CN108175840A - A kind of pure Chinese medicine disinfectant and its equipment - Google Patents
A kind of pure Chinese medicine disinfectant and its equipment Download PDFInfo
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- CN108175840A CN108175840A CN201810148554.4A CN201810148554A CN108175840A CN 108175840 A CN108175840 A CN 108175840A CN 201810148554 A CN201810148554 A CN 201810148554A CN 108175840 A CN108175840 A CN 108175840A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/30—Polygonaceae [Buckwheat family], e.g. red-knees or rhubarb
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/46—Stemonaceae [Stemona family], e.g. croomia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J3/00—Devices or methods specially adapted for bringing pharmaceutical products into particular physical or administering forms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/19—Acanthaceae (Acanthus family)
- A61K36/195—Strobilanthes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/31—Brassicaceae or Cruciferae (Mustard family), e.g. broccoli, cabbage or kohlrabi
- A61K36/315—Isatis, e.g. Dyer's woad
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/57—Magnoliaceae (Magnolia family)
- A61K36/575—Magnolia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/65—Paeoniaceae (Peony family), e.g. Chinese peony
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/708—Rheum (rhubarb)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/756—Phellodendron, e.g. corktree
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/904—Stemonaceae (Stemona family), e.g. croomia
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J2200/00—General characteristics or adaptations
- A61J2200/40—Heating or cooling means; Combinations thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
Abstract
A kind of pure Chinese medicine disinfectant disclosed by the invention and its equipment, are prepared by following steps:A. raw material prepares;B. it impregnates;C. boiling and initial concentration;D. final concentration;E. match liquid.A kind of pure Chinese medicine disinfectant of the present invention is acted synergistically by drug matching, germ can quickly be killed, killed the virus, acting on 35 minutes can make germ or virus be killed or be inactivated, it is quick, without side-effects, and skin can be in direct contact, cross-infection and the propagation of germ virus are avoided, it is non-corrosive to medical instrument, furniture, leather, plastics, tableware, it is also pollution-free to environment.Its advantage is in terms of existing technologies:Preparation process is simple and convenient to operate, and hepatitis A virus and hepatitis B, which are acted on 5 minutes 100%, has complete inactivation effect, and can eliminate AIDS virus antigen.
Description
Technical field
The present invention relates to a kind of medical disinfectant, more particularly to a kind of pure Chinese medicine disinfectant.
Equipment used in above-mentioned pure Chinese medicine disinfectant is prepared the invention further relates to a kind of.
Background technology
At present, hepatitis A virus or hepatitis B endanger the health of human body at any time, although treatment hepatitis A or hepatitis B side
The medicine in face also compares more, but sterilization time is relatively long, slowly effect, curative effect be not notable, and side effect is also relatively more, and prevents first
Liver or the vaccine of hepatitis B have also been prevention effect, and the effect in human body is also to have certain time limit, can not be solved
The certainly infringement of hepatitis A virus or hepatitis B to human body.The present sterilization in market, 100% being of disinfectant for external use killed the virus
Disinfectant is learned, the overwhelming majority is corrosive, such as has stronger corrosivity to skin, metal, and nearly all have to environment
Pollution.
Invention content
The present invention is completed to solve of the prior art insufficient, can be right the object of the present invention is to provide one kind
Hepatitis A virus and hepatitis B, which act on 5 minutes, to be played the role of 100% complete inactivation, can also eliminate AIDS virus antigen, is reached
A kind of action time short, quick pure Chinese medicine disinfectant, and it is environmentally safe, skin can be in direct contact.
