DE1259888B - Verfahren zur Herstellung von Organosiliciumverbindungen - Google Patents
Verfahren zur Herstellung von OrganosiliciumverbindungenInfo
- Publication number
- DE1259888B DE1259888B DEF52522A DEF0052522A DE1259888B DE 1259888 B DE1259888 B DE 1259888B DE F52522 A DEF52522 A DE F52522A DE F0052522 A DEF0052522 A DE F0052522A DE 1259888 B DE1259888 B DE 1259888B
- Authority
- DE
- Germany
- Prior art keywords
- reaction
- compounds
- organosilicon compounds
- preparation
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 7
- 150000003961 organosilicon compounds Chemical class 0.000 title claims description 5
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 18
- 239000003054 catalyst Substances 0.000 claims description 11
- -1 hydrogen silanes Chemical class 0.000 claims description 11
- 229910052697 platinum Inorganic materials 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 6
- 229910052739 hydrogen Inorganic materials 0.000 claims description 6
- 239000001257 hydrogen Substances 0.000 claims description 6
- 150000002894 organic compounds Chemical class 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 description 14
- 229920001296 polysiloxane Polymers 0.000 description 6
- 238000007259 addition reaction Methods 0.000 description 5
- STMDPCBYJCIZOD-UHFFFAOYSA-N 2-(2,4-dinitroanilino)-4-methylpentanoic acid Chemical compound CC(C)CC(C(O)=O)NC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O STMDPCBYJCIZOD-UHFFFAOYSA-N 0.000 description 4
- 125000004429 atom Chemical group 0.000 description 4
- 238000004132 cross linking Methods 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 229910018557 Si O Inorganic materials 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 2
- FDMFUZHCIRHGRG-UHFFFAOYSA-N 3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C=C FDMFUZHCIRHGRG-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 150000001722 carbon compounds Chemical class 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- VXWPONVCMVLXBW-UHFFFAOYSA-M magnesium;carbanide;iodide Chemical compound [CH3-].[Mg+2].[I-] VXWPONVCMVLXBW-UHFFFAOYSA-M 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 150000003377 silicon compounds Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
- C07F15/0006—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table compounds of the platinum group
- C07F15/0086—Platinum compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/18—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
- B01J31/1805—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing nitrogen
- B01J31/181—Cyclic ligands, including e.g. non-condensed polycyclic ligands, comprising at least one complexing nitrogen atom as ring member, e.g. pyridine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/0834—Compounds having one or more O-Si linkage
- C07F7/0838—Compounds with one or more Si-O-Si sequences
- C07F7/0872—Preparation and treatment thereof
- C07F7/0876—Reactions involving the formation of bonds to a Si atom of a Si-O-Si sequence other than a bond of the Si-O-Si linkage
- C07F7/0878—Si-C bond
- C07F7/0879—Hydrosilylation reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1876—Preparation; Treatments not provided for in C07F7/20 by reactions involving the formation of Si-C linkages
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
- B01J2231/32—Addition reactions to C=C or C-C triple bonds
- B01J2231/323—Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
- B01J2531/80—Complexes comprising metals of Group VIII as the central metal
- B01J2531/82—Metals of the platinum group
- B01J2531/828—Platinum
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF52522A DE1259888B (de) | 1967-05-27 | 1967-05-27 | Verfahren zur Herstellung von Organosiliciumverbindungen |
| FR1586857D FR1586857A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-05-27 | 1968-05-22 | |
| US731648A US3567755A (en) | 1967-05-27 | 1968-05-23 | Production of organo-silicon compounds |
| GB24919/68A GB1170888A (en) | 1967-05-27 | 1968-05-24 | Production of Organo-Silicon Compounds |
