CN108096112A - A kind of plant composition with preservative efficacy and preparation method thereof - Google Patents
A kind of plant composition with preservative efficacy and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The present invention relates to a kind of plant composition with preservative efficacy and preparation method thereof, main component is polygonum perfoliatum, calamus extract, annual fleabane herb extract, cork tree, kiss-me, bitter citrus peel extract, bitter bamboo shoot extract, red tea fungus fermented date liquid and Herba Patriniae extract.The anticorrosive composite of the present invention has excellent antibiotic property, has apparent inhibitory action to Escherichia coli, staphylococcus aureus, bacillus subtilis, and application is extensive, can be suitable for the cosmetics of the different dosage forms such as water base, lotion, cream.Raw material sources enrich, production cost is relatively low, have many advantages, such as mild, low irritant, can be suitable for sensibility skin.
Description
Technical field
The present invention relates to a kind of plant compositions with preservative efficacy and preparation method thereof.Specifically with polygonum perfoliatum
For the preparation method of cosmetics preservative prepared by primary raw material.
Background technology
In cosmetics, the effect of preservative is protection product, is allowed to from microbial contamination, extends the shelf longevity of product
Life；Ensure the security of product, prevent consumer from causing possible infection when using the product by microbial contamination.With section
Horizontal progress is ground, industry is also more and more deep to the safety research of preservative, and many tradition have the preservative used, all
It is proven to have certain negative effect.The secret worry of preservative：DMDMH may release formaldehyde；Kathon CG series is chloride, to very much
Skin quality has stimulation；Bronopol may cause the formation of carcinogen nitrosamine；IPBC may cause to take in iodine etc..So peace
The product concept of full plant extracts type preservative is increasingly valued by people.
This product be a kind of raw material sources it is extensive, it is simple for process, of low cost, easy to use, to human temperature and non-stimulated,
And do not cause the naturally renewable plant of secondary environmental pollution again, caused by substitution solves part chemicals needed for processing environment
Bad pollution etc..
Polygonum perfoliatum also known as Herba Lespedezae Cuneatae, the white grass in river etc. pass through the herb of leaf knotweed for polygonaceae platymiscium, are perennial tendril draft,
Distribution is in all parts of the country, resourceful.Contain flavone compound, quassinoids compound, Anthraquinones and new phenylpropyl alcohol in polygonum perfoliatum
Plain sugarcane chaff ester type compound.Polygonum perfoliatum integrates the resources of medicinal plant that antibacterial is subsided a swelling, desinsection is antipruritic, is detoxified as a kind of,
With source it is wide, it is cheap, be not likely to produce drug resistance, without chemicals residue, a variety of pathogens are respectively provided with stronger anti-
The advantages that bacterium acts on, it is among the people extensively using curative for effect.Document CN104172431B discloses a kind of day for food and drink
Right compound preservative is more using Lotus Leafextract, bamboo extractive, licorice, pectin, Ginger P.E, propolis, tea
Phenol, Flos Caryophylli extract etc. have stronger fungistatic effect into being grouped into, and antisepsis is better than the sodium benzoate of same concentration.This is anti-
Rotten agent ingredient is natural, safe and non-toxic；Raw material sources are easy to get extensively；And the original flavor of food and drink and color are not influenced, it is applicable in
In varieties of food items.It is but poor for Germicidal Efficacies such as moulds.
The content of the invention
In order to solve the above problem present in the prior art, the present invention provides one kind using plant extracts as primary raw material
Cosmetics preservative.Raw material sources are extensive, it is simple for process, of low cost, easy to use, to human temperature and non-stimulated, and again
Do not cause secondary environmental pollution.
Technical scheme is as follows：
A kind of plant composition with preservative efficacy, is made of the raw material of following parts by weight：Prickly polygonum extract 15-25
Part；15-25 parts of calamus extract；12-17 parts of annual fleabane herb extract；10-15 parts of cork tree extract；Herba Saxifragae extract 10-20
Part；Bitter tangerine peel 7-12 parts；Bitter bamboo shoot 5-10 parts；3-6 parts of red tea fungus fermented date liquid；2-5 parts of Herba Patriniae extract.
Further, a kind of plant composition with preservative efficacy, is made of the raw material of following parts by weight：Polygonum perfoliatum carries
Take object 20-25；15-20 parts of calamus extract of part；12-15 parts of annual fleabane herb extract；12-15 parts of cork tree extract；Kiss-me carries
Take 12-15 parts of object；Bitter tangerine peel 10-12 parts；Bitter bamboo shoot 5-7 parts；3-4 parts of red tea fungus fermented date liquid；2-3 parts of Herba Patriniae extract.
Present invention additionally comprises a kind of preparation methods of the plant composition with preservative efficacy, comprise the following steps：Successively
The annual fleabane herb of the prickly polygonum extract of 15-25 parts by weight, the calamus extract of 15-25 parts by weight, 12-17 parts by weight is extracted
Object, the cork tree extract of 10-15 parts by weight, the Herba Saxifragae extract of 10-20 parts by weight, bitter tangerine peel, the 5-10 of 7-12 parts by weight
The Herba Patriniae extract of the bitter bamboo shoot of parts by weight, the red tea fungus fermented date liquid of 3-6 parts by weight and 2-5 parts by weight pours into container, and mixing is equal
It is even to get the plant composition with preservative efficacy.
Further, the Herba Polygoni Perfoliati extract is prepared by following steps：By the lever plate of 15-25 parts by weight in formula
Chopping is returned to pour into container, adds in the distilled water of 150 parts by weight, heats 30~120min, filtering is concentrated by evaporation after filtrate mixing
It to 50 parts by weight, pours into the glass or ceramic vessel disinfected, adds in 1, the 2- hexylene glycols of 3 parts by weight, stir evenly rear close
Envelope is preserved to get Herba Polygoni Perfoliati extract.
Further, the calamus extract is prepared by following steps：(1) clean 60~100 parts by weight calamus,
It crushes, is stirred and be sufficiently mixed at room temperature with 75% ethyl alcohol mixed aqueous solution of 120~200 parts by weight, fully impregnate in 3-5h,
Filtering, filtrate are concentrated into 30~50 parts by weight；(2) the calamus filter residue in step (1) is scattered in the distilled water of 150 parts by weight
In, stirring is sufficiently mixed, 1.0~1.2 part by weight of cellulose enzymes of addition under the conditions of 40~55 DEG C, and stirring, fully reaction 2~
5h；(3) 0.7~1.0 parts by weight hemicellulase is added in into the mixed solution of step (2), 2~3h is fully reacted in stirring；
(4) temperature of mixed solution in step (3) is readjusted to 40~50 DEG C, adjusts pH to 4~6, adds in 0.6~1.2 parts by weight
It is stirred after mannase, fully reacts 2~3h；(5) it is neutral that 1.0~1.5 parts by weight are added in into the mixed solution of step (4)
Protease stirs, and after reacting abundant 1~3h, filtering removes filter residue；(6) 120~150 parts by weight are concentrated the filtrate to, with step
(1) the filtrate concentrate mixing in, obtains the calamus extract of 150~200 parts by weight.
Further, the annual fleabane herb extract is prepared by following steps：(1) by 60~100 parts by weight annual fleabane herbs
It cleans, crush, be scattered in 120~200 parts by weight distilled water, stirring is sufficiently mixed；(2) 1 year prepared in step (1)
1.0~1.2 parts by weight hemicellulases are added in fluffy suspension under the conditions of 40~55 DEG C, 2~3h is fully reacted in stirring；(3)
0.6~1.2 parts by weight pectase is added in into the suspension of step (2), 1~2h is fully reacted in stirring；(4) readjust outstanding
The temperature of supernatant liquid adjusts pH to 4~6 to 40~50 DEG C, is stirred after adding in 0.6~1.2 parts by weight mannase, fully reacts
2~3h；(5) 1.0~1.5 parts by weight neutral proteinases are added in into suspension prepared by step (4) to stir, reaction abundant 1~
After 3h, filtering removes filter residue；(6) 120~150 parts by weight are concentrated the filtrate to get annual fleabane herb extract.
