CN109771350A - A kind of skin barrier remediation composition, Essence and preparation method thereof - Google Patents
A kind of skin barrier remediation composition, Essence and preparation method thereof Download PDFInfo
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- CN109771350A CN109771350A CN201910210699.7A CN201910210699A CN109771350A CN 109771350 A CN109771350 A CN 109771350A CN 201910210699 A CN201910210699 A CN 201910210699A CN 109771350 A CN109771350 A CN 109771350A
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Abstract
The invention discloses a kind of skin barrier remediation compositions, contain Herba Violae extract, Fructus Fici extract, trifoliate orange extract and Dendronenthamia japonica var.chinensis extract；The extraction source of the Herba Violae extract is viola mandshurica herb, the Fructus Fici extract extracts the fruit that source is fig, the trifoliate orange extract extracts the dried immature fruit of citron orange that source is trifoliate orange, and the Dendronenthamia japonica var.chinensis extract extracts the fruit that source is Dendronenthamia japonica var.chinensis.Skin barrier remediation composition of the invention is compounded by Herba Violae extract, Fructus Fici extract, trifoliate orange extract and Dendronenthamia japonica var.chinensis extract, is originated from natural plants, and mild safety has effects that preferable skin barrier is repaired, moistening effect is good.The invention also discloses a kind of Essence containing the skin barrier remediation composition, the Essence has preferable skin barrier repairing effect, and is free of irritation chemical component, mildly non-stimulated to skin, good using skin sense, is easy to be absorbed by the skin.
Description
Technical field
The present invention relates to cosmetic technical field more particularly to a kind of skin barrier remediation compositions, Essence and its system
Preparation Method.
Background technique
With advancing age with the deterioration of living environment, the metabolic function of human skin is being gradually reduced, to battalion
The absorption function for supporting substance is also declining, and moisture is easy to be lost；Meanwhile the various harmful substances for being trapped in skin surface also can
Skin is set to gradually lose original elasticity, barrier protection function is also gradually reduced；To cause dry, coarse, decortication, wrinkle etc.
Series skin problem.Therefore, the reparation Yu maintenance of skin barrier have become important a part of people's daily life.
For the generation of more and more skin problems, occurs various product for skin repair in the market.So
And some businessmans are that product is made to achieve the effect that get instant result, and joined the ingredient of some steroids in the product, cause using
Person generates new skin problem, such as: steroid dependent dermatitis.There are also quite a few product containing chemical substance (as chemistry is anti-
Rotten agent etc.), not only there is irritation to skin, be easy to cause the allergic phenomenas such as red swelling of the skin, can also destroy the barrier system of skin
System declines skin moisturizing ability.As the improvement of people's living standards, requirement of the consumer to cosmetics is higher and higher,
It is required that also requiring product natural, safe and healthy and mild while product has skin repair effect.Therefore, exploitation one is needed
Kind has effects that the product that preferable skin barrier is repaired and safety is mild, to meet the needs of people.
Summary of the invention
To solve above-mentioned shortcoming and defect existing in the prior art, the first purpose of this invention is to provide a kind of skin
Skin barrier remediation composition, the skin barrier remediation composition are made of Four Plants extract, and the Four Plants extract
The compounding of object can generate synergistic function, have effects that preferable skin barrier is repaired, safe, mild, be suitble to various skin quality
People use.
Second object of the present invention be to provide a kind of Essence containing the skin barrier remediation composition and its
Preparation method.The Essence contains the skin barrier remediation composition, has effects that preferable skin barrier is repaired.Together
When, the Essence is free of irritation chemical component, mild non-stimulated, natural safety.
To realize its purpose, the technical scheme adopted by the invention is as follows:
A kind of skin barrier remediation composition, containing Herba Violae extract, Fructus Fici extract, trifoliate orange extract and
Dendronenthamia japonica var.chinensis extract；The extraction source of the Herba Violae extract is viola mandshurica herb, and the Fructus Fici extract mentions
The fruit that source is fig is fetched, the trifoliate orange extract extracts the dried immature fruit of citron orange that source is trifoliate orange, the Dendronenthamia japonica var.chinensis extract
Extract the fruit that source is Dendronenthamia japonica var.chinensis.
