CN1287787A - Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor - Google Patents
Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor Download PDFInfo
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- CN1287787A CN1287787A CN 00129782 CN00129782A CN1287787A CN 1287787 A CN1287787 A CN 1287787A CN 00129782 CN00129782 CN 00129782 CN 00129782 A CN00129782 A CN 00129782A CN 1287787 A CN1287787 A CN 1287787A
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Abstract
The present invention relates to the preparation of plant bactericidal insecticide prepared by using traditional Chinese medicinal herbs including rhizoma coptitis, herba houttuyniae, herba menthae, rhubarb, herba plantaginis as material and through cutting, roasting, grinding, extracting, concentrating, blending, etc. The invented product is high in effect, low in toxicity and low in cost. It can beused to treat plant disease and insect pests, such as cotton bollworh, beet armyworm, pieria rapae etc. The pesticide effect can last up to 15-20 days.
Description
The invention belongs to a kind of is plant sterilization insecticide and the production method thereof that raw material is made with the Chinese herbal medicine.
Traditional bactericide such as copper acetate, carbendazim, captan, zineb, Triadimenol etc., insecticide such as ethion, thimet, Rogor, dichlorvos, its shortcoming is that toxicity is big, disease is developed immunity to drugs, and the prevention and elimination of disease and pests effect descends, particularly chemical residual harm person poultry safety, environmental pollution is serious, it is disabled that many medicines have, and the another one reason is the pesticide price height, and the peasant can't accept.
The object of the present invention is to provide a kind of efficient, low toxicity, environmentally safe haves a sense of security to people and animals, and low Chinese herbal medicine sterilization worm agent and the production method thereof of cost.
A kind of Chinese herbal medicine sterilizing insecticide is characterized in that being raw material by traditional Chinese medicine monarch, minister, the compatibility program helping, make with the coptis, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain, is mixed with medicament with following percentage by weight:
Coptis 20--40% cordate houttuynia 15--30%
Peppermint 10--20% rheum officinale 10--20%
Asiatic plantain 5--15
%
The production method of Chinese herbal medicine sterilizing insecticide is characterized in that being made up of the following step by the drug matching synthetic method: section
The coptis, cordate houttuynia, peppermint, rheum officinale, the Asiatic plantain of drying are processed respectively in flakes earlier and joint; Concoct
Drying is processed into the coptis 20--40 gram of joint, squirts for 10 milliliters with 35 degree liquor, dry in the air half-dried after, pour into to do in the pot and fry, do and fry 80--120 ℃ of temperature, the dried stir-fry time is 40-60 minute, coptis top layer is isabelline being advisable;
Drying is processed into the cordate houttuynia 15--30 gram of joint, add 10 milliliters of vinegars after, fried 30--50 minute with pouring into after mixing to do in the pot, do and fry 50--65 ℃ of temperature, play pot when waiting cordate houttuynia to fry into yellowish-brown;
Drying is processed into the thin He 10--20 gram of joint, adds and contains 40
%15 milliliters of saline solutions, dry in the air half-dried after, pour into to do in the pot and fried 60--80 minute, do and fry 40--55 ℃ of a temperature;
The rheum officinale 10--20 gram that dry processing is in blocks adds 15 milliliters of 30% camphor wine, cooks after drying, and doing and frying temperature is 50--60 ℃, does 50--60 minute stir-fry time;
Drying is processed into the Asiatic plantain 5--15 gram of joint, adds 10 milliliters in the rice wine of fermentation, dries in the air to cook after half-dried, and doing and frying temperature is 40--60 ℃, does 30-50 minute stir-fry time; Pulverize
The coptis of concocting, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain are ground into 160--200 purpose fine powder with ball mill respectively, put into the bag of the coptis, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain interior standby respectively; Extract
Respectively the coptis that is ground into powder, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain are respectively added 10--12 times of heavy water of raw material, pour in the extractor at normal temperatures, be heated to 60--110 ℃, be 80--120 minute heat time heating time, filter again,, pour into respectively in the fermentation vat of each label the coptis soup, cordate houttuynia soup, peppermint soup, rheum officinale soup, the Asiatic plantain soup that filter, fermented 15--20 days, fermentation vat often keeps 25--30 ℃; Concentrate
Coptis soup after the fermentation, cordate houttuynia soup, peppermint soup, rheum officinale soup, Asiatic plantain soup, per respectively 100 milliliters of soups add 0.2 milliliter of sulfuric acid and concentrate, and concentration time is 20--40 minute, and post precipitation is standby; Synthetic
Soup behind concentrating and precipitating, by coptis 20--40%, cordate houttuynia 15--30
%, peppermint 10--20
%, rheum officinale 10--20%, Asiatic plantain 5--15
%, percentage by weight carries out compatibility and becomes sterilizing insecticide, and synthetic is to carry out in synthesis reactor, need stir when synthetic 10 minutes, and mixing speed is 1200 rev/mins, and canning sealing becomes product to precipitate 2-4 hour again.
