CN1317001A - 制备脱水糖醇的连续方法 - Google Patents

制备脱水糖醇的连续方法 Download PDF

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Publication number
CN1317001A
CN1317001A CN99810737A CN99810737A CN1317001A CN 1317001 A CN1317001 A CN 1317001A CN 99810737 A CN99810737 A CN 99810737A CN 99810737 A CN99810737 A CN 99810737A CN 1317001 A CN1317001 A CN 1317001A
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CN
China
Prior art keywords
reaction product
reaction
solvent
alcohol
organic solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN99810737A
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English (en)
Chinese (zh)
Inventor
W·C·布里尼加
M·沃勒尔斯
M·A·胡巴德
E·G·蔡
G·克瓦科夫斯茨基
T·H·肖克利
R·雷斯基
U·丁格尔迪森
W·金德
N·科勒
J·里斯
M·汤姆兹克
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EIDP Inc
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EI Du Pont de Nemours and Co
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Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Publication of CN1317001A publication Critical patent/CN1317001A/zh
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/02—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
    • C07D493/04—Ortho-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/04—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members
    • C07D307/18—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having no double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/20—Oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66—Polyesters containing oxygen in the form of ether groups
    • C08G63/668—Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672—Dicarboxylic acids and dihydroxy compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Polyethers (AREA)
  • Saccharide Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN99810737A 1998-09-09 1999-01-11 制备脱水糖醇的连续方法 Pending CN1317001A (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19841032.8 1998-09-09
DE19841032A DE19841032A1 (de) 1998-09-09 1998-09-09 Verfahren zur Herstellung von Anhydrozuckeralkoholen

Publications (1)

Publication Number Publication Date
CN1317001A true CN1317001A (zh) 2001-10-10

Family

ID=7880252

Family Applications (1)

Application Number Title Priority Date Filing Date
CN99810737A Pending CN1317001A (zh) 1998-09-09 1999-01-11 制备脱水糖醇的连续方法

Country Status (11)

Country Link
EP (1) EP1119558A4 (de)
JP (1) JP2002524455A (de)
KR (1) KR20010079763A (de)
CN (1) CN1317001A (de)
AU (1) AU2111299A (de)
BR (1) BR9913612A (de)
CA (1) CA2340348A1 (de)
DE (1) DE19841032A1 (de)
ID (1) ID28701A (de)
TR (1) TR200100701T2 (de)
WO (1) WO2000014081A1 (de)

Cited By (8)

* Cited by examiner, † Cited by third party
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CN103649095A (zh) * 2011-06-02 2014-03-19 株式会社三养吉尼克斯 制备脱水糖醇的方法
CN104736507A (zh) * 2012-10-15 2015-06-24 株式会社三养吉尼克斯 无水糖醇的制备方法
CN104788465A (zh) * 2015-02-10 2015-07-22 沈阳化工大学 一种由山梨醇制异山梨醇的连续化制备方法
CN105073753A (zh) * 2013-02-22 2015-11-18 株式会社三养吉尼克斯 通过氢化糖的连续脱水反应制备无水糖醇的方法
CN105418624A (zh) * 2006-03-09 2016-03-23 阿彻-丹尼尔斯-米德兰公司 脱水糖醇的生产方法
CN106478650A (zh) * 2015-08-26 2017-03-08 Sk新技术株式会社 使用水蒸气产生脱水糖醇的方法
CN106478649A (zh) * 2015-08-26 2017-03-08 Sk新技术株式会社 通过两步反应制备脱水糖醇的方法
CN109134485A (zh) * 2017-06-16 2019-01-04 中国科学院大连化学物理研究所 一种制备异山梨醇的方法

