DE1100019B - Verfahren zur Herstellung von Thiophosphorsaeureestern - Google Patents
Verfahren zur Herstellung von ThiophosphorsaeureesternInfo
- Publication number
- DE1100019B DE1100019B DEF29318A DEF0029318A DE1100019B DE 1100019 B DE1100019 B DE 1100019B DE F29318 A DEF29318 A DE F29318A DE F0029318 A DEF0029318 A DE F0029318A DE 1100019 B DE1100019 B DE 1100019B
- Authority
- DE
- Germany
- Prior art keywords
- solution
- heated
- stirring
- hour
- kill
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 5
- 150000003580 thiophosphoric acid esters Chemical class 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims 2
- 150000002148 esters Chemical class 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 10
- 239000011591 potassium Substances 0.000 claims description 8
- 229910052700 potassium Inorganic materials 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- 125000004093 cyano group Chemical group *C#N 0.000 claims description 7
- 229910052698 phosphorus Inorganic materials 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 3
- 125000003545 alkoxy group Chemical group 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000002947 alkylene group Chemical group 0.000 claims description 2
- 150000005840 aryl radicals Chemical class 0.000 claims description 2
- 125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 claims description 2
- 125000005842 heteroatom Chemical group 0.000 claims description 2
- 150000003254 radicals Chemical class 0.000 claims description 2
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 claims description 2
- 125000000547 substituted alkyl group Chemical group 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical compound OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 claims 1
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 9
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- 239000003921 oil Substances 0.000 description 8
- 241001454295 Tetranychidae Species 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- 230000009885 systemic effect Effects 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 241001124076 Aphididae Species 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000012230 colorless oil Substances 0.000 description 3
- RENMDAKOXSCIGH-UHFFFAOYSA-N Chloroacetonitrile Chemical compound ClCC#N RENMDAKOXSCIGH-UHFFFAOYSA-N 0.000 description 2
- FKLJPTJMIBLJAV-UHFFFAOYSA-N Compound IV Chemical compound O1N=C(C)C=C1CCCCCCCOC1=CC=C(C=2OCCN=2)C=C1 FKLJPTJMIBLJAV-UHFFFAOYSA-N 0.000 description 2
- 125000001188 haloalkyl group Chemical group 0.000 description 2
- 239000005457 ice water Substances 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- QTPJMTACJMLPLL-UHFFFAOYSA-N triethoxy(sulfanylidene)-$l^{5}-phosphane Chemical compound CCOP(=S)(OCC)OCC QTPJMTACJMLPLL-UHFFFAOYSA-N 0.000 description 2
- 241000239290 Araneae Species 0.000 description 1
- 241000118205 Ovicides Species 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- FJBFPHVGVWTDIP-UHFFFAOYSA-N dibromomethane Chemical compound BrCBr FJBFPHVGVWTDIP-UHFFFAOYSA-N 0.000 description 1
- NLFBCYMMUAKCPC-KQQUZDAGSA-N ethyl (e)-3-[3-amino-2-cyano-1-[(e)-3-ethoxy-3-oxoprop-1-enyl]sulfanyl-3-oxoprop-1-enyl]sulfanylprop-2-enoate Chemical compound CCOC(=O)\C=C\SC(=C(C#N)C(N)=O)S\C=C\C(=O)OCC NLFBCYMMUAKCPC-KQQUZDAGSA-N 0.000 description 1
- ARFLASKVLJTEJD-UHFFFAOYSA-N ethyl 2-bromopropanoate Chemical compound CCOC(=O)C(C)Br ARFLASKVLJTEJD-UHFFFAOYSA-N 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 231100000636 lethal dose Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000003151 ovacidal effect Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- XWSLYQXUTWUIKM-UHFFFAOYSA-N trimethoxy(sulfanylidene)-$l^{5}-phosphane Chemical compound COP(=S)(OC)OC XWSLYQXUTWUIKM-UHFFFAOYSA-N 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
