CN1075602A - Efficient Chinese medicine antiseptic and preparation technology thereof - Google Patents
Efficient Chinese medicine antiseptic and preparation technology thereof Download PDFInfo
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- CN1075602A CN1075602A CN 92100929 CN92100929A CN1075602A CN 1075602 A CN1075602 A CN 1075602A CN 92100929 CN92100929 CN 92100929 CN 92100929 A CN92100929 A CN 92100929A CN 1075602 A CN1075602 A CN 1075602A
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- bark
- disinfectant
- ethanol
- tree peony
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Abstract
What the present invention relates to is a kind of material that is used to sterilize and its extracting method.It is with Chinese medicine and additives compositions such as Chinese herb rhubarb, the root bark of tree peony, thick bar, cloves, peppermints.Its preparation technology after earlier Chinese medicine being extracted respectively with alcohol solvent, forms with the additives mixing preparation again.It belongs to pure Chinese medicinal preparation, has no side effect non-corrosiveness; Disinfection Effect is good.
Description
What the present invention relates to is a kind of material that is used to sterilize and its extracting method.
Domestic and international disinfectant used in everyday has over one hundred kind more than at present, they all are chemicals basically, as the most frequently used Peracetic acid, state amyldiacid peroxide, formaldehyde and Lysol, bromogeramine etc., but its weak point mainly is: chemicals all exists certain corrosivity and toxicity, the user is had side effects, environment is produced pollute.Some goods cost is also high.
The objective of the invention is to avoid weak point of the prior art, and the method for a kind of nontoxic, non-corrosive pure middle Types of Medicine disinfectant products and preparation thereof is provided.
Can take following technical scheme to realize purpose.Prepare with the additives that Chinese herb rhubarb, the root bark of tree peony, the bark of official magnolia, cloves, peppermint and ethanol, distilled water, tween and propane diols or glycerine are formed.After medicinal ethanol extracts respectively as solvent in first the general during preparation, evenly promptly get disinfectant of the present invention with the additives mixing preparation again.
Both can adopt their crude drug to rheum officinale, the root bark of tree peony, three Chinese medicines of the bark of official magnolia, also can adopt medicine materical crude slice through processing; Crude drug be can adopt to Chinese medicine cloves, peppermint, the caryophyllus oil, the menthol that therefrom extract also can be adopted.The pattern of medicinal material is to the not influence of drug effect of disinfectant, and just technical process is complicated and simple, adopts medicine materical crude slice, caryophyllus oil, menthol then can make technology simple.
To the tween in the additives, adopt polysorbas20, polysorbate40, polysorbate60, Tween 80 can, be good wherein for Tween 80; Adopting propane diols still is that glycerine composition additives can be selected as one sees fit.Through evidence, the concentration of selected ethanol, propane diols or glycerine does not have influence to the effectiveness of disinfectant in this disinfectant.
In the disinfectant, the extraction medicinal extract of rheum officinale, the root bark of tree peony, three Chinese medicines of the bark of official magnolia is 2～8% by weight, menthol is 0.5～2%, caryophyllus oil is 0.05～0.2%, the consumption of ethanol, distilled water, tween, propane diols or glycerine is 25～35%, 40～50%, 0.1～1%, 10～30% respectively by weight in the additives, and the disinfectant result of use that is mixed with is even more ideal.
Concrete preparation method can be undertaken by following mode:
A, when extracting rheum officinale, pulverize a little with rhubarb decoction pieces, the alcohol solvent that adopts 5～6 times 45～75% adds hot reflux, extracts secondary, and 1～2 hour extraction time at every turn, filtrate is carried out after the ultrafiltration standby again.Can select the milipore filter of molecular weight 100,000 for use.
When b, the extraction root bark of tree peony, the bark of official magnolia, pulverize a little, adopt 4～5 times 95% alcohol solvent to add hot reflux, extract secondary, each 1～2 hour extraction time, filter standby with its medicine materical crude slice.
