CN115554207B - Plant composition and preparation method thereof - Google Patents
Plant composition and preparation method thereof Download PDFInfo
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- CN115554207B CN115554207B CN202211372715.0A CN202211372715A CN115554207B CN 115554207 B CN115554207 B CN 115554207B CN 202211372715 A CN202211372715 A CN 202211372715A CN 115554207 B CN115554207 B CN 115554207B
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- 239000000203 mixture Substances 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000284 extract Substances 0.000 claims abstract description 39
- 239000002537 cosmetic Substances 0.000 claims abstract description 6
- 235000013399 edible fruits Nutrition 0.000 claims description 41
- 241000196324 Embryophyta Species 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 244000044554 Elaeagnus pungens Species 0.000 claims description 19
- 235000013935 Elaeagnus pungens Nutrition 0.000 claims description 19
- 244000225942 Viola tricolor Species 0.000 claims description 13
- 235000004031 Viola x wittrockiana Nutrition 0.000 claims description 12
- 238000010992 reflux Methods 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 9
- 238000001704 evaporation Methods 0.000 claims description 8
- YPUZOECTETYPRF-UHFFFAOYSA-N 1,2,3,4-tetrahydropyrimidine-2-carboxylic acid Chemical compound OC(=O)C1NCC=CN1 YPUZOECTETYPRF-UHFFFAOYSA-N 0.000 claims description 3
- 239000006286 aqueous extract Substances 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- WTVHAMTYZJGJLJ-UHFFFAOYSA-N (+)-(4S,8R)-8-epi-beta-bisabolol Natural products CC(C)=CCCC(C)C1(O)CCC(C)=CC1 WTVHAMTYZJGJLJ-UHFFFAOYSA-N 0.000 claims description 2
- RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 claims description 2
- RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 claims description 2
- 229940036350 bisabolol Drugs 0.000 claims description 2
- HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 4
- 230000003078 antioxidant effect Effects 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 3
- 230000000172 allergic effect Effects 0.000 abstract description 2
- 208000010668 atopic eczema Diseases 0.000 abstract description 2
- 239000006071 cream Substances 0.000 abstract description 2
- 230000003020 moisturizing effect Effects 0.000 abstract description 2
- 239000000049 pigment Substances 0.000 abstract description 2
- 238000011160 research Methods 0.000 abstract description 2
- 230000000638 stimulation Effects 0.000 abstract description 2
- 238000012360 testing method Methods 0.000 description 17
- 239000000243 solution Substances 0.000 description 9
- 239000000523 sample Substances 0.000 description 7
- 238000010790 dilution Methods 0.000 description 6
- 239000012895 dilution Substances 0.000 description 6
- 238000002835 absorbance Methods 0.000 description 5
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 5
- 238000011161 development Methods 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 241000142975 Cornaceae Species 0.000 description 3
- 206010012735 Diarrhoea Diseases 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 238000011068 loading method Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000012488 sample solution Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000007933 dermal patch Substances 0.000 description 2
- 208000001848 dysentery Diseases 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 210000000245 forearm Anatomy 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 230000008591 skin barrier function Effects 0.000 description 2
- 208000010392 Bone Fractures Diseases 0.000 description 1
- 241000755729 Clivia Species 0.000 description 1
- 241000209020 Cornus Species 0.000 description 1
- 241001117772 Elaeagnaceae Species 0.000 description 1
- 241001508399 Elaeagnus Species 0.000 description 1
- 241000471264 Elaeagnus glabra Species 0.000 description 1
- 208000004232 Enteritis Diseases 0.000 description 1
- 206010017076 Fracture Diseases 0.000 description 1
- 235000000404 Poncirus trifoliata Nutrition 0.000 description 1
- 244000202052 Poncirus trifoliata Species 0.000 description 1
- 230000002292 Radical scavenging effect Effects 0.000 description 1
- 206010040914 Skin reaction Diseases 0.000 description 1
- 241001454294 Tetranychus Species 0.000 description 1
- 206010053476 Traumatic haemorrhage Diseases 0.000 description 1
- 240000001717 Vaccinium macrocarpon Species 0.000 description 1
- 235000012545 Vaccinium macrocarpon Nutrition 0.000 description 1
- 235000002118 Vaccinium oxycoccus Nutrition 0.000 description 1
- 241000405217 Viola <butterfly> Species 0.000 description 1
- 244000137773 Viola philippica Species 0.000 description 1
