CN116115508A - Repairing, anti-wrinkle and beautifying mask liquid and preparation method thereof - Google Patents

Abstract

The application relates to a repairing, anti-wrinkle and beautifying mask liquid and a preparation method thereof, wherein the mask liquid comprises the following components in percentage by mass: 0.3 to 0.5 percent of betaine, 0.03 to 0.05 percent of sodium hyaluronate, 0.2 to 0.4 percent of p-hydroxyacetophenone, 0.1 to 0.2 percent of 1, 2-hexanediol, 0.1 to 0.2 percent of thickening agent, 0.08 to 0.12 percent of arginine, 0.42 to 0.62 percent of skin activating agent, 3.2 to 3.5 percent of grape juice, 0.03 to 0.05 percent of glutathione, 0.008 to 0.01 percent of lactobacillus plantarum, 0.1 to 0.2 percent of grape fruit extract, 1 to 3 percent of skin conditioning agent, 3 to 5 percent of butanediol and the balance of water; thickeners include carbomers and hydroxyethylcellulose; skin-activating agents include sodium carboxymethyl-beta-glucan; the skin conditioner comprises radix Cynanchi Atrati extract and herba Cynara scolymi leaf extract. The facial mask has the effects of improving the effects of repairing, resisting wrinkles and beautifying the face of the facial mask.

Description

Repairing, anti-wrinkle and beautifying mask liquid and preparation method thereof

Technical Field

The application relates to the field of skin care products, in particular to a repairing, anti-wrinkle and beautifying facial mask liquid and a preparation method thereof.

Background

In modern society, with the increasing working pressure of people, the problems of serious skin damage, rapid aging, large pores of facial skin, color spots, darkness, acne, wrinkles and the like are caused by the reasons of night stay, irregular diet and age increase, so that more and more people begin to pay attention to skin care, and a series of skin injuries caused by skin aging are expected to be repaired, and the mask is an important step in skin care and has a larger market.

The facial mask sold in the market has various effects of brightening, moisturizing, relieving, whitening and the like, but most of the facial masks in the market have the basic moisturizing and moisturizing effects, people often use the facial mask as daily basic skin care, the facial mask with the effects of whitening, tendering skin and the like is usually used as an emergency, and the effects of whitening and tendering skin of the facial mask often have short duration and are not obvious; therefore, the inventor considers that researching a facial mask with the effects of repairing, anti-wrinkle and beautifying has larger market demand and economic value.

Disclosure of Invention

In order to improve the effects of repairing, resisting and beautifying the face of the mask, the application provides repairing, resisting and beautifying mask liquid and a preparation method thereof.

In a first aspect, the present application provides a repairing, anti-wrinkle and beautifying facial mask liquid, which adopts the following technical scheme:

a repairing anti-wrinkle facial mask liquid comprises the following components in percentage by mass:

phase A: betaine 0.3-0.5%, sodium hyaluronate 0.03-0.05%, p-hydroxyacetophenone 0.2-0.4%, 1, 2-hexanediol 0.1-0.2%, and thickener 0.1-0.2%;

and B phase: arginine 0.08-0.12%;

and C phase: skin activator 0.42-0.62%;

and D phase: 3.2 to 3.5 percent of grape juice, 0.03 to 0.05 percent of glutathione, 0.008 to 0.01 percent of lactobacillus plantarum, 0.1 to 0.2 percent of grape fruit extract, 1 to 3 percent of skin conditioner and 3 to 5 percent of butanediol;

the balance of water;

the thickener comprises carbomer and hydroxyethyl cellulose; the skin activating agent comprises sodium carboxymethyl-beta-glucan; the skin conditioner comprises cynanchum atratum extract and cynara scolymus leaf extract.

