CN109863630A - 锂二次电池用正极活性物质的制造方法 - Google Patents
锂二次电池用正极活性物质的制造方法 Download PDFInfo
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- CN109863630A CN109863630A CN201780062390.7A CN201780062390A CN109863630A CN 109863630 A CN109863630 A CN 109863630A CN 201780062390 A CN201780062390 A CN 201780062390A CN 109863630 A CN109863630 A CN 109863630A
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- active material
- secondary battery
- lithium secondary
- positive active
- lithium
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- 229910052744 lithium Inorganic materials 0.000 title claims abstract description 152
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 title claims abstract description 143
- 239000007774 positive electrode material Substances 0.000 title claims abstract description 117
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 claims abstract description 137
- 239000000203 mixture Substances 0.000 claims abstract description 112
- 230000008569 process Effects 0.000 claims abstract description 111
- 238000001354 calcination Methods 0.000 claims abstract description 93
- 150000002642 lithium compounds Chemical class 0.000 claims abstract description 23
- 239000007769 metal material Substances 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 239000002243 precursor Substances 0.000 claims abstract description 15
- 239000001301 oxygen Substances 0.000 claims description 37
- 229910052760 oxygen Inorganic materials 0.000 claims description 37
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 36
- 239000007789 gas Substances 0.000 claims description 27
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 claims description 24
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 23
- 229910052804 chromium Inorganic materials 0.000 claims description 23
- 239000011651 chromium Substances 0.000 claims description 23
- 229910052808 lithium carbonate Inorganic materials 0.000 claims description 22
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- 229910052758 niobium Inorganic materials 0.000 claims description 5
- 229910052725 zinc Inorganic materials 0.000 claims description 5
- 229910052726 zirconium Inorganic materials 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 4
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- 238000004458 analytical method Methods 0.000 description 16
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- 238000007590 electrostatic spraying Methods 0.000 description 1
- JBTWLSYIZRCDFO-UHFFFAOYSA-N ethyl methyl carbonate Chemical compound CCOC(=O)OC JBTWLSYIZRCDFO-UHFFFAOYSA-N 0.000 description 1
- PQVSTLUFSYVLTO-UHFFFAOYSA-N ethyl n-ethoxycarbonylcarbamate Chemical compound CCOC(=O)NC(=O)OCC PQVSTLUFSYVLTO-UHFFFAOYSA-N 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- RRMGGYGDQCMPKP-UHFFFAOYSA-N gold lithium Chemical compound [Li].[Au] RRMGGYGDQCMPKP-UHFFFAOYSA-N 0.000 description 1
- 239000007770 graphite material Substances 0.000 description 1
- 238000007756 gravure coating Methods 0.000 description 1
- UHUWQCGPGPPDDT-UHFFFAOYSA-N greigite Chemical compound [S-2].[S-2].[S-2].[S-2].[Fe+2].[Fe+3].[Fe+3] UHUWQCGPGPPDDT-UHFFFAOYSA-N 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 150000002466 imines Chemical class 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910000765 intermetallic Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 239000001989 lithium alloy Substances 0.000 description 1
- GLXDVVHUTZTUQK-UHFFFAOYSA-M lithium hydroxide monohydrate Substances [Li+].O.[OH-] GLXDVVHUTZTUQK-UHFFFAOYSA-M 0.000 description 1
- 229940040692 lithium hydroxide monohydrate Drugs 0.000 description 1
