CN110613672A - Face-refreshing and skin-brightening mask composition, mask and preparation method - Google Patents
Face-refreshing and skin-brightening mask composition, mask and preparation method Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention particularly relates to a face-refreshing and skin-brightening mask composition which comprises water, water-phase auxiliary materials and plant extracts, wherein the plant extracts at least comprise an hedera helix leaf/stem extract, a common magnolia bark, a polygonum cuspidatum root extract, pomegranate juice, a helichrysum arenarium extract, a laminaria cuneata extract, a rye seed extract, a tropaeolum majus extract and a folium orthosiphoni extract. The face-refreshing and skin-brightening mask composition can effectively improve the condition that the skin is yellow and dull, and achieves the effect of face-refreshing and skin-brightening. The invention also relates to a preparation method of the whitening and skin-brightening mask composition and a mask containing the whitening and skin-brightening mask composition.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a face-brightening mask composition, a mask and a preparation method.
Background
The facial mask is a category of skin care products, is a carrier of the skin care products, and is applied on the face for beautifying functions such as moisturizing, whitening, anti-aging, grease balancing and the like. The principle of the facial mask is that the facial mask is covered on the face for a short time, so that outside air and pollution are temporarily isolated, the skin temperature is increased, pores of the skin are expanded, sweat gland secretion and metabolism are promoted, the oxygen content of the skin is increased, products of epidermal cell metabolism and accumulated grease substances are favorably removed from the skin, water in the facial mask permeates into the horny layer of the epidermis, the skin becomes soft, and the skin is naturally bright and elastic.
Although the existing facial masks and other products can play a certain role in resisting oxidation and aging, the existing products have certain irritation to the skin after long-term use because the active ingredients are mostly chemical synthetic substances, and the existing facial masks generally can only simply supplement water and retain water, and have poor effects on improving yellow and dull skin.
The present invention has been made in view of the above circumstances.
Disclosure of Invention
In order to solve the technical problem that the prior art cannot provide a mask capable of effectively brightening the skin and achieving the effect of skin rejuvenation, a skin rejuvenation and brightening mask composition, a mask and a preparation method are provided.
The first purpose of the invention is to provide a face-brightening mask composition.
A skin-refreshing and brightening mask composition comprises water, water-phase auxiliary materials and plant extracts, wherein the plant extracts at least comprise an evergreen vine leaf/stem extract, a common magnolia bark, a giant knotweed rhizome extract, pomegranate fruit juice, a helichrysum arenarium extract, a laminaria cuneata extract, a rye seed extract, a tropaeolum majus extract and a clerodendranthus spicatus extract.
Active ingredients of MAGNOLIA cuspidata (magnoli ACUMINATA) bark extract include magnolol, dihydroxydihydromagnolol, magnolol, and dihydromagnolol, which can reduce blood flow near the skin surface in a variety of ways, e.g., vasoconstriction, inhibition of internal or surface angiogenesis, endothelial cell migration, etc. It can improve or eliminate the skin problems of spider veins (i.e. telangiectasia or varicose veins facing the sun) such as blue or purple clusters of veins, dark circles around the eyes and puffy eyes. In addition, the product can also remove fine lines and wrinkles, improve skin elasticity, improve skin firmness and make skin color and luster uniform.
As an embodiment, the magnolia sharonensis bark extract can be prepared by the following method:
a) crushing bark of common magnolia with sharp tips, putting the crushed bark into a solvent, heating the mixture to 30-50 ℃, preserving heat, soaking, filtering, ultrafiltering, and concentrating under reduced pressure to obtain an extract, wherein the solvent is obtained by mixing ethanol and water according to a volume ratio of 1: 15-1;
b) dissolving the extract obtained in the step a) by using ethanol, adsorbing the extract to saturation through a small-pore resin column, washing the small-pore resin column by using water until an effluent liquid is clear, and then eluting the column by using ethanol until the effluent liquid is colorless to obtain an eluent;
c) carrying out reduced pressure rotary distillation concentration on the eluent obtained in the step b) at the temperature of 30-50 ℃ until the solvent is not distilled out any more and the remaining liquid is thick paste to obtain the bark extract of the magnolia sharsii.
The preparation method can be used for obtaining more magnolol, dihydroxy dihydromagnolol, magnolol, dihydromagnolol and other active ingredients, has stable performance, can effectively improve the condition of skin, and can better achieve the effects of firming skin and brightening skin.
As an embodiment, the pomegranate juice can be prepared as follows:
a. selecting fresh pomegranate with smooth skin and tight flesh, crushing the whole pomegranate fruit, and separating pulp from juice;
b. performing ultrasonic treatment for 50-120 minutes at the water temperature of 0-10 ℃, then passing through a macroporous adsorption resin column, washing the resin column with deionized water, and collecting a first effluent;
c. passing the first effluent through a neutral aluminum column, washing with deionized water, and collecting a second effluent;
d. and concentrating the obtained second effluent under reduced pressure to obtain the pomegranate juice.
The pomegranate juice obtained by the preparation method has high contents of anthocyanin, pomegranate polyphenol, vitamin C and linoleic acid, has a better oxidation effect, and can better supplement skin moisture.