- 241001106476 Violaceae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 238000002792 antioxidant assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000004634 cranberry Nutrition 0.000 description 1
- -1 diphenyl picrylphenylhydrazine radical Chemical class 0.000 description 1
- MGJZITXUQXWAKY-UHFFFAOYSA-N diphenyl-(2,4,6-trinitrophenyl)iminoazanium Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1N=[N+](C=1C=CC=CC=1)C1=CC=CC=C1 MGJZITXUQXWAKY-UHFFFAOYSA-N 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 230000007760 free radical scavenging Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011076 safety test Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000035483 skin reaction Effects 0.000 description 1
- 231100000430 skin reaction Toxicity 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000011895 specific detection Methods 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 230000000699 topical effect Effects 0.000 description 1
- 230000036572 transepidermal water loss Effects 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention belongs to the field of plant products, and provides a plant composition and a preparation method thereof. According to the invention, a great amount of researches prove that the extract has good antioxidant effect and moisturizing effect; the skin care cream is not added with various pigments, alcohol and other allergic substances, and is mild and has no stimulation to the skin; can be added into resident cosmetics, and has good popularization and application prospect.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a plant composition and a preparation method thereof.
Background
The genus tetrandra (Cornus) is a plant of the family Cornaceae (Cornaceae), and is named because of the two pairs of symmetrical petal-shaped bracts outside the inflorescence. The four flowers are beautiful in tree shape, and flowers are fully grown when flowers are opened; autumn is the fruit ripe stage, the fruit is red when ripe, and the remaining tree is more than 1 month.
China is one of the origin places of the tetranychus; the fruit is edible; the root Huashan Yaozhen Zhi records that it can treat diarrhea, traumatic hemorrhage, fracture, etc.; at present, the application and development of the four-flower skin barrier repair composition and essence in the fine chemical industry are very rare in China, and only the skin barrier repair composition and essence which can be used for repairing human skin with the viola yedoensis extract, the fig extract and the poncirus trifoliata extract are disclosed in CN 109771350A and a preparation method thereof; however, this patent does not describe the extract of the four flowers more, and the parts, extraction method and specific action used are not studied in one step.
The elaeagnus pungens fruit is the fruit of elaeagnus pungens family of the native plant of China; the other names are yangqiao, sweet stick hammer, clivia, etc.; widely distributed in the regions of the Yangtze river and the south of China; is a natural wild fruit with low awareness degree and has the efficacy of astringing and stopping diarrhea and dysentery. It is commonly used for enteritis, diarrhea and dysentery. At present, the development of the elaeagnus pungens fruit is mostly concentrated on oral administration; in the area of fine chemistry, topical skin compositions such as CN108403521a alone and their use are mentioned as useful for reducing melanin pigmentation of human skin.
Therefore, comprehensive development is necessary for a plurality of native plant resources in China.
Disclosure of Invention
Aiming at the current development situation of the original plants in China, the invention provides a plant composition and a preparation method thereof.
The plant composition is characterized by comprising the following components in parts by mass:
0.3 to 0.5 of tetrahydropyrimidine carboxylic acid;
the four-flower fruit extract is an aqueous extract obtained by peeling fruits of four-flower flowers; the Elaeagnus pungens fruit extract is water extract of Elaeagnus pungens fruit.
In particular, the preparation method of the four-flower fig extract comprises the following steps: peeling the ripe four-flower fruits; extracting with 5-8 times of water at 0-8deg.C, filtering to obtain solution, and evaporating at low temperature to constant weight to obtain four-flower fruit extract.
Further; the preparation method of the four-flower fruit extract comprises the following steps:
(1) Peeling ripe four-flower fruits, and crushing;
(2) Extracting with 5-8 times volume of reflux water at 0-8deg.C for 8-12 hr, wherein the reflux times is 3;
(3) Filtering the extract to obtain solution, evaporating at a temperature of less than or equal to 40deg.C to constant weight to obtain the extract.