- 229910001947 lithium oxide Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- 229910001537 lithium tetrachloroaluminate Inorganic materials 0.000 description 1
- VDVLPSWVDYJFRW-UHFFFAOYSA-N lithium;bis(fluorosulfonyl)azanide Chemical compound [Li+].FS(=O)(=O)[N-]S(F)(=O)=O VDVLPSWVDYJFRW-UHFFFAOYSA-N 0.000 description 1
- QSZMZKBZAYQGRS-UHFFFAOYSA-N lithium;bis(trifluoromethylsulfonyl)azanide Chemical compound [Li+].FC(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F QSZMZKBZAYQGRS-UHFFFAOYSA-N 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229910052960 marcasite Inorganic materials 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000004005 microsphere Substances 0.000 description 1
- 229910052961 molybdenite Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910052982 molybdenum disulfide Inorganic materials 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000004745 nonwoven fabric Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 125000005010 perfluoroalkyl group Chemical group 0.000 description 1
- 125000003367 polycyclic group Chemical group 0.000 description 1
- 229920000867 polyelectrolyte Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 description 1
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 description 1
- 229910052683 pyrite Inorganic materials 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 229910000338 selenium disulfide Inorganic materials 0.000 description 1
- 229960005265 selenium sulfide Drugs 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910052959 stibnite Inorganic materials 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- RCYJPSGNXVLIBO-UHFFFAOYSA-N sulfanylidenetitanium Chemical compound [S].[Ti] RCYJPSGNXVLIBO-UHFFFAOYSA-N 0.000 description 1
- 150000004763 sulfides Chemical class 0.000 description 1
- HXJUTPCZVOIRIF-UHFFFAOYSA-N sulfolane Chemical compound O=S1(=O)CCCC1 HXJUTPCZVOIRIF-UHFFFAOYSA-N 0.000 description 1
- 235000001508 sulfur Nutrition 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical compound FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
- 238000004227 thermal cracking Methods 0.000 description 1
- 229920006259 thermoplastic polyimide Polymers 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 229910000314 transition metal oxide Inorganic materials 0.000 description 1
- 150000003624 transition metals Chemical class 0.000 description 1
- 125000001889 triflyl group Chemical group FC(F)(F)S(*)(=O)=O 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Nickelates
- C01G53/42—Nickelates containing alkali metals, e.g. LiNiO2
- C01G53/44—Nickelates containing alkali metals, e.g. LiNiO2 containing manganese
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
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| JP2016-201566 | 2016-10-13 | ||
| JP2016201566A JP6857482B2 (ja) | 2016-10-13 | 2016-10-13 | リチウム二次電池用正極活物質の製造方法 |
| PCT/JP2017/037171 WO2018070517A1 (ja) | 2016-10-13 | 2017-10-13 | リチウム二次電池用正極活物質の製造方法 |
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| CN109863630A true CN109863630A (zh) | 2019-06-07 |
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| Country | Link |
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| JP (1) | JP6857482B2 (ja) |
| KR (1) | KR102425597B1 (ja) |
| CN (1) | CN109863630A (ja) |
| WO (1) | WO2018070517A1 (ja) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110444756A (zh) * | 2019-08-19 | 2019-11-12 | 湖南金富力新能源股份有限公司 | 用高温反应装置制备的锂离子电池正极材料及制法和应用 |
| CN110459759A (zh) * | 2019-08-19 | 2019-11-15 | 湖南金富力新能源股份有限公司 | 用回转装置制备的锂离子电池正极材料及其制法和应用 |
| CN110935881A (zh) * | 2019-12-30 | 2020-03-31 | 佛山市中研非晶科技股份有限公司 | 非晶纳米晶粉末烘烤装置及应用其的磁粉芯生产线 |