A kind of pure Chinese medicine disinfectant of the present invention, is prepared by following steps:
A. raw material prepares:It is 6-10 parts of the root bark of tree peony, 3-7 parts of Cortex Magnoliae Officinalis, 1-3 parts of honeysuckle, 2-5 parts of Radix Isatidis, 1-3 parts of Cortex Phellodendri, big
98% medicinal alcohol of 7.5 times of 1-3 parts yellow, 1-3 parts of the tuber of stemona and input medicinal material total amount;
B. it impregnates:Medicinal material in step A is put into reaction kettle, 98% medicinal alcohol is added in into reaction kettle, is fully soaked
Transdermal material impregnates 6-12 hours, obtains fully absorbing the wet medicinal material after alcohol;
C. boiling and initial concentration:The wet medicinal material for fully absorbing alcohol obtained in step B is subjected to boiling three times, specifically
It is as follows:First time boiling:80 DEG C are heated to reaction kettle, then 80 DEG C of holding constant temperature 3 hours, filter and liquid is simultaneously evacuated to deposit
In tank, liquid is drawn into concentration tank by unlatching vacuum pressure tank once to be concentrated, and thickening temperature is 80-90 DEG C, pressure dimension
It holds in 2-3 atmospheric pressure;Second of boiling:98% medicinal alcohol of 5.5 times of input medicinal material total amount is added in into reaction kettle, is given
Reaction kettle is heated to 80 DEG C, then 80 DEG C of holding constant temperature 2 hours, filters and simultaneously liquid is evacuated in conservation tank, then inhale liquid
Enter into concentration tank to mix with the liquid that first time boiling obtains and carry out secondary concentration, the temperature of secondary concentration is 80-90 DEG C, pressure
Power maintains 2-3 atmospheric pressure;Third time boiling:98% medical wine of 5.5 times of input medicinal material total amount is added in into reaction kettle
Essence is heated to 80 DEG C to reaction kettle, then 80 DEG C of holding constant temperature 1 hour, filters and simultaneously liquid is evacuated in conservation tank, then by medicine
Liquid is drawn into the liquid obtained in concentration tank with first time boiling and second of boiling and mixes to be concentrated three times, and thickening temperature is
80-90 DEG C, the time control of concentration can obtain initial concentration admixing medical solutions at 50-60 minutes;
D. final concentration:The initial concentration admixing medical solutions obtained in step C are heated, temperature is controlled at 60-70 DEG C,
In 0.6-0.8 atmospheric pressure, heating makes liquid be condensed into the traditional Chinese medicinal ointment that density is 0.9-1 for 50-60 minutes for pressure control, then will
The traditional Chinese medicinal ointment concentrated is released to spare in medicinal liquor barrel, configuration commodity liquid;
E. match liquid:With traditional Chinese medicinal ointment that parts by weight are 1-20 parts, 0.1-5 parts of peppermint, the 98% of 5-30 parts medical wine
Essence and 1-30 parts of distilled water, are configured to required commodity liquid.
A kind of pure Chinese medicine disinfectant of the present invention, is prepared by following steps:A. raw material prepares:6-10 parts of the root bark of tree peony, Cortex Magnoliae Officinalis 3-7
Part, 1-3 parts of honeysuckle, 2-5 parts of Radix Isatidis, 1-3 parts of Cortex Phellodendri, 1-3 parts of rheum officinale, 7.5 times of 1-3 parts of the tuber of stemona and input medicinal material total amount
98% medicinal alcohol;B. it impregnates:Medicinal material in step A is put into reaction kettle, 98% medicinal alcohol is added in into reaction kettle,
Medicinal material is thoroughly impregnated, impregnates 6-12 hours, obtains fully absorbing the wet medicinal material after alcohol;C. boiling and initial concentration:By step B
In obtain fully absorb alcohol wet medicinal material carry out boiling three times, it is specific as follows:First time boiling:80 are heated to reaction kettle
DEG C, then 80 DEG C of holding constant temperature 3 hours, filters and simultaneously liquid is evacuated in conservation tank, opens vacuum pressure tank and is drawn into liquid
It is once concentrated in concentration tank, thickening temperature is 80-90 DEG C, and pressure maintains 2-3 atmospheric pressure;Second of boiling:To anti-
98% medicinal alcohol that 5.5 times of input medicinal material total amount is added in kettle is answered, 80 DEG C are heated to reaction kettle, then keeps 80 DEG C of perseverances
Temperature 2 hours filters and liquid is evacuated in conservation tank, then liquid is drawn into the medicine obtained in concentration tank with first time boiling
Liquid mixing carries out secondary concentration, and the temperature of secondary concentration is 80-90 DEG C, and pressure maintains 2-3 atmospheric pressure;Third time boiling:
98% medicinal alcohol of 5.5 times of input medicinal material total amount is added in into reaction kettle, 80 DEG C is heated to reaction kettle, then keeps 80
DEG C constant temperature 1 hour filters and simultaneously liquid is evacuated in conservation tank, is then drawn into liquid in concentration tank and first time boiling and the
Secondary boiled obtained liquid mixing is concentrated three times, and thickening temperature is 80-90 DEG C, and the time control of concentration is at 50-60 points
Clock can obtain initial concentration admixing medical solutions;D. final concentration:The initial concentration admixing medical solutions obtained in step C are added