Viola mandshurica (scientific name: Viola philippica), alias open country violet, light valve violet etc..Perennial herb belongs to side
Film placenta mesh, Violaceae perennial herb, no aerial stem of plant.The product that acquisition is extracted using viola mandshurica herb as raw material, contains
The esters of glucoside, flavonoids, wax, cerinic acid and unsaturated acids etc. have the function of heat-clearing, detumescence, anti-inflammatory.The viola mandshurica mentions
Take object that can effectively improve skin moisture content in short term and reduce water loss, long-time service can be effectively controlled fat secretion and mention
High skin elasticity.
Fig (Ficus caricaLinn.), is a kind of flowering plant, is under the jurisdiction of Moraceae Ficus, is mainly grown on one
The place in a little torrid zones and temperate zone, belongs to subtropical zone defoliation small arbor.The fruit of fig contains a large amount of pectin, fructose, glucose
And part 'alpha '-hydroxy acids.The Fructus Fici extract can be reduced percutaneous water loss, enhance the moisture retention of skin and softening table
Skin has good moisturizing and repair.
Trifoliate orange (Poncirus trifoliata (L.) Raf.), just entitled trifoliate orange, Chinese endemic tree, Yellow River basin with
Southern area cultivation.Main effective component is Flavonoid substances in its dried immature fruit of citron orange, has excellent antiphlogistic effects.The trifoliate orange dried immature fruit of citron orange
Extract contain poncirin 5000ppm or more, have the function of antiallergic and anti-inflammatory, UVB induction can be protected cells against and generated
Cell death.
Dendronenthamia japonica var.chinensis (Dendrobenthamia angustata (Chun) Fang) also known as mountain lichee, narrowleaf dogwood flower of leaf are to belong to falling
Leaf shrub is to dungarunga.Its fruit protein rich in, vitamin C, amino acid and contain constant necessary to human body
Element and microelement.The Dendronenthamia japonica var.chinensis extract is derived from the fruit portion of Dendronenthamia japonica var.chinensis, has the effects that protection and skin whitening.
The present invention passes through lot of experiments discovery, the Herba Violae extract, the Fructus Fici extract, the Chinese holly
It is obvious in the effect that moisturizing and skin barrier are repaired when tangerine extract and the Dendronenthamia japonica var.chinensis extract are used in compounding simultaneously
Better than one of or two or three collocation, and it is mildly non-stimulated to skin.
Preferably, in the skin barrier remediation composition, by weight, Herba Violae extract: fig is mentioned
Take object: trifoliate orange extract: Dendronenthamia japonica var.chinensis extract=(0.5~2): (0.2~1): (0.6~2.5): (1~2.5).The present invention is logical
Cross experimental studies have found that, the Herba Violae extract, the Fructus Fici extract, the trifoliate orange extract and the Dendronenthamia japonica var.chinensis
When extract is compounded with said ratio, the synergistic function of generation is stronger, preferable to the moisturizing and repairing effect of skin.
Preferably, in the skin barrier remediation composition, by weight, Herba Violae extract: fig is mentioned
Take object: trifoliate orange extract: Dendronenthamia japonica var.chinensis extract=1:0.5:1:1.5.The present invention pass through experimental studies have found that, the viola mandshurica
When extract, the Fructus Fici extract, the trifoliate orange extract and the Dendronenthamia japonica var.chinensis extract are compounded with said ratio, to skin
The moisturizing of skin and repairing effect are best.
The present invention also provides a kind of Essence, contain the skin barrier remediation composition.Preferably, the skin
Weight percent of each component of skin barrier remediation composition in the Essence is as follows: Herba Violae extract 0.5%~
2%, Fructus Fici extract 0.2%~1%, trifoliate orange extract 0.6%~2.5% and Dendronenthamia japonica var.chinensis extract 1%~2.5%.
