CO5160377A1 - Polimerizacion de oxido de etileno utilizando catalizadores de cianuro de metal - Google Patents
Polimerizacion de oxido de etileno utilizando catalizadores de cianuro de metalInfo
- Publication number
- CO5160377A1 CO5160377A1 CO00051076A CO00051076A CO5160377A1 CO 5160377 A1 CO5160377 A1 CO 5160377A1 CO 00051076 A CO00051076 A CO 00051076A CO 00051076 A CO00051076 A CO 00051076A CO 5160377 A1 CO5160377 A1 CO 5160377A1
- Authority
- CO
- Colombia
- Prior art keywords
- ethylene oxide
- metal cyanide
- polymerization
- cyanide catalysts
- polyether
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/08—Saturated oxiranes
- C08G65/10—Saturated oxiranes characterised by the catalysts used
- C08G65/12—Saturated oxiranes characterised by the catalysts used containing organo-metallic compounds or metal hydrides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
- B01J27/26—Cyanides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2615—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen the other compounds containing carboxylic acid, ester or anhydride groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2693—Supported catalysts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0215—Coating
- B01J37/0221—Coating of particles
- B01J37/0223—Coating of particles by rotation
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Toxicology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Polyethers (AREA)
Abstract
Un proceso para preparar un poliéter, que comprende(a) combinar un compuesto iniciador que tiene uno o más grupos oxialquilatables, óxido de etileno y un complejo de catalizador de cianuro de metal para formar una mezcla, y(b) someter la mezcla a condiciones suficientes para etoxilar los grupos oxialquilatables del iniciador para formar un poliéter.
Applications Claiming Priority (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US14307999P | 1999-07-09 | 1999-07-09 | |
US14307899P | 1999-07-09 | 1999-07-09 | |
US14308299P | 1999-07-09 | 1999-07-09 | |
US14308199P | 1999-07-09 | 1999-07-09 | |
US14307599P | 1999-07-09 | 1999-07-09 | |
US20577100P | 2000-05-19 | 2000-05-19 |
Publications (1)
Publication Number | Publication Date |
---|---|
CO5160377A1 true CO5160377A1 (es) | 2002-05-30 |
Family
ID=27558275
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CO00051076A CO5160377A1 (es) | 1999-07-09 | 2000-07-07 | Polimerizacion de oxido de etileno utilizando catalizadores de cianuro de metal |
Country Status (15)
Country | Link |
---|---|
US (1) | US6429342B1 (es) |
EP (1) | EP1200506B1 (es) |
JP (1) | JP2003504468A (es) |
KR (1) | KR20020019949A (es) |
CN (1) | CN1205250C (es) |
AR (1) | AR025544A1 (es) |
AT (1) | ATE323119T1 (es) |
AU (1) | AU5923400A (es) |
BR (1) | BR0013193A (es) |
CA (1) | CA2378466A1 (es) |
CO (1) | CO5160377A1 (es) |
DE (1) | DE60027302T2 (es) |
ES (1) | ES2257302T3 (es) |
MX (1) | MXPA02000310A (es) |
WO (1) | WO2001004183A1 (es) |
Families Citing this family (56)
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CA2401602A1 (en) | 2000-02-29 | 2001-09-07 | Basf Aktiengesellschaft | Method for producing multimetal cyanide compounds |
US6429166B1 (en) * | 2000-05-19 | 2002-08-06 | Dow Global Technologies Inc. | Method for preparing metal cyanide catalyst/polyol initiator slurries |
BR0308674A (pt) * | 2002-03-19 | 2005-02-01 | Dow Global Technologies Inc | Métodos para preparar catalisador de cianeto metálico usando sais metálicos insolúveis |