Heat, at 60-70 DEG C, pressure control makes liquid be condensed into density in 50-60 minutes in 0.6-0.8 atmospheric pressure, heating for temperature control
For the traditional Chinese medicinal ointment of 0.9-1, then the traditional Chinese medicinal ointment concentrated is released to spare in medicinal liquor barrel, configuration commodity liquid;E. match liquid:With
Parts by weight are 1-20 parts of traditional Chinese medicinal ointment, 0.1-5 parts of peppermint, 5-30 parts of 98% medicinal alcohol and 1-30 parts of distillation
Water is configured to required commodity liquid.In this way, newly it is added to rheum officinale, four taste of Cortex Phellodendri, the tuber of stemona and Radix Isatidis in the dispensing of the present invention
Chinese medicine since each Chinese medicine plays the role of sterilization, kills the virus, but is single use effect and has little effect.By filling into
Four kinds of Chinese medicines with original drug matching, the effect of can improving sterilization, kill the virus, not only kill the virus, also enhance and disappear
The effect of swollen, sterilizes the compatibility collaboration killed the virus, and drug effect interacts, and drug effect is stronger, and external application almost also finds no bad anti-
Should, also find no shortcoming.Since Radix Isatidis has the function of clearing heat and detoxicating sterilizing, Radix Isatidis is added in raw material to hepatitis A and hepatitis B
Virus also plays the role of the anti-inflammatory that sterilizes, if be used alone to medicine that kill germ virus function little, external for these years
Boundary thinks that the Chinese medicine of China is not sterilized, and does not kill the virus, Chinese medicine all needs compatible use in fact, can not only enhance drug effect, keep away simultaneously
The characteristics of Chinese medicine sterilizing kills the virus the shortcomings that slow, used by drug matching is exempted from, to hepatitis A virus, hepatitis B and AIDS
Poison can not only kill but also speed is fast.Its advantage is in terms of existing technologies:When germ viruses contact to pure Chinese medicine sterilizes
Agent is killed or is inactivated, can be in direct contact skin, avoid cross-infection and the propagation of germ virus, to doctor for 3-5 minutes
It is non-corrosive to treat instrument, furniture, leather, plastics, tableware, it is also pollution-free to environment, but also white grapes pearl bacterium can be made
With one minute killing rate up to 99.99%, to staphylococcus aureus 1:It is 100% that 2 dilutions, which act on 3 minutes killing rates, right
Hepatitis A virus and hepatitis B, which act on, complete inactivation effect for 5 minutes 100%, quick, significant effect, without side-effects, and
AIDS virus antigen can also be eliminated.
Equipment used in above-mentioned pure Chinese medicine disinfectant is prepared it is a further object of the present invention to provide a kind of:Including connecting successively
Reaction kettle, filter, conservation tank, concentration tank, cooling for reflux tank and the vacuum pressure tank connect, the reaction kettle connect with filter
Logical, the filter is connected with the conservation tank, and the conservation tank is connected with the concentration tank, the concentration tank and the cooling
Return tank connects, and the cooling for reflux tank is connected with the vacuum pressure tank.
Equipment used in a kind of pure Chinese medicine disinfectant of the present invention can also be:
Mateiral pump is equipped between the filter and the conservation tank.
The mateiral pump is stainless steel mateiral pump.
The reaction kettle is equipped with thermometer, pressure gauge and gas outlet.
The concentration tank is equipped with peep hole, gas outlet and discharge port.
Radiator is equipped between the cooling for reflux tank and the vacuum pressure tank.
The vacuum pressure tank is equipped with pressure gauge.
A kind of prepare of the present invention prepares used in above-mentioned pure Chinese medicine disinfectant, including sequentially connected reaction kettle, mistake
Filter, conservation tank, concentration tank, cooling for reflux tank and vacuum pressure tank, the reaction kettle are connected with filter, the filter with
The conservation tank connection, the conservation tank are connected with the concentration tank, and the concentration tank is connected with the cooling for reflux tank, described
Cooling for reflux tank is connected with the vacuum pressure tank.In this way, the medicinal material in reaction kettle is carried out boiling, vacuum pressure tank is opened,
Liquid be sucked by filter it is spare in conservation tank, due to vacuum pressure tank provide vacuum pressure, make gas in cooling for reflux
Tank internal circulation flow, the liquid in conservation tank, which is inhaled into concentration tank, to be concentrated.It has in terms of existing technologies
The advantages of be:It is simple in structure, easy to operate, can effectively reduce production cost, improve production efficiency.
Description of the drawings
Fig. 1 is equipment schematic diagram used in a kind of pure Chinese medicine disinfectant of the present invention.
Figure number explanation
1st, reaction kettle 2, thermometer 3, pressure gauge 4, gas outlet
5th, filter 6, mateiral pump 7, conservation tank 8, concentration tank
10th, peep hole 11, cooling for reflux tank 13, vacuum pressure tank
14th, radiator 15, discharge port
Specific embodiment
Fig. 1 is described in further detail a kind of pure Chinese medicine disinfectant and its equipment of the present invention below in conjunction with the accompanying drawings.
