CN114474890B - 一种吸湿快干面料及其制备方法 - Google Patents
一种吸湿快干面料及其制备方法 Download PDFInfo
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- 239000004744 fabric Substances 0.000 title claims abstract description 59
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- 239000000835 fiber Substances 0.000 claims abstract description 88
- 229920000728 polyester Polymers 0.000 claims abstract description 64
- 238000002156 mixing Methods 0.000 claims abstract description 41
- 229920003043 Cellulose fiber Polymers 0.000 claims abstract description 39
- 239000007788 liquid Substances 0.000 claims abstract description 32
- 238000009941 weaving Methods 0.000 claims abstract description 27
- 229920000742 Cotton Polymers 0.000 claims abstract description 25
- 238000010521 absorption reaction Methods 0.000 claims abstract description 24
- 238000000034 method Methods 0.000 claims abstract description 21
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 36
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- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 30
- 238000002844 melting Methods 0.000 claims description 24
- 230000008018 melting Effects 0.000 claims description 24
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 21
- 238000010438 heat treatment Methods 0.000 claims description 14
- 239000012510 hollow fiber Substances 0.000 claims description 14
- 241000505722 Uraria Species 0.000 claims description 13
- 230000008569 process Effects 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 11
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 10
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- 239000004094 surface-active agent Substances 0.000 claims description 8
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- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000002202 Polyethylene glycol Substances 0.000 claims description 7
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 7
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 7
- 150000001875 compounds Chemical class 0.000 claims description 7
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims description 7
- 239000012153 distilled water Substances 0.000 claims description 7
- 235000003891 ferrous sulphate Nutrition 0.000 claims description 7
- 239000011790 ferrous sulphate Substances 0.000 claims description 7
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 7
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 7
- 229920000570 polyether Polymers 0.000 claims description 7