WO2003080241A1 (en) * | 2002-03-21 | 2003-10-02 | Dow Global Technologies, Inc. | Method for preparing metal cyanide catalyst complexes using partially miscible complexing agents |
WO2003091192A1 (de) | 2002-04-26 | 2003-11-06 | Basf Aktiengesellschaft | C10 -alkanolalkoxylat-gemische und ihre verwendung |
JP4112500B2 (ja) * | 2002-04-26 | 2008-07-02 | ビーエーエスエフ ソシエタス・ヨーロピア | C10−アルカノールアルコキシラート類及びその使用 |
US6835801B2 (en) | 2002-07-19 | 2004-12-28 | Bayer Antwerp, N.V. | Activated starter mixtures and the processes related thereto |
DE10242399A1 (de) * | 2002-09-12 | 2004-03-18 | Basf Ag | Verfahren zur Herstellung von Polyetherolen |
DE10243362A1 (de) | 2002-09-18 | 2004-04-01 | Basf Ag | Herstellung von Alkanolalkoxylaten bei optimierten Reaktionstemperaturen |
DE10243365A1 (de) | 2002-09-18 | 2004-04-01 | Basf Ag | Alkoxylate mit niedrigem Restalkohol-Gehalt |
DE10243366A1 (de) | 2002-09-18 | 2004-04-01 | Basf Ag | Herstellung von Alkoxylaten bei optimierten Reaktionsdrücken |
BR0315469A (pt) * | 2002-11-07 | 2005-08-23 | Dow Global Technologies Inc | Complexo catalisador, polìmero, método para produzir um catalisador de polimerização e método para produzir um poliéter |
DK1565563T3 (da) * | 2002-11-22 | 2013-01-21 | Basf Se | Enzymatisk syntese af polyolacrylater |
WO2004060406A2 (en) | 2002-12-31 | 2004-07-22 | Nektar Therapeutics Al, Corporation | Polymeric reagents comprising a ketone or a related functional group |
US6806348B2 (en) * | 2003-02-11 | 2004-10-19 | Basf Corporation | Process for removing and regenerating a double metal cyanide (DMC) catalyst from a polymer polyol |
US6713599B1 (en) * | 2003-03-31 | 2004-03-30 | Basf Corporation | Formation of polymer polyols with a narrow polydispersity using double metal cyanide (DMC) catalysts |
US6884826B2 (en) * | 2003-06-09 | 2005-04-26 | Bayer Antwerp, N.V. | Process for preparing double metal cyanide catalyzed polyols |
US20050014979A1 (en) * | 2003-07-08 | 2005-01-20 | Eleveld Michiel Barend | Preparation of an alkoxylate composition using a double metal cyanide catalyst |
DE10348420A1 (de) | 2003-10-14 | 2005-05-25 | Basf Ag | C10-Alkanolalkoxylat-Gemische und ihre Verwendung - Neue schaumarme Netzer |
US20050101477A1 (en) * | 2003-11-07 | 2005-05-12 | George Combs | Unsaturated tertiary alcohols as ligands for active dmc catalysts |
CN1961017B (zh) * | 2004-05-31 | 2010-08-25 | 旭硝子株式会社 | 聚氨酯弹性体及其制造方法 |
US20060058182A1 (en) * | 2004-09-13 | 2006-03-16 | Combs George G | Processes for the preparation of double metal cyanide (DMC) catalysts |
CN101048439B (zh) * | 2004-10-25 | 2011-04-13 | 陶氏环球技术公司 | 由植物油基含羟基的材料制成的聚合物多元醇和聚合物分散体 |
AU2005299520A1 (en) * | 2004-10-25 | 2006-05-04 | Dow Global Technologies, Inc. | Prepolymers made from hydroxmethyl-containing polyester polyols derived from fatty acids |
WO2006047431A1 (en) * | 2004-10-25 | 2006-05-04 | Dow Global Technologies, Inc. | Aqueous polyurethane dispersions made from hydroxymethyl containing polyester polyols derived from faty acids |
KR101225352B1 (ko) * | 2004-10-25 | 2013-01-23 | 다우 글로벌 테크놀로지스 엘엘씨 | 히드록시메틸화 폴리에스테르 폴리올을 사용하여 제조된폴리우레탄 카펫 안감 |
JP5085331B2 (ja) * | 2004-10-25 | 2012-11-28 | ダウ グローバル テクノロジーズ エルエルシー | ヒドロキシメチル含有脂肪酸またはそのような脂肪酸のアルキルエステルから作られるポリウレタン |
DE102005012794A1 (de) | 2005-03-19 | 2006-09-21 | Bayer Materialscience Ag | Poly(etherester)polyole und Verfahren zu ihrer Herstellung |
US7495063B2 (en) * | 2006-02-03 | 2009-02-24 | Dow Global Technologies Inc. | Reduced oligomer concentration in high purity polyalkylene glycols |
