CN109805034A - Degradable efficient greenbelt herbicide of one kind and preparation method thereof - Google Patents

Degradable efficient greenbelt herbicide of one kind and preparation method thereof Download PDF

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Publication number
CN109805034A
CN109805034A CN201910146193.4A CN201910146193A CN109805034A CN 109805034 A CN109805034 A CN 109805034A CN 201910146193 A CN201910146193 A CN 201910146193A CN 109805034 A CN109805034 A CN 109805034A
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parts
herbicide
solution
greenbelt
kudzu
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杨沾
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Abstract

The invention discloses a kind of degradable efficient greenbelt herbicides, including following raw material: kudzu, aqueous solution, cottonseed oil, chrysanthemum peach root, fragrant small cup flower, auxiliary agent and active biochemical bacteria solution, with efficient weeding ability, it can degrade simultaneously sufficiently, avoid pollution environment, it can be seen that from test result, the chrysanthemum peach root and fragrant small cup flower that the present invention is added, the degradation capability of herbicide can be effectively improved, the active biochemical bacteria solution that the present invention is added can significantly improve the weeding ability of herbicide, at the same time, the kudzu that the present invention is added has a certain upgrade to the degradation capability and weeding ability of herbicide.

Description

Degradable efficient greenbelt herbicide of one kind and preparation method thereof
Technical field
The present invention relates to a kind of herbicide, specifically a kind of degradable efficient greenbelt herbicide and preparation method thereof.
Background technique
Herbicide, which refers to, can make weeds that withered medicament, also known as herbicide thoroughly or selectively occur, eliminating or Inhibit a substance of plant growth.Sodium chlorate therein, borax, arsenate, trichloroacetic acid for any kind of plant all Play the role of it is withered, effect influenced by herbicide, plant and three factor of environmental condition.It is divided into go out natural disposition and selection by effect Property herbicide, selective herbicide especially nitrophenol, chlorophenol, carbamic derivative majority are all effective.It removes in the world Careless agent development is gradually steady, main development efficiently, low toxicity, wide spectrum, low dosage kind, the small disposable processing of environmental pollution Agent is increasingly becoming mainstream.
Common kind is organic compound, can be widely used for prevention and treatment farmland, orchard, floral nursery, grassland and bare place, The noxious plants such as the ground such as railway line, river, reservoir, warehouse weeds, miscellaneous filling, miscellaneous tree.
Urban green belts are a part indispensable in urban construction, greenbelt have put oxygen, drug abuse, dedusting, sterilization, Noise reduction, sand-proof, the effect for adjusting miniclimate, the weeds of greenbelt growth inside not only influence whether the beauty of greenbelt, and And will affect the normal growth of greenbelt plant, while sanitationman being needed constantly to carry out mechanical chipping, it operates very Trouble.
Summary of the invention
The purpose of the present invention is to provide a kind of degradable efficient greenbelt herbicides, to solve to mention in above-mentioned background technique Out the problem of.
To achieve the above object, the invention provides the following technical scheme:
A kind of degradable efficient greenbelt herbicide, including the following raw material formed by weight: 5-12 parts of kudzu, water-soluble 20-50 parts of liquid, 10-16 parts of cottonseed oil, 6-12 parts of chrysanthemum peach root, fragrant 4-9 parts of small cup flower, 2-6 parts of auxiliary agent and active biochemical bacteria are molten 12-26 parts of liquid.
As a further solution of the present invention: including the following raw material formed by weight: 8-11 parts of kudzu, aqueous solution 25-40 parts, 12-15 parts of cottonseed oil, 7-11 parts of chrysanthemum peach root, fragrant 5-7 parts of small cup flower, 3-5 parts of auxiliary agent and active biochemical bacteria solution 15-20 parts.
As further scheme of the invention: including the following raw material formed by weight: 10 parts of kudzu, aqueous solution 30 Part, 13 parts of cottonseed oil, 8 parts of chrysanthemum peach root, fragrant small cup spend 6 parts, 18 parts of 4 parts of auxiliary agent and activity biochemical bacteria solution.