By adopting the technical scheme, the betaine and the sodium hyaluronate can play a role in moisturizing and locking water by matching; the grape juice can remove pigmentation, help to form skin protein, make skin elastic, tender and smooth, inhibit collagenase by grape fruit extract, promote skin cell activity, and eliminate free radical; the glutathione can remove free radicals in the skin, and meanwhile, the skin can be smooth, fine and glossy, and the effects of whitening, fading spots and resisting aging can be effectively achieved; the lactobacillus plantarum can improve skin moisture, repair skin injury and improve acne; through the synergistic effect of the components and the cooperation of the skin conditioning agent and the skin activating agent, the facial mask liquid prepared by the application has a remarkable repairing effect on skin aging and injury, can promote skin cell revitalization in a short time, improve the content of skin collagen, quickly improve the problem of large skin pores, and can lighten stubborn wrinkles such as wrinkles, so that the skin is tender and bright, and the youthful state is restored.

Preferably, the skin conditioner consists of 0.14-0.16% wt of cynanchum atratum extract, 0.04-0.06% wt of cynara scolymus leaf extract and the balance of solvent.

By adopting the technical scheme, the cynanchum atratum extract is a purely natural super repair factor, can rapidly remove acne and lighten macroscopic acne marks; the cynara scolymus leaf extract has anti-inflammatory property, is beneficial to improving the function of skin immune cells, and has the effects of relieving and eliminating skin allergy; the cynanchum atratum extract and the cynara scolymus leaf extract are matched in a synergistic way, so that on one hand, the anti-inflammatory and anti-acne effects on skin and the like can be better achieved; on the other hand, the two can be matched with other active substances in the facial mask liquid to repair skin barrier, accelerate skin pore shrinkage and promote skin smoothness and tenderness.

Preferably, the skin activator is prepared by compounding 19.35% wt of carboxymethyl-beta-glucan sodium and 80.65% wt of panthenol.

By adopting the technical scheme, the carboxymethyl-beta-glucan sodium has good water solubility, can be completely compatible with other water-soluble components, can effectively excite the activity of specific immune cells, namely Langerhans cells, in the skin, and the activated Langerhans cells secrete various cytokines, so that the damaged skin cells can be effectively repaired, and the skin aging is improved; panthenol is a vitamin B5 derivative, can effectively penetrate into the stratum corneum, is quickly converted into vitamin B5, promotes metabolism of skin cells, can reduce generation of active oxygen free radicals in the skin cells, and has antioxidant effect. The skin activating agent has obvious activating effect through the combination and compounding of the skin activating agent and the mask liquid, and the skin activating agent can play a role in fast resisting wrinkles and tendering skin by matching with other components in the mask liquid; and the two can also be matched with lactobacillus plantarum to realize the regulation of skin flora, thereby helping to maintain an intact skin barrier and repair damage.

Preferably, the mass ratio between the skin activator and the skin conditioner is 1:4.

By adopting the technical scheme, the proportion compounding between the skin activating agent and the skin conditioning agent is further limited, the synergistic cooperation effect between the skin activating agent and other components in the mask liquid can be further improved, the effects of active substances such as grape juice, glutathione, lactobacillus plantarum, grape fruit extracts and the like are further improved under the auxiliary effect of the skin activating agent and the skin conditioning agent, the efficacy of the mask liquid is further improved, and the good cooperation of the skin activating agent and the skin conditioning agent can be further beneficial to prolonging the maintenance time of the mask liquid on the skin, so that the skin after the mask liquid is absorbed can keep a good active state for a long time.

Preferably, the mass ratio of carbomer to hydroxyethyl cellulose in the thickener is 3:1.

By adopting the technical scheme, the carbomer and the hydroxyethyl cellulose are matched according to a specific proportion, so that the stability of a mask liquid system can be obviously improved, the long-acting moisturizing effect of the mask liquid is improved, and the maintenance of the anti-wrinkle beautifying effect of the mask liquid is facilitated.

Preferably, the D phase raw material is also added with chamomile extract accounting for 0.015-0.17% of the total mass percent.

By adopting the technical scheme, the chamomile flower extract can well relieve skin, resist skin sensitivity and has the effects of anti-inflammatory, antibacterial and antioxidant; the addition of the chamomile extract can be matched with a skin conditioner, so that the skin can be conditioned quickly and mildly, the water-oil balance of the skin is promoted, the acne is reduced, the skin aging is slowed down, and the repairing and beautifying effects of the mask liquid are improved.

Preferably, the D phase raw material is also added with hydrolyzed serum protein accounting for 0.08-0.10% of the total mass percent.