Further, the cork tree extract is prepared by following steps：(1) clean 60~100 parts by weight cork trees,
It crushes, is scattered in the distilled water of 120~200 parts by weight, stirring is sufficiently mixed；(2) the cork tree suspension prepared in step (1)
In under the conditions of 40~55 DEG C add in 1.0~1.2 part by weight of cellulose enzymes, stirring, fully react 2~5h；(3) toward step (2)
0.7~1.0 parts by weight hemicellulase is added in the suspension of preparation, 2~3h is fully reacted in stirring；(4) made toward step (3)
Standby suspension adds in 0.6~1.2 parts by weight pectase, and 1~2h is fully reacted in stirring；(5) step (4) preparation is readjusted
Suspension temperature to 40~50 DEG C, adjust pH to 4~6, add in 0.6~1.2 parts by weight mannase after stir, fully
React 2~3h；(6) stirring of 1.0~1.5 parts by weight neutral proteinases is added in, after reacting abundant 1~3h, filtering removes filter residue；
(7) 120~150 parts by weight are concentrated the filtrate to get cork tree extract.
Further, the Herba Patriniae extract is prepared by following steps：(1) 60~75 parts by weight field pennycress are washed
Only, crush, be scattered in 120~150 parts by weight distilled water, stirring is sufficiently mixed；(2) field pennycress prepared in step (1) is hanged
1.0~1.2 part by weight of cellulose enzymes are added in supernatant liquid under the conditions of 40~55 DEG C, 2~5h is fully reacted in stirring；(3) toward step
(2) 0.7~1.0 parts by weight hemicellulase is added in the suspension prepared, 2~3h is fully reacted in stirring；(4) toward step (3)
The suspension of preparation adds in 0.6~1.2 parts by weight pectase, and 1~2h is fully reacted in stirring；(5) step (4) system is readjusted
The temperature of standby suspension adjusts pH to 4~6 to 40~50 DEG C, stirs, fills after adding in 0.6~1.2 parts by weight mannase
Divide reaction 2~3h；(6) stirring of 1.0~1.5 parts by weight neutral proteinases is added in, after reacting abundant 1~3h, filtering removes filter
Slag；(7) 120~150 parts by weight are concentrated the filtrate to get Herba Patriniae extract.
Further, the Herba Saxifragae extract is prepared by following steps：(1) 60~75 parts by weight kiss-mes are washed
Only, crush, be scattered in 120~150 parts by weight distilled water, stirring is sufficiently mixed；(2) kiss-me prepared in step (1) is hanged
1.0~1.2 part by weight of cellulose enzymes are added in supernatant liquid under the conditions of 40~55 DEG C, 2~5h is fully reacted in stirring；(3) toward step
(2) 0.7~1.0 parts by weight hemicellulase is added in the suspension prepared, 2~3h is fully reacted in stirring；(4) toward step (3)
The suspension of preparation adds in 0.6~1.2 parts by weight pectase, and 1~2h is fully reacted in stirring；(5) step (4) system is readjusted
The temperature of standby suspension adjusts pH to 4~6 to 40~50 DEG C, stirs, fills after adding in 0.6~1.2 parts by weight mannase
Divide reaction 2~3h；(6) stirring of 1.0~1.5 parts by weight neutral proteinases is added in, after reacting abundant 1~3h, filtering removes filter
Slag；(7) 120~150 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
Further, the red tea fungus fermented date liquid is prepared by following steps：By the black tea of 2-8 parts by weight, 8-12 weights
Measure the deionized water of the matrimony vine of part, the lily of 2-6 parts by weight, the white granulated sugar of 45-55 parts by weight and 900-1200 parts by weight
Mixing is boiled 100-120 minutes, stands cooled and filtered, deionized water is added in filtrate, and filtrate is made to keep 900-1200 weights
Part is measured, mixing is added in container, is put into the overweight sterilizing of high-temperature sterilization 20 minutes, room temperature is cooled to after sterilizing, adds in 45-60
The black tea mother bacterial liquid of parts by weight, is sealed with gauze, after fermenting 6-9 days at normal temperatures and pressures, is obtained fermented tea with screen filtration and is sent out
Zymotic fluid.
The present invention has the advantages that：
The present invention is extensive with raw material sources, steady performance, to Escherichia coli common in cosmetics, golden yellow
The microorganisms such as staphylococcus, aspergillus niger have good killing effect.And application is extensive, can be suitable for water base, lotion,
The cosmetics of the different dosage forms such as cream.Raw material sources enrich, production cost is relatively low, have many advantages, such as mild, low irritant, can
Suitable for sensibility skin.
Specific embodiment
With reference to specific embodiment, the present invention will be described in detail.
Embodiment one
A kind of plant composition with preservative efficacy, comprises the following steps：The polygonum perfoliatum of 20 parts by weight is extracted successively
Object, the calamus extract of 15 parts by weight, the annual fleabane herb extract of 12 parts by weight, the cork tree extract of 12 parts by weight, 14 parts by weight
Herba Saxifragae extract, the bitter tangerine peel of 7 parts by weight, the bitter bamboo shoot of 5 parts by weight, the red tea fungus fermented date liquid of 3 parts by weight and 2 parts by weight
Herba Patriniae extract pours into container, is uniformly mixed to get the plant composition with preservative efficacy.
Further, the Herba Polygoni Perfoliati extract is prepared by following steps：By the polygonum perfoliatum of 15 parts by weight in formula
Chopping is poured into container, adds in the distilled water of 150 parts by weight, heats 40min, and filtering is concentrated by evaporation after filtrate mixing to 50 weights
Part is measured, is poured into the glass or ceramic vessel disinfected, 1, the 2- hexylene glycols of 3 parts by weight is added in, is sealed after stirring evenly,
Up to Herba Polygoni Perfoliati extract.
Further, the calamus extract is prepared by following steps：(1) 70 parts by weight calamus cleaned, crush,
It is stirred and is sufficiently mixed at room temperature with 75% ethyl alcohol mixed aqueous solution of 140 parts by weight, fully impregnated in 3h, filtered, filtrate is dense
It is reduced to 30 parts by weight；(2) the calamus filter residue in step (1), is scattered in the distilled water of 150 parts by weight, and stirring is sufficiently mixed,
1.0 part by weight of cellulose enzymes are added under the conditions of 40 DEG C, stirs, fully reacts 2h；(3) add into the mixed solution of step (2)
Enter 0.7 parts by weight hemicellulase, stir, fully react 2h；(4) temperature of mixed solution in step (3) is readjusted to 40
DEG C, pH to 4 is adjusted, is stirred after adding in 0.6 parts by weight mannase, fully reacts 2h；(5) toward the mixed solution of step (4)
Middle addition 1.0 parts by weight neutral proteinases stirring, after reacting abundant 1h, filtering removes filter residue；(6) 120 weights are concentrated the filtrate to
Part is measured, is mixed with the filtrate concentrate in step (1), obtains the calamus extract of 150 parts by weight.
Further, the annual fleabane herb extract is prepared by following steps：(1) clean 60 parts by weight annual fleabane herbs,
It crushes, is scattered in 120 parts by weight distilled water, stirring is sufficiently mixed；(2) in the annual fleabane herb suspension prepared in step (1)
1.0 parts by weight hemicellulases are added under the conditions of 40 DEG C, stirs, fully reacts 2h；(3) add into the suspension of step (2)
Enter 0.6 parts by weight pectase, stir, fully react 1h；(4) temperature of suspension is readjusted to 40 DEG C, is adjusted pH to 4, is added
It is stirred after entering 0.6 parts by weight mannase, fully reacts 2h；(5) 1.0 weight are added in into suspension prepared by step (4)
Part neutral proteinase stirring, after reacting abundant 1h, filtering removes filter residue；(6) 120 parts by weight are concentrated the filtrate to get 1 year
Fluffy extract.
