DD155058A5 - Verfahren zum schwefelsaeure-flusssaeure-polieren von glasgegenstaenden - Google Patents
Verfahren zum schwefelsaeure-flusssaeure-polieren von glasgegenstaenden Download PDFInfo
- Publication number
- DD155058A5 DD155058A5 DD80225840A DD22584080A DD155058A5 DD 155058 A5 DD155058 A5 DD 155058A5 DD 80225840 A DD80225840 A DD 80225840A DD 22584080 A DD22584080 A DD 22584080A DD 155058 A5 DD155058 A5 DD 155058A5
- Authority
- DD
- German Democratic Republic
- Prior art keywords
- polishing
- acid
- bath
- sodium
- polishing bath
- Prior art date
Links
- 238000005498 polishing Methods 0.000 title claims abstract description 89
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 239000002253 acid Substances 0.000 title claims abstract description 25
- 238000000034 method Methods 0.000 title claims abstract description 13
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000011521 glass Substances 0.000 claims abstract description 19
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 13
- 238000007517 polishing process Methods 0.000 claims abstract description 13
- 239000011734 sodium Substances 0.000 claims abstract description 13
- 238000005868 electrolysis reaction Methods 0.000 claims abstract description 10
- 229910001414 potassium ion Inorganic materials 0.000 claims abstract description 9
- 229910001415 sodium ion Inorganic materials 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 150000001768 cations Chemical class 0.000 claims abstract description 5
- 239000012528 membrane Substances 0.000 claims abstract description 5
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229910052753 mercury Inorganic materials 0.000 claims abstract description 5
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 9
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 4
- 229910052700 potassium Inorganic materials 0.000 claims description 4
- 239000011591 potassium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 235000006408 oxalic acid Nutrition 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 11
- 239000005401 pressed glass Substances 0.000 abstract description 3
- 239000000470 constituent Substances 0.000 abstract description 2
- 239000005337 ground glass Substances 0.000 abstract description 2
- 229910000567 Amalgam (chemistry) Inorganic materials 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 229910001023 sodium amalgam Inorganic materials 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000003513 alkali Substances 0.000 description 16
- 150000002500 ions Chemical class 0.000 description 13
- 229910052739 hydrogen Inorganic materials 0.000 description 6
- 239000005355 lead glass Substances 0.000 description 6
- 238000001556 precipitation Methods 0.000 description 6
- 238000007598 dipping method Methods 0.000 description 5
- 238000011282 treatment Methods 0.000 description 5
- 239000007795 chemical reaction product Substances 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-M bisulphate group Chemical group S([O-])(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 150000002222 fluorine compounds Chemical class 0.000 description 3
- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 2
- 230000001464 adherent effect Effects 0.000 description 2
- 229910052783 alkali metal Inorganic materials 0.000 description 2
- 229910001413 alkali metal ion Inorganic materials 0.000 description 2
- 229910052936 alkali metal sulfate Inorganic materials 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 229910003460 diamond Inorganic materials 0.000 description 2
