CN109197906A - A kind of air disinfection spray and its preparation method and application - Google Patents
A kind of air disinfection spray and its preparation method and application Download PDFInfo
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- CN109197906A CN109197906A CN201811067523.2A CN201811067523A CN109197906A CN 109197906 A CN109197906 A CN 109197906A CN 201811067523 A CN201811067523 A CN 201811067523A CN 109197906 A CN109197906 A CN 109197906A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/10—Apiaceae or Umbelliferae [Carrot family], e.g. parsley, caraway, dill, lovage, fennel or snakebed
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/14—Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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Abstract
The present invention provides a kind of air disinfection spray and its preparation method and application, the spray includes component A and B component, and the raw material for preparing of the component A includes following components by weight: 0.01-1.35 parts of Fructus Forsythiae, 0.05-0.96 parts of rhizoma ligustici, 0.02-0.72 parts of dried orange peel, 0.15-1.18 parts of cape jasmine, 0.03-2.25 parts of honeysuckle, 0.11-1.86 parts of folium isatidis, 0.07-0.88 parts of dandelion, 0.03-1.22 parts of radix aucklandiae, 0.04-0.85 parts of Asian puccoon, 0.15-1.32 parts of wild chrysanthemum, 10-20 parts of water；The B component includes following components by weight: 0.04-2.58 parts of polyhexamethylene guanide, 0.02-1.33 parts of A.SAP, 30-50 parts of water；The mass ratio of the component A and B component is 1:(3-10)；The spray fungistatic effect is significant.
Description
Technical field
The invention belongs to field of traditional Chinese medicine preparation, it is related to a kind of air disinfection spray and its preparation method and application, especially
It is related to a kind of disinfectant spray and its preparation method and application of environmental type.
Background technique
In the movable environment of people, it is filled with various bacteriums and virus, when the quantity for reaching certain will make human body
At injury.Have much by the common disease of spread of germs, is exactly because in air caused by contained corresponding germ, as lung knot
Core, influenza, pollinosis, meningitis etc., wherein more severe is also by infection through air to the mankind there are also SARS, bird flu
Life and health damage, some are even fatal.In the space of serious pollution, Causative virus is even more to have reached hundreds of
Kind, and air is all-pervasive, can enter respiratory tract, lung, even in blood, it is seen that the disinfection and sterilization of room air must
The property wanted.
CN107715154A discloses a kind of spray conducive to the sterilization that eliminates the unusual smell, and the raw material composition of the spray is by weight
It is as follows to measure part meter: honeysuckle, 30-55 parts, dandelion, 10-25 parts, rhizoma atractylodis, 8-25 parts, eupatorium, 10-20 parts, folium isatidis, 15-
25 parts, cardamom, 15-35 parts, chamomile, 15-30 parts.The invention does not add the chemistry that first diether, freon etc. are harmful to the human body
Ingredient, and fragrant odour can effectively improve air quality without obvious Chinese medicine odor, have good tranquilizing the mind, the prevention upper respiratory tract
Infection, bacteriostasis, it is healthy and safe to human skin without adverse effects such as allergy.But the disinfectant spray of the method preparation
Bactericidal effect need further to be promoted.
CN107899051A discloses a kind of spray for refreshing air, the raw material and its weight proportion of the spray are as follows: wood
3~8 parts of leaf, 10~15 parts of fingered citron blade, 2~6 parts of jasmine petal, 12~17 parts of beeswax, 6~10 parts of folium cortex eucommiae, Morinda officinalis
3~5 parts of leaf, 4~8 parts of mulberry leaf, female wither 10~16 parts of root, 12~18 parts of CedarLeaves, 3~9 points of bergamot, 3~6 parts of folium artemisiae argyi, emulsification
40~50 parts of agent, 90~110 parts of distilled water, 120~150 parts of mixed essential oil.This spray for refreshing air have fresh air,
Remove peculiar smell while, have concurrently sterilization, except formaldehyde, refresh oneself, the effect of expelling parasite, although the invention provide spray have
There is certain bactericidal effect, but do not protrude, it still needs further improvement.