Further, the cork tree extract is prepared by following steps：(1) 60 parts by weight cork trees cleaned, crush,
It is scattered in the distilled water of 120 parts by weight, stirring is sufficiently mixed；(2) in 40 DEG C of items in the cork tree suspension prepared in step (1)
1.0 part by weight of cellulose enzymes are added under part, stirs, fully reacts 2h；(3) 0.7 weight is added in into suspension prepared by step (2)
Part hemicellulase is measured, 2h is fully reacted in stirring；(4) 0.6 parts by weight pectase is added in toward suspension prepared by step (3), stirred
It mixes, fully reacts 1h；(5) temperature of the suspension of step (4) preparation is readjusted to 40 DEG C, is adjusted pH to 4, is added in 0.6 weight
It is stirred after amount part mannase, fully reacts 2h；(6) stirring of 1.0 parts by weight neutral proteinases is added in, after reacting abundant 1h,
Filtering removes filter residue；(7) 120 parts by weight are concentrated the filtrate to get cork tree extract.
Further, the Herba Patriniae extract is prepared by following steps：(1) clean 60 parts by weight field pennycress,
It crushes, is scattered in 120 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare field pennycress suspension in
1.0 part by weight of cellulose enzymes are added under the conditions of 40 DEG C, stirs, fully reacts 2h；(3) add into suspension prepared by step (2)
Enter 0.7 parts by weight hemicellulase, stir, fully react 2h；(4) 0.6 parts by weight fruit is added in toward suspension prepared by step (3)
Glue enzyme, stirring, fully reacts 1h；(5) temperature of the suspension of step (4) preparation is readjusted to 40 DEG C, is adjusted pH to 4, is added
It is stirred after entering 0.6 parts by weight mannase, fully reacts 2h；(6) stirring of 1.0 parts by weight neutral proteinases is added in, reaction is filled
After dividing 1h, filtering removes filter residue；(7) 120 parts by weight are concentrated the filtrate to get Herba Patriniae extract.
Further, the Herba Saxifragae extract is prepared by following steps：(1) clean 60 parts by weight kiss-mes,
It crushes, is scattered in 120 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare kiss-me suspension in
1.0 part by weight of cellulose enzymes are added under the conditions of 40 DEG C, stirs, fully reacts 2h；(3) add into suspension prepared by step (2)
Enter 0.7 parts by weight hemicellulase, stir, fully react 2h；(4) 0.6 parts by weight fruit is added in toward suspension prepared by step (3)
Glue enzyme, stirring, fully reacts 1h；(5) temperature of the suspension of step (4) preparation is readjusted to 40 DEG C, is adjusted pH to 4, is added
It is stirred after entering 0.6 parts by weight mannase, fully reacts 2h；(6) stirring of 1.0 parts by weight neutral proteinases is added in, reaction is filled
After dividing 1h, filtering removes filter residue；(7) 120 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
Further, the red tea fungus fermented date liquid is prepared by following steps：By the black tea of 2 parts by weight, 8 parts by weight
The deionized water mixing of matrimony vine, the lily of 2 parts by weight, the white granulated sugar of 45 parts by weight and 900 parts by weight is boiled 100 minutes,
Cooled and filtered is stood, deionized water is added in filtrate, filtrate is made to keep 900 parts by weight, mixing is added in container, is put into height
The overweight sterilizing of temperature sterilizing 20 minutes, is cooled to room temperature, adds in the black tea mother bacterial liquid of 45 parts by weight, sealed with gauze after sterilizing
Mouthful, after fermenting 6 days at normal temperatures and pressures, red tea fungus fermented date liquid is obtained with screen filtration.
Embodiment two
A kind of plant composition with preservative efficacy, comprises the following steps：The polygonum perfoliatum of 21 parts by weight is extracted successively
Object, the calamus extract of 21 parts by weight, the annual fleabane herb extract of 15 parts by weight, the cork tree extract of 11 parts by weight, 11 parts by weight
Herba Saxifragae extract, the bitter tangerine peel of 9 parts by weight, the bitter bamboo shoot of 5.5 parts by weight, the red tea fungus fermented date liquid of 4 parts by weight and 2.5 weight
The Herba Patriniae extract of part pours into container, is uniformly mixed to get the plant composition with preservative efficacy.
Further, the Herba Polygoni Perfoliati extract is prepared by following steps：By the polygonum perfoliatum of 20 parts by weight in formula
Chopping is poured into container, adds in the distilled water of 150 parts by weight, heats 60min, and filtering is concentrated by evaporation after filtrate mixing to 50 weights
Part is measured, is poured into the glass or ceramic vessel disinfected, 1, the 2- hexylene glycols of 3 parts by weight is added in, is sealed after stirring evenly,
Up to Herba Polygoni Perfoliati extract.
Further, the calamus extract is prepared by following steps：(1) 80 parts by weight calamus cleaned, crush,
It is stirred and is sufficiently mixed at room temperature with 75% ethyl alcohol mixed aqueous solution of 150 parts by weight, fully impregnated in 3.5h, filtering, filtrate
It is concentrated into 40 parts by weight；(2) the calamus filter residue in step (1), is scattered in the distilled water of 150 parts by weight, stirs fully mixed
It closes, 1.1 part by weight of cellulose enzymes is added under the conditions of 50 DEG C, stir, fully react 3h；(3) into the mixed solution of step (2)
0.75 parts by weight hemicellulase is added in, stirs, fully reacts 2.5h；(4) temperature of mixed solution in step (3) is readjusted
To 45 DEG C, pH to 5 is adjusted, is stirred after adding in 1 parts by weight mannase, fully reacts 2.5h；(5) toward the mixing of step (4)
The stirring of 1.1 parts by weight neutral proteinases is added in solution, after reacting abundant 2h, filtering removes filter residue；(6) concentrate the filtrate to
130 parts by weight are mixed with the filtrate concentrate in step (1), obtain the calamus extract of 170 parts by weight.
Further, the annual fleabane herb extract is prepared by following steps：(1) clean 80 parts by weight annual fleabane herbs,
It crushes, is scattered in 150 parts by weight distilled water, stirring is sufficiently mixed；(2) in the annual fleabane herb suspension prepared in step (1)
1.2 parts by weight hemicellulases are added under the conditions of 50 DEG C, stirs, fully reacts 2.5h；(3) into the suspension of step (2)
0.8 parts by weight pectase is added in, stirs, fully reacts 1.5h；(4) readjust the temperature of suspension to 45 DEG C, adjust pH to
4.5, it is stirred after adding in 1.0 parts by weight mannases, fully reacts 2.5h；(5) added in into suspension prepared by step (4)
1.3 parts by weight neutral proteinases stir, and after reacting abundant 1.5h, filtering removes filter residue；(6) 130 weight are concentrated the filtrate to
Part is to get annual fleabane herb extract.
Further, the cork tree extract is prepared by following steps：(1) 80 parts by weight cork trees cleaned, crush,
It is scattered in the distilled water of 150 parts by weight, stirring is sufficiently mixed；(2) in 55 DEG C of items in the cork tree suspension prepared in step (1)
1.2 part by weight of cellulose enzymes are added under part, stirs, fully reacts 2h；(3) 0.7 weight is added in into suspension prepared by step (2)
Part hemicellulase is measured, 2h is fully reacted in stirring；(4) 0.7 parts by weight pectase is added in toward suspension prepared by step (3), stirred
It mixes, fully reacts 1.2h；(5) temperature of the suspension of step (4) preparation is readjusted to 40 DEG C, is adjusted pH to 5, is added in 0.7
It is stirred after parts by weight mannase, fully reacts 2.5h；(6) stirring of 1.2 parts by weight neutral proteinases is added in, reaction is abundant
After 1.5h, filtering removes filter residue；(7) 130 parts by weight are concentrated the filtrate to get cork tree extract.