In the medicament of the present invention, the coptis contains a large amount of berberines, and virus is had the inhibition effect, and the coptis have insecticidal effect, cordate houttuynia contains large number of biological alkali, control influenza to people and play sizable effect, fish raw meat ketone has the stomach toxicity spread effect, peppermint contain the sterilization of a large amount of menthols and lotus alcohol pest-resistant attack effect, peppermint oil has the flavor of delicate fragrance, can lure and draw insect's food-taking, rheum officinale contains the effect that a large amount of yellow ammonium elements, yellow ammonium alkali and yellow ammonium ketone not only can be used as sterilization and disinsection, and the various diseases that can also treat people.Asiatic plantain includes the preceding acid of very high car, the preceding ketone of car, is the disease-resistant guide agent of sterilization, and the present invention forms with above-mentioned various material combinations simultaneously, can produce phytotoxin, and sterilizing power is strong.
Advantage of the present invention: one, efficient sterilizing, desinsection, can trap and kill cotton bollworm, beet armyworm, imported cabbageworm, and the low aqua product of oily content, spray strong adhesion on plant stem-leaf, be easy to by plant absorbing, drug effect was 15--20 days, can trap and kill the extremely strong big instar larvae of Noctuidae 5--6 pesticide resistance in age.Two, can prevent and treat tobacco mosaic, pepper virus disease, cotton cotton bollworm, beet armyworm.Three, with the Chinese herbal medicine be raw material production, low toxicity, pollute for a short time that to the person poultry safety, environmental pollution is few.Four, cost is low, and herbal raw material source is wide, and price is low, and five, production technology is simple, equipment is few, and six, product of the present invention be acidity, pH value 5.4--7.4 uses Shi Buhui and causes that crops root, stem, leaf have poisoning.
Embodiment one, the coptis with drying, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain is cut into slices respectively, the coptis 40 grams squirt for 10 milliliters with 35 degree liquor, the half-dried back 50 minutes temperature of dried stir-fry of drying in the air are 100 ℃, cordate houttuynia 30 grams add to pour into after 10 milliliters of vinegars are mixed to do in the pot to be fried 40 minutes, temperature is 60 ℃, peppermint 15 gram adds and contains 15 milliliters of 40% saline solutions, pour into after drying to do in the pot and fried 70 minutes, baking temperature is 50 ℃, rheum officinale 10 grams, add 15 milliliters of 30% camphor wine, drying in the air cooks after half-dried does and fried 50 minutes, temperature is 55 ℃, Asiatic plantain 5 grams, 10 milliliters in the rice wine that adds fermentation, cook after drying to do and fried 40 minutes, temperature is 50 ℃, the coptis of the above-mentioned process of preparing Chinese medicine, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain is broken into 180 purpose fine powders with ball mill respectively, be divided in the bag standby, the coptis that is ground into powder, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain respectively adds 10 times of heavy water of raw material, pour at normal temperatures and be heated to 100 ℃ in the extractor, be 100 minutes heat time heating time, filters, the coptis soup that filters again, the cordate houttuynia soup, the rheum officinale soup, the Asiatic plantain soup was poured in the fermentation vat of each label fermentation respectively into 18 days, fermentation vat keeps 25 ℃-30 ℃, soup after the fermentation, per respectively 100 milliliters of soups add 0.2 milliliter of sulfuric acid and concentrate concentration time 30 minutes, post precipitation is standby, and the soup behind concentrating and precipitating is by the coptis 40
%, cordate houttuynia 30
%, peppermint 15
%, rheum officinale 10%, Asiatic plantain 5
%In synthesis reactor, synthesize, stirred 10 minutes when synthetic, mixing speed is 1200 rev/mins, filling and sealing becomes product to precipitate 3 hours again, compare with current insecticide with 400 times 800 times of this product dilutions, the contrast medicine is that virus of A bactericide, virus must restrain bactericide, the check plot clear water, test effect saw Table 1, table 2 in 1996
Table 1 Chinese herbal medicine sterilizing insecticide control pepper virus disease field experiment result.