In particular, ripe elaeagnus pungens fruit is denucleated; extracting with 5-8 times of water at 0-8deg.C, filtering to obtain solution, and evaporating at low temperature to constant weight to obtain Elaeagnus pungens fruit extract.
Further; the preparation method of the elaeagnus pungens fruit extract comprises the following steps:
(1) Cleaning ripe fruits of Elaeagnus pungens, crushing, and removing cores;
(2) Extracting with 5-8 times volume of reflux water at 0-8deg.C for 8-12 hr, wherein the reflux times is 3;
(3) Filtering the extract to obtain solution, evaporating at a temperature of less than 40deg.C to constant weight to obtain fructus Elaeagni extract.
In particular, the preparation method of the pansy water comprises the following steps: washing the whole pansy, crushing and squeezing.
The invention also discloses application of the plant composition in resident cosmetics.
The invention has the beneficial effects that:
the plant composition prepared by the invention is mainly three kinds of native plants in China, has long edible history, but is not further developed; according to the invention, a great amount of researches prove that the water extract has good antioxidant effect and moisturizing effect; the skin care cream is not added with various pigments, alcohol and other allergic substances, and is mild and has no stimulation to the skin; can be added into resident cosmetics, and has good popularization and application prospect.
Detailed Description
The present invention will be described in further detail with reference to the following examples, which are not intended to limit the present invention, but are merely illustrative of the present invention. The experimental methods used in the following examples are not specifically described, but the experimental methods in which specific conditions are not specified in the examples are generally carried out under conventional conditions, and the materials, reagents, etc. used in the following examples are commercially available unless otherwise specified.
In the invention, the tetrandra flower is a plant (Dendrobenthamia gigantea) of genus tetrajig of family cornaceae;
the Elaeagnus pungens is plant of Elaeagnus genus of Elaeagnaceae family (Elaeagnus glabra Thunb.);
pansy is a plant of the genus Viola (Viola tricolor l.) in the family violaceae.
The preparation method of the four-flower fig extract comprises the following steps:
(1) Peeling ripe four-flower fruits, and crushing the seeds;
(2) Reflux extracting with water at low temperature for 3 times;
(3) Filtering the solution after extraction, evaporating the solution to constant weight at the temperature of less than or equal to 40 ℃ to obtain a four-flower fruit extract; and (5) standby.
The technical parameters of each step are shown in table 1.
TABLE 1
The preparation method of the elaeagnus pungens fruit extract comprises the following steps:
(1) Cleaning ripe fructus Elaeagni, removing impurities on the surface, cutting the fruit, removing core, and crushing the skin;
(2) Reflux extracting with water at low temperature for 3 times;
(3) Filtering the extract to obtain solution, evaporating at a temperature of less than or equal to 40 ℃ to constant weight to obtain the elaeagnus pungens fruit extract; and (5) standby.
The technical parameters of each step are shown in table 2.
TABLE 2
The preparation method of the pansy water comprises the following steps:
(1) Selecting pansy in the flowering period;
(2) Sucking the attached soil and other impurities, and drying the surface;
(3) Crushing and squeezing pansy, and filtering to remove insoluble substances to obtain pansy water.
The preparation method of the plant composition comprises the following steps:
the prepared four-flower fruit extract, the cranberry fruit extract, the pansy water and the rest raw materials were mixed until all dissolved as shown in table 3 below.
TABLE 3 additive amount (parts by mass)
| Sequence number | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 |
| Four-flower fruit extract serial number | 1 | 1 | 2 | 2 | 3 | 3 |
| Adding amount of four-flower fruit extract | 10 | 15 | 10 | 15 | 10 | 15 |
| Elaeagnus pungens fruit extract serial number | 1 | 1 | 2 | 2 | 3 | 3 |
| Additive amount of extract of Elaeagnus pungens fruit | 8 | 5 | 6 | 6 | 6 | 6 |
| Pansy water addition | 30 | 36 | 36 | 36 | 36 | 36 |
| Bisabolol addition amount | 1 | 1 | 1 | 1 | 1.3 | 1.3 |
| Tetrahydropyrimidine carboxylic acid addition | 0.5 | 0.5 | 0.3 | 0.3 | 0.5 | 0.5 |
Human body skin patch test
The 6 plant compositions obtained were subjected to the human skin patch test in 2022 cosmetic safety technical Specification.