The Helichrysum arenarium flower extract contains abundant flavonoids including quercetin-3-O-beta-D-glucopyranoside (quercetin-3-O-beta-D-glucopyranoside, 1), apigenin-7-D-beta-D-gentiobioside (apigenin 7-O-beta-D-geniobioside, 2), quercetin3-O-rutinoside (quercetin3-O-rutinoside, 3), apigenin-7, 4 '-di-O-glucoside (apigenin-7, 4' -O-beta-D-glucopyranoside-noside, 4), kaempferol-3, 4 '-di-O-glucoside (kaempferol-3, 4' -di-O-beta-D-glucopyranoside, 5) quercetin-3, 3 '-O-diglucose (quercetin-3, 3' -di-O-beta-D-glucopyranoside, 6) and apigenin-7-O-beta-D-glucuronic acid methyl ester (apigenin-7-O-beta-D-glucopyranosiduronic acid methyl ester, 7), and has anti-inflammatory and antioxidant effects.
The Laminaria ochroleuca (LAMINARIA OCHROLEUCA) extract contains lipid cell membrane material with stabilizing effect, special lecithin, alpha oleic acid derivative and vitamins, and is rich in fucoxanthin as photochemical protective agent, and has good antioxidant activity, comprehensive anti-inflammatory, antiaging and sunscreen effects.
The rye (SECALE CEREALE) seed extract is rich in rye arabinoxylan, and can stimulate mechanical and biological functions of fibroblast, significantly improve skin elasticity and tension, and produce durable skin firming effect.
The Tropaeolum maju (Tropaeolum MAJUS) flower extract is extracted from Tropaeolum maju, is rich in polyphenol (p-coumaric acid), can remarkably inhibit the activity of tyrosinase playing a key role in the melanin formation process, reduces the melanin formation, and achieves the effects of inhibiting the melanin formation, preventing color spots and balancing white skin color.
Folium orthosiphoni (Orthosiphon STAMINEUS) extract, also called Orthosiphon aristatus, Orthosiphon aristatus and Java tea, belongs to the genus Orthosiphon of Labiatae, and has strong inhibitory effect on 5-alpha reductase, and can reduce the production of dihydrotestosterone by inhibiting the expression of 5-alpha reductase, thereby reducing the secretion of sebaceous gland oil and achieving the effect of regulating the secretion of oil.
According to the invention, through the mutual synergistic cooperation of the components in the plant extract, the skin quality can be effectively improved, fine wrinkles, eye bags and the like can be removed, the skin can be firmed, and the effects of beautifying and brightening can be achieved.
As an embodiment, the plant extract further includes lavender flower water, ganoderma atrum extract, purslane extract, alpine edelweiss extract, chrysosporium extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract, and snow lotus flower extract.
The lavender floral water has effects of balancing skin oil, killing bacteria, removing scar, promoting cell regeneration, improving pimple, eczema and psoriasis, inhibiting growth of mold, and balancing skin oil. The lavender flower water and other extracts are matched with each other in a synergistic manner, so that a better skin-refreshing and brightening effect can be achieved.
The ganoderma atrum extract is rich in polysaccharide, polypeptide and the like, has obvious effect of delaying senility, can promote and adjust immune function, regulate metabolic balance, promote synthesis of nucleic acid and protein, has the effect of resisting free radicals, promotes DNA synthesis capacity in cell nucleus, can increase division generation of cells and delays senility.
The extract of Leontopodium alpinum can induce the expression of genes related to basement membrane stability, improve the stability of skin structure, and delay aging.
As an embodiment, the peel-brightening mask composition comprises hydrolyzed elastin, lactobacillus/ginseng root fermentation product filtrate.
As an embodiment, the water phase adjuvant comprises butylene glycol, nicotinamide, 1, 2-hexanediol, p-hydroxyacetophenone, polyglycerol-6, glycerol, phenoxyethanol, xanthan gum, allantoin, dipotassium glycyrrhizinate, disodium EDTA, glycerol glucoside, ethylhexyl glycerol, citric acid, sodium benzoate, potassium sorbate, and sodium hyaluronate.
As one embodiment, the peel brightening mask composition comprises the following components:
0.01-20 parts by weight of an ivy leaf/stem extract, 0.01-36 parts by weight of a magnolia sharehanii bark extract, 0.01-30 parts by weight of a polygonum cuspidatum root extract, 0.01-40 parts by weight of pomegranate juice, 0.01-15 parts by weight of an agastache rugosa extract, 0.01-20 parts by weight of a laminaria cuneata extract, 0.01-36 parts by weight of a rye seed extract, 0.01-16 parts by weight of a tropaeolum majus extract and a clerodendranthus spicatus extract, 10-20 parts by weight of lavender water, 0.01-26 parts by weight of a ganoderma atrum extract, 0.01-40 parts by weight of a purslane extract, 0.01-18 parts by weight of a hirsutella alpina extract, 0.01-15 parts by weight of a trufflera alba extract, 0.01-10 parts by weight of a glycyrrhiza glabra root extract, 0.005-10 parts by weight of a nelumbinis extract, 1-36 parts by weight of a hydrolyzed rice extract, 0.002-8 parts by weight of a smallantana flower extract, 0.001-10 parts, 0.001 to 1.6 parts by weight of butylene glycol, 50 to 80 parts by weight of water, 0.002 to 4 parts by weight of nicotinamide, 0.001 to 1.6 parts by weight of 1, 2-hexanediol, 0.001 to 1 part by weight of p-hydroxyacetophenone, 60.001 to 0.6 parts by weight of polyglycerol, 0.001 to 1.5 parts by weight of glycerol, 0.001 to 0.8 parts by weight of phenoxyethanol, 0.02 to 2 parts by weight of xanthan gum, 0.001 to 2.5 parts by weight of allantoin, 0.001 to 0.1 part by weight of dipotassium glycyrrhizinate, 0.001 to 0.5 part by weight of disodium EDTA, 0.001 to 0.8 part by weight of glycerol glucoside, 0.001 to 1 part by weight of ethylhexylglycerol, 0.001 to 0.5 part by weight of citric acid, 0.001 to 0.7 part by weight of sodium benzoate, 0.001 to 0.5 part by weight of potassium sorbate, and 0.004 to 1.5 parts by weight of sodium hyaluronate.