Further, the Herba Patriniae extract is prepared by following steps：(1) clean 75 parts by weight field pennycress,
It crushes, is scattered in 130 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare field pennycress suspension in
1.1 part by weight of cellulose enzymes are added under the conditions of 45 DEG C, stirs, fully reacts 2.5h；(3) into suspension prepared by step (2)
0.8 parts by weight hemicellulase is added in, stirs, fully reacts 2.5h；(4) 0.7 weight is added in toward suspension prepared by step (3)
1.5h is fully reacted in part pectase, stirring；(5) temperature of the suspension of step (4) preparation is readjusted to 45 DEG C, adjusts pH
To 5, stirred after adding in 1 parts by weight mannase, fully react 2.5h；(6) stirring of 1.2 parts by weight neutral proteinases is added in,
After reacting abundant 1.5h, filtering removes filter residue；(7) 130 parts by weight are concentrated the filtrate to get Herba Patriniae extract.
Further, the Herba Saxifragae extract is prepared by following steps：(1) clean 75 parts by weight kiss-mes,
It crushes, is scattered in 130 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare kiss-me suspension in
1.1 part by weight of cellulose enzymes are added under the conditions of 45 DEG C, stirs, fully reacts 3h；(3) add into suspension prepared by step (2)
Enter 0.8 parts by weight hemicellulase, stir, fully react 2.5h；(4) 0.7 parts by weight are added in toward suspension prepared by step (3)
Pectase, stirring, fully reacts 1.5h；(5) readjust step (4) preparation suspension temperature to 45 DEG C, adjust pH to
5, it is stirred after adding in 0.8 parts by weight mannase, fully reacts 2.5h；(6) stirring of 1.2 parts by weight neutral proteinases is added in,
After reacting abundant 2h, filtering removes filter residue；(7) 130 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
Further, the red tea fungus fermented date liquid is prepared by following steps：By the black tea of 5 parts by weight, 10 parts by weight
The deionized water mixing of matrimony vine, the lily of 3 parts by weight, the white granulated sugar of 45 parts by weight and 1000 parts by weight boil 110 points
Clock stands cooled and filtered, deionized water is added in filtrate, and filtrate is made to keep 1000 parts by weight, and mixing is added in container, put
Enter the overweight sterilizing of high-temperature sterilization 20 minutes, room temperature is cooled to after sterilizing, the black tea mother bacterial liquid of 50 parts by weight is added in, uses gauze
After fermenting 7 days at normal temperatures and pressures, red tea fungus fermented date liquid is obtained with screen filtration for sealing.
Embodiment three
A kind of plant composition with preservative efficacy, comprises the following steps：The polygonum perfoliatum of 22 parts by weight is extracted successively
Object, the calamus extract of 16 parts by weight, the annual fleabane herb extract of 13 parts by weight, the cork tree extract of 11 parts by weight, 12 parts by weight
Herba Saxifragae extract, the bitter tangerine peel of 8 parts by weight, the bitter bamboo shoot of 9 parts by weight, the red tea fungus fermented date liquid of 5 parts by weight and 4 parts by weight
Herba Patriniae extract pours into container, is uniformly mixed to get the plant composition with preservative efficacy.
Further, the Herba Polygoni Perfoliati extract is prepared by following steps：By the polygonum perfoliatum of 18 parts by weight in formula
Chopping is poured into container, adds in the distilled water of 150 parts by weight, heats 60min, and filtering is concentrated by evaporation after filtrate mixing to 50 weights
Part is measured, is poured into the glass or ceramic vessel disinfected, 1, the 2- hexylene glycols of 3 parts by weight is added in, is sealed after stirring evenly,
Up to Herba Polygoni Perfoliati extract.
Further, the calamus extract is prepared by following steps：(1) 80 parts by weight calamus cleaned, crush,
It is stirred and is sufficiently mixed at room temperature with 75% ethyl alcohol mixed aqueous solution of 150 parts by weight, fully impregnated in 3.5h, filtering, filtrate
It is concentrated into 40 parts by weight；(2) the calamus filter residue in step (1), is scattered in the distilled water of 150 parts by weight, stirs fully mixed
It closes, 1.15 part by weight of cellulose enzymes is added under the conditions of 45 DEG C, stir, fully react 2.5h；(3) it is molten toward the mixing of step (2)
0.75 parts by weight hemicellulase is added in liquid, stirs, fully reacts 2.5h；(4) mixed solution in step (3) is readjusted
Temperature adjusts pH to 4.5 to 45 DEG C, is stirred after adding in 0.8 parts by weight mannase, fully reacts 2.75h；(5) toward step
(4) stirring of 1.25 parts by weight neutral proteinases is added in mixed solution, after reacting abundant 1.5h, filtering removes filter residue；(6)
130 parts by weight are concentrated the filtrate to, are mixed with the filtrate concentrate in step (1), obtain the calamus extract of 170 parts by weight.
Further, the annual fleabane herb extract is prepared by following steps：(1) clean 90 parts by weight annual fleabane herbs,
It crushes, is scattered in 160 parts by weight distilled water, stirring is sufficiently mixed；(2) in the annual fleabane herb suspension prepared in step (1)
1.1 parts by weight hemicellulases are added under the conditions of 42 DEG C, stirs, fully reacts 2.25h；(3) into the suspension of step (2)
0.7 parts by weight pectase is added in, stirs, fully reacts 1.25h；(4) readjust the temperature of suspension to 48 DEG C, adjust pH to
5.3, it is stirred after adding in 1.0 parts by weight mannases, fully reacts 2.5h；(5) added in into suspension prepared by step (4)
1.35 parts by weight neutral proteinases stir, and after reacting abundant 2h, filtering removes filter residue；(6) 125 parts by weight are concentrated the filtrate to,
Up to annual fleabane herb extract.
Further, the cork tree extract is prepared by following steps：(1) 90 parts by weight cork trees cleaned, crush,
It is scattered in the distilled water of 180 parts by weight, stirring is sufficiently mixed；(2) in 45 DEG C of items in the cork tree suspension prepared in step (1)
1.15 part by weight of cellulose enzymes are added under part, stirs, fully reacts 2.25h；(3) added in into suspension prepared by step (2)
0.75 parts by weight hemicellulase, stirring, fully reacts 2.25h；(4) 0.85 weight is added in toward suspension prepared by step (3)
1.5h is fully reacted in part pectase, stirring；(5) temperature of the suspension of step (4) preparation is readjusted to 48 DEG C, adjusts pH
To 5.7, stirred after adding in 0.95 parts by weight mannase, fully react 2.25h；(6) 1.35 parts by weight neutral proteins are added in
Enzyme stirs, and after reacting abundant 1.25h, filtering removes filter residue；(7) 135 parts by weight are concentrated the filtrate to get cork tree extract.
Further, the Herba Patriniae extract is prepared by following steps：(1) clean 70 parts by weight field pennycress,
It crushes, is scattered in 135 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare field pennycress suspension in
1.15 part by weight of cellulose enzymes are added under the conditions of 45 DEG C, stirs, fully reacts 3.5h；(3) into suspension prepared by step (2)
0.85 parts by weight hemicellulase is added in, stirs, fully reacts 2.25h；(4) 0.75 is added in toward suspension prepared by step (3)
Parts by weight pectase, stirring, fully reacts 1.75h；(5) temperature of the suspension of step (4) preparation is readjusted to 45 DEG C, is adjusted
PH to 4.8 is saved, is stirred after adding in 0.9 parts by weight mannase, fully reacts 2.25h；(6) 1.25 parts by weight neutrality eggs are added in
White enzyme stirring, after reacting abundant 2.25h, filtering removes filter residue；(7) 130 parts by weight are concentrated the filtrate to carry to get field pennycress
Take object.