Table 2 Chinese herbal medicine sterilizing insecticide field control tobacco mosaic experimental result
Embodiment two, with the coptis, cordate houttuynia, peppermint, rheum officinale, the Asiatic plantain of drying cut into slices respectively, the coptis 20 gram, squirt for 10 milliliters with 35 degree liquor, it is 80 ℃ that 40 minutes temperature of stir-fry are done in the half-dried back of drying in the air, cordate houttuynia 15 grams add to pour into after 10 milliliters of vinegars are mixed to do in the pot to be fried 30 minutes, baking temperature is 50 ℃, and rheum officinale 10 grams add 15 milliliters of 40% camphor wine, drying in the air cooks after half-dried does and fried 60 minutes, temperature is 40 ℃, and rheum officinale 15 grams add 30
%15 milliliters of camphor wine, drying in the air, half-dried back is dried fried 50 minutes, temperature is 50 ℃, Asiatic plantain 10 grams, 10 milliliters in the rice wine that adds fermentation, dry the back and do stir-fry 30 minutes, temperature is 40 ℃, the coptis of the above-mentioned process of preparing Chinese medicine, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain is broken into 200 purpose fine powders with ball mill respectively, be divided in the bag standby, the coptis that is ground into powder, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain respectively adds 10 times of heavy water of raw material, pours at normal temperatures and is heated to 80 ℃ in the extractor, and be 80 minutes heat time heating time, filter again, the coptis soup that filters, the cordate houttuynia soup, the rheum officinale soup, the Asiatic plantain soup was poured in the fermentation vat of each label fermentation respectively into 15 days, and fermentation vat keeps 25 ℃-30 ℃, the soup after the fermentation, per respectively 100 milliliters of soups add 0.2 milliliter of sulfuric acid and concentrate, concentration time 20 minutes, post precipitation is standby, and the soup behind concentrating and precipitating is by the coptis 20
%, fish raw meat 15
%, peppermint 10
%, rheum officinale 15
%, Asiatic plantain 10
%Synthesize in synthesis reactor, stirred 10 minutes when synthetic, mixing speed is 1200 rev/mins, and filling and sealing becomes product to precipitate 2 hours again.
| Handle | Investigation strain number | 7 days " Invest, Then Investigate "s after the last dispenser | Remarks | ||
| The diseased plant number | Diseased plant rate % | Anti-efficient % | |||
| Chinese medicine preparation sprays three times | ????602 | ????10 | ????1.7 | ????93.2 | The 4th investigation result after the dispenser for the third time |
| Chinese medicine preparation sprays two times | ????618 | ????13 | ????2.1 | ????90.4 | |
| Chinese medicine preparation sprays one time | ????599 | ????44 | ????7.3 | ????80.4 | |
| Virus of A sprays three times | ????621 | ????11 | ????1.8 | ????90.6 | |
| Virus of A sprays two times | ????607 | ????11 | ????1.8 | ????88.7 | |
| Virus of A sprays one time | ????600 | ????51 | ????8.5 | ????82.1 | |
| Virus must restrain and spray three times | ????611 | ????14 | ????2.3 | ????89.8 | |
| Virus must restrain and spray two times | ????619 | ????9 | ????1.5 | ????87.9 | |
| Virus must restrain and spray one time | ????604 | ????49 | ????8.1 | ????81.8 | |
| Fresh water spraying three times | ????597 | ????186 | ????31.4 | ||
| Fresh water spraying two times | ????620 | ????184 | ????29.7 | ||
| Fresh water spraying one time | ????614 | ????163 | ????26.5 | ||
| Handle | Investigation strain number | 7 days " Invest, Then Investigate "s behind the last medicine | Remarks | ||
| The diseased plant number | Diseased plant rate % | Anti-efficient % | |||
| Chinese medicine preparation sprays three times | ????408 | ????9 | ????2.2 | ????81.3 | The 4th investigation result after the dispenser for the third time |
| Chinese medicine preparation sprays two times | ????411 | ????14 | ????3.4 | ????77.6 | |
| Chinese medicine preparation sprays one time | ????402 | ????16 | ????3.9 | ????76.8 | |
| Virus of A sprays three times | ????406 | ????7 | ????1.7 | ????89.7 | |
| Virus of A sprays two times | ????407 | ????15 | ????3.7 | ????77.9 | |