Further preferably, the peel brightening mask composition comprises the following components:
0.01-8 parts by weight of an ivy leaf/stem extract, 0.01-16 parts by weight of a common magnolia bark extract, 0.01-12 parts by weight of a giant knotweed root extract, 0.01-15 parts by weight of pomegranate juice, 0.2-10 parts by weight of an ashmeadow extract, 0.05-8 parts by weight of a laminaria key-flower extract, 1-10 parts by weight of a rye seed extract, 0.6-10 parts by weight of a tropaeolum extract and a clerodendranthus spicatus extract, 45-80 parts by weight of lavender water, 0.04-12 parts by weight of a ganoderma atrum extract, 0.03-20 parts by weight of a purslane extract, 0.01-10 parts by weight of a hirsutella alpina extract, 0.06-9 parts by weight of a trufflera alba extract, 0.6-7 parts by weight of a glycyrrhiza glabra root extract, 0.5-6 parts by weight of a lotus seed extract, 5-16 parts by weight of a hydrolyzed rice extract, 0.2-3 parts by weight of a smallanthus extract, 1-10 parts by weight of hydrolyzed elastin, 0.01-7 parts, 0.001 to 0.8 part by weight of butanediol, 14 to 16 parts by weight of water, 0.02 to 2.2 parts by weight of nicotinamide, 0.004 to 1 part by weight of 1, 2-hexanediol, 0.01 to 0.6 part by weight of p-hydroxyacetophenone, 60.01 to 0.4 part by weight of polyglycerol, 0.05 to 1 part by weight of glycerol, 0.001 to 0.5 part by weight of phenoxyethanol, 0.1 to 2 parts by weight of xanthan gum, 0.2 to 2.5 parts by weight of allantoin, 0.02 to 0.1 part by weight of dipotassium glycyrrhizinate, 0.01 to 0.3 part by weight of disodium EDTA, 0.05 to 0.5 part by weight of glycerol glucoside, 0.01 to 0.6 part by weight of ethylhexylglycerol, 0.05 to 0.2 part by weight of citric acid, 0.01 to 0.3 part by weight of sodium benzoate, 0.08 to 0.5 part by weight of potassium sorbate, and 0.4 to 1.5 part by weight of sodium hyaluronate.
The components are combined according to the proportion for use, so that a better synergistic effect is achieved, the obtained face-brightening mask composition can better improve various problems of the facial skin, which influence the skin quality and the appearance, and a better face-brightening effect is achieved, and the lavender flower water is adopted as an effective component, plays a role of a solvent, and has a synergistic effect with other plant extracts, so that the face-brightening effect is achieved.
The second objective of the present invention is to provide a preparation method of a skin-brightening mask composition, which comprises the following steps:
s1, mixing water and the water-phase auxiliary material in a nitrogen atmosphere, and heating until the water-phase auxiliary material is completely dissolved to obtain a mixed solution A;
s2, cooling the mixed solution A to 5-10 ℃ under a nitrogen atmosphere, adding plant extracts into the mixed solution A, wherein the plant extracts at least comprise a hedera helix leaf/stem extract, a common magnolia bark, a polygonum cuspidatum root extract, pomegranate juice, a helichrysum arenarium extract, a laminaria cuneata extract, a rye seed extract, a tropaeolum majus extract and a clerodendranthus spicatus extract, and uniformly mixing to obtain a mixed solution B;
s3, cooling the mixed solution B to 10-25 ℃ under nitrogen atmosphere, adding hydrolyzed elastin and lactobacillus/ginseng root fermentation product filtrate, and uniformly mixing to obtain mixed solution C;
and S4, cooling and discharging to obtain the product.
As an embodiment, in step S2, the plant extracts further include lavender flower water, ganoderma atrum extract, purslane extract, alpine edelweiss extract, truffle extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract, and snow lotus flower extract.
As a preferred embodiment, the water phase auxiliary material comprises butanediol, nicotinamide, 1, 2-hexanediol, p-hydroxyacetophenone, polyglycerol-6, glycerol, phenoxyethanol, xanthan gum, allantoin, dipotassium glycyrrhizinate, disodium EDTA, glycerol glucoside, ethylhexyl glycerol, citric acid, sodium benzoate, potassium sorbate and sodium hyaluronate.
The third objective of the present invention is to provide a skin brightening mask, which comprises the skin brightening mask composition as described in any one of the above.