A kind of pure Chinese medicine disinfectant of the present invention, is prepared by following steps:
A. raw material prepares:It is 6-10 parts of the root bark of tree peony, 3-7 parts of Cortex Magnoliae Officinalis, 1-3 parts of honeysuckle, 2-5 parts of Radix Isatidis, 1-3 parts of Cortex Phellodendri, big
98% medicinal alcohol of 7.5 times of 1-3 parts yellow, 1-3 parts of the tuber of stemona and input medicinal material total amount;
B. it impregnates:Medicinal material in step A is put into reaction kettle 1,98% medicinal alcohol is added in into reaction kettle 1, fully
Medicinal material is impregnated with, impregnates 6-12 hours, obtains fully absorbing the wet medicinal material after alcohol;
C. boiling and initial concentration:The wet medicinal material for fully absorbing alcohol obtained in step B is subjected to boiling three times, specifically
It is as follows:First time boiling:80 DEG C are heated to reaction kettle 1, then 80 DEG C of holding constant temperature 3 hours, filter and liquid is simultaneously evacuated to storage
In standby tank 7, liquid is drawn into concentration tank 8 by unlatching vacuum pressure tank 13 once to be concentrated, and thickening temperature is 80-90 DEG C,
Pressure maintains 2-3 atmospheric pressure;Second of boiling:The medical of the 98% of 5.5 times of input medicinal material total amount is added in into reaction kettle 1
Alcohol is heated to 80 DEG C to reaction kettle 1, then 80 DEG C of holding constant temperature 2 hours, filters and simultaneously liquid is evacuated in conservation tank 7, then
Liquid is drawn into the liquid obtained in concentration tank 8 with first time boiling and mixes progress secondary concentration, the temperature of secondary concentration is
80-90 DEG C, pressure maintains 2-3 atmospheric pressure;Third time boiling:5.5 times of input medicinal material total amount is added in into reaction kettle 1
98% medicinal alcohol is heated to 80 DEG C to reaction kettle 1, then 80 DEG C of holding constant temperature 1 hour, filters and liquid simultaneously is evacuated to deposit
In tank 7, then liquid is drawn into the liquid obtained in concentration tank 8 with first time boiling and second of boiling mix progress three times
Concentration, thickening temperature are 80-90 DEG C, and the time control of concentration can obtain initial concentration admixing medical solutions at 50-60 minutes;
D. final concentration:The initial concentration admixing medical solutions obtained in step C are heated, temperature is controlled at 60-70 DEG C,
In 0.6-0.8 atmospheric pressure, heating makes liquid be condensed into the traditional Chinese medicinal ointment that density is 0.9-1 for 50-60 minutes for pressure control, then will
The traditional Chinese medicinal ointment concentrated is released to spare in medicinal liquor barrel, configuration commodity liquid;
E. match liquid:With traditional Chinese medicinal ointment that parts by weight are 1-20 parts, 0.1-5 parts of peppermint, the 98% of 5-30 parts medical wine
Essence and 1-30 parts of distilled water, are configured to required commodity liquid.In this way, firstly because Chinese medicine used is completely dried
Material, the alcohol amount of addition can will not enough have medicinal material, ensure that medicinal material can be impregnated with completely, make the active ingredient in Chinese medicine
It can fully dissolve, to be precipitated;Secondly, in digestion process because medicinal material containing medicinal alcohol in saturation state, second
The alcohol amount that secondary and third time boiling adds in can not have medicinal material, situation about being floated for medicinal material is avoided to occur in pot,
The precipitation of medicinal material active ingredient is influenced, in due course to deflate to reaction kettle 1, controls the conditions of cooking in reaction kettle 1, so as to
Active ingredient in medicinal material is all precipitated, improves yield;Finally, due to the density of required liquid is not achieved in initial concentration, only
It is simply to concentrate to reduce the content of medicinal alcohol and moisture in liquid, so need to carry out liquid last concentration, so as to
Liquid is made to reach required density, is measured with density baumé hydrometer, when liquid density is the density of 0.9-1, is directly opened dense
The liquid concentrated is discarded to spare in medicinal liquor barrel, configuration commodity liquid by the switch of 8 bottom of contracting tank.In this way, the present invention's matches
Rheum officinale, four taste Chinese medicine of Cortex Phellodendri, the tuber of stemona and Radix Isatidis, the work for having sterilization due to each Chinese medicine, killing the virus newly are added in material
With, but be single use effect and have little effect.By filling into four kinds of Chinese medicines, and original drug matching, can improve sterilization,
The effect of the effect of killing the virus not only kills the virus, also enhance detumescence, sterilizes the compatibility collaboration killed the virus, and drug effect is mutual
Effect, drug effect is stronger, and external application almost also finds no adverse reaction, also finds no shortcoming.Since Radix Isatidis has heat-clearing solution
The effect of poison sterilizing, in raw material plus Radix Isatidis also plays the role of the anti-inflammatory that sterilizes to hepatitis A and hepatitis B, if be used alone pair
Kill that germ virus function is little, medical field external for these years thinks that the Chinese medicine of China is not sterilized, and does not kill the virus, in fact in
Medicine all needs compatible use, can not only enhance drug effect, while avoids Chinese medicine sterilizing and kill the virus the shortcomings that slow, passes through drug matching
The characteristics of use, can not only kill hepatitis A virus, hepatitis B and AIDS virus but also speed is fast.In addition, in digestion process
In, boiling three times is all blown open with heating, is warming up to 80 DEG C.
