CO5160375A1 - Metodo para fraccionar poli(oxido de etileno) formado usando un catalizador de cianuro metalico - Google Patents

Metodo para fraccionar poli(oxido de etileno) formado usando un catalizador de cianuro metalico

Info

Publication number
CO5160375A1
CO5160375A1 CO00051057A CO00051057A CO5160375A1 CO 5160375 A1 CO5160375 A1 CO 5160375A1 CO 00051057 A CO00051057 A CO 00051057A CO 00051057 A CO00051057 A CO 00051057A CO 5160375 A1 CO5160375 A1 CO 5160375A1
Authority
CO
Colombia
Prior art keywords
poly
ethylene oxide
molecular weight
fractioning
fraction
Prior art date
Application number
CO00051057A
Other languages
English (en)
Inventor
Katherine S Clement
Louis L Walker
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of CO5160375A1 publication Critical patent/CO5160375A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30Post-polymerisation treatment, e.g. recovery, purification, drying
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/34Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from hydroxy compounds or their metallic derivatives
    • C08G65/46Post-polymerisation treatment, e.g. recovery, purification, drying
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645Metals or compounds thereof, e.g. salts
    • C08G65/2663Metal cyanide catalysts, i.e. DMC's
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/584Recycling of catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)

Abstract

Un método para purificar un polímero de poli(óxido de etileno) que contiene una fracción de menor peso molecular y por lo menos una fracción de mayor peso molecular, caracterizado porque comprende:a) mezclar el polímero de poli(óxido de etileno) con un compuesto o con una mezcla de compuestos, siendo dicho compuesto o dicha mezcla de compuestos un solvente para la fracción de bajo peso molecular, pero no para la fracción de elevado peso molecular, en cantidades relativas y bajo condiciones tales, que se forme una solución de bajo peso molecular en el compuesto o la mezcla de compuestos, yb) separar la solución de fracción de elevado peso molecular.
CO00051057A 1999-07-09 2000-07-07 Metodo para fraccionar poli(oxido de etileno) formado usando un catalizador de cianuro metalico CO5160375A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14307699P 1999-07-09 1999-07-09
US20577300P 2000-05-19 2000-05-19

Publications (1)

Publication Number Publication Date
CO5160375A1 true CO5160375A1 (es) 2002-05-30

Family

ID=26840655

Family Applications (1)

Application Number Title Priority Date Filing Date
CO00051057A CO5160375A1 (es) 1999-07-09 2000-07-07 Metodo para fraccionar poli(oxido de etileno) formado usando un catalizador de cianuro metalico

Country Status (14)

