CN112006960A - Acne-removing and oil-controlling composition and preparation method and application thereof - Google Patents
Acne-removing and oil-controlling composition and preparation method and application thereof Download PDFInfo
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- CN112006960A CN112006960A CN202010966859.3A CN202010966859A CN112006960A CN 112006960 A CN112006960 A CN 112006960A CN 202010966859 A CN202010966859 A CN 202010966859A CN 112006960 A CN112006960 A CN 112006960A
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- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 description 1
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- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9722—Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Animal Behavior & Ethology (AREA)
- Biotechnology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Mycology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Cosmetics (AREA)
Abstract
The application relates to the field of skin care products, and particularly relates to an acne-removing and oil-controlling composition, a preparation method and an application thereof, wherein the acne-removing and oil-controlling composition comprises the following components in parts by mass: 10-15 parts of cascara spicata bark extract; 12-20 parts of a Chinese alangium leaf extract; 100 parts of tea extract; also relates to a preparation method of the acne-removing and oil-controlling composition, which comprises the following steps: the method comprises the following steps: and mixing the cascara Periplaneta bark extract, the cumin leaf extract and the tea leaf extract, and uniformly stirring to obtain the acne-removing and oil-controlling composition. The composition can be used in skin care products, and has the advantages of being not easy to cause irritation to the skin and being capable of increasing the applicable population of the product.
Description
Technical Field
The application relates to the technical field of skin care products, in particular to an acne-removing and oil-controlling composition and a preparation method and application thereof.
Background
Pox, also known as acne, is a chronic inflammatory skin disease very common to the pilosebaceous glands.
The factors such as genetic factors, endocrine dyscrasia, facial cleaning and sanitation, dietary habits, long-term mental stress and the like easily cause sebum metabolic disorder, so that skin grease is excessively exuberant in secretion, excessive sebum mixture gradually deposits at hair follicles to form solid lipid plugs which are difficult to remove, so that follicular keratosis is abnormal due to pore blockage, sebum cannot be normally discharged, small sebaceous globules are gradually formed, skin swelling and protrusion are accompanied by pain, and a weak acid anaerobic environment which is very suitable for reproduction and aggregation of anaerobic propionibacterium acnes is formed in the hair follicles due to the blockage of the hair follicles, so that the anaerobic propionibacterium acnes in the hair follicles is increased and a large amount of sebum is decomposed, a large amount of free fatty acid is formed, the hair follicle wall is damaged, and inflammation of connective tissues around the hair follicles is caused.
The related art generally achieves the aim of removing the pox by adding components with oil control or bacteriostatic effects into skin care products.
In view of the above-mentioned related technologies, the inventor believes that most of the components with oil control or bacteriostatic effects easily irritate the skin or destroy normal flora on the surface of the skin, so that the skin barrier is easily damaged, the moisture retention capacity of the skin is reduced, and further the water-oil balance of the skin is easily disturbed, so that acne is easily repeated, and the applicable population of the product is narrow.
Disclosure of Invention
In order to overcome the defect that the applicable population of the product is narrow, the application provides an acne-removing and oil-controlling composition and a preparation method and application thereof.
In a first aspect, the application provides an acne-removing and oil-controlling composition, which adopts the following technical scheme:
the acne-removing and oil-controlling composition comprises the following components in parts by mass:
10-15 parts of cascara spicata bark extract;
12-20 parts of a Chinese alangium leaf extract;
100 parts of tea extract.
Preferably, the composition comprises the following components in parts by mass:
11-13 parts of cascara spicata bark extract;
14-18 parts of a Chinese alangium leaf extract;
100 parts of tea extract.
By adopting the technical scheme, the cascara sagrada bark extract contains various anthraquinone compounds, has inhibition effects on various bacteria to different degrees, is not easy to generate drug resistance, has the effects of removing superoxide anion free radicals and hydroxyl free radicals, and has an anti-oxidation effect.
Due to the adoption of the tea extract, the existence of tea polyphenol in the tea extract can enhance the water locking capacity of the horny layer of the skin, effectively avoid water loss in skin cells and relieve skin discomfort caused by ultraviolet irradiation.