Preferably, the Essence by forming following weight percentage components: Herba Violae extract 0.5%~
2%, Fructus Fici extract 0.2%~1%, trifoliate orange extract 0.6%~2.5%, Dendronenthamia japonica var.chinensis extract 1%~2.5%, fourth two
Alcohol 3%~8%, pungent glycol 2%~5%, adenosine 0.5%~1%, bisabolol 0.2%~1%, Sensiva SC50 2%~
5%, beta glucan 0.4%~2%, long and thin hot pepper berry extract 0.1%~1%, Radix Pulsatillae extract 0.1%~1%, palpus sunglo mention
Take object 0.1%~1% and water surplus.As it can be seen that Essence of the invention is free of irritation chemical component, and the present invention also passes through
Experimental verification has effects that preferable skin barrier is repaired with Essence made from the formula, mildly non-stimulated to skin, makes
It is good with skin sense, requirement of the person to cosmetics that meet Modern consumer.
Preferably, the Essence by forming following weight percentage components: Herba Violae extract 1%, without flower
Berry extract 0.5%, trifoliate orange extract 1%, Dendronenthamia japonica var.chinensis extract 1.5%, butanediol 5%, pungent glycol 2.5%, adenosine
0.5%, bisabolol 0.5%, Sensiva SC50 2%, beta glucan 1%, long and thin hot pepper berry extract 0.1%, the Chinese bulbul are extracted
Object 0.1%, palpus extractive of usnea 0.1% and water surplus.The present invention is found through experiments that the Essence of the formula is in skin screen
Effect that barrier is repaired is best, and Essence is fine and smooth uniformly, and slim and graceful water profit can quickly be absorbed by the skin utilization.
The present invention also provides a kind of preparation methods of Essence comprising following steps: by water, butanediol and pungent
Glycol is uniformly mixed, and is heated to 80~85 DEG C, is continued 20~30min of insulated and stirred, is then cooled to 60~70 DEG C；It is added and red does not have
Medicine alcohol, adenosine and Sensiva SC50, homogeneous；Beta glucan is added, stirs evenly, defoams, continues to be cooled to 45~50 DEG C, add
Enter Herba Violae extract, Fructus Fici extract, trifoliate orange extract, Dendronenthamia japonica var.chinensis extract, 20~30min of uniform stirring continues
40 DEG C are cooled to, long and thin hot pepper berry extract, Radix Pulsatillae extract, palpus extractive of usnea is added, 20~30min of uniform stirring is made
The Essence.Preferably, the speed of the homogeneous is 8000r/min, time 2min.Preferably, the defoaming is specific
Operation are as follows: 2~3min is placed under the vacuum condition of -0.1MPa.
The invention has the benefit that skin barrier remediation composition of the invention is by Herba Violae extract, fig
Extract, trifoliate orange extract and Dendronenthamia japonica var.chinensis extract compound, and are originated from natural plants, and mild safety has preferable skin
Effect is modified, moistening effect is good.Essence of the invention contains the skin barrier remediation composition, has preferable skin screen
Hinder repairing effect, and is free of irritation chemical component, it is mildly non-stimulated to skin, it is good using skin sense, it is easy to be absorbed by the skin.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, the present invention passes through the following example furtherly
It is bright.It should be understood that the embodiment of the present invention is merely to illustrate technical effect of the invention, protection model and is not intended to limit the present invention
It encloses.In embodiment, method therefor is conventional method unless otherwise instructed.
Examples 1 to 7 is the embodiment of skin barrier remediation composition of the present invention, and group is grouped as shown in table 1.
Meanwhile the present invention is also provided with comparative example 1~4, group is grouped as shown in table 1.
The weight ratio formula of 1 Examples 1 to 7 of table and comparative example 1~4
Embodiment 8~13 is the embodiment of Essence of the present invention, and group is grouped as shown in table 2.Meanwhile the present invention
It is also provided with comparative example 5, group is grouped as shown in table 2.