By adopting the technical scheme, the hydrolyzed serum protein can promote cell regeneration, promote fibroblasts in the dermis to prepare elastin, and the addition of the hydrolyzed serum protein can further promote the activation of the mask liquid on skin cells, quickly fill skin, shrink pores and lighten wrinkles.

In a second aspect, the preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid provided by the application adopts the following technical scheme: a preparation method of repairing, anti-wrinkle and beauty mask liquid comprises the following steps:

s1, mixing and stirring water and the phase A raw materials, heating to 80-82 ℃, stirring until the water and the phase A raw materials are completely dissolved and have no particles, and preserving heat for 30min to obtain a base solution;

s2, cooling to 55-57 ℃, adding the phase B raw material into the base liquid, and uniformly stirring;

s3, cooling to 45-47 ℃, adding the C-phase raw material, and uniformly stirring;

s4, cooling to 40-43 ℃, adding the phase D raw material, and uniformly stirring;

and S5, continuously stirring and cooling to 36-38 ℃, filtering and discharging to obtain the repairing anti-wrinkle facial mask liquid.

By adopting the technical scheme, the specific components are added according to the specific time, the mixing compatibility among the components is good, the stability of the mask liquid system is good, and the components in the mask liquid can play the best matching effect under the proper condition, so that the efficacy of the mask liquid is stable and long.

In summary, the present application includes at least one of the following beneficial technical effects:

1. the mask liquid is added with a plurality of components such as grape juice, grape fruit extract, glutathione, lactobacillus plantarum, skin conditioner, skin activator and the like; through the synergistic effect of the components, the mask liquid prepared by the application has remarkable repairing effect on skin aging and injury, can promote skin cell to recover activity in a short time, improve the content of skin collagen, quickly improve the problem of large skin pores, and can lighten stubborn wrinkles such as wrinkles, so that the skin is tender and bright, and the youthful state is recovered;

2. the skin conditioner comprises the cynanchum atratum extract and the cynara scolymus leaf extract, and the cynanchum atratum extract and the cynara scolymus leaf extract are matched with each other, so that on one hand, the skin conditioner can have better anti-inflammatory and removing effects on skin acne and the like; on the other hand, the two can be matched with other active substances in the facial mask liquid to repair skin barrier, accelerate skin pore shrinkage and promote skin smoothness and tenderness;

3. the application further limits the proportion compounding between the skin activating agent and the skin conditioning agent, can further improve the synergistic coordination effect between the skin activating agent and other components in the mask liquid, further improves the effects of active substances such as grape juice, glutathione, lactobacillus plantarum, grape fruit extracts and the like under the auxiliary effect of the skin activating agent and the skin conditioning agent, further improves the efficacy of the mask liquid, and good coordination of the skin activating agent and the skin conditioning agent can also help to prolong the maintenance time of the mask liquid to the skin, so that the skin after the mask liquid is absorbed can keep a better active state for a long time.

Detailed Description

Preparation example

Preparation example 1

The preparation example discloses a preparation method of a skin activator, which comprises the following steps: adding 1.935kg of sodium carboxymethyl-beta-glucan and 8.065kg of panthenol into an emulsifying pot, mixing, and stirring for 3min at normal temperature and a rotating speed of 100r/min to obtain the skin activator.

Preparation example 2

The preparation example discloses a preparation method of a skin conditioner, which comprises the following specific steps: adding 0.014kg of cynanchum atratum extract, 0.004kg of cynara scolymus leaf extract, 5kg of butanediol and 4.982kg of water into an emulsifying pot, mixing, and stirring at normal temperature and rotating speed of 100r/min for 3min to obtain the skin conditioner.

Preparation example 3

The preparation example discloses a preparation method of a skin conditioner, which comprises the following specific steps: adding 0.016kg of cynanchum atratum extract, 0.006kg of cynara scolymus leaf extract, 5kg of butanediol and 4.978kg of water into an emulsifying pot, mixing, and stirring at normal temperature and rotation speed of 100r/min for 3min to obtain skin conditioner.

