CN1826429B - 使用含过氧化氢的磷酸盐化溶液涂覆金属表面的方法和溶液、制备的金属物品及所述物品的用途 - Google Patents

使用含过氧化氢的磷酸盐化溶液涂覆金属表面的方法和溶液、制备的金属物品及所述物品的用途 Download PDF

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CN1826429B
CN1826429B CN2004800209863A CN200480020986A CN1826429B CN 1826429 B CN1826429 B CN 1826429B CN 2004800209863 A CN2004800209863 A CN 2004800209863A CN 200480020986 A CN200480020986 A CN 200480020986A CN 1826429 B CN1826429 B CN 1826429B
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purposes
ion
salinization
aqueous solution
acid phosphatase
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CN1826429A (zh
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T·尼特施克
R·赖因
E·舍恩费尔德
P·舒巴赫
J·施佩希特
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Chemetall GmbH
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Chemetall GmbH
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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
    • C23C22/364—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/12—Orthophosphates containing zinc cations
    • C23C22/16—Orthophosphates containing zinc cations containing also peroxy-compounds
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C23C22/182—Orthophosphates containing manganese cations containing also zinc cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/07—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing phosphates
    • C23C22/08—Orthophosphates
    • C23C22/18—Orthophosphates containing manganese cations
    • C23C22/182—Orthophosphates containing manganese cations containing also zinc cations
    • C23C22/184—Orthophosphates containing manganese cations containing also zinc cations containing also nickel cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C23C22/36—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates
    • C23C22/364—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations
    • C23C22/365—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides containing also phosphates containing also manganese cations containing also zinc and nickel cations
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/73—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T50/00—Aeronautics or air transport
    • Y02T50/60—Efficient propulsion technologies, e.g. for aircraft

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  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
CN2004800209863A 2003-05-23 2004-05-17 使用含过氧化氢的磷酸盐化溶液涂覆金属表面的方法和溶液、制备的金属物品及所述物品的用途 Expired - Lifetime CN1826429B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10323305A DE10323305B4 (de) 2003-05-23 2003-05-23 Verfahren zur Beschichtung von metallischen Oberflächen mit einer Wasserstoffperoxid enthaltenden Phosphatierungslösung, Phosphatierlösung und Verwendung der behandelten Gegenstände
DE10323305.9 2003-05-23
PCT/EP2004/005282 WO2004104266A1 (de) 2003-05-23 2004-05-17 Verfahren und lösung zur beschichtung von metallischen oberflächen mit einer wasserstoffperoxid enthaltenden phosphatierungslösung, hergestellte metallgenstand und verwendung des gegenstandes

Publications (2)

Publication Number Publication Date
CN1826429A CN1826429A (zh) 2006-08-30
CN1826429B true CN1826429B (zh) 2012-08-08

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CN2004800209863A Expired - Lifetime CN1826429B (zh) 2003-05-23 2004-05-17 使用含过氧化氢的磷酸盐化溶液涂覆金属表面的方法和溶液、制备的金属物品及所述物品的用途

Country Status (13)

Country Link
US (2) US20060278307A1 (enExample)
EP (1) EP1633905B1 (enExample)
JP (1) JP2006528280A (enExample)
CN (1) CN1826429B (enExample)
AT (1) ATE373117T1 (enExample)
AU (1) AU2004241000B2 (enExample)
BR (1) BRPI0410585B1 (enExample)
DE (2) DE10323305B4 (enExample)
DK (1) DK1633905T3 (enExample)
ES (1) ES2294498T3 (enExample)
PT (1) PT1633905E (enExample)
WO (1) WO2004104266A1 (enExample)
ZA (1) ZA200509144B (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005047424A1 (de) * 2005-09-30 2007-04-05 Henkel Kgaa Phosphatierlösung mit Wasserstoffperoxid und chelatbildenden Carbonsäuren
DE102006052919A1 (de) 2006-11-08 2008-05-15 Henkel Kgaa Zr-/Ti-haltige Phosphatierlösung zur Passivierung von Metallverbundoberflächen
KR101272170B1 (ko) * 2006-12-01 2013-06-10 니혼 파커라이징 가부시키가이샤 고 과산화물 자가석출 바스
DE102008000600B4 (de) * 2008-03-11 2010-05-12 Chemetall Gmbh Verfahren zur Beschichtung von metallischen Oberflächen mit einem Passivierungsmittel, das Passivierungsmittel, die hiermit erzeugte Beschichtung und ihre Verwendung
DE102008038653A1 (de) 2008-08-12 2010-03-25 Henkel Ag & Co. Kgaa Sukzessive korrosionsschützende Vorbehandlung von Metalloberflächen in einem Mehrstufenprozess
IT1397902B1 (it) * 2010-01-26 2013-02-04 Np Coil Dexter Ind Srl Processi di pretrattamento alla verniciatura, a basso impatto ambientale, alternativi ai trattamenti tradizionali di fosfatazione.
DE102010030697A1 (de) * 2010-06-30 2012-01-05 Henkel Ag & Co. Kgaa Verfahren zur selektiven Phosphatierung einer Verbundmetallkonstruktion
PL2503025T3 (pl) * 2011-03-22 2013-12-31 Henkel Ag & Co Kgaa Chroniąca przed korozją, wielostopniowa obróbka metalowych elementów konstrukcyjnych o powierzchniach cynkowych
CN103422082B (zh) * 2012-05-17 2017-07-18 中化化工科学技术研究总院 钕铁硼磁性材料锌系磷化液及其使用方法
EP3280830B1 (de) * 2015-04-07 2021-03-31 Chemetall GmbH Verfahren zur gezielten einstellung der elektrischen leitfähigkeit von konversionsbeschichtungen
CN119194461A (zh) 2016-08-24 2024-12-27 Ppg工业俄亥俄公司 用于处理金属基材的碱性组合物
EP3392375B1 (de) * 2017-04-21 2019-11-06 Henkel AG & Co. KGaA Verfahren zur schlammfreien schichtbildenden zinkphosphatierung von metallischen bauteilen in serie
EP3392376A1 (de) 2017-04-21 2018-10-24 Henkel AG & Co. KGaA Verfahren zur schichtbildenden zinkphosphatierung von metallischen bauteilen in serie
WO2019158508A1 (de) * 2018-02-19 2019-08-22 Chemetall Gmbh Verfahren zur selektiven phosphatierung einer verbundmetallkonstruktion
CN108342723B (zh) * 2018-03-19 2020-02-07 常州市春雷浩宇环保科技有限公司 一种适用于锌系磷化液的无渣促进剂
FR3090694B1 (fr) * 2018-12-20 2023-05-26 Univ De Pau Et Des Pays De Ladour Solution de traitement anticorrosion et utilisations
CN115428129A (zh) * 2020-04-14 2022-12-02 三菱瓦斯化学株式会社 钛和/或钛合金的蚀刻液、使用该蚀刻液的钛和/或钛合金的蚀刻方法、以及使用该蚀刻液的基板的制造方法
CA3201412A1 (en) * 2020-12-22 2022-06-30 M-M-Morant-Gmbh Chromium(vi)-free coating agent for metals
CN112899672B (zh) * 2021-01-14 2023-03-17 厦门腾兴隆化工有限公司 一种黑色磷化剂及其制备方法