| Virus of A sprays one time | ????415 | ????15 | ????3.6 | ????69.9 | |
| Virus must restrain and spray three times | ????398 | ????11 | ????2.8 | ????70.1 | |
| Virus must restrain and spray two times | ????416 | ????17 | ????4.1 | ????70.9 | |
| Virus must restrain and spray one time | ????403 | ????20 | ????4.9 | ????68.7 | |
| Fresh water spraying three times | ????402 | ????98 | ????24.4 | ||
| Fresh water spraying two times | ????421 | ????84 | ????19.9 | ||
| Fresh water spraying one time | ????399 | ????101 | ????25.3 | ||
Now 400 times in said herbal medicine plant sterilization insecticide, 800 times are handled experimental result in indoor drug effect to cotton actor worm, beet armyworm:
One, experimental subjects: cotton bollworm, beet armyworm
Two, experimental technique: (cotton bollworm) has Institute of Plant Protection, academy of agricultural sciences, Henan Province that the worm source is provided for 3 ages of the cotton actor worm of examination.If 3 of 400 times, 800 times of Chinese herbal medicine sterilizing insecticides and clear water control treatment, the test of every place squirts cotton leaf for 40 of worms with soup, dry in the air half-dried after, in the box for feeding pests of packing into, investigate once every day, the lethality of investigation cotton bollworm, available following formula calculating:
Treatment region is prevented and treated a back worm number alive * control back, check plot worm number % preventive effect alive
%=(----------------------------------------------) * 100
A worm number * check plot prevents and treats a preceding worm number before handling control
1, cotton bollworm laboratory test results
Table 3 Chinese herbal medicine sterilizing insecticide control cotton bollworm laboratory test results
| Handle | For the examination borer population | One day | Two days | Three days | Four days | ||||
| Dead borer population | Lethality % | Dead borer population | Lethality % | Dead borer population | Lethality % | Dead borer population | Lethality % | ||
| Chinese herbal medicine sterilizing insecticide 400 * | 40 | ?21 | ?52.5 | ?32 | ?80 | ?37 | ?91 | ?40 | ?100 |
| Chinese herbal medicine sterilizing insecticide 800 * | 40 | ?18 | ?45 | ?24 | ?60 | ?27 | ?69.1 | ?36 | ?90 |
| CK | ?40 | ?0 | ?0 | ?0 | ?0 | ?0 | 0 | ?0 | ?0 |
Reach 100 by the visible 400 times of preventive effects of Chinese herbal medicine sterilizing insecticide of table 3
%, 800
Times preventive effect reaches 90
%
Testing the worm of controlling that further proves this invention in the control of indoor beet armyworm imitates
Really, be 3 ages for the examination worm, worm source effluent south insect teaching and research room of agriculture university provides,
400 times, 800 times of Chinese herbal medicine sterilizing insecticides are established 3 processing altogether,
Every place is for 60 of examinations, the medication of Chinese cabbage leaf squirt, dry in the air night half-dried, pack into and support worm
Raise in the case, the death condition of observing beet armyworm every day, add up: in
Herbal plants sterilizing insecticide control beet armyworm laboratory test results sees Table 4.
Table 4 Chinese herbal medicine sterilizing insecticide control beet armyworm laboratory test results
| Handle | For the examination borer population | One day | Two days | Three days | Four days | ||||
| Dead borer population | Lethality % | Dead borer population | Lethality % | Dead borer population | Lethality % | Dead borer population | Lethality % | ||
| Chinese herbal medicine sterilizing insecticide 400 * | 60 | ?34 | ?56.6 | ?46 | ?76.6 | ?56 | ?80 | ?60 | ?100 |
| Chinese herbal medicine sterilizing insecticide 800 * | 60 | ?21 | ?35 | ?32 | ?44 | ?44 | ?73.3 | ?52 | ?86.6 |
| CK | ?60 | ||||||||
As seen from Table 4,400 times of Chinese herbal medicine sterilizing insecticides, 800 times are not only
Effect the control cotton bollworm is remarkable, and 400 times of control beet armyworms, 800
Times preventive effect, 400 times of preventive effects reach 100
%, 800 times of preventive effects reach 86.6%, also phase
When significantly, the practical value of visible this invention.