The composition weight percentage composition (%) of 2 embodiment 8~13 of table and comparative example 5
The preparation method of the Essence includes the following steps: for water, butanediol and pungent glycol to be added in emulsion pot,
Revolving speed stirs evenly under conditions of being 120~150r/min, and is heated to 80~85 DEG C, then 20~30min of insulated and stirred drops
Temperature is to 60~70 DEG C；Bisabolol, adenosine and Sensiva SC50 is added, under the conditions of homogeneous speed is 8000r/min, homogeneous
2min；Beta glucan is added, stirs evenly, it is -0.1MPa that emulsion pot, which is then evacuated to vacuum degree, keeps 2~3min, disappears
Then bubble removing restores to normal pressure, continue to be cooled to 45~50 DEG C, Herba Violae extract, Fructus Fici extract, trifoliate orange is added
Extract, Dendronenthamia japonica var.chinensis extract are continued to be cooled to 40 DEG C, long and thin hot pepper are added with revolving speed 20~30min of uniform stirring of 50r/min
Berry extract, Radix Pulsatillae extract, palpus extractive of usnea are made described with revolving speed 20~30min of uniform stirring of 50r/min
Essence.
One, human skin patch
65 volunteers are selected, the age 20~45 years old, subjects skin's health, no skin disease allergies met subject
Volunteer inclusion criteria, be divided into 13 groups of carry out patch experiments at random, every group uses a kind of sample.Qualified patch device is selected, with
The composition of embodiment 1~13 or Essence about 0.05g are uniformly applied to patch device respectively by closed patch experimental method
Interior, external application special adhesive tape is covered on subject's forearm, removes tested material afterwards for 24 hours, distinguishes the 0th, 4,8,12,24,48h after removal
When observe dermoreaction, record its result according to dermoreaction grade scale in China 2007 editions " cosmetics health specification ".
Human skin patch was seen the results showed that this 65 subjects at the 0th, 4,8,12,24,48 hour
Dermoreaction is examined, wherein 0 skin adverse reaction occurs, illustrates that skin barrier remediation composition and Essence of the invention are pacified
Entirely.
Two, stability experiment
1, resistance to Thermal test: in advance being adjusted constant incubator to 40 DEG C, will be prepared by embodiment 8~13 and comparative example 5
Essence is loaded on respectively in 2 Clear glass bottles and jars, and sample-loading amount is 50g/ bottles, is divided into two groups of A, B.It is placed in constant incubator, A group
It takes out after 24h, B group is taken out after three months, restores respectively to room temperature, observes the cosmetic variation of Essence.
2, it resists cold and tests: refrigerator being adjusted arrive -15 DEG C in advance, by Essence prepared by embodiment 8~13 and comparative example 5
Respectively loaded in 2 Clear glass bottles and jars, sample-loading amount is 50g/ bottles, is divided into two groups of A, B.It is placed in constant incubator, A group is for 24 hours
After take out, B group is taken out after three months, restores respectively to room temperature, observes the cosmetic variation of Essence.
3, room temperature is tested: it is transparent loaded on 10 to weigh Essence prepared by 50g embodiment 8~13 and comparative example 5 respectively
In vial, after placing 6 months under room temperature, the cosmetic variation of Essence is observed.
Experimental result is shown in Table 3.
The Essence stability test result of 3 embodiment 8~13 of table
| Sample | 40℃(24h) | -15℃(24h) | 40 DEG C (3 months) | - 15 DEG C (3 months) | Room temperature (6 months) |
| Embodiment 8 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
| Embodiment 9 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
| Embodiment 10 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
| Embodiment 11 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
| Embodiment 12 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
| Embodiment 13 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
| Comparative example 5 | It is without exception | It is without exception | It is without exception | It is without exception | It is without exception |
It can be seen that from the experimental result of table 3, Essence prepared by embodiment 8~13 all has very well under high and low temperature
Stability, also illustrate that the addition of skin barrier remediation composition does not influence the stability of Essence.