Due to the adoption of the extract of the leaves of the Chinese alangium, the extract of the leaves of the Chinese alangium has better effects of sterilizing and diminishing inflammation, and is beneficial to improving the sterilizing and anti-inflammatory effects of the product.
The oil control and acne removal effects of the skin after the composition is added into a skin care product are good, and the use safety of the product is improved.
Preferably, the acne-removing and oil-controlling composition further comprises the following components in parts by mass:
5-10 parts of chlorella aureocauda extract.
By adopting the technical scheme, the water collecting and water retaining performance of the chlorella aureocauda extract can adjust oil secretion in the skin by adding the chlorella aureocauda extract, and the chlorella aureocauda extract is matched with the rhamnus parviflora bark extract, the cumin leaf extract and the tea leaf extract for use together, so that the moisture retaining effect of the chlorella aureocauda extract is further improved, the water-oil balance of the skin is facilitated, and the oil control effect of the skin is further improved.
Preferably, the acne-removing and oil-controlling composition further comprises the following components in parts by mass:
13-15 parts of tremella extract.
By adopting the technical scheme, the tremella extract has good water absorption performance and film forming performance by adding the tremella extract, and the moisturizing capability and the oil control capability of the skin are further enhanced by matching the tremella extract with the cascara Pelargonii bark extract, the Amur bushy leaf extract and the tea leaf extract.
Preferably, the acne-removing and oil-controlling composition further comprises the following components in parts by mass:
11-13 parts of cactus extract.
By adopting the technical scheme, the cactus extract has better moisturizing capability, contains components with nourishing effect on skin such as amino acid, polysaccharide, superoxide dismutase and the like, has better relieving effect, and can remove free radicals to a certain extent so as to improve the antioxidant effect of the skin.
In a second aspect, the application provides a preparation method of the acne-removing and oil-controlling composition, which adopts the following technical scheme:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
mixing the cascara sagrada bark extract, the Amur bushy leaf extract and the tea leaf extract, and uniformly stirring to obtain the acne-removing and oil-controlling composition.
By adopting the technical scheme, the cascara sagrada bark extract, the amur cork-leaf extract and the tea extract are mixed and uniformly stirred, and the method has the effects of simple production process and convenience for industrial production.
Preferably, when the cascara Persea bark extract, the cumin leaf extract and the tea leaf extract are mixed, the trace microspherical algae extract, the tremella extract and the cactus extract are added, and the mixture is uniformly stirred to obtain the acne-removing and oil-controlling composition.
By adopting the technical scheme, when the birch buckthorn bark extract, the cubeb leaf extract and the tea leaf extract are mixed, the micro-microsphere algae extract, the tremella extract and the cactus extract are added, the stirring is uniform, the compatibility of all the substances is good, and the production operation is simple and convenient.
In a third aspect, the application provides an application of the acne-removing and oil-controlling composition, which adopts the following technical scheme:
the application of the acne-removing and oil-controlling composition is added into a skin care product.
By adopting the technical scheme, the acne-removing and oil-controlling composition is added into the skin care product, so that the skin care product has better acne-removing and oil-controlling effects, and the skin barrier can be better repaired, thereby accelerating the removal of acne and enabling the skin to be quickly recovered to be healthy.
Preferably, the skin care product comprises water, milk, essence, lotion, cream, and facial mask.
By adopting the technical scheme, the acne-removing and oil-controlling composition is added into water, milk, essence, milk, cream and facial mask, so that the water, milk, essence, milk, cream and facial mask have remarkable acne-removing and oil-controlling effects, thereby accelerating the removal of acnes and accelerating the recovery of skin health.
Preferably, the added mass of the acne-removing and oil-controlling composition accounts for 1% -3% of the mass of the skin care product.
By adopting the technical scheme, the acne removing and oil controlling composition accounts for 1-3% of the skin care product, and the acne removing and oil controlling composition in a specific proportion is added, so that the skin care product has a good acne removing effect, and the skin is accelerated to recover health.
In summary, the present application has the following beneficial effects:
1. due to the fact that the cascara sagrada bark extract, the cubeb litsea leaf extract and the tea extract are used in a matched mode, irritation of the cascara sagrada bark extract and the cubeb litsea leaf extract to the skin is relieved, the composition has good acne removing and oil controlling capacity, and therefore after the composition is added to a skin care product, the oil controlling and acne removing effect of the skin is good, and the use safety of the product is improved.