Compared with the prior art, the invention has the following beneficial effects:
the plant extracts of the face-refreshing and skin-brightening mask composition at least contain a plurality of plant functional components such as hedera helix leaf/stem extract, cornia acuminate bark, polygonum cuspidatum root extract, pomegranate fruit juice, helichrysum arenarium extract, laminaria cuneata extract, rye seed extract, tropaeolum majus extract, clerodendranthus spicatus extract and the like, and the face-refreshing and skin-brightening mask composition is rich and high in content of nutrient substances, can obviously improve the yellow and dark skin condition and achieves the effect of face-refreshing and skin-brightening.
The preparation method of the face-refreshing and skin-brightening mask composition is simple in process and convenient for realizing industrialization.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
Example 1
(1) The components of the skin brightening mask composition are as follows:
0.01kg of hedera helix leaf/stem extract, 36kg of common tulip bark extract, 0.01kg of giant knotweed rhizome root extract, 0.01kg of pomegranate juice, 15kg of helichrysum arenarium extract, 0.01kg of laminaria cuneata extract, 36kg of rye seed extract, 0.01kg of tropaeolum majus extract and clerodendrum spicatum extract, 20kg of lavender flower water, 0.01kg of ganoderma atrum extract, 0.01kg of purslane extract, 0.01kg of alpine edelweiss extract, 0.01kg of trufflera cordifolia extract, 0.01kg of glycyrrhiza glabra root extract, 0.005kg of lotus seed extract, 36kg of hydrolyzed rice extract, 0.002kg of snow lotus extract, 10kg of hydrolyzed elastin, 0.01kg of lactobacillus/ginseng root fermentation product filtrate, 0.001kg of butanediol, 10kg of water, 0.002kg of nicotinamide, 0.001kg of 1, 2-hexanediol, 0.001kg of p-hydroxyacetophenone, 0.001kg of polyglycerol-60.001 kg, 0.001kg of phenoxyethanol, 0.02kg of xanthan gum, 0.001kg of allantoin, 0.001kg of dipotassium glycyrrhizinate, 0.5kg of EDTA disodium, 0.8kg of glycerol glucoside, 0.001kg of ethylhexyl glycerol, 0.5kg of citric acid, 0.001kg of sodium benzoate, 0.5kg of potassium sorbate and 1.5kg of sodium hyaluronate.
The preparation method of the face-brightening mask composition comprises the following steps:
the method comprises the following steps:
s1, mixing water and the water-phase auxiliary material in a nitrogen atmosphere, and heating until the water-phase auxiliary material is completely dissolved to obtain a mixed solution A;
s2, cooling the mixed solution A to 5-10 ℃ under a nitrogen atmosphere, adding the plant extracts at least comprising an ivy leaf/stem extract, an acuminate magnolia bark, a polygonum cuspidatum root extract, pomegranate juice, a helichrysum arenarium extract, a laminaria cuneata extract, a rye seed extract, a tropaeolum majus extract, a clerodendranthus spicatus extract, a lavender flower water, a ganoderma atrum extract, a purslane extract, a leontopodium alpinum extract, a trufflera alboloris extract, a glycyrrhiza glabra root extract, a lotus seed extract, a hydrolyzed rice extract and a snow lotus flower extract into the mixed solution A, and uniformly mixing to obtain a mixed solution B;
s3, cooling the mixed solution B to 10-25 ℃ under nitrogen atmosphere, adding hydrolyzed elastin and lactobacillus/ginseng root fermentation product filtrate, and uniformly mixing to obtain mixed solution C;
s4, cooling, sampling, detecting bacteria and fungi to meet the requirements, and discharging to obtain the skin brightening mask composition.
The obtained skin brightening mask composition is injected into a film substrate of the fiber mask through a filling machine and is uniformly distributed, so that the skin brightening mask is obtained.
Example 2
The components of the skin whitening mask composition of this example are as follows:
20kg of hedera helix leaf/stem extract, 36kg of common tulip bark extract, 30kg of giant knotweed rhizome extract, 0.01kg of pomegranate juice, 15kg of helichrysum arenarium extract, 20kg of laminaria cuneata extract, 0.01kg of rye seed extract, 16kg of tropaeolum majus extract and clerodendranthus spicatus extract, 80kg of lavender flower water, 26kg of ganoderma atrum extract, 40kg of purslane extract, 18kg of alpine edelweiss extract, 15kg of chrysosporium extract, 10kg of glabrous greenbrier rhizome extract, 10kg of lotus seed extract, 36kg of hydrolyzed rice extract, 8kg of snow lotus flower extract, 0.001kg of hydrolyzed elastin, 10kg of lactobacillus/ginseng root fermentation product filtrate, 1.6kg of butanediol, 140kg of water, 4kg of nicotinamide, 0.001kg of 1, 2-hexanediol, 1kg of p-hydroxyacetophenone, polyglycerol-60.6 kg, 1.5kg, 0.8kg of ethanol, 2kg of xanthan gum, 2.5kg of allantoin, 0.1kg of dipotassium glycyrrhizinate, 0.001kg of EDTA disodium, 0.001kg of glycerol glucoside, 1kg of ethylhexyl glycerol, 0.001kg of citric acid, 0.7kg of sodium benzoate, 0.001kg of potassium sorbate and 0.004kg of sodium hyaluronate.
