CN114158736B - 适用于特殊医学用途全营养配方食品的复配维生素 - Google Patents
适用于特殊医学用途全营养配方食品的复配维生素 Download PDFInfo
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- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
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- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
- A23L29/35—Degradation products of starch, e.g. hydrolysates, dextrins; Enzymatically modified starches
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
- A23L33/155—Vitamins A or D
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/20—Agglomerating; Granulating; Tabletting
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Mycology (AREA)
- Molecular Biology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicinal Preparation (AREA)
Abstract
本申请提供了一种性质均一、稳定的复配维生素，其适用于包括特殊医学用途全营养配方食品在内的多种成人、儿童、婴儿用营养食品。本申请的复配维生素使用喷雾制粒方法，以麦芽糊精和卡拉胶作为赋形剂制备。
Description
发明领域：
本申请属于食品领域，具体地，本申请提供了一种性质均一、稳定的复配维生素，其适用于包括特殊医学用途全营养配方食品在内的多种成人、儿童、婴儿用营养食品。
背景技术：
乳粉、营养代餐等营养品中常用的维生素包括十余种。虽然用量不高，但这些维持人体正常生理活动所必须的维生素是营养品的必需成分。此类营养品生产规模一般以吨计，售卖包装大小一般为数百克，而实际每次用量基本在数十克的水平上。在这样巨大的规模差异下，无论是实现产品质量均一，还是保证及时有效地提供营养(特别是为婴幼儿、病患等亟需营养的群体提供营养)，产品中各成分的分散均一性均是一个关键生产指标。
此类营养品成分多达仅百种，各种成分含量和颗粒尺寸差异巨大(经过有数个数量级的差异)，而且还存在大量的吸附、包裹等情况。如何将这些成分，特别是含量少而作用显著的维生素成分，快速、充分混合为均一而稳定的产品，是生产中的难题之一。
目前采用的预混料、超微粉碎、喷雾制粒等方法在产品均一性和时间、物料成本上均有不足。
发明内容
针对以上问题，申请人改进了预混维生素混合方法，通过使用特定量的赋形剂组合有效提高了维生素质的混合均匀度。
一方面，本申请提供了一种复配维生素的制备方法，其特征在于，包含喷雾制粒步骤。
进一步地，所述喷雾制粒步骤为：将原料溶于2-4倍质量的30-60摄氏度水中，搅拌均匀；进料温度20-50摄氏度，进风口温度90-150摄氏度；喷雾干燥制备粉体。
进一步地，所述喷雾制粒步骤为：将原料溶于2倍质量的50摄氏度水中，搅拌均匀；进料温度40摄氏度，进风口温度120摄氏度，泵速25％；喷雾干燥制备粉体。
进一步地，所述原料中包含维生素、赋形剂。
进一步地，所述赋形剂为麦芽糊精和卡拉胶。
进一步地，所述赋形剂为麦芽糊精70-90％、卡拉胶2-8％，优选麦芽糊精85％、卡拉胶5％。
进一步地，其中所述维生素包括醋酸视黄酯0.05-0.2％、胆钙化醇0.0005-0.002％、dl-α-醋酸生育酚2-2.5％、植物甲萘醌0.01-0.03％、盐酸硫胺素0.1-0.4％、核黄素0.1-0.3％、盐酸吡哆醇0.1-0.3％、氰钴胺0.0001-0.001％、烟酰胺1-3％、叶酸0.01-0.05％、D-泛酸钙0.1-0.8％、L-抗坏血酸钠2-6％、D-生物素0.001-0.007％；