Equipment used in a kind of above-mentioned pure Chinese medicine disinfectant of the present invention is described further with reference to attached drawing Fig. 1.
The a kind of of the present invention prepares equipment used in above-mentioned pure Chinese medicine disinfectant, including sequentially connected reaction kettle 1, mistake
Filter 5, conservation tank 7, concentration tank 8, cooling for reflux tank 11 and vacuum pressure tank 13, the reaction kettle 1 are connected with filter 5, institute
It states filter 5 to connect with the conservation tank 7, the conservation tank 7 is connected with the concentration tank 8, the concentration tank 8 and the cooling
Return tank 11 connects, and the cooling for reflux tank 11 is connected with the vacuum pressure tank 13.In this way, by the medicinal material in reaction kettle 1 into
Vacuum pressure tank 13 is opened in row boiling, and liquid is made to pass through filter 5 and is entered in conservation tank 7, due to vacuum pressure, air is cold
But 11 internal circulation flow of return tank, the liquid in conservation tank 7, which is inhaled into concentration tank 8, to be concentrated.Whole concentration extractions are complete
Cheng Hou, remaining medicinal material residue can be used for pasture, avoid wasting.In front on the basis of technical solution further preferably
Scheme be:Mateiral pump 6 is equipped between the filter 5 and the conservation tank 7.In this way, the effect of mateiral pump 6 is to take out liquid
Enter into filter 5, liquid enters conservation tank 7 after the filtering by filter 5 medium to be concentrated, filter 5 ensure that into
Enter in conservation tank 7 liquid purity, free from admixture, improve the quality of liquid.Specifically may be used on the basis of technical solution in front
To be:The mateiral pump 6 is stainless steel mateiral pump 6.In this way, because Chinese medicine is easy to generate to the sensibility of ferroso-ferric oxide
Chemical reaction, had both changed the property of Chinese medicine, and had also generated the toxicity being pernicious to people, if may be fatal for taking orally one or two people,
External application generates skin allergic reaction or generates toxic side effect, using stainless steel mateiral pump 6, makes liquid pure, produced by avoiding
Chemical reaction after toxicity, damaged to people.It specifically can also be on the basis of technical solution in front:The reaction kettle
1 is equipped with thermometer 2, pressure gauge 3 and gas outlet 4.In this way, thermometer 2 is used to monitor the boiling temperature in reaction kettle 1, avoid
The precipitation too high or too low for temperature for influencing liquid;The effect of pressure gauge 3 is to monitor the pressure value of reaction kettle 1, is avoided in reaction kettle 1
Pressure crosses the volatilization of ambassador's liquid and causes to waste, and then gas outlet 4 can be put in the temperature or hypertonia in reaction kettle 1
Gas disposal ensures that the pressure in reaction kettle 1 does not exceed preset range.It in front specifically can be on the basis of technical solution
It is:The concentration tank 8 is equipped with peep hole 10, gas outlet 4 and discharge port 15.In this way, peep hole 10 so as to observing at any time
Concentration situation in concentration tank 8, and gas outlet 4 is ensured in concentration tank 8 for deflating when pressure is excessive in concentration tank 8
Pressure is maintained in suitable range, and liquid is avoided to occur the situation of floating roof in concentration process or runs liquid, causes the wave of liquid
Take, after the completion of liquid concentration, the semi-finished product concentrated are picked out from discharge port 15 spare.In front on the basis of technical solution
Specifically it can also be:Radiator 14 is equipped between the cooling for reflux tank 11 and the vacuum pressure tank 13.In this way, radiator 14
Effect be ensure pipeline in pressure and pipeline interior air-flow normal reflow.It is specific on the basis of technical solution in front
It can also be:The vacuum pressure tank 13 is equipped with pressure gauge 3.In this way, pressure gauge 3 is used to monitor the pressure in vacuum pressure tank 13
Power ensures that the air-flow in equipment can be with proper flow.
A kind of pure Chinese medicine disinfectant of the present invention is described further with reference to specific embodiment.