See example 1 for a method of making the peel lightening mask composition.
Example 3
The components of the skin whitening mask composition of this example are as follows:
8kg of hedera helix leaf/stem extract, 16kg of common tulip bark extract, 12kg of giant knotweed rhizome extract, 15kg of pomegranate juice, 10kg of helichrysum arenarium extract, 8kg of laminaria cuneata extract, 10kg of rye seed extract, 10kg of tropaeolum extract and clerodendranthus spicatus extract, 65kg of lavender water, 12kg of ganoderma atrum extract, 20kg of purslane extract, 10kg of alpine edelweiss extract, 9kg of chrysosporium bungei extract, 7kg of glycyrrhiza glabra root extract, 6kg of lotus seed extract, 5kg of hydrolyzed rice extract, 3kg of snow lotus extract, 8kg of hydrolyzed elastin, 5kg of lactobacillus/ginseng root fermentation product filtrate, 0.8kg of butanediol, 15kg of water, 0.02kg of nicotinamide, 1kg of 1, 2-hexanediol, 0.6kg of p-hydroxyacetophenone, 60.4 kg of polyglycerol, 0.05kg, 0.5kg of phenoxyethanol, 0.1kg of xanthan gum, 0.2kg of allantoin, 0.05kg of dipotassium glycyrrhizinate, 0.3kg of EDTA disodium, 0.2kg of glycerol glucoside, 0.6kg of ethylhexyl glycerol, 0.2kg of citric acid, 0.3kg of sodium benzoate, 0.5kg of potassium sorbate and 0.4kg of sodium hyaluronate.
See example 1 for a method of making the peel lightening mask composition.
Example 4
The components of the skin whitening mask composition of this example are as follows:
3kg of hedera helix leaf/stem extract, 7kg of common tulip bark extract, 10kg of giant knotweed rhizome extract, 9kg of pomegranate juice, 2kg of helichrysum arenarium extract, 1kg of laminaria cuneata extract, 3kg of rye seed extract, 3.5kg of tropaeolum majus extract and clerodendranthus spicatus extract, 45kg of lavender flower water, 1kg of ganoderma atrum extract, 6kg of purslane extract, 1.6kg of alpine edelweiss extract, 1.5kg of chrysosporium extract, 2.5kg of glabrous root extract, 4kg of lotus seed extract, 12kg of hydrolyzed rice extract, 0.9kg of snow lotus extract, 5kg of hydrolyzed elastin, 0.5kg of lactobacillus/ginseng root fermentation product filtrate, 0.5kg of butanediol, 16kg of water, 1.2kg of nicotinamide, 0.3 part of 1, 2-hexanediol, 0.1kg of p-hydroxy-hydroxybenzene, 60.2kg of polyglycerol-60.35 kg, 0.35kg of glycerol, 0.1kg of phenoxyethanol, 0.6kg of xanthan gum, 1.8kg of allantoin, 0.1kg of dipotassium glycyrrhizinate, 0.2kg of EDTA disodium, 0.5kg of glycerol glucoside, 0.08kg of ethylhexyl glycerol, 0.1kg of citric acid, 0.03kg of sodium benzoate, 0.08kg of potassium sorbate and 0.9kg of sodium hyaluronate.
See example 1 for a method of making the peel lightening mask composition.
Example 5
The components of the skin whitening mask composition of this example are the same as those of example 1, except that the magnolia bark extract and pomegranate juice are prepared as follows.
Wherein, the magnolia sharplensis bark extract is obtained by the following preparation method:
a) crushing bark of magnolia shariifolia, putting the crushed bark into a solvent, heating the mixture to 30 ℃, preserving heat, soaking, filtering, ultrafiltering, and concentrating under reduced pressure to obtain an extract, wherein the solvent is obtained by mixing ethanol and water according to a volume ratio of 1: 15;
b) dissolving the extract obtained in the step a) by using ethanol, adsorbing the extract to saturation through a small-pore resin column, washing the small-pore resin column by using water until an effluent liquid is clear, and then eluting the column by using ethanol until the effluent liquid is colorless to obtain an eluent;
c) concentrating the eluate obtained in step b) by rotary distillation under reduced pressure at 45 deg.C until the solvent is not evaporated and the remaining liquid is thick paste to obtain cortex Magnoliae officinalis extract.
The pomegranate juice is prepared by the following preparation method:
a. selecting fresh pomegranate with smooth skin and tight flesh, crushing the whole pomegranate fruit, and separating pulp from juice;
b. performing ultrasonic treatment for 120 minutes at the water temperature of 10 ℃, then passing through a macroporous adsorption resin column, washing the resin column with deionized water, and collecting a first effluent;
c. passing the first effluent through a neutral aluminum column, washing with deionized water, and collecting a second effluent;
d. and concentrating the obtained second effluent under reduced pressure to obtain the pomegranate juice.
See example 1 for a method of making the peel lightening mask composition.
Example 6
The components of the skin whitening mask composition of this example are the same as those of example 2, except that the magnolia bark extract and pomegranate juice are prepared as follows.