Skin reactions were observed as standard 30min (after the disappearance of the indentations), 24h and 48h after removal of the plant-containing mixed fermentate, respectively, and the observations were recorded, see table 4.
TABLE 4 human safety test results
| Numbering device | 30min | 24h | 48h |
| Example 1 | Grade 0, 30 | Grade 0, 30 | Grade 0, 30 |
| Example 2 | Grade 0, 30 | Grade 0, 30 | Grade 0, 30 |
| Example 3 | Grade 0, 30 | Grade 0, 30 | Grade 0, 30 |
| Example 4 | Grade 0, 30 | Grade 0, 30 | Grade 0, 30 |
| Example 5 | Grade 0, 30 | Grade 0, 30 | Grade 0, 30 |
| Example 6 | Grade 0, 30 | Grade 0, 30 | Grade 0, 30 |
Sample stability test
(1) Acceleration stability
Taking six prepared embodiments, taking three branches for each embodiment, placing a proper amount of the three branches into a centrifuge tube, sealing a tube orifice, and centrifuging at 3000rpm for 30min; visually observing the morphology; no precipitation, precipitation and other phenomena were observed, and the original appearance was maintained.
(2) Temperature stability
1. Heat resistance test: the temperature of the incubator was adjusted to 40 ℃, three samples of each of the six prepared examples were taken and placed in transparent glass bottles, the sample loading amount was 20 ml/bottle, the bottles were placed in the incubator after being sealed, and the incubator was taken out three months later, and the incubator was returned to room temperature to observe the change in appearance.
2. Cold resistance test: the temperature of the incubator is regulated to-10 ℃, three prepared six examples are taken and arranged in transparent glass bottles, the sample loading amount is 20 ml/bottle, the sealed incubator is placed in the incubator for three months, and the incubator is taken out, returns to room temperature and observes the appearance change.
3. And (3) normal temperature test: three samples of the six prepared examples were taken and placed in transparent glass bottles, the sample loading amount was 20 ml/bottle, and after the bottles were sealed and left at room temperature for 6 months, the appearance change of the essence was observed.
No phenomena such as precipitation and precipitation are observed in the heat resistance test, the cold resistance test and the normal temperature test, and the original appearance is maintained.
Skin moisture loss test
Percutaneous moisture loss (Trans Epidermal Water Loss, TEWL) test was used; the test was performed using a TM300 tester from Courage & Khazaka, germany, and specifically:
each group of examples randomly picked 5 women aged 20 to 40 years without skin disease; the test subjects uniformly smear the sample (0.5 ml) of the example diluted by deionized water for 10 times twice a day in the morning and evening on the inner side of the forearm, and then the same tester respectively tests the percutaneous water loss of the inner side of the forearm after the week 0 and the continuous use to the week 2 and the week 4; specific detection results; the results are shown in Table 5.
The rate of decrease formula for TEWL value is:
TEWL value decrease rate (%) = (A0-An)/a0×100%
Wherein A0 is the 0 th week TEWL value, an is the n th week TEWL value.
TEWL value average decrease rate (%) =sum of decrease rate of TEWL value per group/number of persons per group
TABLE 5 skin moisture loss test results
Antioxidant test
The plant composition prepared in each example was subjected to an antioxidant test for DPPH radical scavenging rate; the specific method comprises the following steps:
experimental materials: diphenyl picrylphenylhydrazine radical (abbreviated as DPPH, sigma, usa);
du800 uv-vis spectrophotometer (Beckman, usa);
the total of 6 groups of test objects, and the sample solution is 10 times diluted by deionized water (namely, the content is 10%) for the plant composition prepared by the above examples.
