CN106852347A - A kind of fragrant even thimerosal and preparation method thereof - Google Patents

A kind of fragrant even thimerosal and preparation method thereof Download PDF

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Publication number
CN106852347A
CN106852347A CN201611139743.2A CN201611139743A CN106852347A CN 106852347 A CN106852347 A CN 106852347A CN 201611139743 A CN201611139743 A CN 201611139743A CN 106852347 A CN106852347 A CN 106852347A
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CN
China
Prior art keywords
parts
thimerosal
mass fraction
elscholtiza
coptis
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Pending
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CN201611139743.2A
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Chinese (zh)
Inventor
张艳军
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Qinzhou University
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Qinzhou University
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Priority to CN201611139743.2A priority Critical patent/CN106852347A/en
Publication of CN106852347A publication Critical patent/CN106852347A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/32Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal

Abstract

The invention discloses a kind of fragrant even thimerosal and preparation method thereof, it is made up of following mass fraction formula components:10 15 parts of the coptis, 79 parts of watery hydrochloric acid, 68 parts of Fructus Corni, 68 parts of cloves, 79 parts of folium artemisiae argyi, 35 parts of sodium hypochlorite, 56 parts of kuh-seng, 79 parts of paniculate swallowwort, 48 parts of elscholtiza, 6 10 parts of lemon grass (Cymbopogon citratus), 37 parts of peppermint, 35 parts of camphortree leaf, production technology of the present invention is easy, detection means is advanced, product quality stabilization, there is remarkable killing and inhibitory action to bacterium, fungi and virus, green, environmental protection, have no toxic side effect, Disinfection Effect is notable.