CN102578168A discloses a kind of spray for the sterilization of pharmacological evaluation room, it is matched by following weight
Made of substance and pharmaceutically acceptable carrier: the achene of Siberian cocklebur, myrrh, the root bark of Chinese wolf-berry, dragon's blood, rheum officinale, safflower, cortex dictamni, Radix Notoginseng,
Viola mandshurica, rhizoma atractylodis, frutus cnidii and indigo naturalis.Although this spray bactericidal effect is obvious, ingredient is simple, cheap,
Only application is sterilized in the lab, is limited to using comparing.
CN107646911A discloses a kind of botanical fungicide, is grouped as by the group of following parts by weight: eucalyptus leaves 6-10
Part, 7-9 parts of aloe, 2-5 parts of pine needle, 1-4 parts of pine bark, 6-8 parts of Jasmine, 4-7 parts of China pink.The fungicide matter of the invention preparation
Ground is mild, nontoxic, environmentally protective, sterilizing ability is strong, fragrant odour.It can be made as spraying, effective fresh air, killing
Bacterium；Also it is used directly for wiping, such as the sterilization of the household goods such as a dishcloth, kitchen desktop, door handle, shoe chest.But
The germicidal efficiency of such fungicide is lower.
Therefore, a kind of spray that environment friendly and pollution-free and bactericidal effect is good how is developed, for the sky of daily life
Gas purification, the guarantee of physical activity health have great importance.
Summary of the invention
In view of the deficiencies of the prior art, the purpose of the present invention is to provide a kind of air disinfection sprays and preparation method thereof
And application purifies air, ensures the purpose of health so that spray can reach effective sterilizing.
To achieve this purpose, the present invention adopts the following technical scheme:
In a first aspect, the spray includes component A and B component, institute the present invention provides a kind of air disinfection spray
The raw material for preparing for stating component A includes following components by weight:
The B component includes following components by weight:
0.04-2.58 parts of polyhexamethylene guanide
0.02-1.33 parts of A.SAP
30-50 parts of water；
The mass ratio of the component A and B component be 1:(3-10), such as can be 1:3,1:4,1:5,1:6,1:7,1:8,
1:9 or 1:10 etc..
Air disinfection spray provided by the invention is formulated using natural, free of contamination raw material, passes through each group division
Reason cooperation, rationally controls content, enables air disinfection spray quickly to kill bacterium and the virus in space, by air
Middle natural bacteria disinfection Effect test, the extinction rate of natural bacteria can reach 97.59% even higher as the result is shown, compared to
The air disinfection spray of existing type, Disinfection Effect is more preferable, and the guarantee effect of purification and health for air is more
It is prominent.
In the present invention, when component A and B component are controlled within the scope of aforementioned proportion, spray may make to reach best effective
Fruit.
In the present invention, Fructus Forsythiae, honeysuckle, dandelion, Asian puccoon, wild chrysanthemum these medicinal materials itself have the function of antibacterial,
After the reasonable formula of compatibility composition, there is synergy bactericidal effect, fungistatic effect can be promoted.
In the present invention, the parts by weight of the Fructus Forsythiae are 0.01-1.35 parts, such as can be 0.01 part, 0.05 part, 0.1
Part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1 part, 1.1 parts, 1.2 parts or 1.35 parts etc..
The application of Fructus Forsythiae at present clinically includes treating acute nephritis, treatment purpura, treatment pulmonary abscess etc., medicinal
It is worth higher.
In the present invention, the parts by weight of the rhizoma ligustici are 0.05-0.96 parts, such as can be 0.05 part, 0.1 part, 0.2
Part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 0.96 part etc..
Rhizoma ligustici is generally used for exterior syndrome due to wind-cold in the field of Chinese medicines, and pain, the treatment of rheumatic arthralgia are pushed up in mountain peak.In the collocation present invention
Other components when, good bactericidal effect can be played.
