CN1790568B - 电介质陶瓷组合物、电子部件和它们的制造方法 - Google Patents
电介质陶瓷组合物、电子部件和它们的制造方法 Download PDFInfo
- Publication number
- CN1790568B CN1790568B CN 200410095402 CN200410095402A CN1790568B CN 1790568 B CN1790568 B CN 1790568B CN 200410095402 CN200410095402 CN 200410095402 CN 200410095402 A CN200410095402 A CN 200410095402A CN 1790568 B CN1790568 B CN 1790568B
- Authority
- CN
- China
- Prior art keywords
- dielectric
- ceramic composition
- oxide
- dielectric ceramic
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 221
- 239000000919 ceramic Substances 0.000 title claims abstract description 107
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 32
- 238000005245 sintering Methods 0.000 claims abstract description 94
- 239000011521 glass Substances 0.000 claims abstract description 92
- 239000002245 particle Substances 0.000 claims abstract description 44
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 claims abstract description 37
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 28
- 229910004298 SiO 2 Inorganic materials 0.000 claims abstract description 25
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 18
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 15
- XLOMVQKBTHCTTD-UHFFFAOYSA-N zinc oxide Inorganic materials [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052788 barium Inorganic materials 0.000 claims abstract description 10
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 10
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 9
- 229910052712 strontium Inorganic materials 0.000 claims abstract description 9
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 9
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 7
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 7
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 7
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 7
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 7
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 7
- 229910011255 B2O3 Inorganic materials 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims description 62
- 238000000034 method Methods 0.000 claims description 44
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 21
- 229910052750 molybdenum Inorganic materials 0.000 claims description 19
- 229910052758 niobium Inorganic materials 0.000 claims description 19
- 229910052715 tantalum Inorganic materials 0.000 claims description 19
- 229910052721 tungsten Inorganic materials 0.000 claims description 19
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 18
- 238000006243 chemical reaction Methods 0.000 claims description 13
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 claims description 12
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 12
- 229910001935 vanadium oxide Inorganic materials 0.000 claims description 12
- 239000010953 base metal Substances 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 4
- 238000003746 solid phase reaction Methods 0.000 claims 2
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 claims 1
- 229910052720 vanadium Inorganic materials 0.000 claims 1
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 abstract description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical group [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 239000012298 atmosphere Substances 0.000 description 26
- 239000003990 capacitor Substances 0.000 description 22
- 239000013078 crystal Substances 0.000 description 19
- 238000000137 annealing Methods 0.000 description 17
- 238000001354 calcination Methods 0.000 description 16
- 239000007789 gas Substances 0.000 description 16
- 238000009413 insulation Methods 0.000 description 16
- 239000011230 binding agent Substances 0.000 description 12
- 230000014759 maintenance of location Effects 0.000 description 12
- 239000003985 ceramic capacitor Substances 0.000 description 11
- 238000010304 firing Methods 0.000 description 11
- 239000004020 conductor Substances 0.000 description 10
- 238000011282 treatment Methods 0.000 description 10
- 239000000843 powder Substances 0.000 description 9
- 239000000758 substrate Substances 0.000 description 9
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 8
- 239000001301 oxygen Substances 0.000 description 8
- 229910052760 oxygen Inorganic materials 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 230000007423 decrease Effects 0.000 description 7
- 238000002844 melting Methods 0.000 description 7
- 230000008018 melting Effects 0.000 description 7
- 229910052573 porcelain Inorganic materials 0.000 description 7
- 229910000990 Ni alloy Inorganic materials 0.000 description 6
- 239000003989 dielectric material Substances 0.000 description 6
- 229910052759 nickel Inorganic materials 0.000 description 6
- 230000009467 reduction Effects 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 4
- 239000000956 alloy Substances 0.000 description 4
- 230000006866 deterioration Effects 0.000 description 4
- 229940028356 diethylene glycol monobutyl ether Drugs 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000011572 manganese Substances 0.000 description 4
- JCGNDDUYTRNOFT-UHFFFAOYSA-N oxolane-2,4-dione Chemical compound O=C1COC(=O)C1 JCGNDDUYTRNOFT-UHFFFAOYSA-N 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 238000010532 solid phase synthesis reaction Methods 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- 239000001856 Ethyl cellulose Substances 0.000 description 3
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 3
- 229910010413 TiO 2 Inorganic materials 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000011248 coating agent Substances 0.000 description 3
- 238000000576 coating method Methods 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 229920001249 ethyl cellulose Polymers 0.000 description 3
