DE1133726B - Verfahren zur Herstellung neuer Perhydrate von Acylierungsprodukten der phosphorigen Saeure - Google Patents
Verfahren zur Herstellung neuer Perhydrate von Acylierungsprodukten der phosphorigen SaeureInfo
- Publication number
- DE1133726B DE1133726B DEH38977A DEH0038977A DE1133726B DE 1133726 B DE1133726 B DE 1133726B DE H38977 A DEH38977 A DE H38977A DE H0038977 A DEH0038977 A DE H0038977A DE 1133726 B DE1133726 B DE 1133726B
- Authority
- DE
- Germany
- Prior art keywords
- phosphorous acid
- alkali
- perhydrates
- acylation products
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 title claims description 23
- 230000010933 acylation Effects 0.000 title claims description 18
- 238000005917 acylation reaction Methods 0.000 title claims description 18
- 238000000034 method Methods 0.000 title claims description 15
- 238000002360 preparation method Methods 0.000 title description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 16
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims description 14
- 229910052698 phosphorus Inorganic materials 0.000 claims description 14
- 239000011574 phosphorus Substances 0.000 claims description 14
- 150000001447 alkali salts Chemical class 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 3
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical class OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 claims description 2
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 claims 1
- 239000000047 product Substances 0.000 description 21
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 19
- 229910052760 oxygen Inorganic materials 0.000 description 19
- 239000001301 oxygen Substances 0.000 description 19
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 125000004429 atom Chemical group 0.000 description 11
- 239000007787 solid Substances 0.000 description 9
- 239000007795 chemical reaction product Substances 0.000 description 8
- 239000000243 solution Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 4
- 235000011121 sodium hydroxide Nutrition 0.000 description 4
- 159000000000 sodium salts Chemical class 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
- QRSFFHRCBYCWBS-UHFFFAOYSA-N [O].[O] Chemical group [O].[O] QRSFFHRCBYCWBS-UHFFFAOYSA-N 0.000 description 2
- WETWJCDKMRHUPV-UHFFFAOYSA-N acetyl chloride Chemical compound CC(Cl)=O WETWJCDKMRHUPV-UHFFFAOYSA-N 0.000 description 2
- 239000012346 acetyl chloride Substances 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000007717 exclusion Effects 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- WYVAMUWZEOHJOQ-UHFFFAOYSA-N propionic anhydride Chemical compound CCC(=O)OC(=O)CC WYVAMUWZEOHJOQ-UHFFFAOYSA-N 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 241001016380 Reseda luteola Species 0.000 description 1
- ISMSDURUTAMCEA-UHFFFAOYSA-N [N].OP(O)(O)=O Chemical class [N].OP(O)(O)=O ISMSDURUTAMCEA-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- -1 nitrogen phosphoric acid compound Chemical class 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- SXYFKXOFMCIXQW-UHFFFAOYSA-N propanedioyl dichloride Chemical compound ClC(=O)CC(Cl)=O SXYFKXOFMCIXQW-UHFFFAOYSA-N 0.000 description 1
- RZWZRACFZGVKFM-UHFFFAOYSA-N propanoyl chloride Chemical compound CCC(Cl)=O RZWZRACFZGVKFM-UHFFFAOYSA-N 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/16—Peroxyhydrates; Peroxyacids or salts thereof containing phosphorus
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3839—Polyphosphonic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
- C07F9/3839—Polyphosphonic acids
- C07F9/386—Polyphosphonic acids containing hydroxy substituents in the hydrocarbon radicals
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3945—Organic per-compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L4/00—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
- D06L4/10—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
- D06L4/15—Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using organic agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Biochemistry (AREA)
- Molecular Biology (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Textile Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL257200D NL257200A (US20030220297A1-20031127-C00009.png) | 1960-03-22 | ||
| NL126199D NL126199C (US20030220297A1-20031127-C00009.png) | 1960-03-22 | ||
| DEH38977A DE1133726B (de) | 1960-03-22 | 1960-03-22 | Verfahren zur Herstellung neuer Perhydrate von Acylierungsprodukten der phosphorigen Saeure |
| CH1010060A CH382160A (de) | 1960-03-22 | 1960-09-07 | Verfahren zur Herstellung von neuen Perverbindungen von Acylierungsprodukten der phosphorigen Säure |
| BE596616A BE596616A (fr) | 1960-03-22 | 1960-10-31 | Procédé de préparation de nouveaux percomposés de produits acylés de l'acide phosphoreux et percomposés ainsi obtenus. |
| FR847730A FR1276899A (fr) | 1960-03-22 | 1960-12-22 | Procédé de préparation de nouveaux percomposés de produits acylés de l'acide phosphoreux et percomposés ainsi obtenus |
| US95497A US3149151A (en) | 1960-03-22 | 1961-03-14 | Per-compounds of acylation products of phosphorous acid |
