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 4
- 239000007858 starting material Substances 0.000 description 41
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 16
- 239000007789 gas Substances 0.000 description 13
- 230000003197 catalytic effect Effects 0.000 description 12
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 10
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 9
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- 229910021529 ammonia Inorganic materials 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 8
- 229910052731 fluorine Inorganic materials 0.000 description 8
- 239000011737 fluorine Substances 0.000 description 8
- 150000002431 hydrogen Chemical class 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- WQOXQRCZOLPYPM-UHFFFAOYSA-N dimethyl disulfide Chemical compound CSSC WQOXQRCZOLPYPM-UHFFFAOYSA-N 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 238000005984 hydrogenation reaction Methods 0.000 description 6
- 239000003921 oil Substances 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 238000005486 sulfidation Methods 0.000 description 6
- 150000003464 sulfur compounds Chemical class 0.000 description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
- 125000004429 atom Chemical group 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 231100000572 poisoning Toxicity 0.000 description 4
- 230000000607 poisoning effect Effects 0.000 description 4
- 229920006395 saturated elastomer Polymers 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 239000000969 carrier Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000000295 fuel oil Substances 0.000 description 3
- 239000003502 gasoline Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- MMZYCBHLNZVROM-UHFFFAOYSA-N 1-fluoro-2-methylbenzene Chemical compound CC1=CC=CC=C1F MMZYCBHLNZVROM-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 2
- 229910017855 NH 4 F Inorganic materials 0.000 description 2
- YTPLMLYBLZKORZ-UHFFFAOYSA-N Thiophene Chemical compound C=1C=CSC=1 YTPLMLYBLZKORZ-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 150000002366 halogen compounds Chemical class 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 150000004763 sulfides Chemical class 0.000 description 2
- 150000003463 sulfur Chemical class 0.000 description 2
- WMXCDAVJEZZYLT-UHFFFAOYSA-N tert-butylthiol Chemical compound CC(C)(C)S WMXCDAVJEZZYLT-UHFFFAOYSA-N 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- LOGFBMFZABHYBI-UHFFFAOYSA-N C(C)(C)(C)[W] Chemical compound C(C)(C)(C)[W] LOGFBMFZABHYBI-UHFFFAOYSA-N 0.000 description 1
- 241000282461 Canis lupus Species 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- AQGDXJQRVOCUQX-UHFFFAOYSA-N N.[S] Chemical compound N.[S] AQGDXJQRVOCUQX-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Inorganic materials 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000004517 catalytic hydrocracking Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000003413 degradative effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000006477 desulfuration reaction Methods 0.000 description 1
- 230000023556 desulfurization Effects 0.000 description 1
- 230000004992 fission Effects 0.000 description 1
- 125000005843 halogen group Chemical group 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000011005 laboratory method Methods 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- YQCIWBXEVYWRCW-UHFFFAOYSA-N methane;sulfane Chemical compound C.S YQCIWBXEVYWRCW-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002829 nitrogen Chemical class 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 125000000446 sulfanediyl group Chemical group *S* 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 229930192474 thiophene Natural products 0.000 description 1
- ZCUFMDLYAMJYST-UHFFFAOYSA-N thorium dioxide Chemical compound O=[Th]=O ZCUFMDLYAMJYST-UHFFFAOYSA-N 0.000 description 1
- 229910003452 thorium oxide Inorganic materials 0.000 description 1
- PBYZMCDFOULPGH-UHFFFAOYSA-N tungstate Chemical compound [O-][W]([O-])(=O)=O PBYZMCDFOULPGH-UHFFFAOYSA-N 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
- C10G49/24—Starting-up hydrotreatment operations
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US226090A US3213012A (en) | 1962-09-25 | 1962-09-25 | Starting up procedure in the hydrocaracking of hydrocarbons |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1267772B true DE1267772B (de) | 1968-05-09 |
Family
ID=22847511