The experimental method comprises the following steps: taking 0.1mL of sample solution, adding 2mL of 60 mu mol/L DPPH solution, uniformly mixing, standing for 30min, adjusting the zero point by using the original solvent, and measuring the absorbance at 517nm to be Ai; uniformly mixing 0.1mL of absolute ethyl alcohol solvent and 2mL of DPPH solution by the same method to determine that the absorbance is Ac; the absorbance was measured for Aj by mixing 0.1mL of the sample solution with 2mL of absolute ethanol solvent. The free radical clearance is calculated according to the following formula; the results are shown in Table 6.
Clearance (%) = [1- (Ai-Aj)/Ac ] ×100%
Wherein Aj reflects the contribution of the sample itself to absorbance; absorbance values after action of Ai sample on DPPH; ac is the absorption of DPPH itself at the measurement wavelength.
TABLE 6 antioxidant assay results
| Numbering device | Clearance (%) |
| Example 1 (10-fold dilution) | 93.2 |
| Example 2 (10-fold dilution) | 94.6 |
| Example 3 (10-fold dilution) | 92.8 |
| Example 4 (10-fold dilution) | 94.1 |
| Example 5 (10-fold dilution) | 93.4 |
| Example 6 (10-fold dilution) | 94.2 |
From the in vitro experimental results, it is shown that: the invention has better free radical scavenging capability.
Claims (3)
1. The plant composition is characterized by comprising the following components in parts by mass:
extract of four flowers and fruits 10-15
5-8 parts of elaeagnus pungens fruit extract
Pansy water 30-36
Bisabolol 1-1.3
0.3 to 0.5 of tetrahydropyrimidine carboxylic acid;
the four-flower fruit extract is an aqueous extract obtained by peeling fruits of four-flower flowers; the elaeagnus pungens fruit extract is an aqueous extract of the fruits of elaeagnus pungens;
the preparation method of the four-flower fruit extract comprises the following steps:
(1) Peeling ripe four-flower fruits, and crushing;
(2) Extracting with 5-8 times volume of reflux water at 0-8deg.C for 8-12 hr, wherein the reflux times is 3;
(3) Filtering the extract to obtain solution, evaporating the solution to constant weight at the temperature of less than or equal to 40 ℃ to obtain a four-flower fruit extract;
the preparation method of the elaeagnus pungens fruit extract comprises the following steps:
(1) Cleaning ripe fruits of Elaeagnus pungens, crushing, and removing cores;
(2) Extracting with 5-8 times volume of reflux water at 0-8deg.C for 8-12 hr, wherein the reflux times is 3;
(3) Filtering the extract to obtain solution, evaporating at a temperature of less than 40deg.C to constant weight to obtain fructus Elaeagni extract.
2. The botanical composition of claim 1, wherein the pansy water is prepared by a process comprising: washing the whole pansy, crushing and squeezing.
3. Use of the phytocomposition according to claim 1 for the preparation of a leave-on cosmetic product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211372715.0A CN115554207B (en) | 2022-11-03 | 2022-11-03 | Plant composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211372715.0A CN115554207B (en) | 2022-11-03 | 2022-11-03 | Plant composition and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115554207A CN115554207A (en) | 2023-01-03 |
| CN115554207B true CN115554207B (en) | 2023-10-31 |
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|---|---|---|---|
| CN202211372715.0A Active CN115554207B (en) | 2022-11-03 | 2022-11-03 | Plant composition and preparation method thereof |
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Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003095884A (en) * | 2001-09-27 | 2003-04-03 | Kankyo Hozen Kenkyusho:Kk | Hair grower material using elaeagnus glabra thunb. |
