CN1199722A - Bacterial active humate and its production - Google Patents

Bacterial active humate and its production Download PDF

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Publication number
CN1199722A
CN1199722A CN 97107503 CN97107503A CN1199722A CN 1199722 A CN1199722 A CN 1199722A CN 97107503 CN97107503 CN 97107503 CN 97107503 A CN97107503 A CN 97107503A CN 1199722 A CN1199722 A CN 1199722A
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kilograms
humic acid
acid salt
disease germs
activated humic
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CN 97107503
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Chinese (zh)
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王家祥
易学良
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Individual
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Individual
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Priority to CN 97107503 priority Critical patent/CN1199722A/en
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Abstract

The bacterial active humate contains biological potassium humate, butyric acid bacteria, saccharomycetes, nitrogen fixing bacteria, humic acid, etc. It is produced through the processes of crushing and oxidizing humus, mixing with organic weak acid for catalysis, stacking for 1-15 days, spraying the solution of other inorganic salt, inoculating strain, natural fermentation for 1-15 days, addition of KOH to regulate pH into neutral and stacking for ripening at room temperature. It has high activity, slowly releasing of fertilizer effect and high fertilizer effect.

Description

A kind of activated humic acid salt and production method thereof of carrying disease germs
The present invention relates to a kind of agricultural fertilizer, it is particularly related to a kind of carry disease germs activated humic acid salt and production method thereof that adopts oxidation style to produce.
Before the present invention proposed, adopting humic acids had been very general situation as agricultural fertilizer.But, natural humate active low, the result of use of fertilizer is not fine.Its reason is the active low of natural humic acid, and effect of fertilizer is not obvious.People have adopted the method for oxidation in order to change this phenomenon, to improve the fertilizer efficiency that matter is planted in corruption, as adopting the way of gas blower air blast, quicken rotten oxidation of planting matter, have improved rotten activity of planting matter to a certain extent.In order to improve the fertilizer efficiency that matter is planted in corruption, also in fertilizer, to transplant mushrooms such as root nodule bacterium, or add additive such as potassiumphosphate etc., its method is a lot, and its purpose all is in order to improve the fertilizer efficiency that matter is planted in corruption.
Also there is relevant technology to disclose in the Chinese patent.As the disclosed application number of Chinese patent application is 93102447.1, and publication number is " brown coal microbial fertilizer and the manufacture method thereof " of CN1081173A, and wherein said brown coal promptly are a kind of of humic acids.Its disclosed technology is that brown coal are pulverized, and introduces bacterial classification, through cultivating, mixing, adds potash fertilizer, phosphate fertilizer, nitrogenous fertilizer etc. again.The purpose of doing so also is to improve the fertilizer efficiency that matter is planted in corruption.But it does not adopt the way of oxidation to improve rotten activity of planting matter, and its effect is very limited.Disclosed another part patent application of Chinese patent also discloses relevant content.Chinese patent application 93114815.4, publication number is called the technology of " five in one special organic fertilizer " for the CN1104617A name, and it melts fertilizer, bacterial manure, chemical fertilizer, little fertilizer, humic acid fertilizer in one based on fertilizer.Its technical spirit is with these Fertilizer Combination, improves its fertilizer efficiency, but its disclosed technology is very insufficient, and technician of the same trade can not implement it.Chinese patent application 95101224.X, publication number is that CN1110674A discloses the patent application of " compound full price fertilizer series product and complete producing technology ", and it has adopted trace element, humic acids, rare earth class material, enzymatic material, active carrier, plant growth hormones, disease-resistant fungus matter etc. to produce so-called compound full price fertilizer.In sum, more than in the disclosed patent application technology, corruption is planted the activity of matter and is not given full play to, fertilizer utilize situation unsatisfactory, the technology of a practicality must be provided, give full play to the potential fertility that matter fertilizer is planted in corruption, make increases in grain production.
The object of the present invention is to provide a kind of method that adopts the oxidation corruption to plant matter, add mushroom thing, rare earth element, produce carry disease germs activated humic acid salt and production method thereof, give full play to the purpose that corruption is planted the potential fertility of matter fertilizer, made increases in grain production to reach.
Purpose of the present invention can realize by following technical measures.
This activated humic acid salt that carries disease germs, its composition is as follows:
In per 1000 kilograms of activated humic acid salt that carry disease germs:
400 kilograms-950 kilograms in biological humic potassium
1,000,000,000-3,000,000,000/gram of butyric bacteria
1,000,000,000-3,000,000,000/gram of yeast