In the present invention, the parts by weight of the dried orange peel are 0.02-0.72 parts, such as can be 0.02 part, 0.1 part, 0.2
Part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part or 0.72 part etc..
Dried orange peel is the dry mature skin of rutaceae orange and its variety, has regulating qi-flowing for strengthening spleen, eliminating dampness and eliminating phlegm,
It can be clinically used for abdominal fullness and distention, deficiency of food is vomited and diarrhoea, coughing with a lot of sputum.
In the present invention, the parts by weight of the cape jasmine are 0.15-1.18 parts, such as can be 0.15 part, 0.2 part, 0.25
Part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1 part or 1.18 parts etc..
Cape jasmine is usually used in treating icteric hepatitis, bruise, hypertension, diabetes and other diseases in tcm clinical practice.Containing sarranine
Anthocyanin base can make weld.
In the present invention, the parts by weight of the honeysuckle are 0.03-2.25 parts, such as can be 0.03 part, 0.1 part, 0.5
Part, 0.8 part, 0.9 part, 1 part, 1.5 parts, 1.85 parts or 2.25 parts etc..
Honeysuckle is known as from ancient times for Caprifoliaceae woodbine honeysuckle and congener dry flower or with the flower just opened
Clearing heat and detoxicating good medicine.The sweet cold air fragrance of its property, for clear heat with drugs of sweet flavour and cold nature without injuring one's stomach, fragrance reaches thoroughly again can eliminating evil.Honeysuckle can declare
Dissipating wind-heat, also kind removing summer-heat blood poison, is used for various febrile diseases, such as body heat, dermexanthesis, macular eruption, heat toxin sore carbuncle, abscess of throat disease,
Significant effect.
In the present invention, the parts by weight of the folium isatidis are 0.11-1.86 parts, such as can be 0.11 part, 0.2 part, 0.4
Part, 0.8 part, 0.9 part, 1 part, 1.5 parts, 1.6 parts or 1.86 parts etc..
Folium isatidis cures mainly the diseases such as hot spot, erysipelas, abscess of throat, aphthae, sore and toxic.In recent years clinically
It is widely applied, in addition to it can be used and control above-mentioned all diseases, and can be used for the strongly fragrant lung of phlegm heat, cough up phlegm yellow thick；Especially it is usually used in popular second encephalitis,
Not only can single be applied to prevention, but also radix bupleuri, honeysuckle flower, Fructus Forsythiae, Radix Isatidis, radix scrophulariae, Radix Rehmanniae can be cooperated etc., can removing summer-heat gas point, battalion point
Heat toxin, can be more appropriate with partial heat type with controlling various encephalitis.
In the present invention, the parts by weight of the dandelion are 0.07-0.88 parts, such as can be 0.07 part, 0.1 part, 0.2
Part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part or 0.88 part etc..
Dandelion alias dandelion, Po Poding, Hua Hualang etc., composite family herbaceos perennial.Capitulum, on seed
There is the bobbles that white pappus is formed, racks after the flowers are in blossom and breed new life to new place.It is public containing Pu in dandelion plant
A variety of health-nutrition ingredients such as English alcohol, taraxacin, choline, organic acid, synanthrin.Nature and flavor are sweet, slight bitter, tremble with fear.Return liver, stomach meridian.Have
Diuresis, laxative, removing jaundice subcutaneous ulcer, cholagogue and other effects.
In the present invention, the parts by weight of the radix aucklandiae are 0.03-1.22 parts, such as can be 0.03 part, 0.1 part, 0.2
Part, 0.3 part, 0.5 part, 0.8 part, 0.9 part, 1 part, 1.2 parts or 1.22 parts etc..
Radix aucklandiae is the root of compositae plant radix aucklandiae, cylindrical or flat round cylindricality.Surface yellowish-brown, taupe or sepia, bolt
Skin has removed mostly, has bright longitudinal furrow and lateral root trace, sometimes visible reticular texture.Gas fragrance is strong and special, bitter after taste elder generation sweet tea, slightly
Pierce tongue.Cure mainly promoting qi circulation and relieving pain, reinforcing spleen to promote digestion.