2. By adding the chlorella aureobasidium extract and using the chlorella aureobasidium extract together with the cascara peltata bark extract, the amur cork tree leaf extract and the tea leaf extract, the moisturizing effect of the chlorella aureobasidium extract is further improved, and the oil control effect of the skin is further improved.
3. The acne-removing and oil-controlling composition is added into the skin care product, so that the skin care product has better acne-removing and oil-controlling effects, the removal of acnes is accelerated, and the skin is quickly recovered to be healthy.
Detailed Description
The information on the source of each raw material component in the following examples and comparative examples is shown in Table 1
TABLE 1
Examples 1 to 5
The embodiment of the application discloses an acne-removing and oil-controlling composition which comprises the following components:
cascara Periplaneta bark extract, folium Hibisci Mutabilis extract, and folium Camelliae sinensis extract.
In examples 1-5, the amounts (in Kg) of each component added are specified in Table 2
TABLE 2
In embodiments 1 to 5, a preparation method of an acne-removing and oil-controlling composition comprises the following specific steps:
adding the cascara sagrada bark extract, the Amur bushy leaf extract and the tea extract into a stirring kettle, stirring at the rotating speed of 100r/min for 5min, and uniformly stirring to obtain the acne-removing and oil-controlling composition.
Example 6
The embodiment of the application discloses an acne-removing and oil-controlling composition:
compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
adding the cascara sagrada bark extract, the Amur bushy leaf extract and the tea extract into a stirring kettle, stirring at the rotating speed of 100r/min for 3min, and uniformly stirring to obtain the acne-removing and oil-controlling composition.
Example 7
The embodiment of the application discloses an acne-removing and oil-controlling composition:
compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
adding the cascara sagrada bark extract, the Amur bushy leaf extract and the tea extract into a stirring kettle, stirring at the rotating speed of 100r/min for 8min, and uniformly stirring to obtain the acne-removing and oil-controlling composition.
Examples 8 to 10
The embodiment of the application discloses an acne-removing and oil-controlling composition:
compared with example 3, the difference is only that:
the acne-removing and oil-controlling composition also comprises the following components:
chlorella minutissima extract.
In examples 6 to 10, the amounts (in Kg) of the respective components added are specified in Table 3
TABLE 3
Adding the Chlorella minutissima extract, the cascara sagrada bark extract, the Amur bushy leaf extract and the tea leaf extract into a stirring kettle, stirring at the rotating speed of 100r/min for 8min, and uniformly stirring to obtain the acne-removing and oil-controlling composition.
Examples 11 to 13
The embodiment of the application discloses an acne-removing and oil-controlling composition:
compared with example 3, the difference is only that:
the acne-removing and oil-controlling composition also comprises the following components:
a tremella extract.
In examples 11-13, the amounts (in Kg) of each component added are specified in Table 4
TABLE 4
Adding Tremella extract, cortex Periplocae Calophyllae extract, folium Hibisci Mutabilis extract, and folium Camelliae sinensis extract into a stirring kettle, stirring at 100r/min for 5min, and stirring to obtain the composition with effects of removing acne and controlling oil.
Examples 14 to 16
The embodiment of the application discloses an acne-removing and oil-controlling composition:
compared with example 3, the difference is only that:
the acne-removing and oil-controlling composition also comprises the following components:
cactus extract.
In examples 14 to 16, the amounts (in Kg) of the respective components added are specified in Table 5
TABLE 5
Adding radix et caulis Opuntiae Dillenii extract, cortex Periplocae Calophyllae extract, radix Inulae Coreanae leaf extract, and folium Camelliae sinensis extract into a stirring kettle, stirring at 100r/min for 3min, and stirring to obtain composition for removing acne and controlling oil.
Examples 17 to 19
The embodiment of the application discloses an acne-removing and oil-controlling composition:
compared with example 3, the difference is only that:
the acne-removing and oil-controlling composition also comprises the following components:
chlorella aureofaciens extract, Tremella extract, and radix et caulis Opuntiae Dillenii extract.