1,000,000,000-3,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
In order to produce the activated humic acid salt that carries disease germs, should be undertaken by following prescription:
1000 kilograms of activated humic acid salt that carry disease germs of every production need:
10 kilograms-20 kilograms of oxygenant double centner-150 kilogram organic monoacids
3 kilograms-4 kilograms of 40 kilograms of-140 kilograms of molybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
3 kilograms-4 kilograms in ferrous sulfate
Above raw material is the industrial chemicals of technical pure level.
681.89 kilograms-843.89 kilograms of matter are planted in the corruption of status nascendi
Concrete production method is: at room temperature the corruption of status nascendi is planted matter and pulverize, send in the reactor, spray oxygenant and carry out oxidizing reaction, place after 1-8 hour, add organic monoacid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 1-15 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 1-15 days, add potassium hydroxide again, adjust its pH value for neutral, stack slaking in 1-10 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.
Above-mentioned oxygenant is hydrogen peroxide (H 2O 2) or potassium permanganate (KMnO 4) organic monoacid is acetic acid (CH 3COOH), molybdate is a Sodium orthomolybdate.
Principle of the present invention is: this product is as a kind of important carrier of all-nutritious active bio-fertilizer and raw material.Its feature be with have to metallic cation produce complexing efficiently, ion exchangeable, have a large amount of nutrition storehouse of nonactive humate that carry disease germs as farm crop, utilize sulfate radical as carrier, macroelement and various trace elements etc. can be absorbed by crop and utilize slowly, effectively, for a long time, adapt to the needs of various different steps farm crop.This product not only can satisfy the absorption of farm crop to the ionic condition element, can also satisfy the needs of crop root to some small molecules, organism, gaseous state nutrition, thus the conversion, the storage that improve biological substance effectively.If this product combines with the fertilizer formula of science, can make join fertilizer and play effect efficient, long-acting, full effect.
This product has the tangible advantage of effect of increasing production compared with the prior art.It is in particular in the following aspects:
1. rotten activity of planting matter effectively improves.Owing to adopted effective oxidation measure, added the strong oxidizer hydrogen peroxide, generate activated humic acid, the activity that makes corruption plant matter is significantly strengthened.
2. adopted trace elements such as molybdenum, nickel, cobalt, made itself and humic acids form metal complex, its fertilizer efficiency is slowly discharged, can not produce the situation that crop is burnt to death, and improve the fertilizer efficiency of little fertilizer.
3. use vitriol as fertilizer sources transportation means, made fertilizer be convenient to crop and absorb, improved the utilization benefit of fertilizer.
4. adopted introduction butyric bacteria, vinelandii, saccharomycetic bacterial classification, and to plant matter with active corruption be carrier, breed these bacteriums in a large number, reached the fertilizer efficiency of bacterial manure.
In sum, this product is planted the approach of matter and is started with from activating corruption, has adopted a technology such as little fertilizer, bacterial manure, formed the activated humic acid salt that carries disease germs, having improved rotten comprehensive fertilizer efficiency of planting matter, had favorable economic benefit and social benefit, is that matter fertilizer is planted in a kind of corruption efficiently.This product both can be used separately, and former section in the middle of can be used as again with composite uses such as fertilizer, inorganic fertilizers, is a kind of ideal humic acid fertilizer.
Description of drawings of the present invention.
Fig. 1. production scheme of the present invention.
Embodiments of the invention:
Embodiment one.
This activated humic acid salt that carries disease germs in per 1000 kilograms activated humic acid salt that carries disease germs, comprises by following material and forming:
In per 1000 kilograms of activated humic acid salt that carry disease germs:
400 kilograms in biological humic potassium
1,000,000,000/gram of butyric bacteria
1,000,000,000/gram of yeast
1,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
For producing the above-mentioned activated humic acid salt that carries disease germs, need to be undertaken by following prescription: 1000 kilograms of activated humic acid salt that carry disease germs of every production need:
10 kilograms of hydrogen peroxide double centner acetic acid
3 kilograms of 40 kilograms of Sodium orthomolybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
3 kilograms in ferrous sulfate
Above raw material is the industrial chemicals of technical pure level.
843.89 kilograms of matter are planted in the corruption of status nascendi
Concrete Production Flow Chart is: at room temperature the corruption of status nascendi is planted matter and pulverize, send in the reactor, spray oxygenant and carry out oxidizing reaction, place after 1 hour, add organic monoacid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 8 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 1 day, add potassium hydroxide again, adjust its pH value for neutral, stack slaking in 5 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.
Embodiment two.
This activated humic acid salt that carries disease germs in per 1000 kilograms activated humic acid salt that carries disease germs, comprises by following material and forming:
In per 1000 kilograms of activated humic acid salt that carry disease germs:
950 kilograms in biological humic potassium
3,000,000,000/gram of butyric bacteria
3,000,000,000/gram of yeast
3,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
For producing the above-mentioned activated humic acid salt that carries disease germs, need to be undertaken by following prescription: 1000 kilograms of activated humic acid salt that carry disease germs of every production need:
20 kilograms of 150 kilograms of acetic acid of hydrogen peroxide
4 kilograms of 140 kilograms of Sodium orthomolybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
4 kilograms in ferrous sulfate
Above raw material is the industrial chemicals of technical pure level.
681.89 kilograms of matter are planted in the corruption of status nascendi
Concrete Production Flow Chart is: at room temperature the corruption of status nascendi is planted matter and pulverize, send in the reactor, spray oxygenant and carry out oxidizing reaction, place after 8 hours, add organic monoacid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 15 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 15 days, add potassium hydroxide again, adjust its pH value for neutral, stack slaking in 10 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.
Embodiment three.
This activated humic acid salt that carries disease germs in per 1000 kilograms activated humic acid salt that carries disease germs, comprises by following material and forming:
760 kilograms in biological humic potassium
2,500,000,000/gram of butyric bacteria
2,500,000,000/gram of yeast
2,500,000,000/gram of vinelandii
Surplus is an activated humic acid.
For producing the above-mentioned activated humic acid salt that carries disease germs, need to be undertaken by following prescription: 1000 kilograms of activated humic acid salt that carry disease germs of every production need
15 kilograms of 120 kilograms of acetic acid of hydrogen peroxide
3.54 kilograms of 90 kilograms of Sodium orthomolybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
4 kilograms in ferrous sulfate
Above raw material is the industrial chemicals of technical pure level.
Surplus is that 767.35 kilograms of matter are planted in the corruption of status nascendi.
Concrete Production Flow Chart is: at room temperature the corruption of status nascendi is planted matter and pulverize, send in the reactor, spray hydrogen peroxide and carry out oxidizing reaction, place after 2 hours, add organic monoacid acetic acid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 2 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 8 days, add potassium hydroxide again, adjusting its pH value is 7.0, stack slaking in 2 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.
Embodiment four.
This activated humic acid salt that carries disease germs in per 1000 kilograms activated humic acid salt that carries disease germs, comprises by following material and forming:
570 kilograms in biological humic potassium
3,000,000,000/gram of butyric bacteria
3,000,000,000/gram of yeast
3,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
For producing the above-mentioned activated humic acid salt that carries disease germs, need to be undertaken by following prescription: 1000 kilograms of activated humic acid salt that carry disease germs of every production need
20 kilograms of 150 kilograms of acetic acid of hydrogen peroxide
3.5 kilograms of 90 kilograms of Sodium orthomolybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
4 kilograms in ferrous sulfate
Above raw material is the industrial chemicals of technical pure level.
Surplus is that matter 732.39 is planted in the corruption of status nascendi.
Concrete Production Flow Chart is: at room temperature the corruption of status nascendi is planted matter and pulverize, send in the reactor, spray hydrogen peroxide and carry out oxidizing reaction, place after 2 hours, add organic monoacid acetic acid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 2 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 8 days, add potassium hydroxide again, adjusting its pH value is 6.5, stack slaking in 2 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.
Embodiment five.
This activated humic acid salt that carries disease germs in per 1000 kilograms activated humic acid salt that carries disease germs, comprises by following material and forming:
886 kilograms in biological humic potassium
3,000,000,000/gram of butyric bacteria
3,000,000,000/gram of yeast
3,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
For producing the above-mentioned activated humic acid salt that carries disease germs, need to be undertaken by following prescription: 1000 kilograms of activated humic acid salt that carry disease germs of every production need
10 kilograms of hydrogen peroxide double centner acetic acid
4 kilograms of 140 kilograms of Sodium orthomolybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
4 kilograms in ferrous sulfate
Above raw material is the industrial chemicals of technical pure level.
Surplus is that 741.89 kilograms of matter are planted in the natural corruption of status nascendi.
Concrete Production Flow Chart is: at room temperature the corruption of status nascendi is planted matter and pulverize, send in the reactor, spray hydrogen peroxide and carry out oxidizing reaction, place after 1 hour, add organic monoacid acetic acid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 10 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 8 days, add potassium hydroxide again, adjusting its pH value is 7.0, stack thermalization in 2 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.