Examples

Examples 1 to 3

Examples 1-3 disclose a repairing anti-wrinkle facial mask liquid, which comprises the following raw materials in percentage by mass:

phase A: betaine 0.3-0.5%, sodium hyaluronate 0.03-0.05%, p-hydroxyacetophenone 0.2-0.4%, 1, 2-hexanediol 0.1-0.2%, and thickener 0.1-0.2%;

and B phase: arginine 0.08-0.12%;

and C phase: skin activator 0.42-0.72%;

and D phase: 3.2 to 3.5 percent of grape juice, 0.03 to 0.05 percent of glutathione, 0.008 to 0.01 percent of lactobacillus plantarum, 0.1 to 0.2 percent of grape fruit extract, 1 to 3 percent of skin conditioner and 3 to 5 percent of butanediol;

the balance of water.

Examples 1-3 also disclose the preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid:

s1, mixing water and a phase A raw material, putting into an emulsifying pot, heating to 80-82 ℃, homogenizing for 3min under the condition of 1000r/min of rotating speed until no particles are completely dissolved, and cooling after heat preservation for 30 min;

s2, cooling to 55-57 ℃, adding the phase B raw material into the base liquid, and stirring for 3min at the rotating speed of 30r/min until the phase B raw material is completely dissolved;

s3, cooling to 45-47 ℃, adding the C-phase raw material, and stirring for 3min at the rotating speed of 70r/min until the C-phase raw material is completely dissolved;

s4, cooling to 40-43 ℃, adding the D-phase raw material, and continuously stirring for 3min at the rotating speed of 70r/min until the D-phase raw material is completely dissolved; and S5, continuously stirring and cooling to 36-38 ℃, and filtering and discharging by using a 200-mesh filter screen to obtain the repairing anti-wrinkle facial mask liquid.

Example 4

Example 4 discloses a repair anti-wrinkle facial mask liquid, which is different from example 3 in that: the mass ratio of the skin activator to the skin conditioner was 1:4.

The amounts of the raw material components (unit: kg) and the stirring temperatures (unit: DEG C) used in examples 1 to 4 are shown in Table 1.

TABLE 1

Examples 5 to 6

Examples 5-6 disclose a repair anti-wrinkle facial mask lotion, which differs from example 3 in that: the phase D raw material is also added with chamomile extract accounting for 0.015-0.017 percent of the total mass.

Examples 7 to 8

Examples 7-8 disclose a repair anti-wrinkle facial mask liquid, which differs from example 3 in that: the phase D raw material is also added with hydrolyzed serum protein accounting for 0.08-0.10 percent of the total mass percent.

Example 9

Example 9 discloses a repair anti-wrinkle facial mask liquid, which is different from example 3 in that: the mass ratio of the skin activator to the skin conditioner is 1:4; the phase D raw material is also added with the chamomile extract accounting for 0.17 percent of the total mass percent and the hydrolyzed serum protein accounting for 0.10 percent of the total mass percent.

The amounts (unit: kg) of the raw material components added in examples 5 to 9 are shown in Table 2.

TABLE 2

Comparative example

Comparative example 1

The preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid is different from the embodiment 3 in that: the skin conditioning agent is replaced with an equal amount of water.

Comparative example 2

The preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid is different from the embodiment 3 in that: the skin activator was replaced with an equal amount of water.

Comparative example 3

The preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid is different from the embodiment 3 in that: the grape fruit extract was replaced with an equal amount of grape juice.

Comparative example 4

The preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid is different from the embodiment 3 in that: glutathione was replaced with an equal amount of water.

Comparative example 5

The preparation method of the repairing, anti-wrinkle and beautifying facial mask liquid is different from the embodiment 3 in that: lactobacillus plantarum was replaced with an equal amount of water.

Comparative example

A commercially available collagen anti-wrinkle repair mask, commodity number: 100035181914 it contains herba Portulacae extract, dipotassium glycyrrhizinate, panthenol, and allantoin as main ingredients.

Performance test

Sample preparation:

the non-woven fabric mask paper with the absorptivity of 90+/-2% and the same regulation is respectively soaked in the mask liquid prepared in the examples 1-9 and the comparative examples 1-5 for 24 hours and then taken out to be used as a test group, the anti-wrinkle repair mask sold in a certain brand in the comparative example is used as a control group, and the moisture contents of the mask in the test group and the control group are consistent within an allowable error range (+ -1%).

