CN112957306A - 一种含有抗敏芳香中草药的护肤品 - Google Patents

一种含有抗敏芳香中草药的护肤品 Download PDF

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CN112957306A
CN112957306A CN202110306281.3A CN202110306281A CN112957306A CN 112957306 A CN112957306 A CN 112957306A CN 202110306281 A CN202110306281 A CN 202110306281A CN 112957306 A CN112957306 A CN 112957306A
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张洪广
姜文明
胡勇
王杰
石星星
王升萍
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China Science And Technology Research Institute Hubei Co ltd
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Abstract

本发明公开了一种含有抗敏芳香中草药的护肤品。由如下重量份数的组分构成：乳木果油3‑5份、胶原蛋白10‑20份、抗敏中草药提取物15‑30份、保湿剂5‑10份、维生素0.1‑1份、水50‑200份。本发明将抗敏芳香中草药加入到护肤品中，赋予护肤品抗敏药效，同时，采用发酵的方法降低抗敏芳香中草药的苦味；采用椰子油和鳄梨油共发酵产生的香气物质，进一步掩盖中草药的苦味，并增加护肤品的香味物质含量。

Description

一种含有抗敏芳香中草药的护肤品
技术领域
本发明属于护肤品制备技术领域，具体涉及一种含有抗敏芳香中草药的护肤品。
背景技术
随着社会经济的不断进步和物质生活的丰富，护肤品种类越来越多，它对人们的精神、形象提升起到了极大的作用。护肤品中添加特殊组分，如营养因子、胶原蛋白、中药组分、维生素等都成为人们研究的一个热点。
在护肤品中添加中草药，赋予了护肤品药效，集美容与治病为一体，收到人们的青睐。抗敏中草药由积雪草、土茯苓、辛夷、鱼腥草、蝉蜕等的提取物组成，其提取物有一股强烈的苦味，添加到护肤品中虽然有药效，但是，其味道难闻，难以被人们接受。
发明内容
本发明的目的在于提供一种含有抗敏芳香中草药的护肤品。
一种含有抗敏芳香中草药的护肤品，由如下重量份数的组分构成：乳木果油3-5份、胶原蛋白10-20份、抗敏中草药提取物15-30份、保湿剂5-10份、维生素0.1-1份、水50-200份。
所述维生素为维生素C、维生素E、谷胱甘肽、维生素A、维生素D中的一种或几种。
所述保湿剂为甘油、乙二醇、丙二醇、丙二醇二缩水甘油醚、聚乙二醇中的一种或几种。
所述抗敏中草药提取物采用如下方法制备：
(1)按照重量份数，取中药成分积雪草12-30份、土茯苓5-10份、辛夷5-10份、鱼腥草10-20份、蝉蜕5-8份；将上述组分混合后打为粉末，过60-100目筛；
(2)加入水50-120份，再加入椰子油5-10份和鳄梨油5-10份，混合搅拌均匀；
(3)接入黑曲霉菌菌液1-3％，在28-32℃条件下发酵20-40h，加热至70-90℃灭菌10-20min；
(4)接入乳酸乳球菌1-3％，在23-27℃条件下发酵40-60h，加热至70-90℃灭菌10-20min，制成发酵物；
(5)加入发酵物质量5-10倍的60-80wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.1-1.3g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。
所述黑曲霉菌菌液中活菌数为1-3X108cfu/mL。
所述乳酸乳球菌菌液中活菌数为5-9X107cfu/mL。
步骤(2)所述搅拌的速率为400-800rpm，搅拌时间10-20min。
本发明的有益效果：本发明将抗敏芳香中草药加入到护肤品中，赋予护肤品抗敏药效，同时，采用发酵的方法降低抗敏芳香中草药的苦味；采用椰子油和鳄梨油共发酵产生的香气物质，进一步掩盖中草药的苦味，并增加护肤品的香味物质含量。
附图说明
图1为不同菌种发酵制备的抗敏中草药提取物苦味值。
图2为加入不同油脂发酵制备的抗敏中草药提取物苦味值。
具体实施方式
为了便于理解本发明，下面将对本发明进行更全面的描述。但是，本发明可以以许多不同的形式来实现，并不限于本文所描述的实施例。相反地，提供这些实施例的目的是使对本发明的公开内容的理解更加透彻全面。
下述实施例采用的黑曲霉购买自中国普通微生物菌种保藏管理中心，保藏编号为CGMCC No:3.11584；乳酸乳球菌购买自中国普通微生物菌种保藏管理中心，保藏编号为CGMCC No:1.12794。
苦味的感观分析评价员根据国标GB/T 14195-93标准方法进行筛选和培训，其中男生5名，女生5名(20-35岁)。采用0～10分制，以L-异亮氨酸(苦味，0.5％)作为标准溶液，评分为10分，参照标准液苦味进行打分。
实施例1抗敏中草药提取物制备方法
(1)按照重量份数，取中药成分积雪草22份、土茯苓7份、辛夷8份、鱼腥草15份、蝉蜕6份；将上述组分混合后打为粉末，过80目筛；
(2)加入上述物料质量8倍的70wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.2g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。经测定上述抗敏中草药提取物的苦味值为9.5±0.3(测定3次取平均值)。
实施例2发酵抗敏中草药提取物制备方法
(1)按照重量份数，取中药成分积雪草22份、土茯苓7份、辛夷8份、鱼腥草15份、蝉蜕6份；将上述组分混合后打为粉末，过80目筛；