Three, skin moisture is lost test
Select 90 volunteers as subject, the age 20~45 years old, subjects skin was healthy, no skin disease allergies,
Meet subject and volunteer inclusion criteria, be divided into 18 groups at random and tested, every group uses a kind of sample.Respectively with embodiment 1
~7 and the skin barrier remediation composition and embodiment 8~13 of comparative example 1~4 and the Essence of comparative example 5 as sample
(total weight parts of the skin barrier remediation composition of Examples 1 to 7 and comparative example 1~4 are 4 parts, and are respectively added in this test
Sample is used as after entering the deionized water of 96 parts by weight).Equivalent sample (0.5g) is uniformly applied to by subject twice sooner or later daily
Then inner forearm is tested the 0th week respectively using the TM300 tester of German CK company and is continued using extremely by same test man
The percutaneous moisture loss of inner forearm after 2nd week, the 4th week, abbreviation TEWL, i.e., every square metre of area scatters and disappears how many grams per hour
Water.
TEWL is very important parameter to the function of assessment skin moisture protective layer, has been obtained in the world extensively
Approval, can be well reflected the integrality of skin barrier function.The TEWL of standard be in the case where having dry skin lossless state,
24 DEG C of environment temperature, ambient humidity measures in the state of being 50%, this test data is tested with this condition and obtained.
TEWL value rate of descent calculation formula is as follows:
TEWL value rate of descent (%)=(A0-An)/A0 × 100%
In formula, A0 is the 0th week TEWL value, and An is n-th week TEWL value.
TEWL value rate of descent is positive value, illustrates that skin barrier is repaired, conversely, skin barrier is not repaired；And
TEWL value rate of descent is bigger, and skin barrier repairing effect is better.The calculation formula of TEWL value average rate of decrease is as follows:
The sum of TEWL value average rate of decrease (%)=every group of TEWL value rate of descent/this group of personnel's number
Experimental test result is shown in Table 4.
4 skin barrier function test result of table
4 interpretation of result of table: the TEWL value average rate of decrease of Examples 1 to 7 is higher, wherein with the TEWL value of embodiment 3
Average rate of decrease highest illustrates that the skin barrier repairing effect of the skin barrier remediation composition of embodiment 3 is best, therefore, this
Invention is using embodiment 3 as the optimization formula of the skin barrier remediation composition.
The TEWL value average rate of decrease of comparative example 1~4 is significantly lower than embodiment 3, illustrates in skin repair composition
It is deposited in terms of repairing skin barrier between Herba Violae extract, Fructus Fici extract, trifoliate orange extract and Dendronenthamia japonica var.chinensis extract
In synergistic function.
The TEWL value average rate of decrease of embodiment 8~13 is higher, wherein most with the TEWL value average rate of decrease of embodiment 9
Height illustrates that the skin barrier repairing effect of the Essence of embodiment 9 is best, and therefore, the present invention is using embodiment 9 as the essence
The optimization formula of liquid.
The TEWL value average rate of decrease of comparative example 5 is significantly lower than embodiment 9, illustrates the skin barrier remediation composition
The preferable skin barrier of Essence can be assigned and repair effect.
Four, using effect example
Using opinion poll point system, the volunteer of 60 20~45 years old age brackets is chosen as object on probation, average mark
At two groups, the Essence of embodiment 9 and the skin repair product of commercially available purchase are tried out respectively.It, will be equal by test product after morning and evening face cleaning
It is even to be applied to face, one month is used continuously, faces to be carried out by test product from smell, moisture retention, absorbability, prosthetic four directions
Scoring.It is best result that the total score of each scoring item, which is 10 points: 10 points, is indicated very well, very satisfied；8~9 points be it is preferable, 5~7
Being divided into can receive, 5 points the following are bad, effect is poor.Every average respectively by test product is finally calculated, the results are shown in Table 5.