Further, the Herba Saxifragae extract is prepared by following steps：(1) clean 70 parts by weight kiss-mes,
It crushes, is scattered in 140 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare kiss-me suspension in
1.15 part by weight of cellulose enzymes are added under the conditions of 48 DEG C, stirs, fully reacts 2.75h；(3) suspension prepared toward step (2)
2.25h is fully reacted in 0.85 parts by weight hemicellulase of middle addition, stirring；(4) 1 weight is added in toward suspension prepared by step (3)
Part pectase is measured, 1.5h is fully reacted in stirring；(5) temperature of the suspension of step (4) preparation is readjusted to 45 DEG C, is adjusted
PH to 5.3 stirs after adding in 0.9 parts by weight mannase, fully reacts 2.25h；(6) 1.25 parts by weight neutral proteins are added in
Enzyme stirs, and after reacting abundant 2h, filtering removes filter residue；(7) 130 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
Further, the red tea fungus fermented date liquid is prepared by following steps：By the black tea of 6 parts by weight, 11 parts by weight
The deionized water mixing of matrimony vine, the lily of 5 parts by weight, the white granulated sugar of 52 parts by weight and 1000 parts by weight boil 108 points
Clock stands cooled and filtered, deionized water is added in filtrate, and filtrate is made to keep 1000 parts by weight, and mixing is added in container, put
Enter the overweight sterilizing of high-temperature sterilization 20 minutes, room temperature is cooled to after sterilizing, the black tea mother bacterial liquid of 57 parts by weight is added in, uses gauze
After fermenting 7 days at normal temperatures and pressures, red tea fungus fermented date liquid is obtained with screen filtration for sealing.
Example IV
A kind of plant composition with preservative efficacy, comprises the following steps：The polygonum perfoliatum of 18 parts by weight is extracted successively
Object, the calamus extract of 17 parts by weight, the annual fleabane herb extract of 15 parts by weight, the cork tree extract of 12 parts by weight, 13 parts by weight
Herba Saxifragae extract, the bitter tangerine peel of 10 parts by weight, the bitter bamboo shoot of 8 parts by weight, the red tea fungus fermented date liquid of 4 parts by weight and 3 parts by weight
Herba Patriniae extract pour into container, be uniformly mixed to get the plant composition with preservative efficacy.
Further, the Herba Polygoni Perfoliati extract is prepared by following steps：By the polygonum perfoliatum of 23 parts by weight in formula
Chopping is poured into container, adds in the distilled water of 150 parts by weight, heats 75min, and filtering is concentrated by evaporation after filtrate mixing to 50 weights
Part is measured, is poured into the glass or ceramic vessel disinfected, 1, the 2- hexylene glycols of 3 parts by weight is added in, is sealed after stirring evenly,
Up to Herba Polygoni Perfoliati extract.
Further, the calamus extract is prepared by following steps：(1) 90 parts by weight calamus cleaned, crush,
It is stirred and is sufficiently mixed at room temperature with 75% ethyl alcohol mixed aqueous solution of 150 parts by weight, fully impregnated in 4h, filtered, filtrate is dense
It is reduced to 40 parts by weight；(2) the calamus filter residue in step (1), is scattered in the distilled water of 150 parts by weight, and stirring is sufficiently mixed,
1.1 part by weight of cellulose enzymes are added under the conditions of 45 DEG C, stirs, fully reacts 3.5h；(3) into the mixed solution of step (2)
0.85 parts by weight hemicellulase is added in, stirs, fully reacts 2.5h；(4) temperature of mixed solution in step (3) is readjusted
To 45 DEG C, pH to 5 is adjusted, is stirred after adding in 0.75 parts by weight mannase, fully reacts 2.5h；(5) toward the mixed of step (4)
It closes and the stirring of 1.25 parts by weight neutral proteinases is added in solution, after reacting abundant 2h, filtering removes filter residue；(6) filtrate is concentrated
It to 140 parts by weight, is mixed with the filtrate concentrate in step (1), obtains the calamus extract of 180 parts by weight.
Further, the annual fleabane herb extract is prepared by following steps：(1) clean 80 parts by weight annual fleabane herbs,
It crushes, is scattered in 180 parts by weight distilled water, stirring is sufficiently mixed；(2) in the annual fleabane herb suspension prepared in step (1)
1.12 parts by weight hemicellulases are added under the conditions of 45 DEG C, stirs, fully reacts 2.5h；(3) into the suspension of step (2)
0.75 parts by weight pectase is added in, stirs, fully reacts 1.2h；(4) readjust the temperature of suspension to 42 DEG C, adjust pH to
4.8, it is stirred after adding in 0.8 parts by weight mannase, fully reacts 2.25h；(5) add into suspension prepared by step (4)
Enter the stirring of 1.35 parts by weight neutral proteinases, after reacting abundant 2.25h, filtering removes filter residue；(6) 130 weights are concentrated the filtrate to
Part is measured to get annual fleabane herb extract.
Further, the cork tree extract is prepared by following steps：(1) 90 parts by weight cork trees cleaned, crush,
It is scattered in the distilled water of 150 parts by weight, stirring is sufficiently mixed；(2) in 45 DEG C of items in the cork tree suspension prepared in step (1)
1.2 part by weight of cellulose enzymes are added under part, stirs, fully reacts 3.5h；(3) 0.9 is added in into suspension prepared by step (2)
Parts by weight hemicellulase, stirring, fully reacts 2h；(4) 1.1 parts by weight pectases are added in toward suspension prepared by step (3),
Stirring, fully reacts 1h；(5) temperature of the suspension of step (4) preparation is readjusted to 45 DEG C, is adjusted pH to 4.8, is added in
It is stirred after 0.9 parts by weight mannase, fully reacts 2.2h；(6) stirring of 1.3 parts by weight neutral proteinases is added in, reaction is filled
After dividing 1.8h, filtering removes filter residue；(7) 130 parts by weight are concentrated the filtrate to get cork tree extract.
Further, the Herba Patriniae extract is prepared by following steps：(1) clean 70 parts by weight field pennycress,
It crushes, is scattered in 140 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare field pennycress suspension in
1.15 part by weight of cellulose enzymes are added under the conditions of 45 DEG C, stirs, fully reacts 2.5h；(3) into suspension prepared by step (2)
0.8 parts by weight hemicellulase is added in, stirs, fully reacts 2.5h；(4) 0.85 weight is added in toward suspension prepared by step (3)
Part pectase is measured, 1.25h is fully reacted in stirring；(5) temperature of the suspension of step (4) preparation is readjusted to 45 DEG C, is adjusted
PH to 5.5 stirs after adding in 1.1 parts by weight mannases, fully reacts 2.5h；(6) 1.25 parts by weight neutral proteins are added in
Enzyme stirs, and after reacting abundant 1.5h, filtering removes filter residue；(7) 125 parts by weight are concentrated the filtrate to extract to get field pennycress
Object.
Further, the Herba Saxifragae extract is prepared by following steps：(1) clean 75 parts by weight kiss-mes,
It crushes, is scattered in 150 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare kiss-me suspension in
1.2 part by weight of cellulose enzymes are added under the conditions of 55 DEG C, stirs, fully reacts 4h；(3) add into suspension prepared by step (2)
Enter 0.9 parts by weight hemicellulase, stir, fully react 2.5h；(4) 0.9 parts by weight are added in toward suspension prepared by step (3)
Pectase, stirring, fully reacts 1.5h；(5) readjust step (4) preparation suspension temperature to 45 DEG C, adjust pH to
5.5, it is stirred after adding in 0.85 parts by weight mannase, fully reacts 2.25h；(6) 1.25 parts by weight neutral proteinases are added in
Stirring, after reacting abundant 2h, filtering removes filter residue；(7) 125 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
Further, the red tea fungus fermented date liquid is prepared by following steps：By the black tea of 6 parts by weight, 10 parts by weight
The deionized water mixing of matrimony vine, the lily of 3 parts by weight, the white granulated sugar of 48 parts by weight and 1000 parts by weight boil 105 points
Clock stands cooled and filtered, deionized water is added in filtrate, and filtrate is made to keep 1000 parts by weight, and mixing is added in container, put
Enter the overweight sterilizing of high-temperature sterilization 20 minutes, room temperature is cooled to after sterilizing, the black tea mother bacterial liquid of 55 parts by weight is added in, uses gauze
After fermenting 8 days at normal temperatures and pressures, red tea fungus fermented date liquid is obtained with screen filtration for sealing.