Wherein, the magnolia sharplensis bark extract is obtained by the following preparation method:
a) crushing bark of magnolia shariifolia, putting the crushed bark into a solvent, heating the mixture to 45 ℃, preserving heat, soaking, filtering, ultrafiltering, and concentrating under reduced pressure to obtain an extract, wherein the solvent is obtained by mixing ethanol and water according to a volume ratio of 1: 7;
b) dissolving the extract obtained in the step a) by using ethanol, adsorbing the extract to saturation through a small-pore resin column, washing the small-pore resin column by using water until an effluent liquid is clear, and then eluting the column by using ethanol until the effluent liquid is colorless to obtain an eluent;
c) concentrating the eluate obtained in step b) by rotary distillation under reduced pressure at 50 deg.C until the solvent is not evaporated and the remaining liquid is thick paste to obtain cortex Magnoliae officinalis extract.
The pomegranate juice is prepared by the following preparation method:
a. selecting fresh pomegranate with smooth skin and tight flesh, crushing the whole pomegranate fruit, and separating pulp from juice;
b. performing ultrasonic treatment for 120 minutes at the water temperature of 0 ℃, then passing through a macroporous adsorption resin column, washing the resin column with deionized water, and collecting a first effluent;
c. passing the first effluent through a neutral aluminum column, washing with deionized water, and collecting a second effluent;
d. and concentrating the obtained second effluent under reduced pressure to obtain the pomegranate juice.
See example 1 for a method of making the peel lightening mask composition.
Example 7
The components of the skin whitening mask composition of this example are the same as those of example 3, except that the magnolia bark extract and pomegranate juice are prepared as follows.
Wherein, the magnolia sharplensis bark extract is obtained by the following preparation method:
a) crushing bark of magnolia shariifolia, putting the crushed bark into a solvent, heating the mixture to 40 ℃, preserving heat, soaking, filtering, ultrafiltering, and concentrating under reduced pressure to obtain an extract, wherein the solvent is obtained by mixing ethanol and water according to a volume ratio of 1: 1;
b) dissolving the extract obtained in the step a) by using ethanol, adsorbing the extract to saturation through a small-pore resin column, washing the small-pore resin column by using water until an effluent liquid is clear, and then eluting the column by using ethanol until the effluent liquid is colorless to obtain an eluent;
c) concentrating the eluate obtained in step b) by rotary distillation under reduced pressure at 38 deg.C until the solvent is not evaporated and the remaining liquid is thick paste to obtain cortex Magnoliae officinalis extract.
The pomegranate juice is prepared by the following preparation method:
a. selecting fresh pomegranate with smooth skin and tight flesh, crushing the whole pomegranate fruit, and separating pulp from juice;
b. performing ultrasonic treatment for 100 minutes at the water temperature of 7 ℃, then passing through a macroporous adsorption resin column, washing the resin column with deionized water, and collecting a first effluent;
c. passing the first effluent through a neutral aluminum column, washing with deionized water, and collecting a second effluent;
d. and concentrating the obtained second effluent under reduced pressure to obtain the pomegranate juice.
See example 1 for a method of making the peel lightening mask composition.
Example 8
The components of the skin whitening mask composition of this example are the same as those of example 4, except that the magnolia bark extract and pomegranate juice are prepared as follows.
Wherein, the magnolia sharplensis bark extract is obtained by the following preparation method:
a) crushing bark of magnolia shariifolia, putting the crushed bark into a solvent, heating the mixture to 35 ℃, preserving heat, soaking, filtering, ultrafiltering, and concentrating under reduced pressure to obtain an extract, wherein the solvent is obtained by mixing ethanol and water according to a volume ratio of 1: 9;
b) dissolving the extract obtained in the step a) by using ethanol, adsorbing the extract to saturation through a small-pore resin column, washing the small-pore resin column by using water until an effluent liquid is clear, and then eluting the column by using ethanol until the effluent liquid is colorless to obtain an eluent;
c) concentrating the eluate obtained in step b) by rotary distillation under reduced pressure at 50 deg.C until the solvent is not evaporated and the remaining liquid is thick paste to obtain cortex Magnoliae officinalis extract.
The pomegranate juice is prepared by the following preparation method:
a. selecting fresh pomegranate with smooth skin and tight flesh, crushing the whole pomegranate fruit, and separating pulp from juice;
b. performing ultrasonic treatment for 50 minutes at the water temperature of 5 ℃, then passing through a macroporous adsorption resin column, washing the resin column with deionized water, and collecting a first effluent;
c. passing the first effluent through a neutral aluminum column, washing with deionized water, and collecting a second effluent;
d. and concentrating the obtained second effluent under reduced pressure to obtain the pomegranate juice.
See example 1 for a method of making the peel lightening mask composition.
Comparative example 1
Referring to example 2, hydrolyzed elastin and lactobacillus/ginseng root fermentation product filtrate were removed from the whitening mask composition of this comparative example, the other components in the whitening mask composition were kept consistent, and the whitening mask composition and the mask were prepared in the same manner.
Comparative example 2
Referring to example 2 above, the whitening and skin-lightening mask composition of this comparative example removed hydrolyzed elastin, lactobacillus/ginseng root fermentation product filtrate, and lavender flower water, ganoderma atrum extract, purslane extract, edelweiss extract, leucotrichum extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract, and snow lotus extract. The other components in the rejuvenation and skin-brightening mask composition are kept consistent, and the rejuvenation and skin-brightening mask composition and the mask have the same preparation method.