Claims (4)

1. activated humic acid salt that carries disease germs is characterized in that it comprises by following material to form:
In per 1000 kilograms of activated humic acid salt that carry disease germs:
400 kilograms-950 kilograms in biological humic potassium
1,000,000,000-3,000,000,000/gram of butyric bacteria
1,000,000,000-3,000,000,000/gram of yeast
1,000,000,000-3,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
2. a kind of activated humic acid salt that carries disease germs according to claim 1 is characterized in that wherein said best composition is:
In per 1000 kilograms of activated humic acid salt that carry disease germs:
950 kilograms in biological humic potassium
3,000,000,000/gram of butyric bacteria
3,000,000,000/gram of yeast
3,000,000,000/gram of vinelandii
Surplus is an activated humic acid.
3. produce the method for the activated humic acid salt that carries disease germs, its special seized with terror being:
A. produce the activated humic acid salt that carries disease germs, undertaken by following prescription:
1000 kilograms of activated humic acid salt that carry disease germs of every production need:
10 kilograms-20 kilograms of oxygenant double centner-150 kilogram organic monoacids
3 kilograms-4 kilograms of 40 kilograms of-140 kilograms of molybdates of potassium hydroxide
Single nickel salt 100 gram rose vitriols 10 grams
3 kilograms-4 kilograms in ferrous sulfate
681.89 kilograms-843.89 kilograms of matter are planted in the corruption of status nascendi
B. at room temperature the corruption of status nascendi being planted matter pulverizes, send in the reactor, spray oxygenant and carry out oxidizing reaction, place after 1-8 hour, add organic monoacid and carry out catalysis, behind the stirring and evenly mixing, stack and sprayed that molybdic acid is received in 1-15 days again, behind the aqueous solution of ferrous sulfate, rose vitriol, single nickel salt, insert butyric bacteria, vinelandii, saccharomycetic bacterial classification, make its natural biology breeding fermentation 1-15 days, add potassium hydroxide again, adjust its pH value for neutral, stack slaking in 1-10 days under the room temperature, promptly form the activated humic acid salt finished product that carries disease germs.
4. the carry disease germs method of activated humic acid salt of production according to claim 3, it is special seized with terror be wherein oxygenant be hydrogen peroxide (H 2O 2) or potassium permanganate (KMnO 4), organic monoacid is acetic acid (CH 3COOH), molybdate is a Sodium orthomolybdate.
CN 97107503 1997-05-21 1997-05-21 Bacterial active humate and its production Pending CN1199722A (en)

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Application Number Priority Date Filing Date Title
CN 97107503 CN1199722A (en) 1997-05-21 1997-05-21 Bacterial active humate and its production

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Application Number Priority Date Filing Date Title
CN 97107503 CN1199722A (en) 1997-05-21 1997-05-21 Bacterial active humate and its production

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CN1199722A true CN1199722A (en) 1998-11-25

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103467144A (en) * 2012-06-06 2013-12-25 福建省诏安县绿洲生化有限公司 Refined fulvic-acid-containing agricultural microbial inoculum and production method thereof
CN104446786A (en) * 2014-11-25 2015-03-25 武汉皓达农业科技有限公司 Method for preparing organic water-soluble fertilizer
CN105838326A (en) * 2016-04-28 2016-08-10 北京联合大学 Ecological rehabilitation promoting snow-melting agent and preparation method thereof
CN106278525A (en) * 2016-07-14 2017-01-04 北京澳佳生态农业股份有限公司 A kind of activated humic acid, containing its chelating fertilizer and preparation method thereof
CN108558568A (en) * 2018-05-04 2018-09-21 保山保农农业开发股份有限公司 A kind of preparation method of the material containing humic acid organic fertilizer
CN109867567A (en) * 2019-04-11 2019-06-11 云南德坤生物科技有限公司 A kind of preparation method of the humic acid biological bacterial manure of the small molecule of base containing potassium carbon
CN111793501A (en) * 2020-08-06 2020-10-20 辜锐 Soil conditioner and preparation method thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103467144A (en) * 2012-06-06 2013-12-25 福建省诏安县绿洲生化有限公司 Refined fulvic-acid-containing agricultural microbial inoculum and production method thereof
CN103467144B (en) * 2012-06-06 2015-01-07 福建省诏安县绿洲生化有限公司 Refined fulvic-acid-containing agricultural microbial inoculum and production method thereof
CN104446786A (en) * 2014-11-25 2015-03-25 武汉皓达农业科技有限公司 Method for preparing organic water-soluble fertilizer
CN105838326A (en) * 2016-04-28 2016-08-10 北京联合大学 Ecological rehabilitation promoting snow-melting agent and preparation method thereof
CN106278525A (en) * 2016-07-14 2017-01-04 北京澳佳生态农业股份有限公司 A kind of activated humic acid, containing its chelating fertilizer and preparation method thereof
CN108558568A (en) * 2018-05-04 2018-09-21 保山保农农业开发股份有限公司 A kind of preparation method of the material containing humic acid organic fertilizer
CN109867567A (en) * 2019-04-11 2019-06-11 云南德坤生物科技有限公司 A kind of preparation method of the humic acid biological bacterial manure of the small molecule of base containing potassium carbon
CN111793501A (en) * 2020-08-06 2020-10-20 辜锐 Soil conditioner and preparation method thereof

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