优选地，醋酸视黄酯0.1054％、胆钙化醇0.0011％、dl-α-醋酸生育酚2.2333％、植物甲萘醌0.0167％、盐酸硫胺素0.2％、核黄素0.1667％、盐酸吡哆醇0.2％、氰钴胺0.0005％、烟酰胺2％、叶酸0.0333％、D-泛酸钙0.6333％、L-抗坏血酸钠4.4047％、D-生物素0.005％。
另一方面，本申请提供了通过上述方法制备的复配维生素产品。
另一方面，本申请提供了上述方法在制备食品中的应用。
进一步地，所述食品为特殊医学用途全营养配方食品。
具体实施方式
实施例1主要试剂和实验方法
麦芽糊精：常规国产种类，符合食品用相关标准；
卡拉胶：河南中辰生物科技有限公司。
包括维生素、矿物质在内其他原料均为常规国产或进口食品级原料。
混合均匀度检测方法：
对同一批次产品，进行10次取样，检测其中的目标成分含量；计算平均值X和标准差S，通过公式CV＝S/X×100％来计算变异系数CV；每批次产品计算3次CV，取CV的平均值。
喷雾制粒：
使用浙江钱江伟岸干燥设备有限公司的PGL-B喷雾干燥制粒机；将原料溶于2倍质量的50摄氏度水中，搅拌均匀；进料温度40摄氏度，进风口温度120摄氏度，泵速25％；喷雾干燥制备粉体。
实施例2复配维生素的制备
申请人验证了大量赋形剂种类和组合(以下仅展示部分代表性配方)，发现适量使用卡拉胶可有有效提高维生素，特别是脂溶性维生素的分散效果。
以下复配维生素配方中的维生素相同，包括：醋酸视黄酯0.1054％、胆钙化醇0.0011％、dl-α-醋酸生育酚2.2333％、植物甲萘醌0.0167％、盐酸硫胺素0.2％、核黄素0.1667％、盐酸吡哆醇0.2％、氰钴胺0.0005％、烟酰胺2％、叶酸0.0333％、D-泛酸钙0.6333％、L-抗坏血酸钠4.4047％、D-生物素0.005％。约90％的赋形剂有区别。
不同赋形剂配方下各种维生素的CV的平均CV％值
结果表明，适当的增稠赋形剂可以有效的提高维生素，特别是脂溶性维生素A、E的分散效果，其对于难溶的维生素也有明显的效果；可能是由于溶液中胶体状态的变化非常敏感，改变增稠赋形剂的种类或者用量时，分散效果很容易发生变化。
实施例3特殊医学用途全营养配方食品实际制备
制备过程中复配维生素使用实施例2中优化的制备方法(85％麦芽糊精+5％卡拉胶赋形剂)制备。
按照以下配方配制特殊医学用途全营养配方食品：
植物脂肪粉59％、固体淀粉糖14.4％、分离乳清蛋白粉10％、柠檬酸钾7％、柠檬酸钠5％、复配矿物质1.5％、磷酸氢钙1.2％、氯化钾0.8％、复配维生素0.6％、氯化钠0.5％。
植物脂肪粉包括麦芽糊精41.7％、植物油24％、固体淀粉糖17.4％、分离乳清蛋白粉15.8％、单，双甘油脂肪酸酯0.69％、L-抗坏血酸钠0.332％、抗坏血酸棕榈酸酯0.03％、生育酚0.03％、磷脂0.018％。
所述复配维生素包含麦芽糊精70-90％、卡拉胶1-8％以及醋酸视黄酯0.05-0.2％、胆钙化醇0.0005-0.002％、dl-α-醋酸生育酚2-2.5％、植物甲萘醌0.01-0.03％、盐酸硫胺素0.1-0.4％、核黄素0.1-0.3％、盐酸吡哆醇0.1-0.3％、氰钴胺0.0001-0.001％、烟酰胺1-3％、叶酸0.01-0.05％、D-泛酸钙0.1-0.8％、L-抗坏血酸钠2-6％、D-生物素0.001-0.007％。复配矿物质包括硫酸铜、硫酸镁、硫酸亚铁、硫酸锌、硫酸锰、碘酸钾、亚硒酸钠。
经检验，产品中矿物质和维生素分布均一，产品性质符合要求：
Claims (3)
1.一种复配维生素的制备方法，其特征在于，所述方法包含喷雾制粒步骤，所述喷雾制粒步骤为：将原料溶于2倍质量的50摄氏度水中，搅拌均匀；进料温度40摄氏度，进风口温度120摄氏度，泵速25％，喷雾干燥制备粉体；所述原料包含醋酸视黄酯0.1054％、胆钙化醇0.0011％、dl-α-醋酸生育酚2.2333％、植物甲萘醌0.0167％、盐酸硫胺素0.2％、核黄素0.1667％、盐酸吡哆醇0.2％、氰钴胺0.0005％、烟酰胺2％、叶酸0.0333％、D-泛酸钙0.6333％、L-抗坏血酸钠4.4047％、D-生物素0.005％以及赋形剂麦芽糊精85％、卡拉胶5％。
2.根据权利要求1所述的方法在制备食品中的应用。
3.根据权利要求2所述的应用，其中所述食品为特殊医学用途全营养配方食品。
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