In examples 17-19, the amounts (in Kg) of each component added are specified in Table 6
TABLE 6
Adding the Chlorella aureocauda extract, Tremella extract, radix et caulis Opuntiae Dillenii extract, cortex Pelargonii Hortori extract, folium Hibisci Munryi extract, and folium Camelliae sinensis extract into a stirring kettle, stirring at 100r/min for 3min, and stirring to obtain the composition for removing acne and controlling oil.
Comparative example 1
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
the method adopts equivalent water to replace the cascara Periplaneta bark extract, the Amur bushy leaf extract and the tea leaf extract.
Comparative example 2
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
the water is used to replace the extract of the leaf of the Chinese pudding and the extract of the tea leaf with the same amount.
Comparative example 3
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
the cascara Periplaneta bark extract and the tea leaf extract are replaced by the same amount of water.
Comparative example 4
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
the method adopts equivalent water to replace the extract of the bark of the cascara Periplaneta and the extract of the leaves of the Amur bristlegrass.
Comparative example 5
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
the extract of the bark of cascara sagrada is replaced by the same amount of water.
Comparative example 6
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
the extract of the leaves of the Chinese pudding is replaced by the same amount of water.
Comparative example 7
Compared with example 3, the difference is only that:
the preparation method of the acne-removing and oil-controlling composition comprises the following steps:
equal amount of water is used to replace the tea extract.
Experimental examples 1 to 14
The application experimental example discloses an essence milk:
the essence milk comprises the following components in parts by mass:
2Kg of acne-removing and oil-controlling composition, 6Kg of glycerin, 4Kg of 1, 3-propylene glycol, 0.8Kg of xanthan gum, 0.6Kg of stearic acid, 0.5Kg of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 5Kg of glyceryl stearate, 0.1Kg of p-hydroxyacetophenone and 82Kg of water.
Acne removing and oil controlling composition of experimental examples 1 to 14 the obtained acne removing and oil controlling compositions prepared in examples 1, 2, 5, 8, 11, 14 and 17 and comparative examples 1 to 7 were used, respectively.
The preparation method of the essence milk comprises the following specific steps:
step 1), adding glycerol, 1, 3-propylene glycol, stearic acid, glycerol stearate, p-hydroxyacetophenone and water into a stirring kettle together, stirring uniformly for 25min at a speed of 60r/min, heating to 85 ℃, standing and preserving heat for 20min to obtain an essence milk premix;
and 2) cooling to 50 ℃, adding the dipotassium glycyrrhizinate and acne-removing and oil-controlling composition, stirring for 60r/min for 15min, stirring uniformly, adding acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and xanthan gum, stirring for 60r/min for 15min, and obtaining the essence milk.
Experimental examples 15 to 28
The application experimental example discloses a smoothing toner:
the smoothing toner comprises the following components in parts by mass:
1Kg of acne-removing and oil-controlling composition, 4Kg of butanediol, 5Kg of glycerin, 0.2Kg of EDTA disodium, 0.05Kg of caprylyl hydroxamic acid, 0.05Kg of p-hydroxyacetophenone, 0.2Kg of triethanolamine, 2Kg of xanthan gum and 89.5Kg of water.
Acne removing and oil controlling composition of experimental examples 15 to 28 the acne removing and oil controlling compositions prepared in examples 1,3, 5, 9, 12, 15 and 18 and comparative examples 1 to 7 were used, respectively.
The preparation method of the smoothing toner comprises the following specific steps:
step 1), adding butanediol, glycerol, EDTA disodium, p-hydroxyacetophenone and water into a stirring kettle together, stirring for 15min at a speed of 60r/min, uniformly stirring, heating to 80 ℃, standing and preserving heat for 20min to obtain a skin softening water premix;
and 2) when the temperature is reduced to 50 ℃, adding the caprylyl hydroximic acid, the triethanolamine and the acne-removing and oil-controlling composition, continuously stirring for 15min at a speed of 60r/min, uniformly stirring, then adding xanthan gum at a speed of 60r/min, continuously stirring for 10min, and uniformly stirring to obtain the smoothing toner.
