CN1829765A - 超吸收剂细微颗粒的附聚方法 - Google Patents
超吸收剂细微颗粒的附聚方法 Download PDFInfo
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- CN1829765A CN1829765A CNA200480021592XA CN200480021592A CN1829765A CN 1829765 A CN1829765 A CN 1829765A CN A200480021592X A CNA200480021592X A CN A200480021592XA CN 200480021592 A CN200480021592 A CN 200480021592A CN 1829765 A CN1829765 A CN 1829765A
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- KVWOTUDBCFBGFJ-UHFFFAOYSA-N tert-butyl 2-methylpropanoate Chemical group CC(C)C(=O)OC(C)(C)C KVWOTUDBCFBGFJ-UHFFFAOYSA-N 0.000 description 1
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- 229910052719 titanium Inorganic materials 0.000 description 1
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- 229910052723 transition metal Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- VPYJNCGUESNPMV-UHFFFAOYSA-N triallylamine Chemical compound C=CCN(CC=C)CC=C VPYJNCGUESNPMV-UHFFFAOYSA-N 0.000 description 1
- ICUTUKXCWQYESQ-UHFFFAOYSA-N triclocarban Chemical compound C1=CC(Cl)=CC=C1NC(=O)NC1=CC=C(Cl)C(Cl)=C1 ICUTUKXCWQYESQ-UHFFFAOYSA-N 0.000 description 1
- 229960003500 triclosan Drugs 0.000 description 1
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- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
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- 125000005591 trimellitate group Chemical group 0.000 description 1
- WXETUDXXEZHSCS-MAVITOTKSA-N vertofix coeur Chemical compound C[C@@H]1CC[C@@]2(C(/CC3)=C\C(C)=O)[C@@H]3C(C)(C)[C@@H]1C2 WXETUDXXEZHSCS-MAVITOTKSA-N 0.000 description 1
- 239000010679 vetiver oil Substances 0.000 description 1
- 229960000834 vinyl ether Drugs 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
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- DGVVWUTYPXICAM-UHFFFAOYSA-N β‐Mercaptoethanol Chemical compound OCCS DGVVWUTYPXICAM-UHFFFAOYSA-N 0.000 description 1
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Thermal Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Polymerisation Methods In General (AREA)
- Polymers With Sulfur, Phosphorus Or Metals In The Main Chain (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Absorbent Articles And Supports Therefor (AREA)
Abstract
Description
颗粒分布[μm] | >850 | <850>600 | <600>300 | <300>150 | <150 |
采用聚丙烯酸酯溶液喷洒之前[重量%] | 0.1 | 0.4 | 0.6 | 56.5 | 42.4 |
采用聚丙烯酸酯溶液喷洒之后[重量%] | 0.2 | 4.6 | 28.6 | 64.9 | 1.7 |
颗粒分布[μm] | >850 | <850>600 | <600>300 | <300>150 | <150 |
采用聚丙烯酸酯溶液喷洒之前[重量%] | 0.1 | 0.2 | 0.4 | 54.3 | 45.7 |
采用聚丙烯酸酯溶液喷洒之后[重量%] | 3.3 | 34.4 | 32.6 | 28.5 | 1.2 |
干燥 | 30min/140℃ | 30min/160℃ | 30min/180℃ | 根据实施例I的生产使用的细微颗粒 |
稳定性 | 17重量% | 18重量% | 17重量% | |
CRC值 | 21.1g/g | 21.1g/g | 17.8g/g | 23g/g |
AAP值 | 9.9g/g | 9.6g/g | 11.7g/g | 18.9g/g |
可溶部分 | 19.8重量% | 18.6重量% | 17.5重量% | 11.2重量% |
含水量 | 4.1重量% | 3.4重量% | 2.1重量% | 3重量% |
反应产物 | CRC[g/g] | AAP 0.7psi[g/g] |
超吸收剂细微颗粒 | 30.5 | 9.5 |
附聚物 | 24.8 | 10.1 |
后交联的附聚物 | 21.5 | 19.0 |
性能 | 附聚物3 |
<150μm的颗粒的比例(研磨之前) | 3.7重量% |
<150μm的颗粒的比例(研磨之后) | 11.2重量% |
>850μm的颗粒的比例(研磨之前) | 34重量% |
在150μm与850μm之间的颗粒的比例(研磨之后) | 88.8重量% |
稳定性值 | 15重量% |
CRC值 | 25.5g/g |
在0.7psi下的AAP值 | 10.6g/g |
可溶部分 | 19.8重量% |
Claims (18)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10334271A DE10334271B4 (de) | 2003-07-25 | 2003-07-25 | Verfahren zur Agglomeration von Superabsorberfeinteilchen, daraus erhältliche Superabsorberpartikel, deren Verwendung sowie diese beinhaltende Verbunde |
DE10334271.0 | 2003-07-25 |
Publications (2)
Publication Number | Publication Date |
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CN1829765A true CN1829765A (zh) | 2006-09-06 |
CN100447184C CN100447184C (zh) | 2008-12-31 |