Test example 1
And (3) testing a product: the masks obtained in examples 1 to 8 of the present invention and comparative examples 1 to 2.
Subject: the population with yellow, dull and lusterless skin was divided for each example into corresponding observation groups of 50 people in each group.
The test method comprises the following steps:
the test subjects in each observation group respectively take 1 piece of the facial mask corresponding to the embodiment, the left face side is cut off and is attached to the right face for 15-30 min (in the time range, the use time of each test subject is ensured to be the same), the left face is not attached or a blank control experiment is carried out, and the control effect of the skin conditions of the left face and the right face of the test subject is observed by naked eyes so as to evaluate the use effect. The test results are shown in table 1 below, using 1 time per day for 1 month.
TABLE 1
The test results show that the face-brightening and skin-brightening mask comprises the extracts of the leaf/stem extract of hedera helix, the bark of common magnolia, the root extract of polygonum cuspidatum, pomegranate juice, the extract of helichrysum arenarium, the extract of laminaria cuneata, the extract of rye seed, the extract of tropaeolum majus, the extract of clerodendranthus spicatus and the like, can effectively improve dark and yellow skin, and achieves a better face-brightening and skin-brightening effect.
Comparative example 1 and comparative example 2 are also embodiments of the present invention, but comparative example 1 and example 2 have relatively reduced effects without adding hydrolyzed elastin, lactobacillus/ginseng root fermentation product filtrate. Comparative example 2 compared to example 2, the effect was relatively reduced compared to example 2 and comparative example 1 without the addition of hydrolyzed elastin, lactobacillus/ginseng root fermentation product filtrate, and lavender flower water, ganoderma atrum extract, purslane extract, alpine edelweiss extract, truffle extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract, and snow lotus flower extract. Therefore, when the mask composition in the mask further comprises lavender flower water, ganoderma atrum extract, purslane extract, alpine edelweiss extract, white truffle extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract and snow lotus herb extract, the skin brightening and rejuvenating effects are better. Furthermore, when the hydrolyzed elastin and the lactobacillus/ginseng root fermentation product filtrate are included, the skin brightening and rejuvenating effect is further improved.
In addition, the four embodiments of examples 5 to 8 have compositions corresponding to those of examples 1 to 4, respectively, and are different only in that the preparation method of the magnolia bark extract and the preparation method of pomegranate juice according to the present invention are adopted, and when the obtained magnolia bark extract and pomegranate juice are used in the skin rejuvenation and brightening mask composition, relatively superior skin improvement effects are achieved.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (10)
1. A face-brightening mask composition comprises water, water-phase auxiliary materials and plant extracts, and is characterized in that the plant extracts at least comprise an evergreen vine leaf/stem extract, a common aucklandia bark, a giant knotweed root extract, pomegranate fruit juice, a helichrysum arenarium extract, a laminaria cuneata extract, a rye seed extract, a tropaeolum extract and a clerodendrum spicatum extract.
2. The peel-brightening mask composition of claim 1, wherein the plant extracts further comprise lavender floral water, ganoderma atrum extract, purslane extract, alpine edelweiss extract, white truffle extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract, and snow lotus extract.
3. The peel skin lightening mask composition of claim 1 or 2, further comprising hydrolyzed elastin, lactobacillus/ginseng root fermentation product filtrate.
4. The rejuvenating and skin lightening mask composition as claimed in claim 3 wherein the water phase excipients comprise butylene glycol, niacinamide, 1, 2-hexanediol, p-hydroxyacetophenone, polyglyceryl-6, glycerin, phenoxyethanol, xanthan gum, allantoin, dipotassium glycyrrhizinate, disodium EDTA, glyceryl glucoside, ethylhexylglycerin, citric acid, sodium benzoate, potassium sorbate, sodium hyaluronate.
5. The peel skin lightening mask composition of claim 4, wherein the mask composition comprises the following ingredients:
0.01-20 parts by weight of an ivy leaf/stem extract, 0.01-36 parts by weight of a magnolia sharehanii bark extract, 0.01-30 parts by weight of a polygonum cuspidatum root extract, 0.01-40 parts by weight of pomegranate juice, 0.01-15 parts by weight of an agastache rugosa extract, 0.01-20 parts by weight of a laminaria cuneata extract, 0.01-36 parts by weight of a rye seed extract, 0.01-16 parts by weight of a tropaeolum majus extract and a clerodendranthus spicatus extract, 20-80 parts by weight of lavender water, 0.01-26 parts by weight of a ganoderma atrum extract, 0.01-40 parts by weight of a purslane extract, 0.01-18 parts by weight of a hirsutella alpina extract, 0.01-15 parts by weight of a trufflera alba extract, 0.01-10 parts by weight of a glycyrrhiza glabra root extract, 0.005-10 parts by weight of a nelumbinis extract, 1-36 parts by weight of a hydrolyzed rice extract, 0.002-8 parts by weight of a smallantana flower extract, 0.001-10 parts, 0.001 to 1.6 parts by weight of butanediol, 10 to 20 parts by weight of water, 0.002 to 4 parts by weight of nicotinamide, 0.001 to 1.6 parts by weight of 1, 2-hexanediol, 0.001 to 1 part by weight of p-hydroxyacetophenone, 60.001 to 0.6 parts by weight of polyglycerol, 0.001 to 1.5 parts by weight of glycerol, 0.001 to 0.8 parts by weight of phenoxyethanol, 0.02 to 2 parts by weight of xanthan gum, 0.001 to 2.5 parts by weight of allantoin, 0.001 to 0.1 part by weight of dipotassium glycyrrhizinate, 0.001 to 0.5 part by weight of disodium EDTA, 0.001 to 0.8 part by weight of glycerol glucoside, 0.001 to 1 part by weight of ethylhexylglycerol, 0.001 to 0.5 part by weight of citric acid, 0.001 to 0.7 part by weight of sodium benzoate, 0.001 to 0.5 part by weight of potassium sorbate, and 0.004 to 1.5 parts by weight of sodium hyaluronate.