Embodiment 1
A. raw material prepares:Root bark of tree peony 25kg, Cortex Magnoliae Officinalis 15kg, honeysuckle 5kg, Radix Isatidis 10kg, Cortex Phellodendri 5kg, rheum officinale 5kg, hundred
98% medicinal alcohol of portion 5kg and 525kg;
B. it impregnates:Medicinal material in step A is put into reaction kettle 1, the 98% medical wine of 525kg is added in into reaction kettle 1
Essence is thoroughly impregnated medicinal material, impregnates 6 hours, obtains fully absorbing the wet medicinal material after alcohol;
C. boiling and initial concentration:The wet medicinal material for fully absorbing alcohol obtained in step B is subjected to boiling three times, specifically
It is as follows:First time boiling:80 DEG C are heated to reaction kettle 1, then 80 DEG C of holding constant temperature 3 hours, filter and liquid is simultaneously evacuated to storage
In standby tank 7, liquid is drawn into concentration tank 8 by unlatching vacuum pressure tank 13 once to be concentrated, and thickening temperature is 80 DEG C, pressure
Maintain 3 atmospheric pressure;Second of boiling:98% medicinal alcohol of 385kg is added in into reaction kettle 1, is heated to reaction kettle 1
To 80 DEG C, then 80 DEG C of holding constant temperature 2 hours, filters and simultaneously liquid is evacuated in conservation tank 7, liquid then is drawn into concentration tank
The liquid obtained in 8 with first time boiling, which mixes, carries out secondary concentration, and the temperature of secondary concentration is 80 DEG C, and pressure maintains 3
Atmospheric pressure;Third time boiling:98% medicinal alcohol of 385kg is added in into reaction kettle 1, is heated to 80 DEG C to reaction kettle 1, so
80 DEG C of holding constant temperature 1 hour afterwards filters and simultaneously liquid is evacuated in conservation tank 7, is then drawn into liquid in concentration tank 8 and first
The liquid mixing that secondary boiling and second of boiling obtain is concentrated three times, and thickening temperature is 80 DEG C, and the time of concentration is 60 points
Clock can obtain initial concentration admixing medical solutions;
D. final concentration:The initial concentration admixing medical solutions obtained in step C are heated, temperature is 60 DEG C, pressure control
For system in 0.8 atmospheric pressure, heating makes liquid be condensed into the traditional Chinese medicinal ointment that density is 1 for 60 minutes, then puts the traditional Chinese medicinal ointment concentrated
Go out into medicinal liquor barrel spare, configuration commodity liquid;
E. match liquid:With the traditional Chinese medicinal ointment of 20kg, the peppermint of 1kg, 98% medicinal alcohol of 54kg and the distilled water of 25kg, match
Required commodity liquid is made.
Embodiment 2
A. raw material prepares:Root bark of tree peony 50kg, Cortex Magnoliae Officinalis 30kg, honeysuckle 10kg, Radix Isatidis 20kg, Cortex Phellodendri 10kg, rheum officinale 5kg,
98% medicinal alcohol of the tuber of stemona 5kg and 975kg;
B. it impregnates:Medicinal material in step A is put into reaction kettle 1, the 98% medical wine of 975kg is added in into reaction kettle 1
Essence is thoroughly impregnated medicinal material, impregnates 12 hours, obtains fully absorbing the wet medicinal material after alcohol;
C. boiling and initial concentration:The wet medicinal material for fully absorbing alcohol obtained in step B is subjected to boiling three times, specifically
It is as follows:First time boiling:80 DEG C are heated to reaction kettle 1, then 80 DEG C of holding constant temperature 3 hours, filter and liquid is simultaneously evacuated to storage
In standby tank 7, liquid is drawn into concentration tank 8 by unlatching vacuum pressure tank 13 once to be concentrated, and thickening temperature is 85 DEG C, pressure
Maintain 2 atmospheric pressure;Second of boiling:98% medicinal alcohol of 715kg is added in into reaction kettle 1, is heated to reaction kettle 1
To 80 DEG C, then 80 DEG C of holding constant temperature 2 hours, filters and simultaneously liquid is evacuated in conservation tank 7, liquid then is drawn into concentration tank
The liquid obtained in 8 with first time boiling, which mixes, carries out secondary concentration, 85 DEG C of the temperature of secondary concentration, and pressure maintains 2 big
Air pressure;Third time boiling:98% medicinal alcohol of 715kg is added in into reaction kettle 1, is heated to 80 DEG C to reaction kettle 1, then
It keeps 80 DEG C of constant temperature 1 hour, filters and simultaneously liquid is evacuated in conservation tank 7, then liquid is drawn into concentration tank 8 and for the first time
The liquid mixing that boiling and second of boiling obtain is concentrated three times, and thickening temperature is 85 DEG C, and the time of concentration is 60 minutes,
It can obtain initial concentration admixing medical solutions;
D. final concentration:The initial concentration admixing medical solutions obtained in step C are heated, temperature is 70 DEG C, pressure control
For system in 0.6 atmospheric pressure, heating makes liquid be condensed into the traditional Chinese medicinal ointment that density is 1 for 50 minutes, then puts the traditional Chinese medicinal ointment concentrated
Go out into medicinal liquor barrel spare, configuration commodity liquid;
E. match liquid:With the traditional Chinese medicinal ointment of 20kg, the peppermint of 1kg, 98% medicinal alcohol of 55kg and the distilled water of 24kg, match
Required commodity liquid is made.