In the present invention, the parts by weight of the Asian puccoon are 0.04-0.85 parts, such as can be 0.04 part, 0.1 part, 0.2
Part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part or 0.85 part etc..
Asian puccoon has effects that certain cure the disease.Such as vaginitis can be controlled, control pityriasis rosea, treating acute and chronic hepatitis etc..
In the present invention, the parts by weight of the wild chrysanthemum are 0.15-1.32 parts, such as can be 0.15 part, 0.2 part, 0.5
Part, 0.8 part, 0.9 part, 1.2 parts or 1.32 parts etc..
Wild chrysanthemum is composite family herbaceos perennial, and wild chrysanthemum cold nature has dispelling wind and heat from the body, subdhing swelling and detoxicating.Malignant boil can be treated
The diseases such as sore carbuncle swollen, abscess of throat, wind-fire red eye, headache and dizziness.
Preferably, the component A further includes 0.05-1 parts of ethyl alcohol, such as can be 0.05 part, 0.06 part, 0.1 part, 0.2
Part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part etc..
Preferably, the component A further includes 0.04-0.87 parts of pueraria lobata, for example, can be 0.04 part, 0.1 part, 0.3 part,
0.5 part, 0.8 part or 0.87 part etc..
Pueraria lobata is the dry root of legume pueraria lobata, practises and claim elegant jessamine.There is expelling pathogenic factors from muscles and skin to bring down a fever, promoting eruption promotes the production of body fluid to quench thirst, and rising Yang stops
The function rushed down.It is usually used in exterior syndrome fever, stiff nape and back, measles without adequate eruption, pyreticosis is thirsty, and the deficiency of Yin is quenched one's thirst, and heat is purged heat dysentery, splenasthenic diarrhea.
In the present invention, pueraria lobata is added into composition, is conducive to the bactericidal effect for promoting composition, is further enhanced spray
The sterilizing ability of mist agent.
In the present invention, the parts by weight of the water of component A be 10-20 parts, such as can be 10 parts, 11 parts, 12 parts, 13 parts,
14 parts, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts or 20 parts etc..
In the present invention, the parts by weight of the polyhexamethylene guanide are 0.04-2.58 parts, such as can be 0.04 part, 0.1
Part, 0.5 part, 1 part, 1.5 parts, 1.8 parts, 2 parts, 2.5 parts or 2.58 parts etc..
In the present invention, polyhexamethylene guanide has nontoxic, colourless, odorless, corrosion-free, wide sterilization spectrum etc. many superior
Property, it is highly suitable for family disinfection.It can be used for the sterilization cleaning of melon fruits and vegetables；For each kind fabric such as clothing, towel, sheet
Sterilization cleaning；And the disinfection for being directly used in the body surfaces such as furniture, carpet, sofa, kitchen utensils, sanitary ware and air is gone out
Bacterium.In addition, in public places, the life security of a large amount of bacterium and the viral infection disease serious harm mankind, sterilizing
As maintenance the essential important link of people's life, therefore, polyhexamethylene guanide be equally well suited for automobile, train,
The sterilization of the public places such as aircraft, steamer, market, hospital, cinema, hotel, restaurant.
In the present invention, the parts by weight of the A.SAP are 0.02-1.33 parts, such as can be 0.02 part, 0.05 part, 0.1
Part, 0.3 part, 0.35 part, 0.5 part, 0.7 part, 0.9 part, 1 part, 1.2 parts or 1.33 parts etc..
A.SAP belongs to natural organic anti-bacterial deodorant, using soybean extraction liquid as main composition.In the present invention, by B group
Addition A.SAP is compounded in point, can cooperate with raising fungistatic effect that suppression is not achieved if dosage is too low with polyhexamethylene guanide
Bacterium effect；It, can be risky to Product Safety if using more than the upper limit.