Test 1, skin pore tightening effect test:

selecting 150 users with large facial skin pores, wherein the ages of the subjects are 18-45 years, the average number of men and women is 15 groups, 14 groups are test groups, 1 group is a control group, each group of the test groups corresponds to a mask sample prepared by an example or a comparative example, and the control group uses the mask sample of the control group; the mask of the test group and the control group was applied 15min before sleeping every night, and the pores at the same position (midpoint of the connecting line between the nasal wings or the nasal wings and the outside of the same side eye angle) of the face of the subject were imaged (amplified by 20 times) using a DIGIMIC800 type skin image analyzer for one month, 3 pictures were taken each time, the pore size was analyzed using the image, and finally, the average value was taken. Comparing the change of the pore diameter numerical value of the skin pores of the subject before and after the sample is used, calculating the pore shrinkage rate, and indicating that the higher the pore shrinkage rate numerical value is, the better the effect of the product on tightening the skin pores is.

Test 2, skin elasticity and firmness recovery test:

150 subjects with loose skin are selected, and the subjects are equally divided into 11 groups according to the number of people for test; the subjects were applied with the test and control group masks 15min before sleeping every night, and skin elasticity before and after use was measured using a skin elasticity meter Corneometer MPA580 for one month, and the rate of change (%) of skin elasticity was calculated and recorded. The rate of change of skin elasticity is calculated by: the change rate (%) = [ (skin elasticity after use-skin elasticity before use)/skin elasticity before use ] ×100%, and the average value of each group test results is taken, the larger the change rate value, the better the skin elasticity recovery.

Test 3, anti-wrinkle effect test:

150 female subjects with wrinkles near the nose and lips (average age of 56 years of female) were selected, and the number of the female subjects was equally divided into 11 groups for the test; the subjects were applied with the test group and the control group masks for 15min before sleeping at night each day, and the average wrinkle depth of the facial wrinkles of the subjects was analyzed by a ViSIA-CR facial image analyzer for one month, and the average wrinkle depth reduction of the wrinkles before and after use was calculated; averaging test results of each group; the larger the wrinkle reduction rate value is, the better anti-wrinkle effect of the product is shown.

Run 4, DPPH-free radical scavenging test:

according to the experimental method in the experimental method of T/SHRH 006-2018 cosmetic-free radical (DPH) scavenging, the mask liquid in the embodiment, the comparative example and the comparative example of the application is tested, and the free radical scavenging rate is calculated, and the higher the scavenging rate is, the stronger the antioxidant and anti-aging capabilities of the product are shown.

The performance test data for runs 1-4 are detailed in Table 3.

TABLE 3 Table 3

According to comparison of performance detection data of examples 1-3 and comparative example in Table 3, the pores are obviously improved after the skin of a subject absorbs the mask liquid prepared in examples 1-3 of the application, the wrinkle is reduced, the skin elasticity is improved, and the anti-oxidation capability of skin aging is improved; the effect of pore astringing is not obvious after the skin of the subject absorbs the commercially available mask liquid in the comparison example, the effect of pore astringing is not obvious, the wrinkle is not desalted, the skin elasticity is improved, but the improvement effect of the mask liquid prepared by the embodiment of the application is not as good.

The application uses various components such as grape juice, grape fruit extract, glutathione, lactobacillus plantarum, skin conditioner, skin activator and the like; through the synergistic effect of the components, the facial mask liquid prepared by the application can greatly improve the activity of skin in a short time, repair skin aging and damage problems such as large pores and deep wrinkles of the skin, enable the skin to be tender and smooth, whiten and lighten and restore the youthful state.

In the embodiment 4 of the application, the combination ratio of the skin activator and the skin conditioner in the mask liquid is further limited, and the accuracy and quantification of the combination ratio can better assist other active ingredients in the mask liquid, so that the repair and activation effects of the mask liquid on the skin are promoted, and the skin performance of a subject after the mask liquid prepared in the embodiment 4 is used is further improved.