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEP1267A Pending DE1267772B (de) | 1962-09-25 | 1963-09-25 | Verfahren zum Anfahren der hydrierenden Spaltung von Kohlenwasserstoffdestillaten |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3213012A (enrdf_load_stackoverflow) |
| DE (1) | DE1267772B (enrdf_load_stackoverflow) |
| FR (1) | FR1374581A (enrdf_load_stackoverflow) |
| GB (1) | GB1050968A (enrdf_load_stackoverflow) |
| NL (2) | NL129111C (enrdf_load_stackoverflow) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1044061A (en) * | 1963-06-07 | 1966-09-28 | British Petroleum Co | Improvements relating to the hydrocatalytic treatment of hydrocarbons |
| US3305477A (en) * | 1964-07-17 | 1967-02-21 | Texaco Inc | Hydrocracking nitrogen-containing feed in the presence of halides |
| US3316169A (en) * | 1964-10-16 | 1967-04-25 | Texaco Inc | Catalytic hydrocracking of hydrocarbons with the use of halogen and sulfur activators |
| US3294674A (en) * | 1964-12-28 | 1966-12-27 | Gulf Research Development Co | Hydrocracking of hydrocarbons with a sulfided tungsten oxide catalyst on a silica-alumina cracking support |
| US3395095A (en) * | 1965-07-01 | 1968-07-30 | Texaco Inc | Hydrocracking of hydrocarbons with the constant addition of sulfur to the reaction zone |
| US3349025A (en) * | 1965-07-15 | 1967-10-24 | Gulf Research Development Co | Hydrocracking with a presulfided tungsten oxide composite catalyst from the group comprising of silver, zinc or thorium on a siliceous carrier |
| US3354076A (en) * | 1965-10-22 | 1967-11-21 | Gulf Research Development Co | Process for the hydrocracking of hydrocarbon oils under reaction conditions so as toretain substantial amounts of aromatics in the naphtha product |
| US3347780A (en) * | 1966-02-04 | 1967-10-17 | Chevron Res | Naphtha hydroconversion to produce lower boiling hydrocarbon products |
| US3336216A (en) * | 1966-03-18 | 1967-08-15 | Chevron Res | Catalytic hydrocracking process with a silica-magnesia cracking base promoted with nickel and tungsten |
| US3505205A (en) * | 1968-04-23 | 1970-04-07 | Gulf Research Development Co | Production of lpg by low temperature hydrocracking |
| US3673108A (en) * | 1969-12-31 | 1972-06-27 | Shell Oil Co | Hydrocracking catalyst activation treatment |
| US3852372A (en) * | 1970-06-25 | 1974-12-03 | Texaco Inc | Isomerization with fluorided composite alumina catalysts |
| US3965253A (en) * | 1972-05-01 | 1976-06-22 | Shell Oil Company | Process for producing hydrogen |
| US3963601A (en) * | 1973-08-20 | 1976-06-15 | Universal Oil Products Company | Hydrocracking of hydrocarbons with a catalyst comprising an alumina-silica support, a group VIII metallic component, a group VI-B metallic component and a fluoride |
| US4040979A (en) * | 1976-02-23 | 1977-08-09 | Uop Inc. | Hydrocarbon conversion catalytic composite |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1109859A (fr) * | 1954-07-30 | 1956-02-02 | Gulf Research Development Co | Procédé d'hydrogénation destructive de mélanges d'hydrocarbures contenant des éléments difficilement vaporisables |
| FR1287661A (fr) * | 1960-03-16 | 1962-03-16 | Universal Oil Prod Co | Procédé pour l'hydrocraquage des huiles hydrocarbonées |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2934492A (en) * | 1956-12-03 | 1960-04-26 | Exxon Research Engineering Co | Hydrogenation of heavy oils |
| US2944005A (en) * | 1958-08-13 | 1960-07-05 | California Research Corp | Catalytic conversion of hydrocarbon distillates |
| US3099617A (en) * | 1960-08-04 | 1963-07-30 | Union Oil Co | Pretreatment of catalyst employed in the hydrocracking of hydrocarbons |
-
0
- GB GB1050968D patent/GB1050968A/en not_active Expired
- NL NL298382D patent/NL298382A/xx unknown
-
1962
- 1962-09-25 US US226090A patent/US3213012A/en not_active Expired - Lifetime
-
1963
- 1963-09-20 FR FR948103A patent/FR1374581A/fr not_active Expired
- 1963-09-25 NL NL129111D patent/NL129111C/xx active
- 1963-09-25 DE DEP1267A patent/DE1267772B/de active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1109859A (fr) * | 1954-07-30 | 1956-02-02 | Gulf Research Development Co | Procédé d'hydrogénation destructive de mélanges d'hydrocarbures contenant des éléments difficilement vaporisables |
| FR1287661A (fr) * | 1960-03-16 | 1962-03-16 | Universal Oil Prod Co | Procédé pour l'hydrocraquage des huiles hydrocarbonées |
Also Published As
| Publication number | Publication date |
|---|---|
| NL129111C (enrdf_load_stackoverflow) | 1965-11-25 |
| GB1050968A (enrdf_load_stackoverflow) | 1900-01-01 |
| FR1374581A (fr) | 1964-10-09 |
| NL298382A (enrdf_load_stackoverflow) | |
| US3213012A (en) | 1965-10-19 |
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