Embodiment five
A kind of plant composition with preservative efficacy, comprises the following steps：The polygonum perfoliatum of 23 parts by weight is extracted successively
Object, the calamus extract of 17 parts by weight, the annual fleabane herb extract of 15 parts by weight, the cork tree extract of 12 parts by weight, 18 parts by weight
Herba Saxifragae extract, the bitter tangerine peel of 8 parts by weight, the bitter bamboo shoot of 6 parts by weight, the red tea fungus fermented date liquid of 3.5 parts by weight and 2.5 weight
The Herba Patriniae extract of part pours into container, is uniformly mixed to get the plant composition with preservative efficacy.
Further, the Herba Polygoni Perfoliati extract is prepared by following steps：By the polygonum perfoliatum of 24 parts by weight in formula
Chopping is poured into container, adds in the distilled water of 150 parts by weight, heats 75min, and filtering is concentrated by evaporation after filtrate mixing to 50 weights
Part is measured, is poured into the glass or ceramic vessel disinfected, 1, the 2- hexylene glycols of 3 parts by weight is added in, is sealed after stirring evenly,
Up to Herba Polygoni Perfoliati extract.
Further, the calamus extract is prepared by following steps：(1) 95 parts by weight calamus cleaned, crush,
It is stirred and is sufficiently mixed at room temperature with 75% ethyl alcohol mixed aqueous solution of 180 parts by weight, fully impregnated in 4.5h, filtering, filtrate
It is concentrated into 40 parts by weight；(2) the calamus filter residue in step (1), is scattered in the distilled water of 150 parts by weight, stirs fully mixed
It closes, 1.1 part by weight of cellulose enzymes is added under the conditions of 45 DEG C, stir, fully react 3.5h；(3) toward the mixed solution of step (2)
2.5h is fully reacted in 0.75 parts by weight hemicellulase of middle addition, stirring；(4) temperature of mixed solution in step (3) is readjusted
Degree adjusts pH to 4.5 to 45 DEG C, is stirred after adding in 0.9 parts by weight mannase, fully reacts 2.5h；(5) toward step (4)
Mixed solution in add in 1.25 parts by weight neutral proteinases stirring, after reacting abundant 1.75h, filtering, remove filter residue；(6) will
Filtrate is concentrated into 130 parts by weight, is mixed with the filtrate concentrate in step (1), obtains the calamus extract of 170 parts by weight.
Further, the annual fleabane herb extract is prepared by following steps：(1) clean 80 parts by weight annual fleabane herbs,
It crushes, is scattered in 180 parts by weight distilled water, stirring is sufficiently mixed；(2) in the annual fleabane herb suspension prepared in step (1)
1.15 parts by weight hemicellulases are added under the conditions of 50 DEG C, stirs, fully reacts 3.5h；(3) into the suspension of step (2)
1 parts by weight pectase is added in, stirs, fully reacts 1.25h；(4) readjust the temperature of suspension to 45 DEG C, adjust pH to
4.8, it is stirred after adding in 0.9 parts by weight mannase, fully reacts 2.25h；(5) add into suspension prepared by step (4)
Enter the stirring of 1.35 parts by weight neutral proteinases, after reacting abundant 2.75h, filtering removes filter residue；(6) 135 weights are concentrated the filtrate to
Part is measured to get annual fleabane herb extract.
Further, the cork tree extract is prepared by following steps：(1) 85 parts by weight cork trees cleaned, crush,
It is scattered in the distilled water of 180 parts by weight, stirring is sufficiently mixed；(2) in 50 DEG C of items in the cork tree suspension prepared in step (1)
1.15 part by weight of cellulose enzymes are added under part, stirs, fully reacts 3.5h；(3) added in into suspension prepared by step (2)
0.75 parts by weight hemicellulase, stirring, fully reacts 2.5h；(4) 1.15 parts by weight are added in toward suspension prepared by step (3)
Pectase, stirring, fully reacts 1.15h；(5) readjust step (4) preparation suspension temperature to 45 DEG C, adjust pH to
5.2, it is stirred after adding in 0.9 parts by weight mannase, fully reacts 2.25h；(6) 1.25 parts by weight neutral proteinases are added in stir
It mixes, after reacting abundant 2h, filtering removes filter residue；(7) 145 parts by weight are concentrated the filtrate to get cork tree extract.
Further, the Herba Patriniae extract is prepared by following steps：(1) clean 70 parts by weight field pennycress,
It crushes, is scattered in 135 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare field pennycress suspension in
1.15 part by weight of cellulose enzymes are added under the conditions of 52 DEG C, stirs, fully reacts 3.75h；(3) suspension prepared toward step (2)
2.25h is fully reacted in 0.85 parts by weight hemicellulase of middle addition, stirring；(4) added in toward suspension prepared by step (3)
0.95 parts by weight pectase, stirring, fully reacts 1.5h；(5) temperature of the suspension of step (4) preparation is readjusted to 45
DEG C, pH to 5.5 is adjusted, is stirred after adding in 0.95 parts by weight mannase, fully reacts 2.5h；(6) 1.35 parts by weight are added in
Neutral proteinase stirs, and after reacting abundant 2h, filtering removes filter residue；(7) 125 parts by weight are concentrated the filtrate to get field pennycress
Extract.
Further, the Herba Saxifragae extract is prepared by following steps：(1) clean 70 parts by weight kiss-mes,
It crushes, is scattered in 135 parts by weight distilled water, stirring is sufficiently mixed；(2) step (1) prepare kiss-me suspension in
1.15 part by weight of cellulose enzymes are added under the conditions of 45 DEG C, stirs, fully reacts 3.5h；(3) into suspension prepared by step (2)
0.85 parts by weight hemicellulase is added in, stirs, fully reacts 2.75h；(4) 1 weight is added in toward suspension prepared by step (3)
1.5h is fully reacted in part pectase, stirring；(5) temperature of the suspension of step (4) preparation is readjusted to 48 DEG C, adjusts pH
To 5.2, stirred after adding in 1.1 parts by weight mannases, fully react 2.25h；(6) 1.35 parts by weight neutral proteinases are added in
Stirring, after reacting abundant 2.25h, filtering removes filter residue；(7) 125 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
Further, the red tea fungus fermented date liquid is prepared by following steps：By the black tea of 5 parts by weight, 10 parts by weight
The deionized water mixing of matrimony vine, the lily of 5 parts by weight, the white granulated sugar of 52 parts by weight and 1150 parts by weight boil 115 points
Clock stands cooled and filtered, deionized water is added in filtrate, and filtrate is made to keep 1150 parts by weight, and mixing is added in container, put
Enter the overweight sterilizing of high-temperature sterilization 20 minutes, room temperature is cooled to after sterilizing, the black tea mother bacterial liquid of 55 parts by weight is added in, uses gauze
After fermenting 7 days at normal temperatures and pressures, red tea fungus fermented date liquid is obtained with screen filtration for sealing.
1 minimal inhibitory concentration unit of table：mg/ml
| Microorganism | Reference examples | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Escherichia coli ATCC29252 | 6.0 | 5.5 | 2.5 | 3.8 | 4.3 | 2.8 |
| Staphylococcus aureus | 12.3 | 7.5 | 0.7 | 2.8 | 2.7 | 3.2 |
| Intestines class salmonella | 6.2 | 8.3 | 5.6 | 3.9 | 4.2 | 3.6 |
| Black-koji mould | 15.3 | 12.3 | 11.8 | 10.9 | 13.7 | 12.1 |
In order to evaluate the irritant effects of product, the female volunteers of 100 30-45 Sui are tested respectively, with
10% lactic acid is reference material, is averaged the irritation and other effects of evaluation product, the results are shown in Table 3.
The allergy number % of 2 volunteer group of table
| 10% creams | 62 |
| Embodiment 1 | 0 |
| Embodiment 2 | 0 |
| Embodiment 3 | 0 |
| Embodiment 4 | 0 |
| Embodiment 5 | 0 |
Table 1,2 statistics indicate that, product of the invention is not only to Escherichia coli common in cosmetics, Staphylococcus aureus
The microorganisms such as bacterium, aspergillus niger have good killing effect.And there is mild, low irritant, it can be suitable for quick
Perceptual skin.
