CN113195411A - 含锂溶液的制备方法 - Google Patents

含锂溶液的制备方法 Download PDF

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Publication number
CN113195411A
CN113195411A CN201980079488.2A CN201980079488A CN113195411A CN 113195411 A CN113195411 A CN 113195411A CN 201980079488 A CN201980079488 A CN 201980079488A CN 113195411 A CN113195411 A CN 113195411A
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CN
China
Prior art keywords
lithium
manganese
containing solution
manganate
lithium manganate
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Pending
Application number
CN201980079488.2A
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English (en)
Chinese (zh)
Inventor
高野雅俊
浅野聪
池田修
松本伸也
工藤阳平
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Sumitomo Metal Mining Co Ltd
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Sumitomo Metal Mining Co Ltd
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Publication date
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Publication of CN113195411A publication Critical patent/CN113195411A/zh
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00—Lithium compounds
    • C01D15/04—Halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/16—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the fluid carrier
    • B01D15/161—Temperature conditioning
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/24—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the treatment of the fractions to be distributed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction, e.g. ion-exchange, ion-pair, ion-suppression or ion-exclusion
    • B01D15/361—Ion-exchange
    • B01D15/362—Cation-exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/42—Selective adsorption, e.g. chromatography characterised by the development mode, e.g. by displacement or by elution
    • B01D15/424—Elution mode
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/3433—Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/34—Regenerating or reactivating
    • B01J20/345—Regenerating or reactivating using a particular desorbing compound or mixture
    • B01J20/3475—Regenerating or reactivating using a particular desorbing compound or mixture in the liquid phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/08—Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/10—Oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/05—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds
    • B01J49/06—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds containing cationic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/53—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/01—Preparation or separation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/12—Complex oxides containing manganese and at least one other metal element
    • C01G45/1207—Permanganates ([MnO4)-] or manganates ([MnO4)2-]
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Environmental & Geological Engineering (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Battery Electrode And Active Subsutance (AREA)
CN201980079488.2A 2018-12-07 2019-12-06 含锂溶液的制备方法 Pending CN113195411A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2018229507 2018-12-07
JP2018-229507 2018-12-07
PCT/JP2019/047811 WO2020116607A1 (ja) 2018-12-07 2019-12-06 リチウム含有溶液の製造方法

Publications (1)

Publication Number Publication Date
CN113195411A true CN113195411A (zh) 2021-07-30

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CN201980079488.2A Pending CN113195411A (zh) 2018-12-07 2019-12-06 含锂溶液的制备方法

Country Status (8)

Country Link
US (1) US20220024776A1 (https=)
EP (1) EP3892588A4 (https=)
JP (1) JP7415948B2 (https=)
CN (1) CN113195411A (https=)
AR (1) AR117244A1 (https=)
AU (1) AU2019395190C1 (https=)
CL (1) CL2021001426A1 (https=)
WO (2) WO2020115948A1 (https=)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115667558A (zh) * 2021-03-31 2023-01-31 住友金属矿山株式会社 含锂溶液的制造方法
CN117920169A (zh) * 2024-01-29 2024-04-26 南京工业大学 低溶损的锂锰氧化物的洗脱剂及制备锰系锂离子筛的方法

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7156322B2 (ja) * 2020-02-17 2022-10-19 住友金属鉱山株式会社 水酸化リチウムの製造方法
CN112791691B (zh) 2020-12-23 2023-07-25 礼思(上海)材料科技有限公司 一种包覆型锂离子筛及其制备方法
DE102021105808A1 (de) 2021-03-10 2022-09-15 EnBW Energie Baden-Württemberg AG Verfahren zur Gewinnung von Lithium aus Sole oder Meerwasser
DE102021108442B4 (de) 2021-04-01 2023-01-26 EnBW Energie Baden-Württemberg AG Verfahren zur Herstellung eines Lithium-Adsorbens
CA3222737A1 (en) * 2021-06-11 2022-12-15 Geo40 Limited Process and system for lithium extraction
CN113368537B (zh) * 2021-06-28 2022-05-24 青海盐湖工业股份有限公司 吸附法利用老卤制备高锂母液的方法和装置
JP2023006193A (ja) 2021-06-30 2023-01-18 住友金属鉱山株式会社 リチウム吸着用造粒体の製造方法
CN116351384A (zh) * 2021-12-28 2023-06-30 比亚迪股份有限公司 锂吸附剂及盐湖提锂方法
JP7513138B1 (ja) * 2023-02-28 2024-07-09 住友金属鉱山株式会社 リチウム含有溶液の製造方法
WO2025253801A1 (ja) * 2024-06-06 2025-12-11 住友化学株式会社 リチウム塩の製造方法、及びリチウム塩の製造システム

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CN101597689A (zh) * 2009-07-08 2009-12-09 中南大学 废旧锂电池中活性物质酸性浸出液的高效净化工艺
US20110219607A1 (en) * 2010-03-12 2011-09-15 Nanjundaswamy Kirakodu S Cathode active materials and method of making thereof
CN106629789A (zh) * 2016-09-12 2017-05-10 中国科学院青海盐湖研究所 一种利用离子交换法提取卤水中锂制备电池级碳酸锂的方法

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CA2459899C (en) * 2001-09-13 2010-11-23 Intec Ltd Zinc recovery process
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CN101597689A (zh) * 2009-07-08 2009-12-09 中南大学 废旧锂电池中活性物质酸性浸出液的高效净化工艺
US20110219607A1 (en) * 2010-03-12 2011-09-15 Nanjundaswamy Kirakodu S Cathode active materials and method of making thereof
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115667558A (zh) * 2021-03-31 2023-01-31 住友金属矿山株式会社 含锂溶液的制造方法
CN117920169A (zh) * 2024-01-29 2024-04-26 南京工业大学 低溶损的锂锰氧化物的洗脱剂及制备锰系锂离子筛的方法

Also Published As

Publication number Publication date
AU2019395190B2 (en) 2022-10-13
AR117244A1 (es) 2021-07-21
WO2020116607A1 (ja) 2020-06-11
US20220024776A1 (en) 2022-01-27
JPWO2020116607A1 (https=) 2020-06-11
CL2021001426A1 (es) 2021-11-26
AU2019395190A1 (en) 2021-06-24
EP3892588A4 (en) 2022-08-31
EP3892588A1 (en) 2021-10-13
AU2019395190C1 (en) 2023-03-16
JP7415948B2 (ja) 2024-01-17
WO2020115948A1 (ja) 2020-06-11

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