In the present invention, in B component water parts by weight be 30-50 parts, such as can be 30 parts, 35 parts, 40 parts, 45 parts or
50 parts etc..
Second aspect, the present invention provides a kind of preparation method of air disinfection spray as described in relation to the first aspect, institutes
Preparation method is stated to include the following steps:
(1) by Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum and optionally
Ground pueraria lobata is added to the water according to the ratio, filters after decoction, collects filtrate and carries out first time concentration, optionally after addition ethyl alcohol, into
Row precipitating is concentrated for second, obtains the extracting solution of component A；
(2) water dilution is added in the extracting solution of the component A obtained to step (1), and polyhexamethylene guanide, A.SAP is then added
Stir to get the air disinfection spray.
Preparation method provided by the invention is simple and easy to do, can sufficiently be concentrated to become the effective component of each component and extract
Liquid, significant effect.
Preferably, the temperature of decoction described in step (1) is 60~100 DEG C, such as can be 60 DEG C, 65 DEG C, 70 DEG C, 75
DEG C, 80 DEG C, 85 DEG C, 90 DEG C, 95 DEG C or 100 DEG C etc..
Preferably, the time of decoction described in step (1) be 1~2h, such as can be 1h, 1.1h, 1.2h, 1.3h,
1.4h, 1.5h, 1.6h, 1.7h, 1.8h, 1.9h or 2h etc..
Preferably, the number of decoction described in step (1) is 2~3 times, such as be can be 2 times or 3 times.
In the present invention, filtered through gauze is used after decoction, and is concentrated after collecting the filtrate for merging and decocting several times.
Preferably, the volume fraction of ethyl alcohol described in step (1) is 90%~95%, for example, can be 90%, 91%,
92%, 93%, 94% or 95% etc..
Preferably, after adding ethyl alcohol, adjustment ethanol content to 60%~80%, such as can be 60%, 62%, 65%,
67%, 68%, 70%, 72%, 75%, 78% or 80% etc..
Preferably, the time of precipitating described in step (1) be 5~20h, such as can be 5h, 7h, 8h, 10h, 12h,
14h, 15h, 18h or 20h etc..
In the present invention, it after precipitating, is concentrated by second, recycles concentrate when there is no ethanol flavor, stop, obtaining
To the extracting solution of component A.
In the present invention, by the amount of addition water and polyhexamethylene guanide, A.SAP in step (2), to control component A and B
The proportionate relationship of component.
Preferably, further include that extracting solution is fitted into aerosol can after being stirred described in step (2), adjust aerosol can
Pressure, obtain the air disinfection spray.
Preferably, the pressure be 0.65~1MPa, such as can be 0.65MPa, 0.7MPa, 0.75MPa, 0.8MPa,
0.85MPa, 0.9MPa, 0.95MPa or 1MPa etc..
Preferably, the preparation method comprises the following steps:
(1) by Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum and optionally
Ground pueraria lobata is added to the water according to the ratio, and 1~2h is decocted at 60~100 DEG C, after repeating 2~3 times, using filtered through gauze, merges and receives
Collect filtrate and carry out first time concentration, optionally addition volume fraction is 90%~95% ethyl alcohol, adjusts ethanol content to 60%
After~80%, carries out 5~20h of precipitating, is concentrated for second, obtain the extracting solution of component A；
(2) water dilution is added in the extracting solution of the component A obtained to step (1), and polyhexamethylene guanide, A.SAP is then added
Stirring, extracting solution is fitted into aerosol can, and the pressure using pure nitrogen gas adjustment aerosol can is 0.65~1MPa, obtains the air
Disinfectant spray.
The third aspect, the present invention provides a kind of air disinfection sprays as described in relation to the first aspect in purification air, kills
Application in bacterium disinfection.
Air disinfection spray provided by the invention, application range is wider, such as can apply in household, and purification is empty
Gas can also directly carry out disinfection for furniture etc.；Can be used in public place, including station, market, hospital etc. occasion into
Row sterilizing.
