CL2021001426A1 - Procedimiento para la producción de una solución que contiene litio - Google Patents

Procedimiento para la producción de una solución que contiene litio

Info

Publication number
CL2021001426A1
CL2021001426A1 CL2021001426A CL2021001426A CL2021001426A1 CL 2021001426 A1 CL2021001426 A1 CL 2021001426A1 CL 2021001426 A CL2021001426 A CL 2021001426A CL 2021001426 A CL2021001426 A CL 2021001426A CL 2021001426 A1 CL2021001426 A1 CL 2021001426A1
Authority
CL
Chile
Prior art keywords
lithium
solution containing
containing lithium
procedure
production
Prior art date
Application number
CL2021001426A
Other languages
English (en)
Inventor
Masatoshi Takano
Satoshi Asano
Osamu Ikeda
Shin-Ya Matsumoto
Yohei Kudo
Original Assignee
Sumitomo Metal Mining Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Metal Mining Co filed Critical Sumitomo Metal Mining Co
Publication of CL2021001426A1 publication Critical patent/CL2021001426A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/04Halides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/16Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the fluid carrier
    • B01D15/161Temperature conditioning
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/10Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/24Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the treatment of the fractions to be distributed
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361Ion-exchange
    • B01D15/362Cation-exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/42Selective adsorption, e.g. chromatography characterised by the development mode, e.g. by displacement or by elution
    • B01D15/424Elution mode
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/34Regenerating or reactivating
    • B01J20/3433Regenerating or reactivating of sorbents or filter aids other than those covered by B01J20/3408 - B01J20/3425
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/34Regenerating or reactivating
    • B01J20/345Regenerating or reactivating using a particular desorbing compound or mixture
    • B01J20/3475Regenerating or reactivating using a particular desorbing compound or mixture in the liquid phase
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/08Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/10Oxides or hydroxides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/05Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds
    • B01J49/06Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds containing cationic exchangers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/53Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for cationic exchangers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/003Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/02Oxides; Hydroxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/12Manganates manganites or permanganates
    • C01G45/1207Permanganates ([MnO]4-) or manganates ([MnO4]2-)
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10Obtaining alkali metals
    • C22B26/12Obtaining lithium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • C22B3/24Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition by adsorption on solid substances, e.g. by extraction with solid resins
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44Treatment or purification of solutions, e.g. obtained by leaching by chemical processes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • General Chemical & Material Sciences (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

El proceso para producir una solución que contiene litio se realiza por adsorción en que se contacta un adsorbente de litio obtenido de óxido de manganeso de litio con un líquido con bajo contenido de litio, obteniendo óxido de manganeso de litio post-adsorción; la elución en que se contacta dicho óxido con una solución de ácido para obtener una solución que contiene litio con manganeso residual; y la oxidación del manganeso para obtener una solución que contiene litio.
CL2021001426A 2018-12-07 2021-05-31 Procedimiento para la producción de una solución que contiene litio CL2021001426A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2018229507 2018-12-07

Publications (1)

Publication Number Publication Date
CL2021001426A1 true CL2021001426A1 (es) 2021-11-26

Family

ID=70973585

Family Applications (1)

Application Number Title Priority Date Filing Date
CL2021001426A CL2021001426A1 (es) 2018-12-07 2021-05-31 Procedimiento para la producción de una solución que contiene litio

Country Status (8)

Country Link
US (1) US20220024776A1 (es)
EP (1) EP3892588A4 (es)
JP (1) JP7415948B2 (es)
CN (1) CN113195411A (es)
AR (1) AR117244A1 (es)
AU (1) AU2019395190C1 (es)
CL (1) CL2021001426A1 (es)
WO (2) WO2020115948A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102021105808A1 (de) 2021-03-10 2022-09-15 EnBW Energie Baden-Württemberg AG Verfahren zur Gewinnung von Lithium aus Sole oder Meerwasser
JP7124917B1 (ja) * 2021-03-31 2022-08-24 住友金属鉱山株式会社 リチウム含有溶液の製造方法
DE102021108442B4 (de) 2021-04-01 2023-01-26 EnBW Energie Baden-Württemberg AG Verfahren zur Herstellung eines Lithium-Adsorbens
CA3222737A1 (en) * 2021-06-11 2022-12-15 Geo40 Limited Process and system for lithium extraction
CN113368537B (zh) * 2021-06-28 2022-05-24 青海盐湖工业股份有限公司 吸附法利用老卤制备高锂母液的方法和装置
JP2023006193A (ja) 2021-06-30 2023-01-18 住友金属鉱山株式会社 リチウム吸着用造粒体の製造方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61171535A (ja) * 1985-01-24 1986-08-02 Agency Of Ind Science & Technol リチウム吸着剤、その製造方法及びそれを用いたリチウム回収方法
JP3388406B2 (ja) 1999-09-22 2003-03-24 独立行政法人産業技術総合研究所 リチウム吸着剤の製造方法
ATE386825T1 (de) 2001-09-13 2008-03-15 Intec Ltd Zinkgewinnungsverfahren
JP4210475B2 (ja) * 2002-06-05 2009-01-21 日鉱金属株式会社 スクラップからのコバルトの回収方法
CN101597689B (zh) * 2009-07-08 2010-12-01 中南大学 废旧锂电池中活性物质酸性浸出液的高效净化工艺
WO2011058841A1 (ja) * 2009-11-10 2011-05-19 財団法人北九州産業学術推進機構 リチウム吸着剤の製造方法及びリチウム吸着剤、リチウム吸着剤用原料、リチウム濃縮方法、リチウム濃縮装置
US20110219607A1 (en) * 2010-03-12 2011-09-15 Nanjundaswamy Kirakodu S Cathode active materials and method of making thereof
US8663361B1 (en) * 2010-05-06 2014-03-04 Sandia Corporation Methods of recovering alkali metals
JP2015020090A (ja) 2013-07-16 2015-02-02 独立行政法人産業技術総合研究所 リチウム吸着材料の製造方法およびリチウム吸着材料
JP6137035B2 (ja) 2014-04-24 2017-05-31 住友金属鉱山株式会社 塩化ニッケル溶液の浄液方法
JP6735192B2 (ja) 2016-09-07 2020-08-05 Jx金属株式会社 リチウムイオン電池スクラップの処理方法
CN106629789B (zh) * 2016-09-12 2018-02-27 中国科学院青海盐湖研究所 一种利用离子交换法提取卤水中锂制备电池级碳酸锂的方法

Also Published As

Publication number Publication date
JP7415948B2 (ja) 2024-01-17
AR117244A1 (es) 2021-07-21
WO2020115948A1 (ja) 2020-06-11
EP3892588A1 (en) 2021-10-13
US20220024776A1 (en) 2022-01-27
AU2019395190A1 (en) 2021-06-24
AU2019395190C1 (en) 2023-03-16
EP3892588A4 (en) 2022-08-31
AU2019395190B2 (en) 2022-10-13
CN113195411A (zh) 2021-07-30
WO2020116607A1 (ja) 2020-06-11
JPWO2020116607A1 (es) 2020-06-11

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