Experimental examples 29 to 42
The application experimental example discloses a face cream:
the face cream comprises the following components in parts by mass:
3Kg of acne-removing and oil-controlling composition, 10Kg of glycerin, 0.5Kg of hyaluronic acid, 0.8Kg of carbomer, 1Kg of squalane, 2Kg of polyglycerol-3 methyl glucose distearate, 0.1Kg of allantoin, 0.2Kg of disodium EDTA, 1Kg of cetyl alcohol, 0.5Kg of hydrogenated lecithin, 1Kg of p-hydroxyacetophenone and 82.9Kg of water.
Acne removing and oil controlling compositions of experimental examples 29 to 42 the acne removing and oil controlling compositions prepared in examples 1, 4, 5, 10, 13, 16 and 19 and comparative examples 1 to 7 were used, respectively.
The preparation method of the face cream comprises the following specific steps:
step 1), adding glycerol, squalane, polyglycerol-3-methyl glucose distearate, EDTA disodium, cetearyl alcohol, hydrogenated lecithin, p-hydroxyacetophenone and water into a stirring kettle together, continuously stirring for 25min at a speed of 60r/min, uniformly stirring, heating to 80 ℃, standing and preserving heat for 20min to obtain a cream premix;
and 2) cooling to 50 ℃, adding the acne-removing and oil-controlling composition, stirring at 60r/min for 5min, stirring uniformly, then adding hyaluronic acid and carbomer at 60r/min, stirring continuously for 10min, and stirring uniformly to obtain the cream.
Experiment 1
Human skin irritation test
The test method comprises the following steps: the test method comprises the following steps: the patch test method adopts 48h closed patch test, and selects 130 healthy volunteers without allergy history, and randomly and averagely divides the healthy volunteers into 26 groups. After cleaning the back of a subject, the spot tester added with the acne-removing and oil-controlling composition prepared in each embodiment and comparative example is pasted on the back by using a non-irritating adhesive tape, the adhesive tape is lightly pressed by fingers after being pasted, so that the adhesive tape is uniformly pasted on the skin for 48 hours, the drying of the spot part of the subject is ordered to be kept within 48 hours, the fierce movement, the scratching of the spot part, the long-time sunlight irradiation and the like are avoided, the spot part is removed after 48 hours and dried, the paste marks disappear after 30 minutes and the like, the judgment is carried out under sufficient light, and the revisit observation is carried out at 72 hours and 96 hours respectively.
The grading standard of adverse reaction in the skin patch test is shown in Table 6
TABLE 6
The results of the skin adverse reactions of the acne-removing and oil-controlling compositions prepared in the examples and comparative examples are shown in Table 7
TABLE 7
According to the comparison of the data of comparative example 2 and comparative example 1 in table 7, the subjects showed suspicious reactions by adding the cascara sagrada bark extract, which proved that the cascara sagrada bark extract had some irritation to the skin.
According to the comparison of the data of comparative example 3 and comparative example 1 in table 7, the subjects showed positive reaction by adding the extract of the leaves of Amur buster, which proved to have strong irritation.
As can be seen from comparison of the data of comparative example 4 and comparative example 1 in table 7, the subjects showed negative reactions by adding the tea extract, demonstrating that the tea extract was mild to the skin.
According to the comparison of the data of comparative examples 5-7 and comparative examples 2-4 in table 7, when the cascara sagrada bark extract, the arnebia root extract and the tea extract are used in combination, the subject has suspicious reaction, which proves that the cascara sagrada bark extract, the arnebia root extract and the tea extract are still irritant to some extent when used in combination.
According to the comparison of the data of example 3 and comparative examples 5-7 in table 7, the subjects showed negative reactions when the cascara spicata bark extract, the arnebia montana leaf extract and the tea leaf extract were used together, which proved that the skin irritation of the cascara spicata bark extract and the arnebia montana leaf extract was significantly reduced after the cascara spicata bark extract, the arnebia montana leaf extract and the tea leaf extract were used together, so that the products were mild to the skin and less likely to cause irritation to the skin.
According to the comparison of the data of the examples 8-10 and the example 3 in the table 7, the subjects showed negative reactions after adding the extract of Micrococcus minimus, which proves that the product is mild to the skin and not easy to irritate the skin after the Micrococcus minimus extract is used together with the cascara Pericarpa bark extract, the Amur bushy leaf extract and the tea leaf extract.