- C07F9/32—Esters thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/1651—Esters of thiophosphoric acids with hydroxyalkyl compounds with further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/1652—Polyol derivatives esterified at least twice by thiophosphoric acid groups
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Molecular Biology (AREA)
- Dentistry (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL255566D NL255566A (US20020051482A1-20020502-M00057.png) | 1959-09-05 | ||
| BE594722D BE594722A (US20020051482A1-20020502-M00057.png) | 1959-09-05 | ||
| NL127248D NL127248C (US20020051482A1-20020502-M00057.png) | 1959-09-05 | ||
| GB941636D GB941636A (US20020051482A1-20020502-M00057.png) | 1959-09-05 | ||
| DEF29318A DE1100019B (de) | 1959-09-05 | 1959-09-05 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
| CH973360A CH388299A (de) | 1959-09-05 | 1960-08-29 | Verfahren zur Herstellung von Thiophosphorsäureestern |
| US53072A US3092649A (en) | 1959-09-05 | 1960-08-31 | Thiophosphoric acid esters and process for their production |
| FR837671A FR1266422A (fr) | 1959-09-05 | 1960-09-02 | Esters de l'acide thiophosphorique et leur procédé de préparation |
| GB30430/60A GB916704A (en) | 1959-09-05 | 1960-09-02 | Dithiophosphoric acid esters |
| NL6902394A NL6902394A (US20020051482A1-20020502-M00057.png) | 1959-09-05 | 1969-02-14 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF29318A DE1100019B (de) | 1959-09-05 | 1959-09-05 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1100019B true DE1100019B (de) | 1961-02-23 |
Family
ID=7093252
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF29318A Pending DE1100019B (de) | 1959-09-05 | 1959-09-05 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Country Status (6)
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1232961B (de) * | 1964-02-27 | 1967-01-26 | Boehringer Sohn Ingelheim | Verfahren zur Herstellung von Estern einiger Saeuren des Phosphors |
| JPS5127736B1 (US20020051482A1-20020502-M00057.png) * | 1970-03-25 | 1976-08-14 | ||
| JPS5128697B1 (US20020051482A1-20020502-M00057.png) * | 1970-11-26 | 1976-08-20 | ||
| JPS5128696B1 (US20020051482A1-20020502-M00057.png) * | 1970-11-26 | 1976-08-20 |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3309371A (en) * | 1963-10-16 | 1967-03-14 | American Cyanamid Co | Organophosphorothioate compounds and method of preparing same |
| US3433865A (en) * | 1963-11-08 | 1969-03-18 | Hooker Chemical Corp | Controlling insects with furoyloxyalkenyl thio phosphates |
| US3326943A (en) * | 1963-11-08 | 1967-06-20 | Hooker Chemical Corp | Furoyloxyalkenyl thio phosphates |
| US3888979A (en) * | 1971-12-24 | 1975-06-10 | Ciba Geigy Corp | Control of pests with o-ethyl-s-(n)-propyl-s-carbamoylalkyl dithiophosphates |
| BE793210A (fr) * | 1971-12-24 | 1973-06-22 | Ciba Geigy | Esters d'acides thiophosphoriques utilisables notamment comme matieres actives de produits phytopharmaceutiques |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE830509C (de) * | 1950-05-24 | 1952-02-04 | Bayer Ag | Verfahren zur Herstellung von neutralen Estern der Thiophosphorsaeure |
| DE956503C (de) * | 1953-07-22 | 1957-01-17 | Geigy Ag J R | Verfahren zur Herstellung neuer Phosphor- bzw. Thiophosphorsaeureester |
| DE1018053B (de) * | 1955-10-29 | 1957-10-24 | Bayer Ag | Verfahren zur Herstellung von S-Chlorbenzylestern der O, O-Dialkyl-thiolphosphorsaeure |