(2)接入菌液2％，菌液中活菌数设定为5X107cfu/mL，在最适温度条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(3)加入上述物料质量8倍的70wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.2g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。
所述菌种选自：酿酒酵母CGMCC NO：2.3866，最适温度25℃；植物乳杆菌CGMCC NO：1.12935，最适温度37℃；黑曲霉CGMCC No:3.11584，最适温度30℃；枯草芽孢杆菌CGMCCNO：1.8886，最适温度37℃；乳酸乳球菌CGMCC No:1.12794，最适温度25℃；测定选用上述菌种发酵后抗敏中草药提取物的苦味值数据。
测定结果见图1，黑曲霉和乳酸乳球菌发酵能够显著降低抗敏中草药提取物的苦味。
实施例3联合发酵抗敏中草药提取物制备方法
(1)按照重量份数，取中药成分积雪草22份、土茯苓7份、辛夷8份、鱼腥草15份、蝉蜕6份；将上述组分混合后打为粉末，过80目筛；
(2)接入黑曲霉菌液2％，菌液中活菌数设定为2X108cfu/mL，在30℃条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(3)接入乳酸乳球菌菌液2％，菌液中活菌数设定为6X107cfu/mL，在25℃条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(4)加入上述物料质量8倍的70wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.2g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。经测定上述抗敏中草药提取物的苦味值为7.3±0.4(测定3次取平均值)。
实施例4联合油脂发酵抗敏中草药提取物制备方法
发明人发现，黑曲霉和乳酸乳球菌发酵植物油脂易产生香味物质，并且能掩盖苦味，本实施例采用如下植物油脂进行实验：大豆油、玉米胚芽油、椰子油、蓖麻油、鳄梨油、羊油、花生油、菜籽油；抗敏中草药提取物制备方法如下：
(1)按照重量份数，取中药成分积雪草22份、土茯苓7份、辛夷8份、鱼腥草15份、蝉蜕6份；将上述组分混合后打为粉末，过80目筛；
(2)加入水80份，再加入油脂14份，混合搅拌均匀；所述搅拌的速率为600rpm，搅拌时间15min；
(3)接入黑曲霉菌液2％，菌液中活菌数设定为2X108cfu/mL，在30℃条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(4)接入乳酸乳球菌菌液2％，菌液中活菌数设定为6X107cfu/mL，在25℃条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(5)加入上述物料质量8倍的70wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.2g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。
测定结果见图2，加入椰子油、鳄梨油发酵能够显著降低抗敏中草药提取物的苦味值。
实施例5复合油脂发酵抗敏中草药提取物制备方法
(1)按照重量份数，取中药成分积雪草22份、土茯苓7份、辛夷8份、鱼腥草15份、蝉蜕6份；将上述组分混合后打为粉末，过80目筛；
(2)加入水80份，再加入椰子油7份、鳄梨油7份，混合搅拌均匀；所述搅拌的速率为600rpm，搅拌时间15min；
(3)接入黑曲霉菌液2％，菌液中活菌数设定为2X108cfu/mL，在30℃条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(4)接入乳酸乳球菌菌液2％，菌液中活菌数设定为6X107cfu/mL，在25℃条件下发酵30h，加热至80℃灭菌15min，制成发酵物；
(5)加入上述物料质量8倍的70wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.2g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。经测定上述抗敏中草药提取物的苦味值为4.6±0.1(测定3次取平均值)。
实施例6
一种含有抗敏芳香中草药的护肤品，由如下重量份数的组分构成：乳木果油4份、胶原蛋白15份、实施例5制备的抗敏中草药提取物22份、甘油7份、维生素C 0.1份、维生素E0.1份、水100份。
实施例7
一种含有抗敏芳香中草药的护肤品，由如下重量份数的组分构成：乳木果油3份、胶原蛋白10份、实施例5制备的抗敏中草药提取物15份、乙二醇5份、维生素C 0.02份、维生素E 0.02份、谷胱甘肽0.03份、维生素A 0.01份、维生素D 0.03份、水50份。
实施例8
一种含有抗敏芳香中草药的护肤品，由如下重量份数的组分构成：乳木果油5份、胶原蛋白18份、实施例5制备的抗敏中草药提取物28份、丙二醇9份、维生素C 0.4份、维生素E 0.4份、水200份。
实施例9
一种含有抗敏芳香中草药的护肤品，由如下重量份数的组分构成：乳木果油5份、胶原蛋白10份、实施例5制备的抗敏中草药提取物25份、丙二醇二缩水甘油醚7份、谷胱甘肽0.1份、维生素A 0.1份、维生素D 0.2份、水150份。
以上所述实施例仅表达了本发明的几种实施方式，其描述较为具体和详细，但并不能因此而理解为对发明专利范围的限制。应当指出的是，对于本领域的普通技术人员来说，在不脱离本发明构思的前提下，还可以做出若干变形和改进，这些都属于本发明的保护范围。因此，本发明专利的保护范围应以所附权利要求为准。