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* Cited by examiner, † Cited by third party
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WO2001092266A2 (en) * 2000-05-26 2001-12-06 E.I. Dupont De Nemours And Company Process for the manufacture of anhydro sugar alcohols
CN1430619A (zh) * 2000-05-26 2003-07-16 纳幕尔杜邦公司 制备脱水糖醇的连续法及其使用的反应器
FR2810040B1 (fr) * 2000-06-09 2004-04-09 Roquette Freres Procede de purification d'une composition contenant au moins un produit de deshydratation interne d'un sucre hydrogene
KR100772255B1 (ko) * 2000-06-09 2007-11-01 로께뜨프레르 수소화 당의 내부 탈수물을 1종 이상 함유하는 조성물의정제 방법
US6849748B2 (en) 2000-11-01 2005-02-01 Archer-Daniels-Midland Company Process for the production of anhydrosugar alcohols
US7439352B2 (en) 2000-11-01 2008-10-21 Archer-Daniels-Midland Company Process for the production of anhydrosugar alcohols
FR2832407B1 (fr) * 2001-11-20 2005-07-01 Roquette Freres Procede de preparation d'une composition contenant au moins un produit de deshydratation interne d'un sucre hydrogene
US6831181B2 (en) * 2002-04-17 2004-12-14 E. I. Dupont De Nemours And Co. High yield byproduct recycle process for anhydro sugar alcohols
US6818781B2 (en) * 2002-04-17 2004-11-16 E. I. Du Pont De Nemours And Company Simultaneous reaction and separation process for the manufacture of dianhydro sugar alcohols
US6867296B2 (en) 2002-04-17 2005-03-15 E. I. Du Pont De Nemours And Company Recovery and purification of anhydro sugar alcohols from a vapor stream
US6864378B2 (en) 2002-04-17 2005-03-08 E. I. Du Pont De Nemours And Company Integrated continuous process for anhydro sugar alcohol manufacture
US7728156B2 (en) 2006-01-26 2010-06-01 Battelle Memorial Institute Method of performing sugar dehydration and catalyst treatment
US7615652B2 (en) 2006-01-26 2009-11-10 Battelle Memorial Institute Two-stage dehydration of sugars
US7772412B2 (en) * 2006-01-26 2010-08-10 Battelle Memorial Institute Methods for dehydration of sugars and sugar alcohols
US7649099B2 (en) 2006-01-26 2010-01-19 Battelle Memorial Institute Method of forming a dianhydrosugar alcohol
GB0713598D0 (en) * 2007-07-13 2007-08-22 Ici Ltd Cyclic ethers
JP5635228B2 (ja) * 2008-02-18 2014-12-03 帝人株式会社 ポリカーボネート樹脂組成物
JP5635227B2 (ja) * 2008-02-18 2014-12-03 帝人株式会社 光拡散性ポリカーボネート樹脂組成物
EP2100972A1 (de) 2008-03-13 2009-09-16 BIOeCON International Holding N.V. Verfahren zum Umwandeln von Polysacchariden in einem geschmolzenen Salzhydrat
US9765084B2 (en) 2008-04-10 2017-09-19 Iowa Corn Promotion Board Recovery and refining of dianhydrosugars
US9120806B2 (en) * 2008-04-10 2015-09-01 Iowa Corn Promotion Board Dianhydrosugar production process
WO2010106052A1 (en) 2009-03-17 2010-09-23 Bioecon International Holding N.V. Process for converting polysaccharides in an inorganic molten salt hydrate
EP2408937A1 (de) 2009-03-17 2012-01-25 BIOeCON International Holding N.V. Verfahren zur umwandlung von polysacchariden in ein anorganisches geschmolzenes salzhydrat
BRPI1009270A2 (pt) 2009-03-17 2016-05-03 Bioecon Int Holding Nv processo para converter um material contendo polissacarídeo a um aditivo de combustível ou a um material substituto de combustível, e, uso de açúcares dianidro derivados
EP2408782A1 (de) 2009-03-17 2012-01-25 BIOeCON International Holding N.V. Verfahren zur umwandlung von polysacchariden in ein anorganisches geschmolzenes salzhydrat
US9090550B2 (en) 2010-07-30 2015-07-28 Archer Daniels Midland Company Microwave assisted synthesis of dehydrated sugar derivatives hydroxymethylfurfural, levulinic acid, anhydrosugar alcohols, and ethers thereof
KR101172615B1 (ko) * 2010-12-15 2012-08-08 주식회사 삼양제넥스 무수당 알코올의 증류 방법 및 이를 이용한 무수당 알코올의 제조 방법
EP2615093A1 (de) 2012-01-16 2013-07-17 BIOeCON International Holding N.V. Isolierung von anhydro Zucker Hexitols mittels selektiven Adsorbentien
KR101388676B1 (ko) 2012-05-11 2014-04-25 주식회사 삼양제넥스 박막증류를 통한 고순도 무수당 알코올의 제조방법
CA2889661C (en) 2012-10-31 2019-07-02 Archer Daniels Midland Company Improved method of making internal dehydration products of sugar alcohols
KR101455740B1 (ko) 2012-11-08 2014-11-04 주식회사 삼양제넥스 결정화 공정 폐기물을 사용하여 수율을 항상시킨 고순도 무수당 알코올의 제조방법
KR101452903B1 (ko) * 2012-11-08 2014-10-23 주식회사 삼양제넥스 결정화 공정 폐기물의 재결정물을 사용하여 수율을 항상시킨 고순도 무수당 알코올의 제조방법
KR101475388B1 (ko) 2012-12-14 2014-12-23 주식회사 삼양제넥스 하이드롤을 이용한 무수당 알코올의 제조방법
KR101624567B1 (ko) * 2013-02-22 2016-05-26 주식회사 삼양사 박막증류에 이은 컬럼증류를 채택한 단일 증류단계를 포함하는 고순도 무수당 알코올의 제조방법
JP6347545B2 (ja) * 2014-07-16 2018-06-27 国立大学法人北海道大学 糖アルコールの脱水用固体触媒、およびその触媒を使用する二無水糖アルコールの製造方法。
KR102280247B1 (ko) * 2014-10-16 2021-07-21 에스케이이노베이션 주식회사 공비증류를 이용한 무수당 알코올의 제조방법
KR102299182B1 (ko) * 2014-10-16 2021-09-08 에스케이이노베이션 주식회사 고압 반응에 의한 무수당 알코올의 제조방법
US10752638B2 (en) 2014-10-16 2020-08-25 Sk Innovation Co., Ltd. Method for producing anhydrosugar alcohol by high-pressure reaction
KR20160077000A (ko) 2014-12-23 2016-07-01 에스케이이노베이션 주식회사 무수당 알코올의 효과적인 생산 및 정제 방법
KR20160076999A (ko) * 2014-12-23 2016-07-01 에스케이이노베이션 주식회사 무수당 알코올의 연속적인 생산방법
ES2827527T3 (es) 2015-02-24 2021-05-21 Archer Daniels Midland Co Fabricación y purificación de isoididas
JP6852263B2 (ja) * 2016-02-08 2021-03-31 三菱ケミカル株式会社 アンヒドロ糖アルコールの製造方法
FR3048970B1 (fr) 2016-03-16 2019-07-19 Roquette Freres Procede de fabrication de dianhydrohexitol avec une etape de distillation sur un evaporateur a couche mince
FR3050456B1 (fr) 2016-04-25 2018-04-27 Roquette Freres Procede de fabrication de cristaux de dianhydrohexitol avec une etape d'evapocristallisation des eaux meres de premiere cristallisation
KR102238298B1 (ko) * 2020-02-27 2021-04-12 주식회사 삼양사 무수당 알코올의 디에테르를 고순도로 정제하는 방법
KR102152693B1 (ko) * 2020-02-28 2020-09-08 주식회사 삼양사 수율이 개선된 무수당 알코올의 디에테르 제조 방법