C, the rheum officinale ultrafiltrate of a preface gained is mixed with the root bark of tree peony, the bark of official magnolia filtrate of b preface gained, becomes proportion 1.15～1.20(B at 60 ℃～80 ℃ concentrating under reduced pressure) medicinal extract, standby.
D, caryophyllus oil, menthol are as the criterion with an amount of 95% ethanol mixing, standby.
After extracting above each standby material, elder generation mixes medicinal extract and tween, propane diols or the glycerine of c preface during preparation, then it is mixed with d preface spares, add ethanol while stirring with distilled water diluting, place, get upper clear supernate and promptly get disinfectant, can carry out can, seal.
Relative other goods of disinfectant that make by the technical program have the following advantages:
1, it belongs to pure Chinese medicinal preparation, human body is had no side effect, and LD50＞20g/Kg, non-corrosiveness, free from environmental pollution.
2, Disinfection Effect is good: this disinfectant sterilizing power is strong, to Escherichia coli (8099 strain) effect one minute, killing rate 99.99%, one minute killing rate 100% of dialogue staphylococcus (8032 strain) effect, disinfectant and 1: 2 dilution do diplococcus (No. 29106) and 3 minutes killing rates of staphylococcus aureus (No. 26001) effect are 100%; First, hepatitis type B virus there is deactivation, complete inactivation in HAV and the HBsAg five minutes; HIV antigen is had the elimination effect, and the ELISA acquired immune deficiency syndrome (AIDS) kit of Roche company is adopted in experiment.
3, this disinfectant is deposited 1 year its constant utility.
Claims (4)
1, a kind of disinfectant is characterized in that: the additive preparing that it adopts Chinese herb rhubarb, the root bark of tree peony, the bark of official magnolia, cloves, peppermint and ethanol, distilled water, tween and propane diols or glycerine to form forms.
2, a kind of preparation technology who is used for the described disinfectant of claim 1 is characterized in that: after medicinal ethanol extracts respectively as solvent in its first general, again with the additives mixing preparation.
3, disinfectant as claimed in claim 1, it is characterized in that: the extraction medicinal extract of rheum officinale, the root bark of tree peony, three Chinese medicines of the bark of official magnolia is 2～8% by weight, menthol 0.5～2%, caryophyllus oil 0.05～0.2%, the consumption of ethanol, distilled water, tween, propane diols or glycerine is respectively 25～35%, 40～50%, 0.1～1%, 10～30% by weight in the additives.
4, preparation technology as claimed in claim 2 is characterized in that:
A, when extracting rheum officinale, adopt 45～75% alcohol solvent to add hot reflux 1～2h, its filtrate is carried out after the ultrafiltration standby again;
When b, the extraction root bark of tree peony, the bark of official magnolia, the alcohol solvent of employing 95% adds hot reflux 1～2h, filters standby;
C, a, rheum officinale ultrafiltrate are mixed with b, the root bark of tree peony, bark of official magnolia filtrate, become the medicinal extract of proportion 1.15～1.20 standby at 60～80 ℃ of concentrating under reduced pressure;
D, caryophyllus oil, menthol is standby with an amount of 95% ethanol mixing;
Elder generation mixes medicinal extract and tween, propane diols or the glycerine of C preface during preparation, mixes with d then, adds the ethanol with distilled water diluting while stirring, places, gets supernatant and promptly get disinfectant.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92100929 CN1075602A (en) | 1992-02-22 | 1992-02-22 | Efficient Chinese medicine antiseptic and preparation technology thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 92100929 CN1075602A (en) | 1992-02-22 | 1992-02-22 | Efficient Chinese medicine antiseptic and preparation technology thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1075602A true CN1075602A (en) | 1993-09-01 |