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- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 3
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- 239000011425 bamboo Substances 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 2
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- 230000000694 effects Effects 0.000 abstract description 12
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- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
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Abstract
本发明公开了一种吸湿快干面料及其制备方法,将乌拉草纤维与棉纤维进行混纺,得到混纺纱,再经织造得到亲水内层;将异形聚酯纤维进行混纺,再经纺织形成中间层;将改性纤维素纤维与棉纤维、异形聚酯纤维进行混纺,得到复合纱线,再经经纬织造得到外层;将外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料。本发明制备的吸湿快干面料的吸湿速干效果明显,织物具有一定的抗黄变性能和抗菌性能,并且制备方法简单,制备工艺易操作,适合工业化生产。
Description
技术领域
本发明涉及纺织面料技术领域,具体涉及一种吸湿快干面料及其制备方法。
背景技术
随着人们对身体健康的重视,越来越多的人选择运动健身,在运动过程中产生的汗液很容易贴附在人体表面,不仅会造成运动者烦躁,更会使织物内外表面滋生细菌或真菌,并且穿戴几次之后织物往往更易出现黄变现象,进而影响织物的美观,缩短使用寿命。因此,需要一种能够将机体产生的汗液湿气及时的排到织物表面并尽快挥发,达到干爽的效果,并且还需要具有一定抑菌耐黄变的效果。而市面上出现了速干织物一般是通过后整理技术赋予织物一定的吸湿排汗功能,但随着洗涤次数的增加,吸湿速干功能急剧下降;还有一种吸湿速干面料是通过织物原料纤维的结构形态改变,借助毛细管效应改善吸湿、导湿性能,但其很少具有抗菌、耐黄变功效。
中国专利CN111172651A公开了一种吸湿快干双层针织面料的制备方法,其特征是:先编织内层具有导湿作用同时外层具有吸湿作用的双层针织面料,再对内层表面进行轻度非连续亲水整理且对外层表面进行轻度非连续疏水整理,制得吸湿快干双层针织面料;轻度非连续亲水整理的过程即对内层表面的局部区域进行亲水整理并控制其亲水性弱于外层亲水区域的过程;轻度非连续疏水整理的过程即对外层表面的局部区域进行疏水整理并控制其疏水性弱于内层疏水区域的过程。但该织物的吸湿速干效果不佳。
发明内容
有鉴于此,本发明提供一种吸湿快干面料及其制备方法,以解决上述技术问题。
为实现上述目的,本发明提供如下技术方案:一种吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至102℃~113℃,滴加浓度为22vt%~28vt%的双氧水,继续处理50分钟~100分钟,降温至50℃~55℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到120份~220份浓度为1.2wt%~1.5wt%的硫酸亚铁溶液中,浸渍30分钟~50分钟,甩掉表面多余液体放到处理液中,升温至82℃~88℃,20分钟后滴加双氧水,继续升温至100℃~108℃,处理100分钟~135分钟,经水洗、干燥后再放到无水乙醇中浸泡40分钟~55分钟,干燥后得到改性纤维素纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比(30~45):(55~70)进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比(45~65):(20~40):15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将步骤S50得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;
步骤S70,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料。
其中,聚酯纤维具有较高的湿屈服模量,在湿润状态下也能保持织物与肌肤的微气候状态,提高舒适性,再通过异形纺丝,制作成管状中空的聚酯纤维,赋予一定的毛细效应,干燥速率远大于棉纤维,具有强大的透气性和良好的吸湿控制效果保证织物面料干燥;乌拉草是一种无菌根,对细菌和真菌具有抑制作用,对于织物的内层来说,即使可以将水分及时传输到中间层和表层,但内层仍会存在部分液体,长期这样易滋生细菌,对皮肤进行伤害,选用乌拉草作为内层原料一方面起到透气排汗的作用,一方面还可以杀菌除臭。
进一步地,步骤S10中,上述聚酯纤维的粘度在0.66~0.68dl/g之间,熔点为256℃,含水量在0.3%~0.5%。水解马来酸酐的应用有很多,在与表面活性剂并用时可以提高对织物的保护作用,预防织物泛黄;接枝共聚是对纤维素纤维进行改性的重要方法之一,先在纤维素纤维表面引入二价铁离子,可与双氧水作用产生自由基,为介质提供更多的活性点,用来接枝马来酸酐上的羧酸基,在保持纤维素纤维固有的优点外,还可以赋予纤维素纤维抗黄变的性能。纤维素纤维具有透气清凉、吸湿排汗、亲肤舒适的特点,