| BE715646D BE715646A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1967-05-27 | 1968-05-24 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF52522A DE1259888B (de) | 1967-05-27 | 1967-05-27 | Verfahren zur Herstellung von Organosiliciumverbindungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1259888B true DE1259888B (de) | 1968-02-01 |
Family
ID=7105515
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF52522A Pending DE1259888B (de) | 1967-05-27 | 1967-05-27 | Verfahren zur Herstellung von Organosiliciumverbindungen |
Country Status (5)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2159991A1 (de) * | 1971-12-03 | 1973-06-14 | Dynamit Nobel Ag | Siliciumhaltige dioxolanderivate und ihre verwendung zur herstellung von epoxygruppen enthaltenden organosilanestern |
| FR2419296A1 (fr) * | 1978-03-08 | 1979-10-05 | Consortium Elektrochem Ind | Procede pour fixer sur une liaison multiple aliphatique de l'hydrogene lie a du silicium |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4417069A (en) * | 1983-02-22 | 1983-11-22 | General Electric Company | Method of preparing β-phenylethylchlorosilanes |
| US4530879A (en) * | 1983-03-04 | 1985-07-23 | Minnesota Mining And Manufacturing Company | Radiation activated addition reaction |
| US4600484A (en) * | 1983-12-06 | 1986-07-15 | Minnesota Mining And Manufacturing Company | Hydrosilation process using a (η5 -cyclopentadienyl)tri(σ-aliphatic) platinum complex as the catalyst |
| US4510094A (en) * | 1983-12-06 | 1985-04-09 | Minnesota Mining And Manufacturing Company | Platinum complex |
| JPH0747595B2 (ja) * | 1986-10-30 | 1995-05-24 | 東レ・ダウコ−ニング・シリコ−ン株式会社 | エポキシ基含有ジシラザンおよびその製造方法 |
| US5145886A (en) * | 1988-05-19 | 1992-09-08 | Minnesota Mining And Manufacturing Company | Radiation activated hydrosilation reaction |
| DE3828926A1 (de) * | 1988-08-26 | 1990-03-01 | Hoechst Ag | Verfahren zur herstellung von (aryl)-(dimethyl)-(3-arylpropyl)-silanen |
| US4916169A (en) * | 1988-09-09 | 1990-04-10 | Minnesota Mining And Manufacturing Company | Visible radiation activated hydrosilation reaction |
| US4898961A (en) * | 1989-07-17 | 1990-02-06 | Dow Corning Corporation | Method for preparing alkenylsilanes |
| US6046250A (en) * | 1990-12-13 | 2000-04-04 | 3M Innovative Properties Company | Hydrosilation reaction utilizing a free radical photoinitiator |
| US6376569B1 (en) * | 1990-12-13 | 2002-04-23 | 3M Innovative Properties Company | Hydrosilation reaction utilizing a (cyclopentadiene)(sigma-aliphatic) platinum complex and a free radical photoinitiator |
| JP2005150235A (ja) | 2003-11-12 | 2005-06-09 | Three M Innovative Properties Co | 半導体表面保護シート及び方法 |
| US20080014532A1 (en) * | 2006-07-14 | 2008-01-17 | 3M Innovative Properties Company | Laminate body, and method for manufacturing thin substrate using the laminate body |
| US20090017248A1 (en) * | 2007-07-13 | 2009-01-15 | 3M Innovative Properties Company | Layered body and method for manufacturing thin substrate using the layered body |
| US20090017323A1 (en) * | 2007-07-13 | 2009-01-15 | 3M Innovative Properties Company | Layered body and method for manufacturing thin substrate using the layered body |
| US7891636B2 (en) * | 2007-08-27 | 2011-02-22 | 3M Innovative Properties Company | Silicone mold and use thereof |
| JP5551602B2 (ja) * | 2007-11-01 | 2014-07-16 | スリーエム イノベイティブ プロパティズ カンパニー | マスター型複製方法 |
| JP2010062269A (ja) * | 2008-09-02 | 2010-03-18 | Three M Innovative Properties Co | ウェーハ積層体の製造方法、ウェーハ積層体製造装置、ウェーハ積層体、支持層剥離方法、及びウェーハの製造方法 |
| EP2500009A1 (en) | 2011-03-17 | 2012-09-19 | 3M Innovative Properties Company | Dental ceramic article, process of production and use thereof |
| US9102845B2 (en) | 2012-07-19 | 2015-08-11 | 3M Innovative Properties Company | Functionalized isobutylene-isoprene copolymer composition |
| US9994740B2 (en) | 2013-05-31 | 2018-06-12 | 3M Innovative Properties Company | Fluoroalkyl silicones |
| WO2015050928A1 (en) | 2013-10-04 | 2015-04-09 | 3M Innovative Properties Company | Fluoroalkyl silicone compositions |
| CN105612165B (zh) | 2013-10-04 | 2018-05-25 | 3M创新有限公司 | 氟代烷基硅烷及其涂层 |
| KR20160140811A (ko) | 2014-03-31 | 2016-12-07 | 쓰리엠 이노베이티브 프로퍼티즈 캄파니 | 플루오로알킬 실리콘 |
| WO2016032794A1 (en) | 2014-08-27 | 2016-03-03 | 3M Innovative Properties Company | Novel polyfluoroalkylated alkenes and silicone compounds prepared therefrom |