Country Link
US (1) US6552163B1 (es)
EP (1) EP1204695B1 (es)
JP (1) JP2003504469A (es)
KR (1) KR100628674B1 (es)
CN (1) CN1129627C (es)
AR (1) AR024684A1 (es)
AT (1) ATE380836T1 (es)
AU (1) AU5920800A (es)
BR (1) BR0011793A (es)
CA (1) CA2376201A1 (es)
CO (1) CO5160375A1 (es)
DE (1) DE60037431T2 (es)
MX (1) MXPA02000299A (es)
WO (1) WO2001004184A1 (es)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MXPA04009145A (es) 2002-03-21 2004-11-26 Dow Global Technologies Inc Metodo para preparar complejos catalizadores de cianuro de metal usando agentes formadores de complejo parcialmente miscibles.
CN100348643C (zh) * 2002-11-07 2007-11-14 陶氏环球技术公司 应用可聚合络合试剂制备金属氰化物催化剂的方法
ES2352455T3 (es) * 2004-10-25 2011-02-18 Dow Global Technologies Inc. Polímeros polioles y dispersiones de polímeros obtenidas a partir de materiales que contienen hidroxilo basados en aceites vegetales.
MX2007004991A (es) * 2004-10-25 2007-06-14 Dow Global Technologies Inc Poliuretanos hechos de acidos grasos conteniendo hidroxi-metilo o esteres de alquilo de tales acidos grasos.
RU2375945C2 (ru) * 2004-10-25 2009-12-20 Дау Глобал Текнолоджиз, Инк. Полиуретановая основа коврового покрытия, полученная с использованием гидроксиметилированных (сложный полиэфир) полиолов
JP5000523B2 (ja) * 2004-10-25 2012-08-15 ダウ グローバル テクノロジーズ エルエルシー 脂肪酸に由来するヒドロキシメチル含有ポリエステルポリオールから製造されたプレポリマー
KR101237677B1 (ko) * 2004-10-25 2013-02-27 다우 글로벌 테크놀로지스 엘엘씨 지방산으로부터 유도된 히드록시메틸-함유 폴리에스테르폴리올로부터 제조된 수성 폴리우레탄 분산액
CN104193984B (zh) * 2014-09-02 2016-06-08 科之杰新材料集团有限公司 一种混凝土减水剂用不饱和烯基聚醚单体及其制备方法
CN104262613B (zh) * 2014-10-13 2016-06-22 辽宁奥克医药辅料股份有限公司 一种含有环氧乙烷杂质的聚乙二醇的精制方法
JP7192767B2 (ja) * 2017-06-16 2022-12-20 株式会社大阪ソーダ ポリエーテル重合体
JP7393330B2 (ja) * 2018-04-18 2023-12-06 株式会社カネカ ポリエーテルの製造方法
EP3567067A1 (de) * 2018-05-08 2019-11-13 Covestro Deutschland AG Abtrennung von doppelmetallcyanid-katalysator
JP7240859B2 (ja) * 2018-11-26 2023-03-16 株式会社カネカ 精製ポリエーテルの製造方法、及び硬化性組成物の製造方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3278458A (en) * 1963-02-14 1966-10-11 Gen Tire & Rubber Co Method of making a polyether using a double metal cyanide complex compound
US3478109A (en) * 1967-07-28 1969-11-11 Eastman Kodak Co Solvent extraction of polymeric glycols using methanol
US3546331A (en) * 1967-12-26 1970-12-08 Union Carbide Corp Surface crystallization of poly(2,2,4,4-tetramethylcyclobutanediol - 1,3)carbonates by organic solvent/organic nonsolvent liquid solutions
US4684715A (en) * 1984-05-07 1987-08-04 The Firestone Tire & Rubber Company Extraction of rubber and/or resin from rubber containing plants with a monophase solvent mixture
DE3607946A1 (de) * 1986-03-11 1987-09-17 Basf Ag Verfahren zur einengung der molekulargewichtsverteilung von polytetrahydrofuran und von copolymerisaten aus tetrahydrofuran und alkylenoxiden
US5010047A (en) * 1989-02-27 1991-04-23 Arco Chemical Technology, Inc. Recovery of double metal cyanide complex catalyst from a polymer
US5198471A (en) * 1989-09-11 1993-03-30 Rensselaer Polytechnic Institute Polymer recycling by selective dissolution
IT1241077B (it) * 1990-03-22 1993-12-29 Donegani Guido Ist Procedimento per il frazionamento in continuo di polimeri ed apparecchiatura adatta allo scopo
US5426175A (en) * 1991-07-15 1995-06-20 Phillips Petroleum Company Deashing process for polyolefins
US5470813A (en) * 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5756604A (en) * 1995-08-31 1998-05-26 Hodogaya Chemical Co., Ltd. Process for producing polyether, and process for recycling and reusing herteropolyacid
US5800711A (en) 1996-10-18 1998-09-01 Mdv Technologies, Inc. Process for the fractionation of polyoxyalkylene block copolymers
US6043299A (en) * 1996-10-31 2000-03-28 Shell Oil Company Process for the extraction of material from multi-phase systems
DE19706331A1 (de) * 1997-02-19 1998-08-20 Mueller Herbert Dr Verfahren zur Gewinnung von Polytetramethylenetherglykolen mit enger Molmassenverteilung
US5844070A (en) * 1997-05-16 1998-12-01 Arco Chemical Technology, L.P. Process for rapid activation of double metal cyanide catalysts

Also Published As

Publication number Publication date
US6552163B1 (en) 2003-04-22
BR0011793A (pt) 2002-03-12
KR100628674B1 (ko) 2006-09-27
ATE380836T1 (de) 2007-12-15
JP2003504469A (ja) 2003-02-04
WO2001004184A1 (en) 2001-01-18
CN1358209A (zh) 2002-07-10
DE60037431D1 (de) 2008-01-24
CN1129627C (zh) 2003-12-03
CA2376201A1 (en) 2001-01-18
DE60037431T2 (de) 2008-11-27
MXPA02000299A (es) 2002-06-21
KR20020019950A (ko) 2002-03-13
EP1204695B1 (en) 2007-12-12
AU5920800A (en) 2001-01-30
EP1204695A1 (en) 2002-05-15
AR024684A1 (es) 2002-10-23

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