进一步地,步骤S10中,上述多段控温熔融的温度分别为270℃~285℃、285℃~300℃、280℃~305℃、278℃~315℃、278℃~315℃。
进一步地,步骤S10中,上述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm。
进一步地,步骤S20中,上述纤维素纤维选自粘胶纤维、竹纤维、莫代尔纤维中的任一种。
进一步地,步骤S30中,上述亲水内层中乌拉草纤维与棉纤维的重量比为37:63。
进一步地,步骤S50中,上述外层中改性纤维素纤维、棉纤维、异形聚酯纤维的重量比为55:30:15。
进一步地,步骤S60中,上述吸湿速干整理液的原料包括:0.2wt%~1.4wt%聚乙二醇、0.4wt%~2.5wt%吐温60、0.5wt%~1.8wt%聚醚多元醇、12wt%~30wt%水分散型聚氨酯复合物、8wt%~18wt%乙二醇,余量为水。
进一步地,步骤S70中,上述烘干、烘焙的具体过程为:先放到80~98℃的烘干机内烘干3~5分钟,再172~176℃烘焙20秒。
本发明的另一发明目的在于提供一种吸湿快干面料,根据上述的制备方法制备而成。
从上述的技术方案可以看出,本发明的优点是:
1.本发明吸湿快干面料包括亲水内层、中间层和快干外层,其中亲水内层以具有吸湿性能优异的棉纤维与乌拉草进行混纺得到的混纺纱为原料,在快速吸水的同时,还可以对肌肤提供一定的抗菌功能,防止潮湿环境滋生细菌而对肌肤造成伤害,中间层以吸湿排汗性能优异的异形聚酯纤维为原料,可以将亲水内层吸收的液体及时排出,并引导外层,外层由改性纤维素纤维、棉纤维和异形聚酯纤维组成,并通过吸湿速干整理液的处理,速干效果明显;
2.由于长期实现吸湿、排湿、干燥功能,面料很容易出现变色泛黄等现象,在外层面料中添加改性纤维素纤维,可以提高织物的抗黄变性能,保持衣物的颜色艳丽,提高织物的使用寿命;
3.本发明制备的吸湿快干面料的吸湿速干效果明显,织物具有一定的抗黄变性能和抗菌性能,并且制备方法简单,制备工艺易操作,适合工业化生产。
除了上面所描述的目的、特征和优点之外,本发明还有其它的目的、特征和优点。下面将对本发明作进一步详细的说明。
具体实施方式
以下对本发明的实施例进行详细说明,但是本发明可以由权利要求限定和覆盖的多种不同方式实施。
实施例1
一种吸湿快干面料及其制备方法
吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;上述聚酯纤维的粘度在0.67dl/g之间,熔点为256℃,含水量在0.4%;上述多段控温熔融的温度分别为278℃、290℃、295℃、285℃、285℃;上述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至108℃,滴加浓度为25vt%的双氧水,继续处理75分钟,降温至52℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到170份浓度为1.3wt%的硫酸亚铁溶液中,浸渍40分钟,甩掉表面多余液体放到处理液中,升温至85℃,20分钟后滴加双氧水,继续升温至104℃,处理115分钟,经水洗、干燥后再放到无水乙醇中浸泡50分钟,干燥后得到改性纤维素纤维;上述纤维素纤维为粘胶纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比37:63进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比55:30:15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将步骤S50得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;上述吸湿速干整理液的原料包括:0.8wt%聚乙二醇、1.5wt%吐温60、1.2wt%聚醚多元醇、20wt%水分散型聚氨酯复合物、13wt%乙二醇,余量为水;
步骤S70,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料;上述烘干、烘焙的具体过程为:先放到89℃的烘干机内烘干4分钟,再174℃烘焙20秒。
实施例2
一种吸湿快干面料及其制备方法
吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;上述聚酯纤维的粘度在0.66dl/g之间,熔点为256℃,含水量在0.3%;上述多段控温熔融的温度分别为270℃、285℃、280℃、278℃、315℃;上述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至102℃,滴加浓度为22vt%的双氧水,继续处理50分钟,降温至50℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到120份浓度为1.2wt%的硫酸亚铁溶液中,浸渍30分钟,甩掉表面多余液体放到处理液中,升温至82℃,20分钟后滴加双氧水,继续升温至100℃,处理100分钟,经水洗、干燥后再放到无水乙醇中浸泡40分钟,干燥后得到改性纤维素纤维;上述纤维素纤维为竹纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比30:70进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比45:40:15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将步骤S50得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;上述吸湿速干整理液的原料包括:0.2wt%聚乙二醇、0.4wt%吐温60、0.5wt%聚醚多元醇、12wt%水分散型聚氨酯复合物、8wt%乙二醇,余量为水;