Compared with the existing technology, the invention has the following advantages:
Air disinfection spray provided by the invention is formulated using natural, free of contamination raw material, passes through each group division
Reason cooperation, rationally controls content, enables air disinfection spray quickly to kill bacterium and the virus in space, by air
Middle natural bacteria disinfection Effect test, the extinction rate of natural bacteria can reach 97.59% even higher as the result is shown, compared to
The air disinfection spray of existing type, Disinfection Effect is more preferable, and the guarantee effect of purification and health for air is more
It is prominent, it can be adapted for air cleaning in various situations, sterilizing, market application prospect is extensive.
Specific embodiment
The technical scheme of the invention is further explained by means of specific implementation.Those skilled in the art should be bright
, the described embodiments are merely helpful in understanding the present invention, should not be regarded as a specific limitation of the invention.
Embodiment 1
The present embodiment provides a kind of air disinfection spray, including component A and B component, the mass ratioes of component A and B component
For 1:5, wherein the raw material for preparing of component A includes following components by weight:
B component includes following components by weight:
1.25 parts of polyhexamethylene guanide；
1.12 parts of A.SAP
40 parts of water；
(1) according to the ratio by Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum
It is added to the water, decocts 1.5h at 80 DEG C, after being repeated 2 times, using filtered through gauze, merge and collect filtrate progress first time concentration,
Volume fraction is added as 95% ethyl alcohol, after adjustment ethanol content to 80%, carries out precipitating 10h, second of concentration is recycled to nothing
Ethanol flavor obtains the extracting solution of component A；
(2) the water dilution of proportional quantity is added in the extracting solution of the component A obtained to step (1), and the poly- of proportional quantity is then added
Hexa-methylene guanidine, A.SAP stirring, extracting solution is fitted into aerosol can, and the pressure using pure nitrogen gas adjustment aerosol can is 0.8MPa,
Obtain air disinfection spray.
Embodiment 2
The present embodiment provides a kind of air disinfection spray, including component A and B component, the mass ratioes of component A and B component
For 1:10, wherein the raw material for preparing of component A includes following components by weight:
The B component includes following components by weight:
2.58 parts of polyhexamethylene guanide；
1.33 parts of A.SAP
50 parts of water；
(1) according to the ratio by Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum
It is added to the water, decocts 2h at 60 DEG C, after being repeated 3 times, using filtered through gauze, merge and collect filtrate progress first time concentration, add
Adding volume fraction is 90% ethyl alcohol, and adjustment ethanol content carries out precipitating 20h to after 60%, is concentrated for second, and no second is recycled to
Alcohol taste obtains the extracting solution of component A；
(2) the water dilution of proportional quantity is added in the extracting solution of the component A obtained to step (1), and the poly- of proportional quantity is then added
Hexa-methylene guanidine, A.SAP stirring, extracting solution is fitted into aerosol can, and the pressure using pure nitrogen gas adjustment aerosol can is
0.65MPa obtains air disinfection spray.
Embodiment 3
The present embodiment provides a kind of air disinfection spray, including component A and B component, the mass ratioes of component A and B component
For 1:3, wherein the raw material for preparing of component A includes following components by weight:
The B component includes following components by weight:
0.04 part of polyhexamethylene guanide；
0.02 part of A.SAP
30 parts of water；
(1) Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum, pueraria lobata are pressed
Proportion is added to the water, and decocts 1h at 100 DEG C, and after being repeated 2 times, using filtered through gauze, it is dense for the first time to merge collection filtrate progress
Contracting adds volume fraction as 95% ethyl alcohol, after adjustment ethanol content to 80%, carries out precipitating 5h, be concentrated, be recycled to for the second time
Without ethanol flavor, the extracting solution of component A is obtained；
(2) the water dilution of proportional quantity is added in the extracting solution of the component A obtained to step (1), and the poly- of proportional quantity is then added
Hexa-methylene guanidine, A.SAP stirring, extracting solution is fitted into aerosol can, and the pressure using pure nitrogen gas adjustment aerosol can is 1MPa, is obtained
To air disinfection spray.