Embodiment 3
A. raw material prepares:Root bark of tree peony 30kg, Cortex Magnoliae Officinalis 35kg, honeysuckle 15kg, Radix Isatidis 15kg, Cortex Phellodendri 15kg, rheum officinale 10kg,
98% medicinal alcohol of the tuber of stemona 10kg and 975kg;
B. it impregnates:Medicinal material in step A is put into reaction kettle 1, the 98% medical wine of 975kg is added in into reaction kettle 1
Essence is thoroughly impregnated medicinal material, impregnates 10 hours, obtains fully absorbing the wet medicinal material after alcohol;
C. boiling and initial concentration:The wet medicinal material for fully absorbing alcohol obtained in step B is subjected to boiling three times, specifically
It is as follows:First time boiling:80 DEG C are heated to reaction kettle 1, then 80 DEG C of holding constant temperature 3 hours, filter and liquid is simultaneously evacuated to storage
In standby tank 7, liquid is drawn into concentration tank 8 by unlatching vacuum pressure tank 13 once to be concentrated, and thickening temperature is 90 DEG C, pressure
Maintain 2 atmospheric pressure;Second of boiling:98% medicinal alcohol of 715kg is added in into reaction kettle 1, is heated to reaction kettle 1
To 80 DEG C, then 80 DEG C of holding constant temperature 2 hours, filters and simultaneously liquid is evacuated in conservation tank 7, liquid then is drawn into concentration tank
The liquid obtained in 8 with first time boiling, which mixes, carries out secondary concentration, and the temperature of secondary concentration is 90 DEG C, and pressure maintains 2
Atmospheric pressure;Third time boiling:98% medicinal alcohol of 715kg is added in into reaction kettle 1, is heated to 80 DEG C to reaction kettle 1, so
80 DEG C of holding constant temperature 1 hour afterwards filters and simultaneously liquid is evacuated in conservation tank 7, is then drawn into liquid in concentration tank 8 and first
The liquid mixing that secondary boiling and second of boiling obtain is concentrated three times, and thickening temperature is 90 DEG C, and the time of concentration is 50 points
Clock can obtain initial concentration admixing medical solutions;
D. final concentration:The initial concentration admixing medical solutions obtained in step C are heated, temperature is 70 DEG C, pressure control
For system in 0.6 atmospheric pressure, heating makes liquid be condensed into the traditional Chinese medicinal ointment that density is 1 for 60 minutes, then puts the traditional Chinese medicinal ointment concentrated
Go out into medicinal liquor barrel spare, configuration commodity liquid;
E. match liquid:With the traditional Chinese medicinal ointment of 20kg, the peppermint of 1kg, 98% medicinal alcohol of 50kg and the distilled water of 24kg, match
Required commodity liquid is made.
It is above-mentioned that only several specific embodiments in the present invention are illustrated, but can not be as the protection model of the present invention
Enclose, it is every according to the present invention in design spirit made by equivalent change or modification, be deemed to fall the present invention protection
Range.