6. The peel skin lightening mask composition of claim 5, wherein the mask composition comprises the following ingredients:
0.01-8 parts by weight of an ivy leaf/stem extract, 0.01-16 parts by weight of a common magnolia bark extract, 0.01-12 parts by weight of a giant knotweed root extract, 0.01-15 parts by weight of pomegranate juice, 0.2-10 parts by weight of an ashmeadow extract, 0.05-8 parts by weight of a laminaria key-flower extract, 1-10 parts by weight of a rye seed extract, 0.6-10 parts by weight of a tropaeolum extract and a clerodendranthus spicatus extract, 45-80 parts by weight of lavender water, 0.04-12 parts by weight of a ganoderma atrum extract, 0.03-20 parts by weight of a purslane extract, 0.01-10 parts by weight of a hirsutella alpina extract, 0.06-9 parts by weight of a trufflera alba extract, 0.6-7 parts by weight of a glycyrrhiza glabra root extract, 0.5-6 parts by weight of a lotus seed extract, 5-16 parts by weight of a hydrolyzed rice extract, 0.2-3 parts by weight of a smallanthus extract, 1-10 parts by weight of hydrolyzed elastin, 0.01-7 parts, 0.001 to 0.8 part by weight of butanediol, 14 to 16 parts by weight of water, 0.02 to 2.2 parts by weight of nicotinamide, 0.004 to 1 part by weight of 1, 2-hexanediol, 0.01 to 0.6 part by weight of p-hydroxyacetophenone, 60.01 to 0.4 part by weight of polyglycerol, 0.05 to 1 part by weight of glycerol, 0.001 to 0.5 part by weight of phenoxyethanol, 0.1 to 2 parts by weight of xanthan gum, 0.2 to 2.5 parts by weight of allantoin, 0.02 to 0.1 part by weight of dipotassium glycyrrhizinate, 0.01 to 0.3 part by weight of disodium EDTA, 0.05 to 0.5 part by weight of glycerol glucoside, 0.01 to 0.6 part by weight of ethylhexylglycerol, 0.05 to 0.2 part by weight of citric acid, 0.01 to 0.3 part by weight of sodium benzoate, 0.08 to 0.5 part by weight of potassium sorbate, and 0.4 to 1.5 part by weight of sodium hyaluronate.
7. The preparation method of the face-brightening mask composition is characterized by comprising the following steps:
s1, mixing water and the water-phase auxiliary material in a nitrogen atmosphere, and heating until the water-phase auxiliary material is completely dissolved to obtain a mixed solution A;
s2, cooling the mixed solution A to 5-10 ℃ under a nitrogen atmosphere, adding plant extracts into the mixed solution A, wherein the plant extracts at least comprise an hedera helix leaf/stem extract, an acuminate magnolia bark extract, a polygonum cuspidatum root extract, pomegranate juice, a helichrysum arenarium extract, a laminaria cuneata extract, a rye seed extract, a tropaeolum majus extract and a clerodendranthus spicatus extract, and uniformly mixing to obtain a mixed solution B;
s3, adding hydrolyzed elastin and lactobacillus/ginseng root fermentation product filtrate when the temperature of the mixed solution B is reduced to 10-25 ℃ under nitrogen atmosphere, and uniformly mixing to obtain a mixed solution C;
and S4, cooling and discharging to obtain the product.
8. The method of preparing the face-brightening mask composition of claim 7, wherein in step S2, the plant extracts further comprise lavender flower water, ganoderma atrum extract, purslane extract, alpine edelweiss extract, white truffle extract, glycyrrhiza glabra root extract, lotus seed extract, hydrolyzed rice extract, and snow lotus extract.
9. The method of preparing a skin rejuvenating and brightening mask composition as claimed in claim 8, wherein said aqueous phase adjuvant comprises butylene glycol, niacinamide, 1, 2-hexanediol, p-hydroxyacetophenone, polyglycerin-6, glycerin, phenoxyethanol, xanthan gum, allantoin, dipotassium glycyrrhizinate, disodium EDTA, glycerol glucoside, ethylhexylglycerin, citric acid, sodium benzoate, potassium sorbate, sodium hyaluronate.
10. A peel skin lightening mask comprising the peel skin lightening mask composition of any one of claims 1 to 6.
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| CN115068387B (en) * | 2022-07-11 | 2024-04-26 | 润芳可(上海)生物科技有限公司 | Plant composition and application thereof in cosmetics |
| CN115487022B (en) * | 2022-11-18 | 2023-03-17 | 云南典润洋科技有限公司 | Pressure control device for high-pressure oxygen-enriched cabin |
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