Description

A kind of fragrant even thimerosal and preparation method thereof
Technical field
The present invention relates to thimerosal field, in particular to a kind of fragrant even thimerosal and preparation method thereof.
Background technology
Sterilization is the process to being killed by the pathogenic microorganism of protection organism and its surrounding environment, is passed for eliminating Dye source, cut-out route of transmission, the generation for controlling infectious disease have vital effect with diffusion.In Animal husbandry production During using it is more be chemosterilant, these preparations from it is proper be effective.But respectively have its deficiency, such as portion Divide toxic disinfectant, excitant, metal protection, environmental disruption etc.;Many disinfectants influence the strong of animal in various degree Health, is not suitable for band animal sterilization;Operating system will have safeguard procedures;Peculiar smell can not be eliminated quickly after sterilization, and long-term use can be right Animal has danger for accumulating poisoning etc..When such as " 84 " thimerosal air concentration is higher, mucous membrane, skin to human body have stronger thorn Swash or damage;Ozone concentration more than 0.3mg/m3, overlong time can make skin produce erythema or cause ophthalmia and ozone poisoning purification, Alopecia, fall the side effects such as eyebrow;Hydrogen peroxide long term is damaged to rat, particularly male mouse Liver and kidney function and lung, testis Evil, Long Term Contact have to skin and mucous membrane excitement, skin irritation and it is temporary bleach, redness, foaming, eye illness, gastrorrhagia, sternly Blindness, necrosis, pulmonary edema can be caused during weight;Formaldehyde has stimulation, sensitization and mutagenesis, and main harm shows as right Mucocutaneous stimulation, formaldehyde is magma noxious material, can be combined with protein, respiratory tract occur serious when high concentration is sucked Stimulation and oedema, Eye irritation, headache, direct skin contact formaldehyde can cause allergic dermatitis, color spot, necrosis, suck highly concentrated Bronchial astehma, high-concentration formaldehyde or a kind of genotoxicity material, the feelings that animal sucks in high concentration can be induced during degree formaldehyde Under condition, rhinopharyngeal neoplasm can be caused;Peracetic acid has severe corrosive, property unstable etc..
The content of the invention
The invention provides a kind of fragrant even thimerosal and preparation method thereof, production technology of the present invention is easy, detection means elder generation Enter, product quality stabilization, there is remarkable killing and inhibitory action to bacterium, fungi and virus, green, environmentally friendly, nontoxic pair is made With Disinfection Effect is notable.
To achieve the above object, the present invention provides following technical scheme:
A kind of fragrant even thimerosal and preparation method thereof, is made up of following mass fraction formula components:Coptis 10-15 parts, it is dilute Hydrochloric acid 7-9 parts, Fructus Corni 6-8 parts, cloves 6-8 parts, folium artemisiae argyi 7-9 parts, sodium hypochlorite 3-5 parts, kuh-seng 5-6 parts, paniculate swallowwort 7-9 Part, elscholtiza 4-8 parts, lemon grass (Cymbopogon citratus) 6-10 parts, peppermint 3-7 parts, camphortree leaf 3-5 parts.
Further:It is made up of following mass fraction formula components:10 parts of the coptis, 7 parts of watery hydrochloric acid, 6 parts of Fructus Corni, cloves 6 Part, 7 parts of folium artemisiae argyi, 3 parts of sodium hypochlorite, 5 parts of kuh-seng, 7 parts of paniculate swallowwort, 4 parts of elscholtiza, 6 parts of lemon grass (Cymbopogon citratus), 3 parts of peppermint, 3 parts of camphortree leaf.
Further:It is made up of following mass fraction formula components:12.5 parts of the coptis, 8 parts of watery hydrochloric acid, 7 parts of Fructus Corni, cloves 7 parts, 8 parts of folium artemisiae argyi, 4 parts of sodium hypochlorite, 5.5 parts of kuh-seng, 8 parts of paniculate swallowwort, 6 parts of elscholtiza, 8 parts of lemon grass (Cymbopogon citratus), 5 parts of peppermint, camphortree leaf 4 Part.
Further:It is made up of following mass fraction formula components:15 parts of the coptis, 9 parts of watery hydrochloric acid, 8 parts of Fructus Corni, cloves 8 Part, 9 parts of folium artemisiae argyi, 5 parts of sodium hypochlorite, 6 parts of kuh-seng, 9 parts of paniculate swallowwort, 8 parts of elscholtiza, 10 parts of lemon grass (Cymbopogon citratus), 7 parts of peppermint, camphortree leaf 5 Part.
Further:Preparation method of the present invention has following steps:
Step one, selection Chinese medicine material, dispensing is carried out according to mass fraction, is fitted into Chinese medicine extracting tank after being well mixed, To the water that 8~10 times of quality of material is added in tank, secondary, 1.0~1.5 hours every time, releasing extract solution are decocted;
Step 2, filtration, it is 1.10~1.30 (70~80 DEG C of surveys) that filtrate decompression is concentrated into relative density, when being cooled to room temperature Surplus stock is slowly added to, makes alcohol content up to 40%~70%, be sufficiently stirred for, after standing 12 hours, take supernatant standby;
Step 3, it is added in supernatant, after stirring, adds water and be settled to the volume of 4~8 times of quality of material, stirs evenly, Filtration, gets product.
The beneficial effects of the invention are as follows:Production technology of the present invention is easy, and detection means is advanced, product quality stabilization, to thin Bacterium, fungi and virus have remarkable killing and an inhibitory action, green, environmental protection, have no toxic side effect, and Disinfection Effect is notable.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment one:
A kind of fragrant even thimerosal is made up of following mass fraction formula components:Coptis 10-15 parts, watery hydrochloric acid 7-9 parts, mountain Zhu Cornel 6-8 parts, cloves 6-8 parts, folium artemisiae argyi 7-9 parts, sodium hypochlorite 3-5 parts, kuh-seng 5-6 parts, paniculate swallowwort 7-9 parts, elscholtiza 4-8 parts, lemon 6-10 parts, peppermint 3-7 parts, camphortree leaf 3-5 parts of lemon grass.
Embodiment two:
A kind of fragrant even thimerosal is made up of following mass fraction formula components:10 parts of the coptis, 7 parts of watery hydrochloric acid, Fructus Corni 6 Part, 6 parts of cloves, 7 parts of folium artemisiae argyi, 3 parts of sodium hypochlorite, 5 parts of kuh-seng, 7 parts of paniculate swallowwort, 4 parts of elscholtiza, 6 parts of lemon grass (Cymbopogon citratus), 3 parts of peppermint, camphor tree 3 parts of leaf.
Embodiment three:
A kind of fragrant even thimerosal is made up of following mass fraction formula components:12.5 parts of the coptis, 8 parts of watery hydrochloric acid, Fructus Corni 7 Part, 7 parts of cloves, 8 parts of folium artemisiae argyi, 4 parts of sodium hypochlorite, 5.5 parts of kuh-seng, 8 parts of paniculate swallowwort, 6 parts of elscholtiza, 8 parts of lemon grass (Cymbopogon citratus), 5 parts of peppermint, 4 parts of camphortree leaf.
Example IV:
A kind of fragrant even thimerosal is made up of following mass fraction formula components:15 parts of the coptis, 9 parts of watery hydrochloric acid, Fructus Corni 8 Part, 8 parts of cloves, 9 parts of folium artemisiae argyi, 5 parts of sodium hypochlorite, 6 parts of kuh-seng, 9 parts of paniculate swallowwort, 8 parts of elscholtiza, 10 parts of lemon grass (Cymbopogon citratus), 7 parts of peppermint, 5 parts of camphortree leaf.
Embodiment five:
A kind of preparation method preparation method of fragrant even thimerosal comprises the following steps:
Step one, selection Chinese medicine material, dispensing is carried out according to mass fraction, is fitted into Chinese medicine extracting tank after being well mixed, To the water that 8~10 times of quality of material is added in tank, secondary, 1.0~1.5 hours every time, releasing extract solution are decocted;
Step 2, filtration, it is 1.10~1.30 (70~80 DEG C of surveys) that filtrate decompression is concentrated into relative density, when being cooled to room temperature Surplus stock is slowly added to, makes alcohol content up to 40%~70%, be sufficiently stirred for, after standing 12 hours, take supernatant standby;
Step 3, it is added in supernatant, after stirring, adds water and be settled to the volume of 4~8 times of quality of material, stirs evenly, Filtration, gets product.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined May be appreciated other embodiment.