The foregoing is merely the embodiment of the present invention, are not intended to limit the scope of the invention, every to utilize this hair
The equivalent structure or equivalent flow shift that bright description is made directly or indirectly is used in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (10)
1. a kind of plant composition with preservative efficacy, which is characterized in that be made of the raw material of following parts by weight：Polygonum perfoliatum carries
Take 15-25 parts of object；15-25 parts of calamus extract；12-17 parts of annual fleabane herb extract；10-15 parts of cork tree extract；Kiss-me carries
Take 10-20 parts of object；Bitter tangerine peel 7-12 parts；Bitter bamboo shoot 5-10 parts；3-6 parts of red tea fungus fermented date liquid；2-5 parts of Herba Patriniae extract.
2. a kind of plant composition with preservative efficacy as described in claim 1, which is characterized in that by following parts by weight
Raw material forms：20-25 parts of prickly polygonum extract；15-20 parts of calamus extract；12-15 parts of annual fleabane herb extract；Cork tree extract
12-15 parts；12-15 parts of Herba Saxifragae extract；Bitter tangerine peel 10-12 parts；Bitter bamboo shoot 5-7 parts；3-4 parts of red tea fungus fermented date liquid；Field pennycress
2-3 parts of extract.
3. a kind of preparation method of the plant composition with preservative efficacy, which is characterized in that comprise the following steps：Successively will
The prickly polygonum extract of 15-25 parts by weight, the calamus extract of 15-25 parts by weight, 12-17 parts by weight annual fleabane herb extract,
The cork tree extract of 10-15 parts by weight, the Herba Saxifragae extract of 10-20 parts by weight, the bitter tangerine peel of 7-12 parts by weight, 5-10 weight
The bitter bamboo shoot, the red tea fungus fermented date liquid of 3-6 parts by weight and the Herba Patriniae extract of 2-5 parts by weight of part pour into container, are uniformly mixed, i.e.,
There must be the plant composition of preservative efficacy.
4. a kind of preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that described
Herba Polygoni Perfoliati extract is prepared by following steps：The polygonum perfoliatum chopping of 15-25 parts by weight in formula is poured into container, is added in
The distilled water of 150 parts by weight, heats 30~120min, and filtering is concentrated by evaporation to 50 parts by weight after filtrate mixing, pours into and disinfect
Glass or ceramic vessel in, add in 1, the 2- hexylene glycols of 3 parts by weight, be sealed to shoulder plate after stirring evenly and return extraction
Object.
5. a kind of preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that described
Calamus extract is prepared by following steps：
（1）60~100 parts by weight calamus are cleaned, are crushed, with 75% ethyl alcohol mixed aqueous solution of 120 ~ 200 parts by weight in room temperature
Lower stirring is sufficiently mixed, and is fully impregnated in 3-5h, and filtering, filtrate is concentrated into 30~50 parts by weight；
（2）In step（1）In calamus filter residue, be scattered in the distilled water of 150 parts by weight, stirring is sufficiently mixed, in 40~55
1.0~1.2 part by weight of cellulose enzymes are added under the conditions of DEG C, 2~5h is fully reacted in stirring；
（3）Toward step（2）Mixed solution in add in 0.7~1.0 parts by weight hemicellulase, stirring, fully react 2~3h；
（4）Readjust step（3）The temperature of middle mixed solution adjusts pH to 4~6 to 40~50 DEG C, adds in 0.6~1.2 weight
It is stirred after amount part mannase, fully reacts 2~3h；
（5）Toward step（4）Mixed solution in add in the stirring of 1.0~1.5 parts by weight neutral proteinases, after reacting abundant 1~3h,
Filtering removes filter residue；
（6）120~150 parts by weight are concentrated the filtrate to, with step（1）In filtrate concentrate mixing, obtain 150~200 weights
Measure the calamus extract of part.
6. a kind of preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that described
Annual fleabane herb extract is prepared by following steps：
（1）60~100 parts by weight annual fleabane herbs are cleaned, are crushed, are scattered in 120 ~ 200 parts by weight distilled water, are stirred fully mixed
It closes；
（2）In step（1）1.0~1.2 parts by weight half fibers are added in the annual fleabane herb suspension of middle preparation under the conditions of 40~55 DEG C
2~3h is fully reacted in the plain enzyme of dimension, stirring；
（3）Toward step（2）Suspension in add in 0.6~1.2 parts by weight pectase, stirring, fully react 1~2h；
（4）The temperature of suspension is readjusted to 40~50 DEG C, adjusts pH to 4~6, adds in 0.6~1.2 parts by weight mannosan
It is stirred after enzyme, fully reacts 2~3h；
（5）Toward step（4）The stirring of 1.0~1.5 parts by weight neutral proteinases is added in the suspension of preparation, reacts abundant 1~3h
Afterwards, filter, remove filter residue；
（6）120~150 parts by weight are concentrated the filtrate to get annual fleabane herb extract.
7. a kind of preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that described
Cork tree extract is prepared by following steps：
（1）60~100 parts by weight cork trees are cleaned, are crushed, are scattered in the distilled water of 120 ~ 200 parts by weight, are stirred fully mixed
It closes；
（2）In step（1）1.0~1.2 part by weight of cellulose enzymes are added in the cork tree suspension of preparation under the conditions of 40~55 DEG C,
2~5h is fully reacted in stirring；
（3）Toward step（2）0.7~1.0 parts by weight hemicellulase of addition in the suspension of preparation, stirring, fully reaction 2~
3h；
（4）Toward step（3）The suspension of preparation adds in 0.6~1.2 parts by weight pectase, and 1~2h is fully reacted in stirring；
（5）Readjust step（4）The temperature of the suspension of preparation adjusts pH to 4~6 to 40~50 DEG C, adds in 0.6~1.2
It is stirred after parts by weight mannase, fully reacts 2~3h；
（6）The stirring of 1.0~1.5 parts by weight neutral proteinases is added in, after reacting abundant 1~3h, filtering removes filter residue；
（7）120~150 parts by weight are concentrated the filtrate to get cork tree extract.
8. a kind of preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that described
Herba Patriniae extract is prepared by following steps：
（1）60~75 parts by weight field pennycress are cleaned, are crushed, are scattered in 120 ~ 150 parts by weight distilled water, are stirred fully mixed
It closes；
（2）In step（1）1.0~1.2 part by weight of cellulose are added in the field pennycress suspension of preparation under the conditions of 40~55 DEG C
2~5h is fully reacted in enzyme, stirring；
（3）Toward step（2）0.7~1.0 parts by weight hemicellulase of addition in the suspension of preparation, stirring, fully reaction 2~
3h；
（4）Toward step（3）The suspension of preparation adds in 0.6~1.2 parts by weight pectase, and 1~2h is fully reacted in stirring；
（5）Readjust step（4）The temperature of the suspension of preparation adjusts pH to 4~6 to 40~50 DEG C, adds in 0.6~1.2
It is stirred after parts by weight mannase, fully reacts 2~3h；
（6）The stirring of 1.0~1.5 parts by weight neutral proteinases is added in, after reacting abundant 1~3h, filtering removes filter residue；
（7）120~150 parts by weight are concentrated the filtrate to get Herba Patriniae extract.
9. a kind of preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that described
Herba Saxifragae extract is prepared by following steps：
（1）60~75 parts by weight kiss-mes are cleaned, are crushed, are scattered in 120 ~ 150 parts by weight distilled water, are stirred fully mixed
It closes；
（2）In step（1）1.0~1.2 part by weight of cellulose are added in the kiss-me suspension of preparation under the conditions of 40~55 DEG C
2~5h is fully reacted in enzyme, stirring；
（3）Toward step（2）0.7~1.0 parts by weight hemicellulase of addition in the suspension of preparation, stirring, fully reaction 2~
3h；
（4）Toward step（3）The suspension of preparation adds in 0.6~1.2 parts by weight pectase, and 1~2h is fully reacted in stirring；
（5）Readjust step（4）The temperature of the suspension of preparation adjusts pH to 4~6 to 40~50 DEG C, adds in 0.6~1.2
It is stirred after parts by weight mannase, fully reacts 2~3h；
（6）The stirring of 1.0~1.5 parts by weight neutral proteinases is added in, after reacting abundant 1~3h, filtering removes filter residue；
（7）120~150 parts by weight are concentrated the filtrate to get Herba Saxifragae extract.
