CN118632823B - 含SiO2Al2O3溶胶溶液的合成方法和多孔质氧化铝膜的形成方法 - Google Patents

含SiO2Al2O3溶胶溶液的合成方法和多孔质氧化铝膜的形成方法

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Publication number
CN118632823B
CN118632823B CN202380019058.8A CN202380019058A CN118632823B CN 118632823 B CN118632823 B CN 118632823B CN 202380019058 A CN202380019058 A CN 202380019058A CN 118632823 B CN118632823 B CN 118632823B
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solution
sio
sol
sol solution
concentration
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CN118632823A (zh
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长谷川章
冈田治
中村宽美
小笠原静香
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Research On New Energy Of Corp
Institute of National Colleges of Technologies Japan
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Research On New Energy Of Corp
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/02—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the alkali- or alkaline earth metals or beryllium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/031—Precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/141—Preparation of hydrosols or aqueous dispersions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/44—Dehydration of aluminium oxide or hydroxide, i.e. all conversions of one form into another involving a loss of water
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5025—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with ceramic materials
    • C04B41/5031—Alumina
    • C—CHEMISTRY; METALLURGY
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    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/85—Coating or impregnation with inorganic materials
    • C04B41/87—Ceramics
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/12—Silica and alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00793—Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/0081—Uses not provided for elsewhere in C04B2111/00 as catalysts or catalyst carriers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Structural Engineering (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Dispersion Chemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
CN202380019058.8A 2022-03-25 2023-03-20 含SiO2Al2O3溶胶溶液的合成方法和多孔质氧化铝膜的形成方法 Active CN118632823B (zh)

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Application Number Priority Date Filing Date Title
JP2022-050413 2022-03-25
JP2022050413 2022-03-25
PCT/JP2023/010790 WO2023182247A1 (ja) 2022-03-25 2023-03-20 ＳｉＯ２Ａｌ２Ｏ３含有ゾル溶液の合成方法、及び、多孔質アルミナ膜の形成方法

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US (2) US12343703B2 (https=)
EP (1) EP4458771B1 (https=)
JP (1) JP7678492B2 (https=)
KR (1) KR102753605B1 (https=)
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JP7678492B2 (ja) 2022-03-25 2025-05-16 株式会社ルネッサンス・エナジー・リサーチ ＳｉＯ２Ａｌ２Ｏ３含有ゾル溶液の合成方法、及び、多孔質アルミナ膜の形成方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101535182A (zh) * 2006-11-08 2009-09-16 日产化学工业株式会社 二氧化硅-氧化铝复合溶胶及其制造方法
CN103339061A (zh) * 2011-01-14 2013-10-02 株式会社新生能源研究 多孔质氧化铝材料及其制造方法、以及催化剂

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1275412B (it) * 1995-06-01 1997-08-05 Enichem Spa Procedimento per la preparazione di ossidi misti silice-allumina porosi in forma sferica
JP4065944B2 (ja) 2002-12-25 2008-03-26 独立行政法人産業技術総合研究所 高耐熱・高強度アルミナ多孔体の製造法
CN101225248A (zh) * 2007-01-16 2008-07-23 财团法人工业技术研究院 显色材料及其制备方法
JP2009061383A (ja) 2007-09-06 2009-03-26 Nagoya Institute Of Technology 耐熱性アルミナ担体とその製造方法
KR101137929B1 (ko) 2010-05-31 2012-05-09 에스케이하이닉스 주식회사 비휘발성 메모리 장치 및 그 제조 방법
EP2808081A4 (en) 2012-01-23 2015-08-26 N E Chemcat Corp BARIUM SULPHATE CONTAINING ALUMINUM MATERIAL AND EXHAUST GAS CLEANING CATALYST THEREOF
WO2014051091A1 (ja) 2012-09-28 2014-04-03 Dic株式会社 α－アルミナ微粒子及びその製造方法
CN108854870A (zh) * 2017-05-11 2018-11-23 北京化工大学 一种高纯度硅铝溶胶的制备方法
CN110844911A (zh) * 2019-12-20 2020-02-28 黄冈师范学院 一种利用含氟硅渣直接制备高纯白炭黑的方法
US20230105883A1 (en) 2020-03-26 2023-04-06 Renaissance Energy Research Corporation Porous alumina and catalyst
JP7678492B2 (ja) 2022-03-25 2025-05-16 株式会社ルネッサンス・エナジー・リサーチ ＳｉＯ２Ａｌ２Ｏ３含有ゾル溶液の合成方法、及び、多孔質アルミナ膜の形成方法

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101535182A (zh) * 2006-11-08 2009-09-16 日产化学工业株式会社 二氧化硅-氧化铝复合溶胶及其制造方法
CN103339061A (zh) * 2011-01-14 2013-10-02 株式会社新生能源研究 多孔质氧化铝材料及其制造方法、以及催化剂

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
姚楠等.溶胶凝胶法制备中孔分布集中的氧化物及混合氧化物催化材料.中国科学（B辑）.2001,第31卷(第4期),355-363. *
无定型Al2O3-2SiO2制备及地质聚合反应机理研究;郑广俭;中国博士学位论文全文数据库;20120715;第工程科技Ⅰ辑卷(第第7期期);51-53 *
无定形Al2O3-2SIO2制备及地质聚合反应机理研究;郑广俭;中国博士学位论文全文数据库工程科技Ⅰ辑;20120715(第7期);51-53 *
溶胶凝胶法制备中孔分布集中的氧化物及混合氧化物催化材料;姚楠等;中国科学（B辑）;20010831;第31卷(第4期);355-363 *

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WO2023182247A1 (ja) 2023-09-28
CN118632823A (zh) 2024-09-10
JP7678492B2 (ja) 2025-05-16
JPWO2023182247A1 (https=) 2023-09-28
US20250288974A1 (en) 2025-09-18
US20250041832A1 (en) 2025-02-06
US12440825B2 (en) 2025-10-14
KR20240125048A (ko) 2024-08-19
KR102753605B1 (ko) 2025-01-10
EP4458771A1 (en) 2024-11-06
US12343703B2 (en) 2025-07-01
EP4458771A4 (en) 2025-05-07
DK4458771T3 (da) 2026-02-09
EP4458771B1 (en) 2025-12-24

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