Every average of the table 5 by test product
It can be seen that from the result of table 5, the Essence of the embodiment of the present invention 9 in smell, moistening effect, absorbability and repairs effect
Effect on fruit is preferable, hence it is evident that is better than commercial product.Reflect according to user, the Essence of embodiment 9 is fine and smooth uniformly, slim and graceful water
Profit, absorbs fast, does not stick after greasy, clearly, there are also certain anti-inflammatory effects.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of skin barrier remediation composition, which is characterized in that contain Herba Violae extract, Fructus Fici extract, trifoliate orange
Extract and Dendronenthamia japonica var.chinensis extract；The extraction source of the Herba Violae extract is viola mandshurica herb, and the fig mentions
The fruit that source is fig that extracts of object is taken, the trifoliate orange extract extracts the dried immature fruit of citron orange that source is trifoliate orange, the Dendronenthamia japonica var.chinensis
Extract extracts the fruit that source is Dendronenthamia japonica var.chinensis.
2. skin barrier remediation composition as described in claim 1, which is characterized in that by weight, the viola mandshurica
Extract: Fructus Fici extract: trifoliate orange extract: Dendronenthamia japonica var.chinensis extract=(0.5~2): (0.2~1): (0.6~2.5): (1
~2.5).
3. skin barrier remediation composition as claimed in claim 2, which is characterized in that by weight, the viola mandshurica
Extract: Fructus Fici extract: trifoliate orange extract: Dendronenthamia japonica var.chinensis extract=1:0.5:1:1.5.
4. a kind of Essence, which is characterized in that contain skin barrier remediation composition as claimed in any one of claims 1 to 3.
5. Essence as claimed in claim 4, which is characterized in that containing following weight percentage components: viola mandshurica mentions
Take object 0.5%~2%, Fructus Fici extract 0.2%~1%, trifoliate orange extract 0.6%~2.5% and Dendronenthamia japonica var.chinensis extract 1%
~2.5%.
6. Essence as claimed in claim 5, which is characterized in that by forming following weight percentage components: viola mandshurica
Extract 0.5%~2%, Fructus Fici extract 0.2%~1%, trifoliate orange extract 0.6%~2.5%, Dendronenthamia japonica var.chinensis extract
1%~2.5%, butanediol 3%~8%, pungent glycol 2%~5%, adenosine 0.5%~1%, bisabolol 0.2%~1%, second
Base hexyl glycerol 2%~5%, beta glucan 0.4%~2%, long and thin hot pepper berry extract 0.1%~1%, Radix Pulsatillae extract
It 0.1%~1%, must extractive of usnea 0.1%~1% and water surplus.
7. Essence as claimed in claim 6, which is characterized in that by forming following weight percentage components: viola mandshurica
Extract 1%, Fructus Fici extract 0.5%, trifoliate orange extract 1%, Dendronenthamia japonica var.chinensis extract 1.5%, butanediol 5%, pungent glycol
2.5%, adenosine 0.5%, bisabolol 0.5%, Sensiva SC50 2%, beta glucan 1%, long and thin hot pepper berry extract 0.1%,
Radix Pulsatillae extract 0.1%, palpus extractive of usnea 0.1% and water surplus.
8. a kind of preparation method of Essence as claimed in claims 6 or 7, which comprises the steps of:
Water, butanediol and pungent glycol are uniformly mixed, are heated to 80~85 DEG C, continues 20~30min of insulated and stirred, then cools down
To 60~70 DEG C；Bisabolol, adenosine and Sensiva SC50, homogeneous is added；Beta glucan is added, stirs evenly, defoams, after
It is continuous to be cooled to 45~50 DEG C, Herba Violae extract, Fructus Fici extract, trifoliate orange extract, Dendronenthamia japonica var.chinensis extract is added, uniformly
20~30min is stirred, continues to be cooled to 40 DEG C, long and thin hot pepper berry extract, Radix Pulsatillae extract, palpus extractive of usnea is added, uniformly
20~30min is stirred, the Essence is made.
9. preparation method as claimed in claim 8, which is characterized in that the speed of the homogeneous is 8000r/min, and the time is
2min。
10. preparation method as claimed in claim 8, which is characterized in that the concrete operations of the defoaming are as follows: -0.1MPa's
2~3min is placed under vacuum condition.
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| CN115554207A (en) * | 2022-11-03 | 2023-01-03 | 北京植物医生生物科技有限公司 | Plant composition and preparation method thereof |
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| CN109771350B (en) | 2021-09-28 |
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