According to the comparison of the data of examples 11-13 and example 3 in table 7, the subjects showed negative reactions after adding the tremella extract, which proves that the combination of the tremella extract with the cascara spicata bark extract, the cubeb litsea leaf extract and the tea leaf extract makes the product milder to the skin and less prone to cause irritation to the skin.
According to the comparison of the data of the examples 14-16 and the example 3 in the table 7, the test subject showed a negative reaction after adding the cactus extract, which proves that the product is mild to the skin and not easy to cause irritation to the skin after the nandina parviflora extract is used together with the rhamnus parviflora bark extract, the lonicera confusa leaf extract and the tea leaf extract.
Experiment 2
Propionibacterium acnes bacteriostasis test
According to a culture medium for operation of 'cosmetic hygiene standards' 2015 edition, a bacterial liquid preparation method and an inoculation method, the skin care products prepared in the experimental examples 1-42 are subjected to a propionibacterium acnes bacteriostasis test, the bacteriostasis rate represents the bacteriostasis result, the higher the bacteriostasis rate is, the better the bacteriostasis effect of the skin care products is proved, and the lower the bacteriostasis rate is, the worse the bacteriostasis effect of the skin care products is proved.
Experiment 3
Evaluation of oil control Effect
The test population is selected to be 15-35 years old and 126 people in total, each group comprises 3 people, half of men and women, the face has obvious acnes and acnes, the test population accords with the volunteer selection standard of a subject, the test population is continuously used for 14 days after 2 times every day, and other skin care products or hormone products cannot be used in the test process. The sebum value was determined after 14 days by the test persons' return, using the model SM815 test method, brand Courage-Khazaka, Germany, and the treatment effect was recorded, the sebum value reduction being obtained by subtracting the sebum value before use from the sebum value after 14 days.
The detection data of the essence milk in the experiments 1-2 are shown in a table 8, the detection data of the smoothing toner is shown in a table 9, and the detection data of the cream is shown in a table 10.
TABLE 8
TABLE 9
Watch 10
According to the comparison of the data of the experimental example 9 and the experimental example 8 in the table 8, the bacteriostasis rate of the skin care product is obviously increased by adding the cascara spicata bark extract into the essence milk, so that the cascara spicata bark extract can effectively inhibit propionibacterium acnes, the reduction value of the sebum value of the skin is improved to a certain extent, and the cascara spicata bark extract is proved to have a certain oil control capability, so that the repair of pox is facilitated, and the acne removing effect of the product is improved.
According to the comparison of the data of the experimental example 10 and the experimental example 8 in table 8, the bacteriostatic rate of the skin care product is obviously reduced by adding the extract of the leaves of the ambumleaf into the essence milk, which proves that the extract of the leaves of the ambumleaf can obviously inhibit propionibacterium acnes, the decrease value of the sebum value is not greatly changed, and that the oil control capability of the extract of the leaves of the ambumleaf on the skin is poor, so that the extract of the leaves of the ambumleaf can promote the repair of acnes to a certain extent, and similarly, the data of the experimental example 24 and the experimental example 22 in table 9 and table 10, and the data of the experimental example 38 and the experimental example 36 prove that the effect of the extract of the leaves of the ambumleaf added into the smoothing toner and the facial cream is similar, so that the effect of the extract of the leaves added into the.
According to the comparison of the data of the experimental example 11 and the experimental example 8 in table 8, the reduction value of sebum is obviously improved by adding the tea extract into the essence milk, so that the tea extract has better oil control capability and lower bacteriostatic rate, and the tea extract has poorer bacteriostatic effect, so that the tea extract can promote the repair of acne to a certain extent, and similarly, the data of the experimental example 25 and the experimental example 22 in tables 9 and 10, and the data of the experimental example 39 and the experimental example 36 prove that the effect of adding the tea extract into the smoothing toner and the facial cream is similar, so that the effect of adding the tea extract into the skin care product is similar to the effect of adding the tea extract into the essence milk.