| GB9618/61A GB903816A (en) | 1960-03-22 | 1961-03-16 | Per-compounds of acylation products of phosphorous acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEH38977A DE1133726B (de) | 1960-03-22 | 1960-03-22 | Verfahren zur Herstellung neuer Perhydrate von Acylierungsprodukten der phosphorigen Saeure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1133726B true DE1133726B (de) | 1962-07-26 |
Family
ID=7153789
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEH38977A Pending DE1133726B (de) | 1960-03-22 | 1960-03-22 | Verfahren zur Herstellung neuer Perhydrate von Acylierungsprodukten der phosphorigen Saeure |
Country Status (6)
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1217950B (de) * | 1965-02-25 | 1966-06-02 | Henkel & Cie Gmbh | Verfahren zur Herstellung neuer Perhydrate von Aminoalkylphosphonsaeuren |
| DE1300563B (de) * | 1965-05-13 | 1969-08-07 | Procter & Gamble | Verfahren zur Herstellung von AEthan-1-hydroxy-1, 1-diphosphonsaeure |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3394083A (en) * | 1963-08-15 | 1968-07-23 | Monsanto Co | Effervescent builder compositions and detergent compositions containing the same |
| DE1496916B1 (de) * | 1964-09-22 | 1969-10-23 | Monsanto Co | Cyanidfreies,galvanisches Bad und Verfahren zum Abscheiden galvanischer UEberzuege |
| US4440646A (en) * | 1965-08-24 | 1984-04-03 | Plains Chemical Development Co. | Chelation |
| US3471406A (en) * | 1965-09-07 | 1969-10-07 | Plains Chem Dev Co | Detergent compositions containing methane tri and tetra phosphonic acid compounds |
| US4020091A (en) * | 1965-10-28 | 1977-04-26 | Plains Chemical Development Co. | Chelation |
| US4254063A (en) * | 1979-05-07 | 1981-03-03 | Betz Laboratories, Inc. | Method for preparing oligomeric ester chain condensates of substituted 1-hydroxy-1,1-diphosphonic acid |
| US4802990A (en) * | 1987-07-30 | 1989-02-07 | Inskeep Jr Eugene L | Solution and method for dissolving minerals |
| US5369099A (en) * | 1993-04-22 | 1994-11-29 | CH2 O Incorporated | Method and composition for inhibiting the formation of hardwater deposits on fruit |
| WO1995023510A1 (en) * | 1993-04-22 | 1995-09-08 | Ch2O Incorporated | A method of inhibiting the formation of crystalline mineral deposits in soil |
| US5930950A (en) * | 1993-04-22 | 1999-08-03 | Ch20 Incorporated | Method of inhibiting the formation of crystalline mineral deposits in soil |
| US5736256A (en) * | 1995-05-31 | 1998-04-07 | Howard A. Fromson | Lithographic printing plate treated with organo-phosphonic acid chelating compounds and processes relating thereto |
| US8513176B2 (en) | 2006-08-02 | 2013-08-20 | Ch2O Incorporated | Disinfecting and mineral deposit eliminating composition and methods |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2119523A (en) * | 1933-07-28 | 1938-06-07 | Bohme H Th Ag | Pyrophosphate ester bleaching agent |
| US2350850A (en) * | 1941-03-26 | 1944-06-06 | Watzel Rudolf | Process for the production of nitrogen-phosphoric acid compounds |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1914312A (en) * | 1928-08-18 | 1933-06-13 | Degussa | Process for the manufacture of compositions of hydrogen-peroxidephosphate |
| US1914311A (en) * | 1928-08-21 | 1933-06-13 | Degussa | Process for the incorporation of active oxygen in organic compounds |
| GB355016A (en) * | 1929-08-10 | 1931-08-20 | Gustav Schoenberg | A process for preparing hydrogen peroxide-phosphate compounds |
| DE973122C (de) * | 1949-03-11 | 1959-12-03 | Hoechst Ag | Verfahren zur Herstellung geformter Waschmittel |
| US3055897A (en) * | 1959-08-08 | 1962-09-25 | Therachemie Chem Therapeut | Process for the production of triazineperhydrate compounds |
-
0
- NL NL257200D patent/NL257200A/xx unknown
- NL NL126199D patent/NL126199C/xx active
-
1960
- 1960-03-22 DE DEH38977A patent/DE1133726B/de active Pending
- 1960-09-07 CH CH1010060A patent/CH382160A/de unknown
- 1960-10-31 BE BE596616A patent/BE596616A/fr unknown
-
1961
- 1961-03-14 US US95497A patent/US3149151A/en not_active Expired - Lifetime
- 1961-03-16 GB GB9618/61A patent/GB903816A/en not_active Expired
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2119523A (en) * | 1933-07-28 | 1938-06-07 | Bohme H Th Ag | Pyrophosphate ester bleaching agent |
| US2350850A (en) * | 1941-03-26 | 1944-06-06 | Watzel Rudolf | Process for the production of nitrogen-phosphoric acid compounds |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1217950B (de) * | 1965-02-25 | 1966-06-02 | Henkel & Cie Gmbh | Verfahren zur Herstellung neuer Perhydrate von Aminoalkylphosphonsaeuren |
| DE1300563B (de) * | 1965-05-13 | 1969-08-07 | Procter & Gamble | Verfahren zur Herstellung von AEthan-1-hydroxy-1, 1-diphosphonsaeure |
Also Published As
| Publication number | Publication date |
|---|---|
| NL257200A (US20030220297A1-20031127-C00009.png) | |
| BE596616A (fr) | 1961-05-02 |
| NL126199C (US20030220297A1-20031127-C00009.png) | |
| CH382160A (de) | 1964-09-30 |
| GB903816A (en) | 1962-08-22 |
| US3149151A (en) | 1964-09-15 |
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