Comparative example 1
The difference of this comparative example and embodiment 1 is only that this comparative example does not include Fructus Forsythiae, remaining is same as Example 1
Air disinfection spray is prepared.
Comparative example 2
The difference of this comparative example and embodiment 1 is only that this comparative example does not include honeysuckle, remaining with 1 phase of embodiment
It is same that air disinfection spray is prepared.
Comparative example 3
The difference of this comparative example and embodiment 1 is only that this comparative example does not include dandelion, remaining with 1 phase of embodiment
It is same that air disinfection spray is prepared.
Comparative example 4
The difference of this comparative example and embodiment 1 is only that this comparative example does not include Asian puccoon, remaining is same as Example 1
Air disinfection spray is prepared.
Comparative example 5
The difference of this comparative example and embodiment 1 is only that this comparative example does not include wild chrysanthemum, remaining with 1 phase of embodiment
It is same that air disinfection spray is prepared.
Comparative example 6
The difference of this comparative example and embodiment 1 is only that the mass ratio of component A and B component is 1:1 in this comparative example, makees
For air disinfection spray.
Comparative example 7
The difference of this comparative example and embodiment 1 is only that the mass ratio of component A and B component is 1:12 in this comparative example, makees
For air disinfection spray.
Comparative example 8
The difference of this comparative example and embodiment 1 is only that this comparative example does not include polyhexamethylene guanide, remaining with implementation
Example 1 is identical to be prepared air disinfection spray.
Comparative example 9
The difference of this comparative example and embodiment 1 is only that this comparative example does not include A.SAP, remaining is same as Example 1
Air disinfection spray is prepared.
Comparative example 10
The difference of this comparative example and embodiment 1 is only that this comparative example does not include B component, remaining is same as Example 1
Air disinfection spray is prepared.
Performance test:
The air disinfection spray of above-described embodiment 1-3 and comparative example 1-10 is subjected to air sterilization effect field test.
Test basis: it is tested referring to 2.1.3.5 in Ministry of Public Health's " disinfection technology standard " (2002 editions), randomly selects one
(volume is about 40m for office3), natural bacteria sampling is carried out with air microorganism sampler in unmanned situation, as
Sample (positive control) before sterilizing.The office is closed, air disinfection spray is sprayed in office air, sprays 2mL/
m3, it after acting on 5min, then is once sampled, as the experiment sample after disinfection, carries out viable bacteria culture and count, test temperature 20
℃±1℃.Test is repeated 3 times, and calculates average value, as shown in table 1 (in table 1 data be 3 times test obtained average value).
Table 1
By the comparison of embodiment 1-3 and comparative example 1-10 it is found that air disinfection spray provided by the invention, effect is most
It is good；When additionally addition pueraria lobata, bactericidal effect is promoted；And lacked in the spray one of ingredient such as Fructus Forsythiae,
Honeysuckle, dandelion, Asian puccoon, wild chrysanthemum etc., bactericidal effect is declined, but extinction rate is also 90% or so；And work as this hair
When the too high levels of bright component A, the bactericidal effect of product is poor, and only 82.16% or so；And when the content of B component of the present invention
When excessively high, the safety of product is unable to reach requirement at this time, can not carry out using；When having lacked poly- six in air disinfection spray
Methylene guanidine or
When A.SAP, extinction rate only has more than 60% at this time, and bactericidal effect is excessively poor；And in the absence of B component, this space-time
The bactericidal effect of gas disinfectant spray is worst.
In addition, air disinfection spray provided by the invention not only has good bactericidal effect, and by a variety of
The compounding of ingredient, is beneficial to health, and environment protecting is excellent.For the sterilizing, net being applied under various complex environments
Change air, has good effect, application prospect is extensive.