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US6379474B1 (en) * 1997-08-06 2002-04-30 Henkel Kommanditgesellschaft Auf Aktien Phosphating method accelerated by N-oxides
WO2002070781A2 (de) * 2001-03-06 2002-09-12 Chemetall Gmbh Verfahren zum aufbringen eines phosphatüberzuges und verwendung der derart phosphatierten metallteile
WO2002070782A2 (de) * 2001-03-06 2002-09-12 Chemetall Gmbh Verfahren zur beschichtung von metallischen oberflächen und verwendung der derart beschichteten substrate
CN1372602A (zh) * 2000-03-07 2002-10-02 坎梅陶尔股份有限公司 涂敷磷酸盐覆层的方法和磷酸盐化金属部件的应用

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DE4306446A1 (de) * 1993-03-02 1994-09-08 Metallgesellschaft Ag Verfahren zur Erleichterung der Kaltumformung
JPH08302477A (ja) * 1994-12-06 1996-11-19 Nippon Parkerizing Co Ltd 金属材料用りん酸亜鉛系化成処理液および処理方法
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DE19958192A1 (de) * 1999-12-02 2001-06-07 Henkel Kgaa Verfahren zur Phosphatierung, Nachspülung und kathodischer Elektrotauchlackierung
CA2358625A1 (en) * 2000-10-10 2002-04-10 Henkel Corporation Phosphate conversion coating
DE10118552A1 (de) * 2001-04-14 2002-10-17 Henkel Kgaa Bestimmung der Beschleunigerkonzentration in Phosphatierbäder
DE10155976A1 (de) * 2001-11-14 2003-05-22 Henkel Kgaa Steuerung der Beschleunigerkonzentration in Phosphatierbäder
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US6379474B1 (en) * 1997-08-06 2002-04-30 Henkel Kommanditgesellschaft Auf Aktien Phosphating method accelerated by N-oxides
CN1372602A (zh) * 2000-03-07 2002-10-02 坎梅陶尔股份有限公司 涂敷磷酸盐覆层的方法和磷酸盐化金属部件的应用
WO2002070781A2 (de) * 2001-03-06 2002-09-12 Chemetall Gmbh Verfahren zum aufbringen eines phosphatüberzuges und verwendung der derart phosphatierten metallteile
WO2002070782A2 (de) * 2001-03-06 2002-09-12 Chemetall Gmbh Verfahren zur beschichtung von metallischen oberflächen und verwendung der derart beschichteten substrate

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AU2004241000A1 (en) 2004-12-02
ZA200509144B (en) 2007-03-28
AU2004241000B2 (en) 2009-05-14
BRPI0410585B1 (pt) 2014-09-16
PT1633905E (pt) 2007-12-20
CN1826429A (zh) 2006-08-30
ES2294498T3 (es) 2008-04-01
EP1633905A1 (de) 2006-03-15
DE10323305B4 (de) 2006-03-30
WO2004104266A1 (de) 2004-12-02
DE502004004961D1 (de) 2007-10-25
JP2006528280A (ja) 2006-12-14
ATE373117T1 (de) 2007-09-15
BRPI0410585A (pt) 2006-06-20
US20060278307A1 (en) 2006-12-14
DE10323305A1 (de) 2004-12-16
DK1633905T3 (da) 2008-01-14
US20110180186A1 (en) 2011-07-28
EP1633905B1 (de) 2007-09-12

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