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Application Number | Title | Priority Date | Filing Date |
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CNB200480021592XA Expired - Lifetime CN100447184C (zh) | 2003-07-25 | 2004-07-22 | 超吸收剂细微颗粒的附聚方法 |
Country Status (9)
Country | Link |
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US (2) | US7776984B2 (zh) |
EP (1) | EP1648956B1 (zh) |
JP (1) | JP4694481B2 (zh) |
CN (1) | CN100447184C (zh) |
AT (1) | ATE357473T1 (zh) |
BR (1) | BRPI0412929A (zh) |
DE (2) | DE10334271B4 (zh) |
TW (1) | TWI367781B (zh) |
WO (1) | WO2005012406A1 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101925623B (zh) * | 2008-01-29 | 2013-11-06 | 巴斯夫欧洲公司 | 生产吸水性聚合物颗粒的方法 |
CN104394895A (zh) * | 2012-04-17 | 2015-03-04 | 巴斯夫欧洲公司 | 制备表面后交联吸水性聚合物颗粒的方法 |
CN106164099A (zh) * | 2014-06-13 | 2016-11-23 | 株式会社Lg化学 | 超吸收性聚合物的制备方法及由其制备的超吸收性聚合物 |
CN106413765A (zh) * | 2014-05-13 | 2017-02-15 | 宝洁公司 | 附聚的超吸收聚合物颗粒 |
CN115558050A (zh) * | 2022-09-27 | 2023-01-03 | 赤壁市高质量发展研究院有限公司 | 一种声学增强材料块、其反相乳液聚合制备方法和应用 |
Families Citing this family (44)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7169843B2 (en) * | 2003-04-25 | 2007-01-30 | Stockhausen, Inc. | Superabsorbent polymer with high permeability |
DE10334271B4 (de) * | 2003-07-25 | 2006-02-23 | Stockhausen Gmbh | Verfahren zur Agglomeration von Superabsorberfeinteilchen, daraus erhältliche Superabsorberpartikel, deren Verwendung sowie diese beinhaltende Verbunde |
EP1769004B1 (de) | 2004-06-21 | 2017-08-09 | Evonik Degussa GmbH | Wasserabsorbierendes polysaccharid sowie ein verfahren zu seiner herstellung |
EP1629854B1 (en) * | 2004-07-20 | 2010-10-13 | The Procter & Gamble Company | Surface cross-linked superabsorbent polymer particles and methods of making them |
SG159540A1 (en) * | 2005-02-15 | 2010-03-30 | Nippon Catalytic Chem Ind | Water absorbing agent, water absorbing article and method for production of water absorbing agent |
US20090068440A1 (en) * | 2005-06-20 | 2009-03-12 | Gunther Bub | Production of acrolein, acrylic acid and water-absorbent polymer structures made from glycerine |
DE102005055497A1 (de) * | 2005-11-18 | 2007-05-31 | Stockhausen Gmbh | Geruchsbindende superabsorbierende Zusammensetzung |
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CN106413765A (zh) * | 2014-05-13 | 2017-02-15 | 宝洁公司 | 附聚的超吸收聚合物颗粒 |
CN106164099A (zh) * | 2014-06-13 | 2016-11-23 | 株式会社Lg化学 | 超吸收性聚合物的制备方法及由其制备的超吸收性聚合物 |
CN106164099B (zh) * | 2014-06-13 | 2018-02-09 | 株式会社Lg化学 | 超吸收性聚合物的制备方法及由其制备的超吸收性聚合物 |
US10023703B2 (en) | 2014-06-13 | 2018-07-17 | Lg Chem, Ltd. | Preparation method of superabsorbent polymer and superabsorbent polymer prepared thereby |
US10208171B2 (en) | 2014-06-13 | 2019-02-19 | Lg Chem, Ltd. | Preparation method of superabsorbent polymer and superabsorbent polymer prepared thereby |
CN115558050A (zh) * | 2022-09-27 | 2023-01-03 | 赤壁市高质量发展研究院有限公司 | 一种声学增强材料块、其反相乳液聚合制备方法和应用 |
CN115558050B (zh) * | 2022-09-27 | 2023-04-11 | 赤壁市高质量发展研究院有限公司 | 一种声学增强材料块、其反相乳液聚合制备方法和应用 |
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EP1648956B1 (de) | 2007-03-21 |
DE502004003295D1 (de) | 2007-05-03 |
BRPI0412929A (pt) | 2006-09-26 |
JP4694481B2 (ja) | 2011-06-08 |
DE10334271B4 (de) | 2006-02-23 |
EP1648956A1 (de) | 2006-04-26 |
US20070015860A1 (en) | 2007-01-18 |
TWI367781B (en) | 2012-07-11 |
DE10334271A1 (de) | 2005-02-24 |
US20100234531A1 (en) | 2010-09-16 |
TW200518833A (en) | 2005-06-16 |
WO2005012406A1 (de) | 2005-02-10 |
JP2006528708A (ja) | 2006-12-21 |
ATE357473T1 (de) | 2007-04-15 |
US8367774B2 (en) | 2013-02-05 |
US7776984B2 (en) | 2010-08-17 |
CN100447184C (zh) | 2008-12-31 |
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