In the embodiments 5 and 6, the mother chrysanthemum extract is added into the mask liquid, and the addition of the mother chrysanthemum extract can be matched with the skin conditioner, so that the skin can be quickly and mildly conditioned, the skin aging is slowed down, and the repairing and beautifying effects of the mask liquid are improved; in the embodiments 7 and 8, hydrolyzed serum proteins are added into the mask liquid, and the addition of the hydrolyzed serum proteins can further promote the activation of the mask liquid on skin cells, so that the mask liquid can quickly fill skin, shrink pores and reduce wrinkles; the mask liquid prepared in examples 5-8 of the application has better effects on skin tendering, wrinkle resistance and repair than the mask liquid prepared in examples 1-3. In the embodiment 9, the combination ratio of the skin activator and the skin conditioner is limited, the chamomile extract and the hydrolyzed serum protein are added at the same time, the components of the mask liquid prepared in the embodiment 9 are matched with each other, the mask liquid is more stable and perfect, and the improvement effect of the mask liquid prepared in the embodiment 9 on the skin of a subject is more remarkable.

The foregoing are all preferred embodiments of the present application, and are not intended to limit the scope of the present application in any way, therefore: all equivalent changes in structure, shape and principle of this application should be covered in the protection scope of this application.

Claims (8)

1. A repairing, anti-wrinkle and beautifying facial mask liquid is characterized in that: comprises the following components in percentage by mass:

phase A: betaine 0.3-0.5%, sodium hyaluronate 0.03-0.05%, p-hydroxyacetophenone 0.2-0.4%, 1, 2-hexanediol 0.1-0.2%, and thickener 0.1-0.2%;

and B phase: arginine 0.08-0.12%;

and C phase: skin activator 0.42-0.62%;

and D phase: 3.2 to 3.5 percent of grape juice, 0.03 to 0.05 percent of glutathione, 0.008 to 0.01 percent of lactobacillus plantarum, 0.1 to 0.2 percent of grape fruit extract, 1 to 3 percent of skin conditioner and 3 to 5 percent of butanediol;

the balance of water;

the thickener comprises carbomer and hydroxyethyl cellulose; the skin activating agent comprises sodium carboxymethyl-beta-glucan; the skin conditioner comprises cynanchum atratum extract and cynara scolymus leaf extract.

2. The repair anti-wrinkle facial mask liquid according to claim 1, wherein: the skin conditioner comprises 0.14-0.16 wt% of cynanchum atratum extract, 0.04-0.06 wt% of cynara scolymus leaf extract and the balance of solvent.

3. The repair anti-wrinkle facial mask liquid according to claim 1, wherein: the skin activator is prepared by compounding 19.35% wt of carboxymethyl-beta-glucan sodium and 80.65% wt of panthenol.

4. The repair anti-wrinkle facial mask liquid according to claim 1, wherein: the mass ratio between the skin activator and the skin conditioner is 1:4.

5. The repair anti-wrinkle facial mask liquid according to claim 1, wherein: the mass ratio of carbomer to hydroxyethyl cellulose in the thickener is 3:1.

6. The repair anti-wrinkle facial mask liquid according to claim 1, wherein: the phase D raw material is also added with chamomile extract accounting for 0.015-0.17% of the total mass percent.

7. A repair anti-wrinkle facial mask liquid according to any one of claims 1-6, characterized in that: the D phase raw material is also added with hydrolyzed serum protein accounting for 0.08-0.10 percent of the total mass percent.

8. A method for preparing the repairing, anti-wrinkle and beautifying facial mask liquid according to any one of claims 1-7, which is characterized in that: the method comprises the following steps:

s1, mixing and stirring water and the phase A raw materials, heating to 80-82 ℃, stirring until the water and the phase A raw materials are completely dissolved and have no particles, and preserving heat for 30min to obtain a base solution;

s2, cooling to 55-57 ℃, adding the phase B raw material into the base liquid, and uniformly stirring;

s3, cooling to 45-47 ℃, adding the C-phase raw material, and uniformly stirring;

s4, cooling to 40-43 ℃, adding the phase D raw material, and uniformly stirring;

and S5, continuously stirring and cooling to 36-38 ℃, filtering and discharging to obtain the repairing anti-wrinkle facial mask liquid.