According to the comparison of the data of the experimental example 12 and the experimental example 10 in the table 8, the bacteriostatic rate is further improved by adding the tea extract and the kuhseng leaf extract into the essence milk, the reduction value of the sebum value is obviously improved, and the inhibition effect of the propionibacterium acnes is improved and the oil control capability of the skin is improved after the tea extract and the kuhseng leaf extract are used together, so that the acne removing effect of the product is better, and similarly, the data of the experimental examples 26 and 24, the experimental example 40 and the experimental example 38 in the tables 9 and 10 prove that the effects of the tea extract and the kuhseng leaf extract added into the skin softening lotion and the face cream are similar, so that the effect of the tea extract and the kuhseng leaf extract added into the skin care product is similar to the effect of the tea extract and the kuhseng leaf extract added into.
According to the comparison of the data of the experimental example 13 and the experimental example 9 in the table 8, the bacteriostatic rate is improved to a certain extent by adding the tea extract and the cascara spicata bark extract into the essence milk, which proves that the inhibition rate of propionibacterium acnes can be improved to a certain extent after the tea extract and the cascara spicata bark extract are matched, the reduction value of sebum value is obviously improved, the oil control effect of the tea extract and the cascara spicata bark extract on skin is better, the tea extract is beneficial to removing redundant grease from skin and accelerating the removal of acnes, and similarly, the data of the experimental examples 27 and 23, the experimental example 41 and the experimental example 37 in the tables 9 and 10 prove that the tea extract and the cascara spicata bark extract are matched and added into the smoothing toner and the face cream to have similar effects, therefore, the effect of the tea extract and the Perilla frutescens bark extract added into the skin care product is similar to the effect of the tea extract and the Perilla frutescens bark extract added into the essence milk.
According to the comparison of the data of the experimental example 14 and the experimental examples 9 and 10 in the table 8, the bacteriostatic rate of the skin care product is not greatly changed and the reduction value of the sebum value is not greatly changed by adding the cubeb litsea tree leaf extract and the cubeb litsea tree bark extract into the essence milk for matching use, so that the cubeb litsea tree leaf extract and the cubeb litsea tree bark extract after matching use are proved to have insignificant change on the propionibacterium acnes and little influence on the oil control capability of the extracted skin care product, and similarly, the data of the experimental examples 28 and the experimental examples 23 and 24, the experimental examples 42 and the experimental examples 37 and 38 in the tables 9 and 10 prove that the cubeb litsea tree leaf extract and the cubeb litsea tree bark extract have similar effects on the addition of the cubeba bark extract into the smoothing toner and the facial cream, therefore, the effect of the extract of the Amur brazil leaves and the extract of the bark of the cascara sagrada added into the skin care product is similar to the effect of the extract added into the essence milk.
According to the comparison of the data of the experimental example 2 and the experimental examples 12-14 in the table 8, the bacteriostatic rate of the skin care product is further improved and the sebum value reduction value is further improved by adding the tea extract, the cubeb sikaki leaf extract and the cubeb sikamea bark extract into the essence milk for use together, so that the inhibition effect on propionibacterium acnes is improved after the tea extract, the cubeb sikaki leaf extract and the cubeb sikamea bark extract are combined together, the oil control capability of the skin care product is also improved, and the acne removing effect of the skin care product is further improved, and similarly, the data of the experimental examples 16 and the experimental examples 26-28, the experimental example 30 and the experimental examples 40-42 in the tables 9 and 10 prove that the tea extract, the cubeb sikaki leaf extract and the cubia sikamea bark extract are combined together and added into the smoothing toner and the face cream, therefore, the effect of the tea extract, the cubeb litsea leaf extract and the peruvian rhamnus bark extract which are matched and added into the skin care product is similar to the effect of the tea extract, the cubeb litsea leaf extract and the peruvian rhamnus bark extract which are added into the essence milk.
According to comparison of the data of the experimental example 4 and the experimental examples 1-3 in the table 8, the reduction value of sebum value after the addition of the chlorella vulgaris extract is further improved by adding the chlorella vulgaris extract into the essence milk, and the result proves that the oil control capability of the skin care product can be obviously improved after the chlorella vulgaris extract is added, so that the skin care product is favorably helped to prevent the generation of acnes and quicken the removal of the acnes, and the acne removal capability of the skin care product is better.