Family
ID=4938879
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 92100929 Withdrawn CN1075602A (en) | 1992-02-22 | 1992-02-22 | Efficient Chinese medicine antiseptic and preparation technology thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1075602A (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1055611C (en) * | 1994-09-15 | 2000-08-23 | 江苏省农药研究所 | Safe sanitary pesticide and disinfectant compound |
| CN1061218C (en) * | 1997-12-09 | 2001-01-31 | 贾春健 | Agricultural liquid traditional Chinese medicine bactericide |
| CN1101652C (en) * | 2000-10-12 | 2003-02-19 | 李世芳 | Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor |
| CN101953894A (en) * | 2010-08-27 | 2011-01-26 | 姚传凤 | Method for extracting drug killing hepatitis C viruses from clove |
| CN103493851A (en) * | 2013-09-25 | 2014-01-08 | 合肥智上农业开发有限公司 | Traditional Chinese medicine disinfectant prepared employing film technology |
| CN104026173A (en) * | 2014-06-24 | 2014-09-10 | 杨美田 | Disinfectant special for inspection instrument in inspection department and preparation method of disinfectant |
| CN104397077A (en) * | 2014-11-26 | 2015-03-11 | 成都顺发消洗科技有限公司 | Novel sterilizing solution |
| CN107693605A (en) * | 2017-09-22 | 2018-02-16 | 田阳县群姐砂糖橘专业合作社 | A kind of sugar orange disinfectant and preparation method thereof |
| CN108175840A (en) * | 2018-02-13 | 2018-06-19 | 段增军 | A kind of pure Chinese medicine disinfectant and its equipment |
| CN115039797A (en) * | 2022-03-24 | 2022-09-13 | 福建省农业科学院亚热带农业研究所（福建省农业科学院蔗麻研究中心） | Clove essential oil antibacterial mixed solution and application thereof |
-
1992
- 1992-02-22 CN CN 92100929 patent/CN1075602A/en not_active Withdrawn
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1055611C (en) * | 1994-09-15 | 2000-08-23 | 江苏省农药研究所 | Safe sanitary pesticide and disinfectant compound |
| CN1061218C (en) * | 1997-12-09 | 2001-01-31 | 贾春健 | Agricultural liquid traditional Chinese medicine bactericide |
| CN1101652C (en) * | 2000-10-12 | 2003-02-19 | 李世芳 | Chinese herb medicinal plant type fungicidal and insecticidal agent, and prepn. therefor |
| CN101953894A (en) * | 2010-08-27 | 2011-01-26 | 姚传凤 | Method for extracting drug killing hepatitis C viruses from clove |
| CN103493851A (en) * | 2013-09-25 | 2014-01-08 | 合肥智上农业开发有限公司 | Traditional Chinese medicine disinfectant prepared employing film technology |
| CN104026173A (en) * | 2014-06-24 | 2014-09-10 | 杨美田 | Disinfectant special for inspection instrument in inspection department and preparation method of disinfectant |
| CN104026173B (en) * | 2014-06-24 | 2016-05-11 | 李淑娟 | A kind of clinical laboratory inspection apparatus appropriative disinfector and preparation method thereof |
| CN104397077A (en) * | 2014-11-26 | 2015-03-11 | 成都顺发消洗科技有限公司 | Novel sterilizing solution |
| CN107693605A (en) * | 2017-09-22 | 2018-02-16 | 田阳县群姐砂糖橘专业合作社 | A kind of sugar orange disinfectant and preparation method thereof |
| CN108175840A (en) * | 2018-02-13 | 2018-06-19 | 段增军 | A kind of pure Chinese medicine disinfectant and its equipment |
| CN115039797A (en) * | 2022-03-24 | 2022-09-13 | 福建省农业科学院亚热带农业研究所（福建省农业科学院蔗麻研究中心） | Clove essential oil antibacterial mixed solution and application thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C03 | Withdrawal of patent application (patent law 1993) | ||
| WW01 | Invention patent application withdrawn after publication |