| DE1032247B (de) * | 1954-12-04 | 1958-06-19 | Bayer Ag | Verfahren zur Herstellung von organischen Phosphorverbindungen |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA494562A (en) * | 1948-02-04 | 1953-07-21 | American Cyanamid Company | Carbamylalkyl phosphates and method of preparation |
| US2494284A (en) * | 1949-01-12 | 1950-01-10 | American Cyanamid Co | Cyanoalkyl phosphates and method of preparation |
| US2611728A (en) * | 1949-11-01 | 1952-09-23 | Standard Oil Dev Co | Insecticidal compositions containing substituted aliphatic esters of diethyl dithiophosphoric acid |
| US2736726A (en) * | 1952-03-28 | 1956-02-28 | Geigy Ag J R | Basic phosphoric acid esters |
| US2767206A (en) * | 1953-12-30 | 1956-10-16 | Shell Dev | Alicyclic esters of phosphoric acids |
| LU35028A1 (US20020051482A1-20020502-M00057.png) * | 1955-02-16 | 1900-01-01 | ||
| NL101816C (US20020051482A1-20020502-M00057.png) * | 1955-05-03 | |||
| US2879283A (en) * | 1955-06-06 | 1959-03-24 | Monsanto Chemicals | Sulfoalkyl phosphorothioates and metal salts thereof |
| NL95444C (US20020051482A1-20020502-M00057.png) * | 1955-06-14 | |||
| US2884354A (en) * | 1955-08-30 | 1959-04-28 | Hercules Powder Co Ltd | Dithiophosphate insecticides |
| US2895982A (en) * | 1956-04-09 | 1959-07-21 | Shell Dev | Complex nitrophenyl phosphates |
| US2882198A (en) * | 1956-07-16 | 1959-04-14 | Fmc Corp | Pesticidal phosphorus esters |
| US2890947A (en) * | 1956-11-14 | 1959-06-16 | Pure Oil Co | Gasoline motor fuel |
| FR1186899A (fr) * | 1957-04-02 | 1959-09-03 | Hoechst Ag | Esters bis-phosphoriques neutres et leur préparation |
-
0
- BE BE594722D patent/BE594722A/xx unknown
- GB GB941636D patent/GB941636A/en active Active
- NL NL127248D patent/NL127248C/xx active
- NL NL255566D patent/NL255566A/xx unknown
-
1959
- 1959-09-05 DE DEF29318A patent/DE1100019B/de active Pending
-
1960
- 1960-08-29 CH CH973360A patent/CH388299A/de unknown
- 1960-08-31 US US53072A patent/US3092649A/en not_active Expired - Lifetime
- 1960-09-02 GB GB30430/60A patent/GB916704A/en not_active Expired
-
1969
- 1969-02-14 NL NL6902394A patent/NL6902394A/xx unknown
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE830509C (de) * | 1950-05-24 | 1952-02-04 | Bayer Ag | Verfahren zur Herstellung von neutralen Estern der Thiophosphorsaeure |
| DE956503C (de) * | 1953-07-22 | 1957-01-17 | Geigy Ag J R | Verfahren zur Herstellung neuer Phosphor- bzw. Thiophosphorsaeureester |
| DE1032247B (de) * | 1954-12-04 | 1958-06-19 | Bayer Ag | Verfahren zur Herstellung von organischen Phosphorverbindungen |
| DE1018053B (de) * | 1955-10-29 | 1957-10-24 | Bayer Ag | Verfahren zur Herstellung von S-Chlorbenzylestern der O, O-Dialkyl-thiolphosphorsaeure |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1232961B (de) * | 1964-02-27 | 1967-01-26 | Boehringer Sohn Ingelheim | Verfahren zur Herstellung von Estern einiger Saeuren des Phosphors |
| JPS5127736B1 (US20020051482A1-20020502-M00057.png) * | 1970-03-25 | 1976-08-14 | ||
| JPS5128697B1 (US20020051482A1-20020502-M00057.png) * | 1970-11-26 | 1976-08-20 | ||
| JPS5128696B1 (US20020051482A1-20020502-M00057.png) * | 1970-11-26 | 1976-08-20 |
Also Published As
| Publication number | Publication date |
|---|---|
| GB941636A (US20020051482A1-20020502-M00057.png) | |
| NL255566A (US20020051482A1-20020502-M00057.png) | |
| GB916704A (en) | 1963-01-23 |
| NL6902394A (US20020051482A1-20020502-M00057.png) | 1969-04-25 |
| NL127248C (US20020051482A1-20020502-M00057.png) | |
| US3092649A (en) | 1963-06-04 |
| CH388299A (de) | 1965-02-28 |
| BE594722A (US20020051482A1-20020502-M00057.png) |
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