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105418624A (zh) * 2006-03-09 2016-03-23 阿彻-丹尼尔斯-米德兰公司 脱水糖醇的生产方法
CN103649095B (zh) * 2011-06-02 2016-01-20 株式会社三养吉尼克斯 制备脱水糖醇的方法
CN103649095A (zh) * 2011-06-02 2014-03-19 株式会社三养吉尼克斯 制备脱水糖醇的方法
CN104736507A (zh) * 2012-10-15 2015-06-24 株式会社三养吉尼克斯 无水糖醇的制备方法
CN104736507B (zh) * 2012-10-15 2019-05-21 株式会社三养社 无水糖醇的制备方法
CN105073753B (zh) * 2013-02-22 2017-04-26 株式会社三养社 通过氢化糖的连续脱水反应制备无水糖醇的方法
CN105073753A (zh) * 2013-02-22 2015-11-18 株式会社三养吉尼克斯 通过氢化糖的连续脱水反应制备无水糖醇的方法
CN104788465A (zh) * 2015-02-10 2015-07-22 沈阳化工大学 一种由山梨醇制异山梨醇的连续化制备方法
CN106478650A (zh) * 2015-08-26 2017-03-08 Sk新技术株式会社 使用水蒸气产生脱水糖醇的方法
CN106478649A (zh) * 2015-08-26 2017-03-08 Sk新技术株式会社 通过两步反应制备脱水糖醇的方法
CN106478649B (zh) * 2015-08-26 2019-05-28 Sk新技术株式会社 通过两步反应制备脱水糖醇的方法
CN106478650B (zh) * 2015-08-26 2019-06-04 Sk新技术株式会社 使用水蒸气产生脱水糖醇的方法
CN109134485A (zh) * 2017-06-16 2019-01-04 中国科学院大连化学物理研究所 一种制备异山梨醇的方法

Also Published As

Publication number Publication date
JP2002524455A (ja) 2002-08-06
CA2340348A1 (en) 2000-03-16
TR200100701T2 (tr) 2001-07-23
EP1119558A4 (de) 2002-01-09
EP1119558A1 (de) 2001-08-01
AU2111299A (en) 2000-03-27
ID28701A (id) 2001-06-28
WO2000014081A1 (en) 2000-03-16
DE19841032A1 (de) 2000-03-16
BR9913612A (pt) 2001-10-30
KR20010079763A (ko) 2001-08-22

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