| CN116438683A (zh) * | 2020-11-17 | 2023-07-14 | 住友化学株式会社 | 锂金属复合氧化物的制造方法 |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6673538B2 (ja) | 2017-11-21 | 2020-03-25 | 日立金属株式会社 | リチウムイオン二次電池用正極活物質の製造方法及び熱処理装置 |
| CN109037633B (zh) * | 2018-07-31 | 2022-02-22 | 湖南德景源科技有限公司 | 一种利用回转窑热处理生产改性高镍正极材料的方法 |
| JP6646129B1 (ja) * | 2018-12-07 | 2020-02-14 | 住友化学株式会社 | リチウム二次電池用正極活物質の製造方法 |
| KR102168640B1 (ko) * | 2020-04-21 | 2020-10-21 | (주)탑전지 | 스피넬 복합고용체 산화물을 포함하는 양극 활물질, 이의 제조 방법, 및 이를 포함하는 리튬 이차 전지 |
| JP6936909B1 (ja) * | 2020-08-07 | 2021-09-22 | Ｂａｓｆ戸田バッテリーマテリアルズ合同会社 | 非水電解質二次電池用正極活物質及びそれを用いた非水電解質二次電池 |
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| JP2002260655A (ja) * | 2001-02-28 | 2002-09-13 | Nichia Chem Ind Ltd | リチウムイオン二次電池用正極活物質の製造方法 |
| JP2011058785A (ja) * | 2009-09-14 | 2011-03-24 | Takasago Ind Co Ltd | ロータリーキルンおよび当該ロータリーキルンにより製造される電池材料 |
| CN102812583A (zh) * | 2011-03-29 | 2012-12-05 | Jx日矿日石金属株式会社 | 锂离子电池用正极活性物质的制造方法及锂离子电池用正极活性物质 |
| CN104201323A (zh) * | 2014-07-07 | 2014-12-10 | 上海电力学院 | 氧化铝包覆钴酸锂正极材料的制备方法 |
| CN105428589A (zh) * | 2015-11-13 | 2016-03-23 | 江苏南大紫金锂电智能装备有限公司 | 锂电池正极材料智能生产工艺 |
| JP2016106358A (ja) * | 2015-12-25 | 2016-06-16 | 信越化学工業株式会社 | 非水電解質二次電池用負極活物質の製造方法 |
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| JPH11139829A (ja) * | 1997-11-04 | 1999-05-25 | Nikki Chemcal Co Ltd | リチウムイオン二次電池用正極材の製造方法 |
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| JP4394068B2 (ja) * | 2005-12-26 | 2010-01-06 | Ａｇｃセイミケミカル株式会社 | リチウム二次電池用正極物質及びその製造方法 |
| WO2010113512A1 (ja) * | 2009-04-03 | 2010-10-07 | パナソニック株式会社 | リチウムイオン二次電池用正極活物質及びその製造方法並びにリチウムイオン二次電池 |
| JP2012201525A (ja) * | 2011-03-24 | 2012-10-22 | Toho Material Kk | 複合金属酸化物の製造方法 |
| WO2012132072A1 (ja) * | 2011-03-29 | 2012-10-04 | Jx日鉱日石金属株式会社 | リチウムイオン電池用正極活物質の製造方法及びリチウムイオン電池用正極活物質 |
| JP2015196621A (ja) * | 2014-04-01 | 2015-11-09 | 日本化学工業株式会社 | 硫化リチウムの製造方法及び無機固体電解質の製造方法 |
-
2016
- 2016-10-13 JP JP2016201566A patent/JP6857482B2/ja active Active
-
2017
- 2017-10-13 CN CN201780062390.7A patent/CN109863630A/zh active Pending
- 2017-10-13 KR KR1020197009989A patent/KR102425597B1/ko active IP Right Grant
- 2017-10-13 WO PCT/JP2017/037171 patent/WO2018070517A1/ja active Application Filing
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| JP2002260655A (ja) * | 2001-02-28 | 2002-09-13 | Nichia Chem Ind Ltd | リチウムイオン二次電池用正極活物質の製造方法 |
| JP2011058785A (ja) * | 2009-09-14 | 2011-03-24 | Takasago Ind Co Ltd | ロータリーキルンおよび当該ロータリーキルンにより製造される電池材料 |
| CN102812583A (zh) * | 2011-03-29 | 2012-12-05 | Jx日矿日石金属株式会社 | 锂离子电池用正极活性物质的制造方法及锂离子电池用正极活性物质 |
| CN104201323A (zh) * | 2014-07-07 | 2014-12-10 | 上海电力学院 | 氧化铝包覆钴酸锂正极材料的制备方法 |
| CN105428589A (zh) * | 2015-11-13 | 2016-03-23 | 江苏南大紫金锂电智能装备有限公司 | 锂电池正极材料智能生产工艺 |
| JP2016106358A (ja) * | 2015-12-25 | 2016-06-16 | 信越化学工業株式会社 | 非水電解質二次電池用負極活物質の製造方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110444756A (zh) * | 2019-08-19 | 2019-11-12 | 湖南金富力新能源股份有限公司 | 用高温反应装置制备的锂离子电池正极材料及制法和应用 |
| CN110459759A (zh) * | 2019-08-19 | 2019-11-15 | 湖南金富力新能源股份有限公司 | 用回转装置制备的锂离子电池正极材料及其制法和应用 |
| CN110444756B (zh) * | 2019-08-19 | 2020-12-01 | 湖南金富力新能源股份有限公司 | 用高温反应装置制备的锂离子电池正极材料及制法和应用 |
| CN110935881A (zh) * | 2019-12-30 | 2020-03-31 | 佛山市中研非晶科技股份有限公司 | 非晶纳米晶粉末烘烤装置及应用其的磁粉芯生产线 |
| CN116438683A (zh) * | 2020-11-17 | 2023-07-14 | 住友化学株式会社 | 锂金属复合氧化物的制造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JP6857482B2 (ja) | 2021-04-14 |
| JP2018063853A (ja) | 2018-04-19 |
| KR102425597B1 (ko) | 2022-07-26 |
| KR20190062432A (ko) | 2019-06-05 |
| WO2018070517A1 (ja) | 2018-04-19 |
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Application publication date: 20190607 |