Claims (7)

1.一种含有抗敏芳香中草药的护肤品，其特征在于，由如下重量份数的组分构成：乳木果油3-5份、胶原蛋白10-20份、抗敏中草药提取物15-30份、保湿剂5-10份、维生素0.1-1份、水50-200份。
2.根据权利要求1所述含有抗敏芳香中草药的护肤品，其特征在于，所述维生素为维生素C、维生素E、谷胱甘肽、维生素A、维生素D中的一种或几种。
3.根据权利要求1所述含有抗敏芳香中草药的护肤品，其特征在于，所述保湿剂为甘油、乙二醇、丙二醇、丙二醇二缩水甘油醚、聚乙二醇中的一种或几种。
4.根据权利要求1所述含有抗敏芳香中草药的护肤品，其特征在于，所述抗敏中草药提取物采用如下方法制备：
(1)按照重量份数，取中药成分积雪草12-30份、土茯苓5-10份、辛夷5-10份、鱼腥草10-20份、蝉蜕5-8份；将上述组分混合后打为粉末，过60-100目筛；
(2)加入水50-120份，再加入椰子油5-10份和鳄梨油5-10份，混合搅拌均匀；
(3)接入黑曲霉菌菌液1-3％，在28-32℃条件下发酵20-40h，加热至70-90℃灭菌10-20min；
(4)接入乳酸乳球菌1-3％，在23-27℃条件下发酵40-60h，加热至70-90℃灭菌10-20min，制成发酵物；
(5)加入发酵物质量5-10倍的60-80wt％乙醇溶液，渗漉提取，提取液回收并浓缩至密度为1.1-1.3g/cm3的浸膏，气流粉碎得到抗敏中草药提取物。
5.根据权利要求1所述含有抗敏芳香中草药的护肤品，其特征在于，所述黑曲霉菌菌液中活菌数为1-3X108cfu/mL。
6.根据权利要求1所述含有抗敏芳香中草药的护肤品，其特征在于，所述乳酸乳球菌菌液中活菌数为5-9X107cfu/mL。
7.根据权利要求1所述含有抗敏芳香中草药的护肤品，其特征在于，步骤(2)所述搅拌的速率为400-800rpm，搅拌时间10-20min。
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