- 235000019325 ethyl cellulose Nutrition 0.000 description 3
- 239000007791 liquid phase Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000003973 paint Substances 0.000 description 3
- 230000009257 reactivity Effects 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 239000004925 Acrylic resin Substances 0.000 description 2
- 229920000178 Acrylic resin Polymers 0.000 description 2
- 229920002799 BoPET Polymers 0.000 description 2
- 101100513612 Microdochium nivale MnCO gene Proteins 0.000 description 2
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 2
- -1 carbonates Chemical class 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 238000000280 densification Methods 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000003475 lamination Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 238000004017 vitrification Methods 0.000 description 2
- 239000003232 water-soluble binding agent Substances 0.000 description 2
- DURPTKYDGMDSBL-UHFFFAOYSA-N 1-butoxybutane Chemical compound CCCCOCCCC DURPTKYDGMDSBL-UHFFFAOYSA-N 0.000 description 1
- 229910000881 Cu alloy Inorganic materials 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910000807 Ga alloy Inorganic materials 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 229910001252 Pd alloy Inorganic materials 0.000 description 1
- 229910002367 SrTiO Inorganic materials 0.000 description 1
- 241000779819 Syncarpia glomulifera Species 0.000 description 1
- 229940022682 acetone Drugs 0.000 description 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000007772 electrode material Substances 0.000 description 1
- 239000002003 electrode paste Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 229910052747 lanthanoid Inorganic materials 0.000 description 1
- 150000002602 lanthanoids Chemical class 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- PPNAOCWZXJOHFK-UHFFFAOYSA-N manganese(2+);oxygen(2-) Chemical class [O-2].[Mn+2] PPNAOCWZXJOHFK-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000002902 organometallic compounds Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000001739 pinus spp. Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 description 1
- 238000010405 reoxidation reaction Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 229910052706 scandium Inorganic materials 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 238000005476 soldering Methods 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000003836 solid-state method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 229940036248 turpentine Drugs 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
Landscapes
- Inorganic Insulating Materials (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Ceramic Capacitors (AREA)
- Fixed Capacitors And Capacitor Manufacturing Machines (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP420609/03 | 2003-12-18 | ||
| JP2003420609A JP4267438B2 (ja) | 2003-12-18 | 2003-12-18 | 誘電体磁器組成物、電子部品及びこれらの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1790568A CN1790568A (zh) | 2006-06-21 |
| CN1790568B true CN1790568B (zh) | 2010-06-09 |
Family
ID=34782081
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410095402 Expired - Lifetime CN1790568B (zh) | 2003-12-18 | 2004-12-17 | 电介质陶瓷组合物、电子部件和它们的制造方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP4267438B2 (enrdf_load_stackoverflow) |
| CN (1) | CN1790568B (enrdf_load_stackoverflow) |
| TW (1) | TW200529261A (enrdf_load_stackoverflow) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7923395B2 (en) | 2005-04-07 | 2011-04-12 | Kemet Electronics Corporation | C0G multi-layered ceramic capacitor |
| JP4809036B2 (ja) * | 2005-10-27 | 2011-11-02 | 京セラ株式会社 | 積層セラミックコンデンサおよびその製法 |
| JP4678022B2 (ja) * | 2007-11-26 | 2011-04-27 | Ｔｄｋ株式会社 | 誘電体磁器組成物の製造方法 |
| JP2010040798A (ja) | 2008-08-06 | 2010-02-18 | Murata Mfg Co Ltd | 積層セラミックコンデンサ |
| JP5532505B2 (ja) * | 2009-07-23 | 2014-06-25 | 日本電気硝子株式会社 | コンデンサー用ガラスフィルム |
| JP6076331B2 (ja) * | 2012-03-19 | 2017-02-08 | 株式会社村田製作所 | セラミック電子部品 |
| JP7099212B2 (ja) * | 2018-09-13 | 2022-07-12 | Tdk株式会社 | 誘電体組成物および電子部品 |
| JP7196484B2 (ja) * | 2018-09-13 | 2022-12-27 | Tdk株式会社 | 誘電体組成物および電子部品 |
| CN113457668B (zh) * | 2020-03-31 | 2023-08-08 | 中国石油化工股份有限公司 | 一种高比热容基质材料及其制备方法与应用 |
| US12051545B2 (en) | 2021-08-02 | 2024-07-30 | Taiyo Yuden Co., Ltd. | Ceramic electronic device including dielectric layer containing perovskite compound with yttria-stabilized zirconia, and manufacturing method of same |
| JP2023136757A (ja) | 2022-03-17 | 2023-09-29 | 太陽誘電株式会社 | セラミック電子部品、誘電体材料、及びセラミック電子部品の製造方法 |
| CN115340376B (zh) * | 2022-06-28 | 2023-08-08 | 清华大学深圳国际研究生院 | 一种ltcc用陶瓷基板及其制备方法和应用 |
| CN118545997B (zh) * | 2024-07-24 | 2024-09-24 | 湖南省新化县鑫星电子陶瓷有限责任公司 | 一种高介电性能电子陶瓷及其制备方法 |
| CN119661212A (zh) * | 2024-12-09 | 2025-03-21 | 华南理工大学 | 一种低温烧结且低损耗的锰锌铁氧体材料及其制备方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1317459A (zh) * | 2000-04-07 | 2001-10-17 | 株式会社村田制作所 | 非还原性介电陶瓷和使用该陶瓷的单块陶瓷电容器 |
| CN1359874A (zh) * | 2000-12-20 | 2002-07-24 | 松下电器产业株式会社 | 电介质瓷器组合物和电介质器件 |
-
2003
- 2003-12-18 JP JP2003420609A patent/JP4267438B2/ja not_active Expired - Lifetime
-
2004
- 2004-12-03 TW TW93137351A patent/TW200529261A/zh not_active IP Right Cessation
- 2004-12-17 CN CN 200410095402 patent/CN1790568B/zh not_active Expired - Lifetime
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1317459A (zh) * | 2000-04-07 | 2001-10-17 | 株式会社村田制作所 | 非还原性介电陶瓷和使用该陶瓷的单块陶瓷电容器 |
| CN1359874A (zh) * | 2000-12-20 | 2002-07-24 | 松下电器产业株式会社 | 电介质瓷器组合物和电介质器件 |
Also Published As
| Publication number | Publication date |
|---|---|
| TW200529261A (en) | 2005-09-01 |
| TWI326092B (enrdf_load_stackoverflow) | 2010-06-11 |
| JP4267438B2 (ja) | 2009-05-27 |
| CN1790568A (zh) | 2006-06-21 |
| JP2005179105A (ja) | 2005-07-07 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20100609 |