| US9975834B2 (en) | 2014-08-27 | 2018-05-22 | 3M Innovative Properties Company | Polyfluoroalkylated alkenes and silicon compounds prepared therefrom |
| US9938307B2 (en) | 2014-08-27 | 2018-04-10 | 3M Innovative Properties Company | Polyfluoroalkylated alkenes and silane compounds prepared therefrom |
| US20240294815A1 (en) | 2021-08-02 | 2024-09-05 | 3M Innovative Properties Company | Hydrosilylation based beta-diketone primers for adhesion to metal |
-
1967
- 1967-05-27 DE DEF52522A patent/DE1259888B/de active Pending
-
1968
- 1968-05-22 FR FR1586857D patent/FR1586857A/fr not_active Expired
- 1968-05-23 US US731648A patent/US3567755A/en not_active Expired - Lifetime
- 1968-05-24 GB GB24919/68A patent/GB1170888A/en not_active Expired
- 1968-05-24 BE BE715646D patent/BE715646A/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2159991A1 (de) * | 1971-12-03 | 1973-06-14 | Dynamit Nobel Ag | Siliciumhaltige dioxolanderivate und ihre verwendung zur herstellung von epoxygruppen enthaltenden organosilanestern |
| FR2419296A1 (fr) * | 1978-03-08 | 1979-10-05 | Consortium Elektrochem Ind | Procede pour fixer sur une liaison multiple aliphatique de l'hydrogene lie a du silicium |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1586857A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1970-03-06 |
| US3567755A (en) | 1971-03-02 |
| BE715646A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1968-10-16 |
| GB1170888A (en) | 1969-11-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE1259888B (de) | Verfahren zur Herstellung von Organosiliciumverbindungen | |
| DE69218115T2 (de) | Organopolysiloxane und Verfahren zur Herstellung | |
| DE2646726C2 (de) | Die Anlagerung verzögerndes Mittel bei der durch Platinkatalysator geförderten und bei Raumtemperatur erfolgenden Anlagerung von Si-gebundenem Wasserstoff an mindestens 50 Si-Atome je Molekul und aliphatische Mehrfachbindungen enthaltendes Organopolysiloxan | |
| DE60114177T2 (de) | Verfahren zur kondensation von verbindungen, die siliciumgebundene hydroxyl-oder alkoxygruppen enthalten | |
| DE69032905T2 (de) | Platinkatalysator, Verfahren für seine Herstellung und härtbare Siloxanzusammensetzungen, die diesen Katalysator enthalten | |
| DE1262271B (de) | Verfahren zur Herstellung von Organosiliciumverbindungen | |
| DE1214234B (de) | Verfahren zur Herstellung von neuen Organosiliciumverbindungen mit Oximgruppen enthaltenden Resten | |
| EP0075703A1 (de) | Verfahren zur Addition von organischen Siliciumverbindungen mit SiH-Gruppen an Verbindungen mit olefinischen Doppelbindungen | |
| DE1495918A1 (de) | Verfahren zur Herstellung von Organ?siliciumverbindungen mit organischem Rhodiumkomplex als Katalysator | |
| EP2250214B1 (de) | Verfahren zur herstellung von siliconpolyethern | |
| DE1570446C3 (de) | Verfahren zur Herstellung von Organosiloxanblockmisch polymeren | |
| EP0170287B1 (de) | Verfahren zum Stabilisieren von Organopolysiloxan | |
| DE69722096T2 (de) | Alkylsubstituierte Siloxane und alkylsubstituierte Polyetherflüssigkeiten | |
| DE2500930A1 (de) | Kontinuierliches verfahren fuer die herstellung von polysiloxanoelen | |
| DE69721762T2 (de) | Verfahren zur herstellung von siliconölen durch hydrosilylierung von polyorganohydrogensiloxanen und sauerstoff- enthaltenden cylischen verbindungen in anwesenheit eines heterogenes katalysator | |
| EP1940852B1 (de) | Verfahren zur hydrosilylierung | |
| DE2251297C3 (de) | Verfahren zur Herstellung von Organosiliciumverbindungen | |
| DE1768785B2 (de) | Verfahren zur Herstellung von Organosiliciumverbindungen | |
| DE1935167A1 (de) | Amino-alkoxy-alkenyl-polysiloxane | |
| EP0117503B1 (de) | Verfahren zum Stabilisieren von Organopolysiloxanen | |
| DE2724822A1 (de) | Verfahren zum anlagern von si-gebundenem wasserstoff an aliphatische mehrfachbindung | |
| DE2133105B2 (de) | Verfahren zur Herstellung härtbarer Fluororganopolysiloxanharze | |
| DE1618836A1 (de) | Verfahren zur Herstellung von Organotrisiloxanen | |
| EP0193748A1 (de) | Verfahren zur Erhöhung des Molekulargewichts von Diorgano(poly)siloxan | |
| DE1125180B (de) | Verfahren zur Hydrolyse von Chlorsilanen mit unmittelbar an Silicium gebundenem Wasserstoff bzw. organofunktionellen Gruppen |