The Applicant declares that the present invention is explained by the above embodiments air disinfection spray and its preparation side of the invention
Method and application, but the invention is not limited to above-mentioned method detaileds, that is, do not mean that the present invention must rely on above-mentioned method detailed
It could implement.It should be clear to those skilled in the art, any improvement in the present invention, to each raw material of product of the present invention
Equivalence replacement and addition, the selection of concrete mode of auxiliary element etc., all fall within protection scope of the present invention and the open scope
Within.
Claims (10)
1. a kind of air disinfection spray, which is characterized in that the spray includes component A and B component, the system of the component A
Standby raw material includes following components by weight:
The B component includes following components by weight:
0.04-2.58 parts of polyhexamethylene guanide
0.02-1.33 parts of A.SAP
30-50 parts of water；
The mass ratio of the component A and B component is 1:(3-10).
2. air disinfection spray according to claim 1, which is characterized in that the component A further includes ethyl alcohol 0.05-1
Part.
3. air disinfection spray according to claim 1 or 2, which is characterized in that the component A further includes pueraria lobata
0.04-0.87 parts.
4. the preparation method of air disinfection spray according to any one of claim 1-3, which is characterized in that the system
Preparation Method includes the following steps:
(1) by Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum and optionally Pueraria lobota
Root is added to the water according to the ratio, filters after decoction, collects filtrate and carries out first time concentration, optionally after addition ethyl alcohol, is sunk
It forms sediment, be concentrated for second, obtain the extracting solution of component A；
(2) water dilution is added in the extracting solution of the component A obtained to step (1), and polyhexamethylene guanide, A.SAP stirring is then added
Obtain the air disinfection spray.
5. the preparation method according to claim 4, which is characterized in that the temperature of decoction described in step (1) is 60~100
℃。
6. preparation method according to claim 4 or 5, which is characterized in that the time of decoction described in step (1) be 1~
2h；
Preferably, the number of decoction described in step (1) is 2~3 times.
7. the preparation method according to any one of claim 4-6, which is characterized in that the body of ethyl alcohol described in step (1)
Fraction is 90%~95%；
Preferably, after adding ethyl alcohol, adjustment ethanol content to 60%~80%；
Preferably, the time of precipitating described in step (1) is 5~20h.
8. the preparation method according to any one of claim 4-7, which is characterized in that stirring described in step (2) terminates
Afterwards, further include that extracting solution is fitted into aerosol can, adjust the pressure of aerosol can, obtain the air disinfection spray；
Preferably, the pressure is 0.65~1MPa.
9. the preparation method according to any one of claim 4-8, which is characterized in that the preparation method includes following step
It is rapid:
(1) by Fructus Forsythiae, rhizoma ligustici, dried orange peel, cape jasmine, honeysuckle, folium isatidis, dandelion, radix aucklandiae, Asian puccoon, wild chrysanthemum and optionally Pueraria lobota
Root is added to the water according to the ratio, and 1~2h is decocted at 60~100 DEG C, after repeating 2~3 times, using filtered through gauze, merges and collects filter
The ethyl alcohol that liquid progress first time concentration, optionally addition volume fraction are 90%~95%, adjustment ethanol content to 60%~
After 80%, carries out 5~20h of precipitating, is concentrated for second, obtain the extracting solution of component A；
(2) water dilution is added in the extracting solution of the component A obtained to step (1), and polyhexamethylene guanide, A.SAP stirring is then added,
Extracting solution is fitted into aerosol can, the pressure using pure nitrogen gas adjustment aerosol can is 0.65~1MPa, obtains the air disinfection
Spray.
10. air disinfection spray according to any one of claim 1-3 answering in purification air, sterilizing
With.
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| CN201811067523.2A CN109197906A (en) | 2018-09-13 | 2018-09-13 | A kind of air disinfection spray and its preparation method and application |
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| CN111317759A (en) * | 2020-03-06 | 2020-06-23 | 大连正润环保工程有限公司 | Traditional Chinese medicine anion disinfectant and preparation method thereof |
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| CN111109301A (en) * | 2019-12-31 | 2020-05-08 | 张立波 | Composite disinfectant and preparation method and application thereof |
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