Claims (8)
1. a kind of pure Chinese medicine disinfectant, it is characterised in that:It is prepared by following steps:
A. raw material prepares:6-10 parts of the root bark of tree peony, 3-7 parts of Cortex Magnoliae Officinalis, 1-3 parts of honeysuckle, 2-5 parts of Radix Isatidis, 1-3 parts of Cortex Phellodendri, rheum officinale 1-3
98% medicinal alcohol of 7.5 times of part, 1-3 parts of the tuber of stemona and input medicinal material total amount;
B. it impregnates:Medicinal material in step A is put into reaction kettle, 98% medicinal alcohol is added in into reaction kettle, is thoroughly impregnated medicine
Material impregnates 6-12 hours, obtains fully absorbing the wet medicinal material after alcohol;
C. boiling and initial concentration:The wet medicinal material for fully absorbing alcohol obtained in step B is subjected to boiling three times, specifically such as
Under:First time boiling:80 DEG C are heated to reaction kettle, then 80 DEG C of holding constant temperature 3 hours, filter and liquid is simultaneously evacuated to conservation tank
In, liquid is drawn into concentration tank by unlatching vacuum pressure tank once to be concentrated, and thickening temperature is 80-90 DEG C, and pressure maintains
In 2-3 atmospheric pressure;Second of boiling:98% medicinal alcohol of 5.5 times of input medicinal material total amount is added in into reaction kettle, to anti-
Kettle is answered to be heated to 80 DEG C, then 80 DEG C of holding constant temperature 2 hours, filter and simultaneously liquid is evacuated in conservation tank, then suck liquid
The liquid obtained into concentration tank with first time boiling, which mixes, carries out secondary concentration, and the temperature of secondary concentration is 80-90 DEG C, pressure
Maintain 2-3 atmospheric pressure;Third time boiling:98% medicinal alcohol of 5.5 times of input medicinal material total amount is added in into reaction kettle,
80 DEG C are heated to reaction kettle, then 80 DEG C of holding constant temperature 1 hour, filter and simultaneously liquid is evacuated in conservation tank, then by liquid
It is drawn into the liquid obtained in concentration tank with first time boiling and second of boiling and mixes and concentrated three times, thickening temperature is
80-90 DEG C, the time control of concentration can obtain initial concentration admixing medical solutions at 50-60 minutes;
D. final concentration:The initial concentration admixing medical solutions obtained in step C are heated, temperature control is at 60-70 DEG C, pressure
In 0.6-0.8 atmospheric pressure, heating makes liquid be condensed into the traditional Chinese medicinal ointment that density is 0.9-1 for 50-60 minutes for control, then will concentration
Good traditional Chinese medicinal ointment is released to spare in medicinal liquor barrel, configuration commodity liquid;
E. match liquid:With traditional Chinese medicinal ointment that parts by weight are 1-20 parts, 0.1-5 parts of peppermint, 5-30 parts of 98% medicinal alcohol and
1-30 parts of distilled water is configured to required commodity liquid.
2. a kind of equipment used in pure Chinese medicine disinfectant described in claim 1, it is characterised in that:Including sequentially connected anti-
Kettle, filter, conservation tank, concentration tank, cooling for reflux tank and vacuum pressure tank are answered, the reaction kettle is connected with filter, described
Filter is connected with the conservation tank, and the conservation tank is connected with the concentration tank, the concentration tank and the cooling for reflux tank
Connection, the cooling for reflux tank are connected with the vacuum pressure tank.
3. equipment used in a kind of pure Chinese medicine disinfectant according to right wants 2, it is characterised in that:The filter and institute
It states and mateiral pump is equipped between conservation tank.
4. equipment used in a kind of pure Chinese medicine disinfectant according to right wants 3, it is characterised in that:The mateiral pump is not
Become rusty steel mateiral pump.
5. equipment used in a kind of pure Chinese medicine disinfectant according to claim 4, it is characterised in that:On the reaction kettle
Equipped with thermometer, pressure gauge and gas outlet.
6. equipment used in a kind of pure Chinese medicine disinfectant according to claim 5, it is characterised in that:On the concentration tank
Equipped with peep hole, gas outlet and discharge port.
7. equipment used in a kind of pure Chinese medicine disinfectant according to claim 2-6 any one claims, special
Sign is:Radiator is equipped between the cooling for reflux tank and the vacuum pressure tank.
8. equipment used in a kind of pure Chinese medicine disinfectant according to claim 7, it is characterised in that:The vacuum pressure
Tank is equipped with pressure gauge.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109288728A (en) * | 2018-11-27 | 2019-02-01 | 南通优护优家卫生用品有限公司 | The alcohol disinfecting agent that can be foamed |
CN115463449A (en) * | 2022-09-13 | 2022-12-13 | 太极集团重庆涪陵制药厂有限公司 | Traditional chinese medicine constant temperature filtration system |
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CN1075602A (en) * | 1992-02-22 | 1993-09-01 | 天津市中医研究所 | Efficient Chinese medicine antiseptic and preparation technology thereof |
WO2006035561A1 (en) * | 2004-09-28 | 2006-04-06 | Xirem Laboratory, Inc. | Antipathogenic house, disinfectant for houses, disinfectant for living organisms and feed and drinking water for animals |
CN103054923A (en) * | 2013-01-04 | 2013-04-24 | 霸王(广州)有限公司 | Method and device for carrying out dynamic and continuous circulating extraction on total triterpenoid saponin in yerbadetajo herb medicinal material |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109288728A (en) * | 2018-11-27 | 2019-02-01 | 南通优护优家卫生用品有限公司 | The alcohol disinfecting agent that can be foamed |
CN115463449A (en) * | 2022-09-13 | 2022-12-13 | 太极集团重庆涪陵制药厂有限公司 | Traditional chinese medicine constant temperature filtration system |
CN115463449B (en) * | 2022-09-13 | 2024-04-12 | 太极集团重庆涪陵制药厂有限公司 | Traditional chinese medicine constant temperature infiltration system |
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Application publication date: 20180619 |