CS203196B2 - Method of removing nitrosamines from dinitroanilines by the action of hydrochloric acid or gaseous hydrogen chloride - Google Patents

Method of removing nitrosamines from dinitroanilines by the action of hydrochloric acid or gaseous hydrogen chloride Download PDF

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Publication number
CS203196B2
CS203196B2 CS784725A CS472578A CS203196B2 CS 203196 B2 CS203196 B2 CS 203196B2 CS 784725 A CS784725 A CS 784725A CS 472578 A CS472578 A CS 472578A CS 203196 B2 CS203196 B2 CS 203196B2
Authority
CS
Czechoslovakia
Prior art keywords
hydrogen chloride
nitrosamine
chloride gas
alkyl
dinitroaniline
Prior art date
Application number
CS784725A
Other languages
Czech (cs)
English (en)
Inventor
Richard F Eizember
Kathleen R Vogler
William N Cannon
Original Assignee
Lilly Co Eli
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lilly Co Eli filed Critical Lilly Co Eli
Publication of CS203196B2 publication Critical patent/CS203196B2/cs

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82Purification; Separation; Stabilisation; Use of additives
    • C07C209/84Purification
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00Compounds containing amino groups bound to a carbon skeleton
    • C07C211/43Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
    • C07C211/44Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
    • C07C211/52Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring the carbon skeleton being further substituted by halogen atoms or by nitro or nitroso groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
CS784725A 1977-07-18 1978-07-14 Method of removing nitrosamines from dinitroanilines by the action of hydrochloric acid or gaseous hydrogen chloride CS203196B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US81655877A 1977-07-18 1977-07-18
US87883478A 1978-02-17 1978-02-17

Publications (1)

Publication Number Publication Date
CS203196B2 true CS203196B2 (en) 1981-02-27

Family

ID=27124088

Family Applications (1)

Application Number Title Priority Date Filing Date
CS784725A CS203196B2 (en) 1977-07-18 1978-07-14 Method of removing nitrosamines from dinitroanilines by the action of hydrochloric acid or gaseous hydrogen chloride

Country Status (21)

Country Link
JP (1) JPS5822102B2 (es)
AR (1) AR221846A1 (es)
AU (1) AU516698B2 (es)
BG (1) BG34182A3 (es)
BR (1) BR7804599A (es)
CA (1) CA1081256A (es)
CS (1) CS203196B2 (es)
DD (1) DD137222A5 (es)
DE (1) DE2831119C2 (es)
DK (1) DK152113C (es)
ES (1) ES471821A1 (es)
FR (1) FR2398044A1 (es)
GB (1) GB1599930A (es)
HU (1) HU182483B (es)
IE (1) IE47127B1 (es)
IL (1) IL55142A (es)
IT (1) IT1097822B (es)
MX (1) MX5203E (es)
NL (1) NL189911C (es)
PL (1) PL119759B1 (es)
RO (1) RO75656A (es)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0019281B1 (de) * 1979-05-21 1982-12-29 Hoechst Aktiengesellschaft Verfahren zur Entfernung von Nitrosierungsmittel(n) aus nitrierten aromatischen Verbindungen
DE2926947C2 (de) * 1979-07-04 1982-03-18 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von Nitrosierungsmittel (n) aus nitrierten aromatischen Verbindungen
DE3345157A1 (de) * 1983-12-14 1985-06-27 Hoechst Ag, 6230 Frankfurt Verfahren zur herstellung von nitrosaminfreien n,n-disubstituierten nitroaromatischen aminen und deren stabilisierung gegen nitrosaminbildung
IT1195822B (it) * 1986-08-12 1988-10-27 I Pi Ci Spa Procedimento per la purificazione della trifluralina
IT1293450B1 (it) * 1997-07-14 1999-03-01 Finchimica Srl Procedimento per la purificazione di dinitroaniline.
WO2016110965A1 (ja) * 2015-01-07 2016-07-14 三菱日立パワーシステムズ株式会社 ニトロソ化合物の処理方法および処理装置
CN109320424B (zh) * 2017-07-31 2021-12-21 江苏永安化工有限公司 一种二甲戊灵的纯化方法
CN116735760B (zh) * 2023-08-16 2024-02-09 山东道可化学有限公司 一种氟乐灵中n,n-二丙基亚硝胺的检测方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4134917A (en) * 1977-04-25 1979-01-16 American Cyanamid Company Method for the denitrosation of organic nitrosamines

Also Published As

Publication number Publication date
MX5203E (es) 1983-04-25
DK152113B (da) 1988-02-01
ES471821A1 (es) 1979-10-01
IE47127B1 (en) 1983-12-28
RO75656A (ro) 1981-04-20
IT1097822B (it) 1985-08-31
BG34182A3 (en) 1983-07-15
FR2398044B1 (es) 1980-10-31
DE2831119A1 (de) 1979-02-08
NL7807576A (nl) 1979-01-22
DK152113C (da) 1988-06-20
BR7804599A (pt) 1979-03-20
PL119759B1 (en) 1982-01-30
IL55142A (en) 1981-06-29
NL189911B (nl) 1993-04-01
DE2831119C2 (de) 1983-05-26
IE781430L (en) 1979-01-18
IL55142A0 (en) 1978-09-29
IT7825724A0 (it) 1978-07-14
JPS5422329A (en) 1979-02-20
DK319378A (da) 1979-01-19
PL208500A1 (pl) 1979-07-02
NL189911C (nl) 1993-09-01
JPS5822102B2 (ja) 1983-05-06
DD137222A5 (de) 1979-08-22
AU516698B2 (en) 1981-06-18
GB1599930A (en) 1981-10-07
AR221846A1 (es) 1981-03-31
FR2398044A1 (fr) 1979-02-16
AU3805878A (en) 1980-01-17
HU182483B (en) 1984-01-30
CA1081256A (en) 1980-07-08

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