- 239000010432 diamond Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 229910000497 Amalgam Inorganic materials 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 150000001340 alkali metals Chemical group 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 238000005267 amalgamation Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 150000002892 organic cations Chemical class 0.000 description 1
- -1 oxalic acid Chemical class 0.000 description 1
- 238000011045 prefiltration Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- ABTOQLMXBSRXSM-UHFFFAOYSA-N silicon tetrafluoride Chemical compound F[Si](F)(F)F ABTOQLMXBSRXSM-UHFFFAOYSA-N 0.000 description 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
- 238000004528 spin coating Methods 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- DGCPSAFMAXHHDM-UHFFFAOYSA-N sulfuric acid;hydrofluoride Chemical compound F.OS(O)(=O)=O DGCPSAFMAXHHDM-UHFFFAOYSA-N 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 235000015041 whisky Nutrition 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C03C15/02—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
- C03C15/02—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface
- C03C15/025—Surface treatment of glass, not in the form of fibres or filaments, by etching for making a smooth surface for polishing crystal glass, i.e. lead glass
Landscapes
- Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
- Removal Of Specific Substances (AREA)
- Cleaning By Liquid Or Steam (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2949383A DE2949383C2 (de) | 1979-12-07 | 1979-12-07 | Verfahren zur Schwefelsäure-Flußsäure-Polieren von Glasgegenständen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DD155058A5 true DD155058A5 (de) | 1982-05-12 |
Family
ID=6087901
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DD80225840A DD155058A5 (de) | 1979-12-07 | 1980-12-08 | Verfahren zum schwefelsaeure-flusssaeure-polieren von glasgegenstaenden |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4332649A (enExample) |
| EP (1) | EP0030361B1 (enExample) |
| JP (1) | JPS5939380B2 (enExample) |
| AT (1) | ATE6766T1 (enExample) |
| BG (1) | BG39975A3 (enExample) |
| CA (1) | CA1151514A (enExample) |
| CS (1) | CS221940B2 (enExample) |
| DD (1) | DD155058A5 (enExample) |
| DE (1) | DE2949383C2 (enExample) |
| IE (1) | IE50486B1 (enExample) |
| PL (1) | PL124685B1 (enExample) |
Families Citing this family (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3215963A1 (de) * | 1982-04-29 | 1983-11-03 | Licentia Patent-Verwaltungs-Gmbh, 6000 Frankfurt | Verfahren zum verbessern des netzverhaltens von glasoberflaechen |
| ES8500612A1 (es) * | 1982-10-13 | 1984-11-16 | Saelzle Erich | Metodo de pulir articulos de vidrio |
| US5120605A (en) * | 1988-09-23 | 1992-06-09 | Zuel Company, Inc. | Anti-reflective glass surface |
| US4944986A (en) * | 1988-09-23 | 1990-07-31 | Zuel Company | Anti-reflective glass surface |
| US5164018A (en) * | 1992-03-18 | 1992-11-17 | Barcelona Jr Russell L | Water-spot remover containing hydrofluoric acid, ammonium fluoride, and an alcohol |
| DE4217057A1 (de) * | 1992-05-22 | 1993-11-25 | Saelzle Erich | Verfahren zur Verminderung der Blei- und/oder Bariumemission von Blei und/oder Barium enthaltenden Kristallglasgegenständen bei Berührung mit einer flüssigen Phase |
| US5391258A (en) * | 1993-05-26 | 1995-02-21 | Rodel, Inc. | Compositions and methods for polishing |
| KR0180850B1 (ko) | 1996-06-26 | 1999-03-20 | 구자홍 | 유리기판 에칭장치 |
| US6630052B1 (en) | 1996-06-26 | 2003-10-07 | Lg. Philips Lcd Co., Ltd. | Apparatus for etching glass substrate |
| KR100265556B1 (ko) * | 1997-03-21 | 2000-11-01 | 구본준 | 식각장치 |