Claims (2)
1, a kind of Chinese herbal medicine sterilizing insecticide is characterized in that being raw material by traditional Chinese medicine monarch, minister, the compatibility program helping, make with the coptis, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain, is mixed with medicament with following percentage by weight:
Coptis 20--40% cordate houttuynia 15--30
%
Peppermint 10--20
%Rheum officinale 10--20
%
Asiatic plantain 5--15%
2, the production method of the described Chinese herbal medicine sterilizing insecticide of a kind of claim 1 is characterized in that being made up of the following step by the drug matching synthetic method: a) section is processed the coptis, cordate houttuynia, peppermint, rheum officinale, the Asiatic plantain of drying respectively in flakes earlier and joint; B) concoct
Drying is processed into the coptis 20--40 gram of joint, squirts for 10 milliliters with 35 degree liquor, dry in the air half-dried after, pour into to do in the pot and fry, do and fry 80--120 ℃ of temperature, the dried stir-fry time is 40-60 minute, coptis top layer is isabelline being advisable;
Drying is processed into the cordate houttuynia 15--30 gram of joint, add 10 milliliters of vinegars after, fried 30--50 minute with pouring into after mixing to do in the pot, do and fry 50--65 ℃ of temperature, play pot when waiting cordate houttuynia to fry into yellowish-brown;
Drying is processed into the thin He 10--20 gram of joint, adds and contains 40
%15 milliliters of saline solutions, dry in the air half-dried after, pour into to do in the pot and fried 60--80 minute, do and fry 40--55 ℃ of a temperature;
The rheum officinale 10--20 gram that dry processing is in blocks adds 15 milliliters of 30% camphor wine, cooks after drying, and doing and frying temperature is 50--60 ℃, does 50--60 minute stir-fry time;
Drying is processed into the Asiatic plantain 5--15 gram of joint, adds 10 milliliters in the rice wine of fermentation, dries in the air to cook after half-dried, and doing and frying temperature is 40--60 ℃, does 30-50 minute stir-fry time; C) pulverize
The coptis of concocting, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain are ground into 160--200 purpose fine powder with ball mill respectively, put into the bag of the coptis, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain interior standby respectively; D) extract
Respectively the coptis that is ground into powder, cordate houttuynia, peppermint, rheum officinale, Asiatic plantain are respectively added 10--12 times of heavy water of raw material, pour in the extractor at normal temperatures, be heated to 60--110 ℃, be 80--120 minute heat time heating time, filter again,, pour into respectively in the fermentation vat of each label the coptis soup, cordate houttuynia soup, peppermint soup, rheum officinale soup, the Asiatic plantain soup that filter, fermented 15--20 days, fermentation vat often keeps 25--30 ℃; E) concentrate
Coptis soup after the fermentation, cordate houttuynia soup, peppermint soup, rheum officinale soup, Asiatic plantain soup, per respectively 100 milliliters of soups add 0.2 milliliter of sulfuric acid and concentrate, and concentration time is 20--40 minute, and post precipitation is standby; F) synthetic
Soup behind concentrating and precipitating is by coptis 20--40
%, cordate houttuynia 15--30
%, peppermint 10--20
%, rheum officinale 10--20
%, Asiatic plantain 5--15%, percentage by weight carry out compatibility and become sterilizing insecticide, and synthetic is to carry out in synthesis reactor, need stir when synthetic 10 minutes, and mixing speed is 1200 rev/mins, and canning sealing becomes product to precipitate 2-4 hour again.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00129782A CN1101652C (en) | 2000-10-12 | 2000-10-12 | Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00129782A CN1101652C (en) | 2000-10-12 | 2000-10-12 | Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1287787A true CN1287787A (en) | 2001-03-21 |
| CN1101652C CN1101652C (en) | 2003-02-19 |
Family
ID=4593731
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN00129782A Expired - Fee Related CN1101652C (en) | 2000-10-12 | 2000-10-12 | Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1101652C (en) |
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