步骤S70,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料;上述烘干、烘焙的具体过程为:先放到80℃的烘干机内烘干3分钟,再172℃烘焙20秒。
实施例3
一种吸湿快干面料及其制备方法
吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;上述聚酯纤维的粘度在0.68dl/g之间,熔点为256℃,含水量在0.5%;上述多段控温熔融的温度分别为285℃、300℃、305℃、278℃、315℃;上述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至113℃,滴加浓度为28vt%的双氧水,继续处理100分钟,降温至55℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到220份浓度为1.5wt%的硫酸亚铁溶液中,浸渍50分钟,甩掉表面多余液体放到处理液中,升温至88℃,20分钟后滴加双氧水,继续升温至108℃,处理135分钟,经水洗、干燥后再放到无水乙醇中浸泡55分钟,干燥后得到改性纤维素纤维;上述纤维素纤维为莫代尔纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比45:55进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比65:20:15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将步骤S50得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;上述吸湿速干整理液的原料包括:1.4wt%聚乙二醇、2.5wt%吐温60、1.8wt%聚醚多元醇、30wt%水分散型聚氨酯复合物、18wt%乙二醇,余量为水;
步骤S70,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料;上述烘干、烘焙的具体过程为:先放到98℃的烘干机内烘干5分钟,再176℃烘焙20秒。
实施例4
一种吸湿快干面料及其制备方法
吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;上述聚酯纤维的粘度在0.66~0.68dl/g之间,熔点为256℃,含水量在0.3%;上述多段控温熔融的温度分别为280℃、290℃、300℃、300℃、290℃;上述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至110℃,滴加浓度为26vt%的双氧水,继续处理60分钟,降温至50℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到150份浓度为1.4wt%的硫酸亚铁溶液中,浸渍60分钟,甩掉表面多余液体放到处理液中,升温至86℃,20分钟后滴加双氧水,继续升温至102℃,处理110分钟,经水洗、干燥后再放到无水乙醇中浸泡45分钟,干燥后得到改性纤维素纤维;上述纤维素纤维为粘胶纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比40:60进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比60:25:15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将步骤S50得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;上述吸湿速干整理液的原料包括:0.4wt%聚乙二醇、2.0wt%吐温60、0.8wt%聚醚多元醇、25wt%水分散型聚氨酯复合物、10wt%乙二醇,余量为水;
步骤S70,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料;上述烘干、烘焙的具体过程为:先放到85℃的烘干机内烘干6分钟,再170℃烘焙20秒。
对比例1
一种吸湿快干面料及其制备方法
吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到丝束,将丝束进行卷绕牵伸,得到聚酯纤维;上述聚酯纤维的粘度在0.67dl/g之间,熔点为256℃,含水量在0.4%;上述多段控温熔融的温度分别为278℃、290℃、295℃、285℃、285℃;上述纺丝组件上的喷丝孔为常规圆形喷丝孔;
步骤S20,将乌拉草纤维与棉纤维以重量比37:63进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S30,将步骤S10得到的聚酯纤维进行混纺,再经纺织形成中间层;
步骤S40,将粘胶纤维与棉纤维、步骤S10得到的聚酯纤维以重量比55:30:15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S50,将步骤S40得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;上述吸湿速干整理液的原料包括:0.8wt%聚乙二醇、1.5wt%吐温60、1.2wt%聚醚多元醇、20wt%水分散型聚氨酯复合物、13wt%乙二醇,余量为水;