| US6327011B2 (en) * | 1997-10-20 | 2001-12-04 | Lg Electronics, Inc. | Liquid crystal display device having thin glass substrate on which protective layer formed and method of making the same |
| KR100272513B1 (ko) | 1998-09-08 | 2001-01-15 | 구본준 | 유리기판의 식각장치 |
| KR100308157B1 (ko) | 1998-10-22 | 2001-11-15 | 구본준, 론 위라하디락사 | 액정표시소자용 유리기판 |
| US6083840A (en) * | 1998-11-25 | 2000-07-04 | Arch Specialty Chemicals, Inc. | Slurry compositions and method for the chemical-mechanical polishing of copper and copper alloys |
| WO2001078116A2 (en) * | 2000-04-11 | 2001-10-18 | Cabot Microelectronics Corporation | System for the preferential removal of silicon oxide |
| JP2002087844A (ja) * | 2000-09-14 | 2002-03-27 | Sony Corp | 表示パネルの製造方法 |
| US6929861B2 (en) | 2002-03-05 | 2005-08-16 | Zuel Company, Inc. | Anti-reflective glass surface with improved cleanability |
| DE10228116A1 (de) * | 2002-06-24 | 2004-01-29 | Sälzle, Erich, Dr. | Verfahren zum Polieren von Glasgegenständen |
| US20040035696A1 (en) * | 2002-08-21 | 2004-02-26 | Reinhard Fred P. | Apparatus and method for membrane electrolysis for process chemical recycling |
| JP4324742B2 (ja) * | 2006-04-28 | 2009-09-02 | シャープ株式会社 | 研磨ガラス基板の製造方法 |
| US9926225B2 (en) | 2011-12-30 | 2018-03-27 | Corning Incorporated | Media and methods for etching glass |
| WO2013181213A1 (en) | 2012-05-31 | 2013-12-05 | Corning Incorporated | Systems and methods for acid-treating glass articles |
| CN110828290A (zh) * | 2018-08-10 | 2020-02-21 | 东莞新科技术研究开发有限公司 | 一种硅片的清洗方法及硅片 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3321388A (en) * | 1962-08-09 | 1967-05-23 | Asahi Denka Kogyo Kk | Process for coordinated operation of diaphragm and mercury cathode electrolytic cells |
| DE1189681B (de) * | 1963-10-26 | 1965-03-25 | Erich Saelzle Dipl Chem Dr | Verfahren zum Polieren von Gegenstaenden aus Kristall- oder Bleikristallglas |
| DE1496666C3 (de) * | 1965-05-26 | 1974-04-04 | Erich Dipl.-Chem.Dr. 8000 Muenchen Saelzle | Verfahren zum Polieren von Glasgegenständen in einem Flußsäure und Schwefelsäure enthaltenden Polierbad |
| US3560281A (en) * | 1967-10-02 | 1971-02-02 | Owens Illinois Inc | Process for regenerating an acid bath |
| DE1920009B2 (de) * | 1969-04-19 | 1971-11-11 | Dunchen, Hannes, 3340 Wolfen buttel | Verfahren und vorrichtung zum behandeln von feststoffhaltiger poliersaeure |
-
1979
- 1979-12-07 DE DE2949383A patent/DE2949383C2/de not_active Expired
-
1980
- 1980-11-19 US US06/208,452 patent/US4332649A/en not_active Expired - Lifetime
- 1980-12-02 JP JP55170194A patent/JPS5939380B2/ja not_active Expired
- 1980-12-03 EP EP80107553A patent/EP0030361B1/de not_active Expired
- 1980-12-03 AT AT80107553T patent/ATE6766T1/de not_active IP Right Cessation
- 1980-12-05 CA CA000366267A patent/CA1151514A/en not_active Expired
- 1980-12-05 IE IE2557/80A patent/IE50486B1/en not_active IP Right Cessation
- 1980-12-05 PL PL1980228290A patent/PL124685B1/pl unknown
- 1980-12-05 CS CS808563A patent/CS221940B2/cs unknown
- 1980-12-08 BG BG049912A patent/BG39975A3/xx unknown
- 1980-12-08 DD DD80225840A patent/DD155058A5/de not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CA1151514A (en) | 1983-08-09 |
| JPS5692137A (en) | 1981-07-25 |
| CS221940B2 (en) | 1983-04-29 |
| IE50486B1 (en) | 1986-04-30 |
| PL228290A1 (enExample) | 1981-08-21 |
| EP0030361A1 (de) | 1981-06-17 |
| EP0030361B1 (de) | 1984-03-21 |
| DE2949383B1 (de) | 1980-12-11 |
| IE802557L (en) | 1981-06-12 |
| ATE6766T1 (de) | 1984-04-15 |
| PL124685B1 (en) | 1983-02-28 |
| BG39975A3 (en) | 1986-09-15 |
| DE2949383C2 (de) | 1982-01-21 |
| US4332649A (en) | 1982-06-01 |
| JPS5939380B2 (ja) | 1984-09-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ENJ | Ceased due to non-payment of renewal fee |