A kind of 10. preparation method of the plant composition with preservative efficacy as claimed in claim 3, which is characterized in that institute
Red tea fungus fermented date liquid is stated to be prepared by following steps：By the black tea of 2-8 parts by weight, the matrimony vine of 8-12 parts by weight, 2-6 parts by weight
Lily, 45-55 parts by weight white granulated sugar and 900-1200 parts by weight deionized water mixing boil 100-120 minutes,
Cooled and filtered is stood, deionized water is added in filtrate, filtrate is made to keep 900-1200 parts by weight, mixing is added in container,
The overweight sterilizing of high-temperature sterilization 20 minutes is put into, room temperature is cooled to after sterilizing, adds in the black tea mother bacterial liquid of 45-60 parts by weight,
It is sealed with gauze, after fermenting 6-9 days at normal temperatures and pressures, red tea fungus fermented date liquid is obtained with screen filtration.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108685802A (en) * | 2018-08-07 | 2018-10-23 | 广东丸美生物技术股份有限公司 | Anticorrosive composite and its preparation method and application |
| CN108852936A (en) * | 2018-08-07 | 2018-11-23 | 广东丸美生物技术股份有限公司 | Anticorrosive composite for cosmetics and preparation method thereof, purposes and cosmetics |
| CN108904379A (en) * | 2018-08-07 | 2018-11-30 | 广东丸美生物技术股份有限公司 | Cotton rose leaf extract and preparation method thereof, anticorrosive composite and preparation method thereof and cosmetic composition |
| CN108904378A (en) * | 2018-08-07 | 2018-11-30 | 广东丸美生物技术股份有限公司 | Tianshan Mountains violet extract and preparation method thereof, anticorrosive composite and preparation method thereof and cosmetic composition |
| CN108938486A (en) * | 2018-08-07 | 2018-12-07 | 广东丸美生物技术股份有限公司 | Anticorrosive composite and its preparation method and application |
| CN108992375A (en) * | 2018-08-07 | 2018-12-14 | 广东丸美生物技术股份有限公司 | Anticorrosive composite for cosmetics and preparation method thereof, purposes and cosmetics |
| CN109010168A (en) * | 2018-08-07 | 2018-12-18 | 广东丸美生物技术股份有限公司 | Radix Sangusorbae extract and preparation method thereof, anticorrosive composite and preparation method thereof and cosmetic composition |
| CN110215413A (en) * | 2018-03-02 | 2019-09-10 | 广州华狮化妆品科技有限公司 | A kind of the eye & lip makeup remover for long wear formulas cosmetics and preparation method of double gel rubber systems |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103083210A (en) * | 2013-01-25 | 2013-05-08 | 王恩瀚 | Medicine composition with skin whitening effect as well as preparation method and application thereof |
| CN104435379A (en) * | 2014-10-27 | 2015-03-25 | 文佳颖 | Plant extract compound capable of inhibiting bacteria, resisting inflammation, stopping bleeding and relieving pain and application of plant extract compound |
| CN105310898A (en) * | 2015-11-03 | 2016-02-10 | 北京一轻研究院 | Skin-whitening composition |
| CN106963676A (en) * | 2017-03-24 | 2017-07-21 | 福建师范大学 | A kind of kiss-me bactericidal composition and preparation method thereof |
| CN107296874A (en) * | 2017-06-29 | 2017-10-27 | 合肥川迪医药技术有限公司 | A kind of pharmaceutical composition of anti-inflammation and preparation method thereof |
-
2018
- 2018-01-12 CN CN201810031096.6A patent/CN108096112B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103083210A (en) * | 2013-01-25 | 2013-05-08 | 王恩瀚 | Medicine composition with skin whitening effect as well as preparation method and application thereof |
| CN104435379A (en) * | 2014-10-27 | 2015-03-25 | 文佳颖 | Plant extract compound capable of inhibiting bacteria, resisting inflammation, stopping bleeding and relieving pain and application of plant extract compound |
| CN105310898A (en) * | 2015-11-03 | 2016-02-10 | 北京一轻研究院 | Skin-whitening composition |
| CN106963676A (en) * | 2017-03-24 | 2017-07-21 | 福建师范大学 | A kind of kiss-me bactericidal composition and preparation method thereof |
| CN107296874A (en) * | 2017-06-29 | 2017-10-27 | 合肥川迪医药技术有限公司 | A kind of pharmaceutical composition of anti-inflammation and preparation method thereof |
Non-Patent Citations (8)
| Title |
|---|
| 刘春生等: "《精编本草纲目药物彩色图鉴》", 31 January 2016, 山西科学技术出版社 * |
| 常敏毅: "《实用抗癌草药》", 31 March 1996, 中国医药科技出版社 * |
| 文洪宇等: ""应用于中药提取分离中的酶的综述"", 《中国医药指南》 * |
| 李广勋: "《中药药理毒理与临床》", 31 December 1992, 天津科技翻译出版公司 * |
| 梅全喜: "《现代中药药理与临床应用手册.第3版》", 31 October 2016, 中国中医药出版社 * |
| 潘远根等: "《湖南药物.第1卷》", 31 December 2004, 湖南科学技术出版社 * |
| 窦国祥等: "《老年人饮食指南》", 30 June 1986, 原子能出版社 * |
| 范文昌等: "《广东地产清热解毒药物大全》", 31 July 2011, 中医古籍出版社 * |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110215413A (en) * | 2018-03-02 | 2019-09-10 | 广州华狮化妆品科技有限公司 | A kind of the eye & lip makeup remover for long wear formulas cosmetics and preparation method of double gel rubber systems |
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| CN108685802A (en) * | 2018-08-07 | 2018-10-23 | 广东丸美生物技术股份有限公司 | Anticorrosive composite and its preparation method and application |
| CN108852936A (en) * | 2018-08-07 | 2018-11-23 | 广东丸美生物技术股份有限公司 | Anticorrosive composite for cosmetics and preparation method thereof, purposes and cosmetics |
| CN108904379A (en) * | 2018-08-07 | 2018-11-30 | 广东丸美生物技术股份有限公司 | Cotton rose leaf extract and preparation method thereof, anticorrosive composite and preparation method thereof and cosmetic composition |
| CN108904378A (en) * | 2018-08-07 | 2018-11-30 | 广东丸美生物技术股份有限公司 | Tianshan Mountains violet extract and preparation method thereof, anticorrosive composite and preparation method thereof and cosmetic composition |
| CN108938486A (en) * | 2018-08-07 | 2018-12-07 | 广东丸美生物技术股份有限公司 | Anticorrosive composite and its preparation method and application |
| CN108992375A (en) * | 2018-08-07 | 2018-12-14 | 广东丸美生物技术股份有限公司 | Anticorrosive composite for cosmetics and preparation method thereof, purposes and cosmetics |
| CN109010168A (en) * | 2018-08-07 | 2018-12-18 | 广东丸美生物技术股份有限公司 | Radix Sangusorbae extract and preparation method thereof, anticorrosive composite and preparation method thereof and cosmetic composition |
| CN108852936B (en) * | 2018-08-07 | 2019-09-13 | 广东丸美生物技术股份有限公司 | Anticorrosive composite for cosmetics and preparation method thereof, purposes and cosmetics |
| CN108685802B (en) * | 2018-08-07 | 2019-10-18 | 广东丸美生物技术股份有限公司 | Anticorrosive composite and its preparation method and application |
| CN108938486B (en) * | 2018-08-07 | 2019-10-18 | 广东丸美生物技术股份有限公司 | Anticorrosive composite and its preparation method and application |
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