Claims (5)

1. a kind of perfume connects thimerosal, it is characterised in that:It is made up of following mass fraction formula components:
Coptis 10-15 parts, watery hydrochloric acid 7-9 parts, Fructus Corni 6-8 parts, cloves 6-8 parts, folium artemisiae argyi 7-9 parts, sodium hypochlorite 3-5 parts, hardship 5-6 parts, paniculate swallowwort 7-9 parts, elscholtiza 4-8 parts, lemon grass (Cymbopogon citratus) 6-10 parts, peppermint 3-7 parts, camphortree leaf 3-5 parts of ginseng.
2. a kind of perfume according to claim 1 connects thimerosal, it is characterised in that:By following mass fraction formula components group Into:
10 parts of the coptis, 7 parts of watery hydrochloric acid, 6 parts of Fructus Corni, 6 parts of cloves, 7 parts of folium artemisiae argyi, 3 parts of sodium hypochlorite, 5 parts of kuh-seng, paniculate swallowwort 7 Part, 4 parts of elscholtiza, 6 parts of lemon grass (Cymbopogon citratus), 3 parts of peppermint, 3 parts of camphortree leaf.
3. a kind of perfume according to claim 1 connects thimerosal, it is characterised in that:By following mass fraction formula components group Into:
12.5 parts of the coptis, 8 parts of watery hydrochloric acid, 7 parts of Fructus Corni, 7 parts of cloves, 8 parts of folium artemisiae argyi, 4 parts of sodium hypochlorite, 5.5 parts of kuh-seng, Xu are long 8 parts of minister in ancient times, 6 parts of elscholtiza, 8 parts of lemon grass (Cymbopogon citratus), 5 parts of peppermint, 4 parts of camphortree leaf.
4. a kind of perfume according to claim 1 connects thimerosal, it is characterised in that:By following mass fraction formula components group Into:
15 parts of the coptis, 9 parts of watery hydrochloric acid, 8 parts of Fructus Corni, 8 parts of cloves, 9 parts of folium artemisiae argyi, 5 parts of sodium hypochlorite, 6 parts of kuh-seng, paniculate swallowwort 9 Part, 8 parts of elscholtiza, 10 parts of lemon grass (Cymbopogon citratus), 7 parts of peppermint, 5 parts of camphortree leaf.
5. a kind of a kind of perfume according to claim 1 connects the preparation method of thimerosal, it is characterised in that:Including following step Suddenly:
Step one, selection Chinese medicine material, dispensing is carried out according to mass fraction, is fitted into Chinese medicine extracting tank after being well mixed, to tank The water of middle 8~10 times of quality of material of addition, decocts secondary, 1.0~1.5 hours every time, releasing extract solution;
Step 2, filtration, it is 1.10~1.30 (70~80 DEG C of surveys) that filtrate decompression is concentrated into relative density, is cooled to slow during room temperature Surplus stock is added, makes alcohol content up to 40%~70%, be sufficiently stirred for, after standing 12 hours, take supernatant standby;
Step 3, it is added in supernatant, after stirring, adds water and be settled to the volume of 4~8 times of quality of material, stir evenly, filters Cross, get product.
CN201611139743.2A 2016-12-12 2016-12-12 A kind of fragrant even thimerosal and preparation method thereof Pending CN106852347A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111466419A (en) * 2020-04-13 2020-07-31 天津市璇叶环保科技有限公司 Food-grade sodium hypochlorite disinfectant and preparation process thereof
CN111602670A (en) * 2020-06-11 2020-09-01 天津市璇叶环保科技有限公司 Safe food-grade sodium hypochlorite additive

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178862A (en) * 2011-04-27 2011-09-14 北京生泰尔生物科技有限公司 Preparation and quality detection methods of Xianglian disinfectant
CN104920504A (en) * 2015-05-06 2015-09-23 魏士威 Air disinfectant

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178862A (en) * 2011-04-27 2011-09-14 北京生泰尔生物科技有限公司 Preparation and quality detection methods of Xianglian disinfectant
CN104920504A (en) * 2015-05-06 2015-09-23 魏士威 Air disinfectant

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111466419A (en) * 2020-04-13 2020-07-31 天津市璇叶环保科技有限公司 Food-grade sodium hypochlorite disinfectant and preparation process thereof
CN111602670A (en) * 2020-06-11 2020-09-01 天津市璇叶环保科技有限公司 Safe food-grade sodium hypochlorite additive

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Application publication date: 20170616