JP2007284586A (ja) * | 2006-04-18 | 2007-11-01 | Asahi Glass Co Ltd | ポリエーテルモノオールの製造方法 |
US20080132729A1 (en) * | 2006-12-01 | 2008-06-05 | Mcdaniel Kenneth G | Continuous process for the production of ethoxylates |
CN101578130A (zh) * | 2007-01-11 | 2009-11-11 | 陶氏环球技术公司 | 烷氧基化物混合物表面活性剂 |
US7834082B2 (en) * | 2007-01-17 | 2010-11-16 | Bayer Materialscience Llc | Polyether-polysiloxane polyols |
US7473677B2 (en) * | 2007-04-16 | 2009-01-06 | Bayer Materialscience Llc | High productivity process for alkylphenol ethoxylates |
US20080255378A1 (en) * | 2007-04-16 | 2008-10-16 | Bayer Materialscience Llc | High productivity process for non-phenolic ethoxylates |
BRPI0909922A2 (pt) | 2008-06-18 | 2019-03-06 | Dow Global Technologies Inc | método para remover triglicerídeos reticulados a partir de uma espuma e uso de um surfactante não-iônico |
WO2010072029A1 (en) | 2008-12-25 | 2010-07-01 | Dow Global Technologies Inc. | Surfactant compositions with wide ph stability |
WO2011034878A2 (en) * | 2009-09-15 | 2011-03-24 | Union Carbide Chemicals & Plastics Technology Llc | Silicone replacements for personal care compositions |
JP2011124546A (ja) | 2009-10-14 | 2011-06-23 | Rohm & Haas Electronic Materials Llc | 半導体ウェハを清浄化しマイクロエッチングする方法 |
JP2011205058A (ja) | 2009-12-17 | 2011-10-13 | Rohm & Haas Electronic Materials Llc | 半導体基体をテクスチャ化する改良された方法 |
EP2236493A1 (en) | 2010-01-27 | 2010-10-06 | Shell Internationale Research Maatschappij B.V. | Preparation of alkoxysulfates |
CN102958887A (zh) * | 2010-06-29 | 2013-03-06 | 陶氏环球技术有限责任公司 | 支链仲醇烷氧基化表面活性剂及其制备方法 |
CN103080229B (zh) | 2010-06-30 | 2015-07-22 | 陶氏环球技术有限责任公司 | 用于织物加工的支链的仲醇烷氧基化物表面活性剂 |
CN103270012A (zh) * | 2010-11-23 | 2013-08-28 | 陶氏环球技术有限责任公司 | 支链仲醇烷氧基化物表面活性剂及制备它们的方法 |
SG192049A1 (en) * | 2011-02-24 | 2013-08-30 | Shell Int Research | Process and reactor system for the preparation of polyether polyols |
HUE044968T2 (hu) * | 2011-04-04 | 2019-11-28 | Henkel Ag & Co Kgaa | Katalizátor egy epoxid polimerizálására és egy epoxid és széndioxid kopolimerizálására |
CN103946270B (zh) | 2011-11-22 | 2016-09-14 | 西奥公司 | 使用非金属引发剂合成高分子量peo |
EP2861065B1 (en) * | 2012-06-18 | 2017-03-15 | Basf Se | Agroformulations containing a lactone based alkoxylate |
FR3073517A1 (fr) | 2017-11-10 | 2019-05-17 | Arkema France | Sulfates d'alcools secondaires alcoxyles |
FR3073519A1 (fr) * | 2017-11-10 | 2019-05-17 | Arkema France | Alcool secondaire alcoxyle |
FR3073521A1 (fr) | 2017-11-10 | 2019-05-17 | Arkema France | Ester de phosphate d'alcool secondaire |
CA3129644A1 (en) | 2019-02-19 | 2020-08-27 | Dow Global Technologies Llc | Enhanced crude oil recovery from subterranean crude oil-bearing sandstone reservoirs |
FR3102177B1 (fr) | 2019-10-18 | 2023-05-19 | Arkema France | Alcools alcoxylés et coiffés |
CA3163453A1 (en) | 2020-01-09 | 2021-07-15 | Rostislav KAMKIN | Method for flotation of a phosphate-containing ore |
FR3111901B1 (fr) | 2020-06-30 | 2023-02-17 | Arkema France | PROCÉdÉ D’ALCOXYLATION AMÉLIORÉ |
CA3240573A1 (en) | 2021-12-16 | 2023-06-22 | Yusen QIAO | Novel nonionic surfactants and processes to make them |
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---|---|---|---|---|
GB1063525A (en) | 1963-02-14 | 1967-03-30 | Gen Tire & Rubber Co | Organic cyclic oxide polymers, their preparation and tires prepared therefrom |
US3278458A (en) * | 1963-02-14 | 1966-10-11 | Gen Tire & Rubber Co | Method of making a polyether using a double metal cyanide complex compound |
US3689532A (en) | 1969-10-14 | 1972-09-05 | Rohm & Haas | Process for polyoxyalkylation |