| JP2003342190A (en) * | 2002-03-19 | 2003-12-03 | Fancl Corp | Anti-helicobacter pylori composition |
| JP2005119978A (en) * | 2003-10-14 | 2005-05-12 | Intoron:Kk | Cosmetic |
| KR20080078753A (en) * | 2007-02-24 | 2008-08-28 | 제주대학교 산학협력단 | Method for extraction of antioxidants and cosmeceuticals from plant resources |
| CN105746804A (en) * | 2016-03-20 | 2016-07-13 | 柴华 | Preparation process of aster tataricus and iris tea powder |
| CN108283590A (en) * | 2018-03-08 | 2018-07-17 | 诺斯贝尔化妆品股份有限公司 | A kind of anticorrosive composite and preparation method thereof |
| CN108403521A (en) * | 2011-03-28 | 2018-08-17 | 玫琳凯有限公司 | Topical skin composition and application thereof |
| CN109771350A (en) * | 2019-03-19 | 2019-05-21 | 广州睿森生物科技有限公司 | A kind of skin barrier remediation composition, Essence and preparation method thereof |
| CN110200880A (en) * | 2019-07-25 | 2019-09-06 | 广州睿森生物科技有限公司 | A kind of composition and its preparing the application in oxidation resistant product |
| CN110691630A (en) * | 2017-08-02 | 2020-01-14 | 巴斯夫美容护理法国公司 | Use of extract of rambutan peel for moisturizing skin and/or mucous membranes |
| CN111096917A (en) * | 2020-01-19 | 2020-05-05 | 广州妮趣化妆品有限公司 | Long-acting anti-dandruff itching-relieving composition and application thereof |
| CN113440443A (en) * | 2020-03-25 | 2021-09-28 | 湖南御家化妆品制造有限公司 | Moisturizing composition, application thereof, essence and moisturizing mask |
| TW202142243A (en) * | 2020-02-04 | 2021-11-16 | 日商Ａｄｅｋａ股份有限公司 | External composition for improving skin quality, cosmetic compostion and method for improving skin quality |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2918291C (en) * | 2013-07-22 | 2022-12-06 | Universite Du Quebec A Chicoutimi | Use of plant extracts against herpes simplex virus |
-
2022
- 2022-11-03 CN CN202211372715.0A patent/CN115554207B/en active Active
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003095884A (en) * | 2001-09-27 | 2003-04-03 | Kankyo Hozen Kenkyusho:Kk | Hair grower material using elaeagnus glabra thunb. |
| JP2003342190A (en) * | 2002-03-19 | 2003-12-03 | Fancl Corp | Anti-helicobacter pylori composition |
| JP2005119978A (en) * | 2003-10-14 | 2005-05-12 | Intoron:Kk | Cosmetic |
| KR20080078753A (en) * | 2007-02-24 | 2008-08-28 | 제주대학교 산학협력단 | Method for extraction of antioxidants and cosmeceuticals from plant resources |
| CN108403521A (en) * | 2011-03-28 | 2018-08-17 | 玫琳凯有限公司 | Topical skin composition and application thereof |
| CN105746804A (en) * | 2016-03-20 | 2016-07-13 | 柴华 | Preparation process of aster tataricus and iris tea powder |
| CN110691630A (en) * | 2017-08-02 | 2020-01-14 | 巴斯夫美容护理法国公司 | Use of extract of rambutan peel for moisturizing skin and/or mucous membranes |
| CN108283590A (en) * | 2018-03-08 | 2018-07-17 | 诺斯贝尔化妆品股份有限公司 | A kind of anticorrosive composite and preparation method thereof |
| CN109771350A (en) * | 2019-03-19 | 2019-05-21 | 广州睿森生物科技有限公司 | A kind of skin barrier remediation composition, Essence and preparation method thereof |
| CN110200880A (en) * | 2019-07-25 | 2019-09-06 | 广州睿森生物科技有限公司 | A kind of composition and its preparing the application in oxidation resistant product |
| CN111096917A (en) * | 2020-01-19 | 2020-05-05 | 广州妮趣化妆品有限公司 | Long-acting anti-dandruff itching-relieving composition and application thereof |
| TW202142243A (en) * | 2020-02-04 | 2021-11-16 | 日商Ａｄｅｋａ股份有限公司 | External composition for improving skin quality, cosmetic compostion and method for improving skin quality |
| CN113440443A (en) * | 2020-03-25 | 2021-09-28 | 湖南御家化妆品制造有限公司 | Moisturizing composition, application thereof, essence and moisturizing mask |
Non-Patent Citations (1)
| Title |
|---|
| 中国亚热带常见园林植物清除DPPH自由基活性研究;何云核, 胡丰林, 陆瑞利, 彭代启, 刘卿;园艺学报(05);第563-567页 * |
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