步骤S60,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料;上述烘干、烘焙的具体过程为:先放到89℃的烘干机内烘干4分钟,再174℃烘焙20秒。
对比例2
一种吸湿快干面料及其制备方法
吸湿快干面料的制备方法,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;上述聚酯纤维的粘度在0.67dl/g之间,熔点为256℃,含水量在0.4%;上述多段控温熔融的温度分别为278℃、290℃、295℃、285℃、285℃;上述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至108℃,滴加浓度为25vt%的双氧水,继续处理75分钟,降温至52℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到170份浓度为1.3wt%的硫酸亚铁溶液中,浸渍40分钟,甩掉表面多余液体放到处理液中,升温至85℃,20分钟后滴加双氧水,继续升温至104℃,处理115分钟,经水洗、干燥后再放到无水乙醇中浸泡50分钟,干燥后得到改性纤维素纤维;上述纤维素纤维为粘胶纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比37:63进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比55:30:15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将亲水内层、中间层和外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料;上述烘干、烘焙的具体过程为:先放到89℃的烘干机内烘干4分钟,再174℃烘焙20秒。
实验例
为了进一步说明本发明的技术进步性,现采用实验进一步说明。
实验方法:根据GB/T21655.1-2008对实施例1~4及对比例1~2制备的织物进行吸水率、滴水扩散时间测试,根据FZ/T01071-2008对芯吸高度进行测试,根据GB/T12704-1991进行测试,结果如表1所示。
对本发明制备的织物进行洗涤,测试洗涤1次,洗涤20次,洗涤100次后织物的抗黄变性,以及洗涤100次后织物的大肠杆菌抑菌率,结果如表2所示。
表1
表2
以上仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (8)
1.一种吸湿快干面料的制备方法,其特征在于,包括以下步骤:
步骤S10,将聚酯纤维进行干燥至含水量≤40ppm,放到螺杆挤压机中多段控温熔融,经过滤器过滤后进入纺丝组件喷丝,得到中空丝束,将中空丝束进行卷绕牵伸,得到异形聚酯纤维;
步骤S20,将马来酸酐和蒸馏水混合并加热至溶液澄清透明,再加入氯化铜,搅拌混合后升温至102℃~113℃,滴加浓度为22vt%~28vt%的双氧水,继续处理50分钟~100分钟,降温至50℃~55℃,再加入表面活性剂,得到处理液;将100份纤维素纤维放到120份~220份浓度为1.2 wt%~1.5wt%的硫酸亚铁溶液中,浸渍30分钟~50分钟,甩掉表面多余液体放到处理液中,升温至82℃~88℃,20分钟后滴加双氧水,继续升温至100℃~108℃,处理100分钟~135分钟,经水洗、干燥后再放到无水乙醇中浸泡40分钟~55分钟,干燥后得到改性纤维素纤维;
步骤S30,将乌拉草纤维与棉纤维以重量比(30~45):(55~70)进行混纺,得到混纺纱,再经织造得到亲水内层;
步骤S40,将步骤S10得到的异形聚酯纤维进行混纺,再经纺织形成中间层;
步骤S50,将步骤S20得到的改性纤维素纤维与棉纤维、步骤S10得到的异形聚酯纤维以重量比(45~65):(20~40):15进行混纺,得到复合纱线,再经经纬织造得到外层;
步骤S60,将步骤S50得到的外层浸扎在吸湿速干整理液中,二浸二轧,得到预处理外层;
步骤S70,将亲水内层、中间层和预处理外层通过粘合的方式进行复合,再经烘干、烘焙,得到吸湿快干面料
步骤S20中,所述纤维素纤维选自粘胶纤维、竹纤维、莫代尔纤维中的任一种;
步骤S60中,所述吸湿速干整理液的原料包括:0.2wt%~1.4wt%聚乙二醇、0.4wt%~2.5wt%吐温60、0.5wt%~1.8wt%聚醚多元醇、12wt%~30wt%水分散型聚氨酯复合物、8wt%~18wt%乙二醇,余量为水。
2.根据权利要求1所述的制备方法,其特征在于,步骤S10中,所述聚酯纤维的粘度在0.66~0.68dl/g之间,熔点为256℃,含水量在0.3%~0.5%。
3.根据权利要求1所述的制备方法,其特征在于,步骤S10中,所述多段控温熔融的温度分别为270℃~285℃、285℃~300℃、280℃~305℃、278℃~315℃、278℃~315℃。
4.根据权利要求1所述的制备方法,其特征在于,步骤S10中,所述纺丝组件上的喷丝孔为中空椭圆形,孔深为0.5mm。
5.根据权利要求1所述的制备方法,其特征在于,步骤S30中,所述亲水内层中乌拉草纤维与棉纤维的重量比为37:63。
6.根据权利要求1所述的制备方法,其特征在于,步骤S50中,所述外层中改性纤维素纤维、棉纤维、异形聚酯纤维的重量比为55:30:15。
7.根据权利要求1所述的制备方法,其特征在于,步骤S70中,所述烘干、烘焙的具体过程为:先放到80~98℃的烘干机内烘干3~5分钟,再172~176℃烘焙20秒。
8.一种吸湿快干面料,其特征在于,根据权利要求1~7中任一项所述的制备方法制备而成。
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