JPS5230489B2 (es) | 1974-06-08 | 1977-08-09 | ||
DE3142041C2 (de) * | 1981-10-23 | 1983-09-15 | Th. Goldschmidt Ag, 4300 Essen | Verfahren zur Herstellung von Polyoxyalkylenethern |
JPH0710801B2 (ja) | 1987-05-14 | 1995-02-08 | 三洋化成工業株式会社 | (メタ)アクリル酸エステルの製造法 |
US4877906A (en) | 1988-11-25 | 1989-10-31 | Arco Chemical Technology, Inc. | Purification of polyols prepared using double metal cyanide complex catalysts |
US4985491A (en) | 1989-10-05 | 1991-01-15 | Olin Corporation | Polyurethane sealants made using high molecular weight polyols prepared with double metal cyanide catalysts |
JP2999789B2 (ja) | 1990-02-23 | 2000-01-17 | 旭硝子株式会社 | ポリエーテル類の製造方法 |
US5144093A (en) | 1991-04-29 | 1992-09-01 | Olin Corporation | Process for purifying and end-capping polyols made using double metal cyanide catalysts |
JPH08208426A (ja) | 1995-02-03 | 1996-08-13 | Nippon Oil & Fats Co Ltd | 化粧品基材 |
US5563221A (en) | 1995-06-21 | 1996-10-08 | Arco Chemical Technology, L.P. | Process for making ethylene oxide-capped polyols from double metal cyanide-catalyzed polyols |
US5679764A (en) | 1995-11-06 | 1997-10-21 | Arco Chemical Technology, L.P. | Process of oxyalkylation employing solid, heterogeneous MgO catalyst |
US5856369A (en) | 1996-07-30 | 1999-01-05 | Osi Specialties, Inc. | Polyethers and polysiloxane copolymers manufactured with double metal cyanide catalysts |
JP3244632B2 (ja) | 1996-09-03 | 2002-01-07 | 矢崎総業株式会社 | 多段コネクタ |
US5714428A (en) | 1996-10-16 | 1998-02-03 | Arco Chemical Technology, L.P. | Double metal cyanide catalysts containing functionalized polymers |
DE69825168T2 (de) * | 1997-08-25 | 2005-07-28 | Arco Chemical Technology, L.P., Greenville | Herstellung von funktionalisierten polyethern |
-
2000
- 2000-07-07 AR ARP000103500A patent/AR025544A1/es unknown
- 2000-07-07 WO PCT/US2000/018664 patent/WO2001004183A1/en active IP Right Grant
- 2000-07-07 KR KR1020027000245A patent/KR20020019949A/ko not_active Application Discontinuation
- 2000-07-07 AU AU59234/00A patent/AU5923400A/en not_active Abandoned
- 2000-07-07 AT AT00945262T patent/ATE323119T1/de not_active IP Right Cessation
- 2000-07-07 CO CO00051076A patent/CO5160377A1/es unknown
- 2000-07-07 ES ES00945262T patent/ES2257302T3/es not_active Expired - Lifetime
- 2000-07-07 CN CNB00809991XA patent/CN1205250C/zh not_active Expired - Fee Related
- 2000-07-07 EP EP00945262A patent/EP1200506B1/en not_active Revoked
- 2000-07-07 JP JP2001509395A patent/JP2003504468A/ja active Pending
- 2000-07-07 MX MXPA02000310A patent/MXPA02000310A/es unknown
- 2000-07-07 CA CA002378466A patent/CA2378466A1/en not_active Abandoned
- 2000-07-07 US US09/611,499 patent/US6429342B1/en not_active Expired - Fee Related
- 2000-07-07 DE DE60027302T patent/DE60027302T2/de not_active Revoked
- 2000-07-07 BR BR0013193-8A patent/BR0013193A/pt not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
BR0013193A (pt) | 2002-07-02 |
WO2001004183A1 (en) | 2001-01-18 |
DE60027302T2 (de) | 2007-01-18 |
EP1200506B1 (en) | 2006-04-12 |
KR20020019949A (ko) | 2002-03-13 |
US6429342B1 (en) | 2002-08-06 |
ATE323119T1 (de) | 2006-04-15 |
CN1360607A (zh) | 2002-07-24 |
EP1200506A1 (en) | 2002-05-02 |
CA2378466A1 (en) | 2001-01-18 |
MXPA02000310A (es) | 2002-06-21 |
JP2003504468A (ja) | 2003-02-04 |
CN1205250C (zh) | 2005-06-08 |
AU5923400A (en) | 2001-01-30 |
DE60027302D1 (de) | 2006-05-24 |
ES2257302T3 (es) | 2006-08-01 |
AR025544A1 (es) | 2002-12-04 |
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