According to comparison of data of experimental example 5 and experimental examples 1-3 in table 8, the white fungus extract is added into the essence milk, so that the sebum value reduction value of the skin is further improved, the white fungus extract can improve the moisture retention capacity of the skin to a certain extent, and thus the skin is helped to regulate water and oil balance, and the skin is helped to remove pox, and similarly, the data of experimental example 19 and experimental examples 15-17 in tables 9 and 10, and the data of experimental example 33 and experimental examples 29-31 prove that the effect of the white fungus extract added into the skin care product is similar to that of the white fungus extract added into the essence milk.
According to the comparison of the data of the experimental example 6 and the experimental examples 1-3 in the table 8, the cactus extract is added into the essence milk, so that the sebum value reduction value of the skin is further improved, the cactus extract can improve the water replenishing and moisturizing capability of the product to a certain extent, the oil control capability of the skin is improved, the oil discharge in the skin is reduced, and the skin can be helped to dispel acnes, and similarly, the data of the experimental example 20 and the experimental examples 15-17 in the tables 9 and 10, and the data of the experimental example 34 and the experimental examples 29-31 prove that the cactus extract is similar to the effect of being added into the smoothing toner and the facial cream, so that the effect of being added into the skin care product is similar to the effect of being added into the essence milk.
The specific experimental examples are only for explaining the present application and are not limiting to the present application, and those skilled in the art can make modifications without inventive contribution to the experimental examples as required after reading the present specification, but all of them are protected by patent laws within the scope of the claims of the present application.
Claims (10)
1. The acne-removing and oil-controlling composition is characterized by comprising the following components in parts by mass:
10-15 parts of cascara spicata bark extract;
12-20 parts of a Chinese alangium leaf extract;
100 parts of tea extract.
2. The composition for removing acne and controlling oil according to claim 1, which is characterized in that: the paint comprises the following components in parts by mass:
11-13 parts of cascara spicata bark extract;
14-18 parts of a Chinese alangium leaf extract;
100 parts of tea extract.
3. The composition for removing acne and controlling oil according to claim 1, which is characterized in that: the acne-removing and oil-controlling composition also comprises the following components in parts by weight:
5-10 parts of chlorella aureocauda extract.
4. The composition for removing acne and controlling oil according to claim 1, which is characterized in that: the acne-removing and oil-controlling composition also comprises the following components in parts by weight:
13-15 parts of tremella extract.
5. The composition for removing acne and controlling oil according to claim 1, which is characterized in that: the acne-removing and oil-controlling composition also comprises the following components in parts by weight:
11-13 parts of cactus extract.
6. The preparation method of the acne-removing and oil-controlling composition is characterized by comprising the following steps: the method comprises the following steps:
mixing the cascara sagrada bark extract, the Amur bushy leaf extract and the tea leaf extract, and uniformly stirring to obtain the acne-removing and oil-controlling composition.
7. A method of preparing a moisturizing and skin barrier maintenance composition according to claim 6, characterized in that: mixing the cascara Periplaneta bark extract, the folium Ilicis Purpureae extract and the tea extract, adding the Micrococcus Microphyllum extract, the tremella extract and the cactus extract, and stirring uniformly to obtain the acne-removing and oil-controlling composition.
8. The application of the acne-removing and oil-controlling composition is characterized in that: the acne-removing and oil-controlling composition is added into a skin care product.
9. Use of the composition for removing acne and controlling oil according to claim 8, characterized in that: the skin care product comprises smoothing toner, essence milk, essence liquid, cream, emulsion, cream and facial mask.
10. Use of the composition for removing acne and controlling oil according to claim 8, characterized in that: the acne removing and oil controlling composition accounts for 1-3% of the skin care product by weight.
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| CN114948844A (en) * | 2022-06-13 | 2022-08-30 | 广州多多化妆品有限公司 | Sulphur-light illusion eye shadow |
| CN117045578A (en) * | 2023-09-12 | 2023-11-14 | 广东科盈科技有限公司 | Acne-removing and oil-controlling composition containing motor Gastrodia elata extract and application thereof |
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