As further scheme of the invention: the auxiliary agent is specially alkenyl succinic anhydride, phosphoric anhydride, asparagine, apple One of tartaric acid or alkyl polyglycoside.
As further scheme of the invention: the aqueous solution is specially that mass fraction is that 92-95wt% acetone is water-soluble Liquid.
A kind of preparation method of degradable efficient greenbelt herbicide, which comprises the following steps:
1), kudzu after drying is crushed to after 10-20 mesh obtains kudzu powder and is added in aqueous solution, cottonseed oil is then added It is ultrasonically treated after mixing with auxiliary agent, and is filtered, washed and obtains kudzu solution after being concentrated and obtain kudzu extraction Object solution for standby;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, i.e., The water that temperature is 45 DEG C, volume is 6 times of rumen fluid amounts, the active biochemical that 7 times of rumen fluid opportunistic pathogen amounts are made are put into seed cylinder Bacterium solution for standby;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 10-15wt%, then crushes, crosses 150-180 mesh Sieve is uniformly mixed after dry, then carries out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added in wall material solution after mixing After matter, spray drying, cooling degradable efficient greenbelt herbicide.
As further scheme of the invention: in step 1), the frequency of ultrasonic treatment is 52-55kHz, ultrasonic treatment Power is 650-700W, and the time of ultrasonic treatment is 3-5min.
A kind of degradable efficient greenbelt herbicide is preparing the application in herbicidal product.
Compared with prior art, the beneficial effects of the present invention are: degradable efficient greenbelt herbicide prepared by the present invention Including following raw material: kudzu, aqueous solution, cottonseed oil, chrysanthemum peach root, fragrant small cup flower, auxiliary agent and active biochemical bacteria solution have height The weeding ability of effect, while can degrade sufficiently, environment is avoided pollution, as can be seen that the present invention was added from test result Chrysanthemum peach root and fragrant small cup flower, can effectively improve the degradation capability of herbicide, the active biochemical bacteria solution energy that the present invention is added The weeding ability of herbicide is enough significantly improved, at the same time, degradation capability and weeding of the kudzu that the present invention is added to herbicide Ability has a certain upgrade.
Specific embodiment
Technical solution of the present invention is described in more detail With reference to embodiment.
Embodiment 1
A kind of degradable efficient greenbelt herbicide, including the following raw material formed by weight: 5 parts of kudzu, aqueous solution 20 parts, 10 parts of cottonseed oil, 6 parts of chrysanthemum peach root, fragrant small cup spend 4 parts, 2 parts of auxiliary agent and 12 parts of active biochemical bacteria solution.
Specifically, the auxiliary agent is specially alkenyl succinic anhydride in the present embodiment.
Specifically, the aqueous solution is specially that mass fraction is 92wt% aqueous acetone solution in the present embodiment.
A kind of preparation method of degradable efficient greenbelt herbicide, which comprises the following steps:
1) kudzu after drying, is crushed to 10 mesh to obtain being added in aqueous solution after kudzu powder, be then added cottonseed oil and Auxiliary agent is ultrasonically treated after mixing, and is filtered, washed and obtains kudzu solution after being concentrated and obtain kudzu extract Solution for standby;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, i.e., The water that temperature is 45 DEG C, volume is 6 times of rumen fluid amounts, the active biochemical that 7 times of rumen fluid opportunistic pathogen amounts are made are put into seed cylinder Bacterium solution for standby;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 10wt%, then crushed, 150 meshes are crossed, it is dry After be uniformly mixed, then carry out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added in wall material solution after mixing After matter, spray drying, cooling degradable efficient greenbelt herbicide.
Specifically, the frequency of ultrasonic treatment is 52kHz in the present embodiment step 1), the power of ultrasonic treatment is 650W, is surpassed The time of sonication is 3min.
Embodiment 2
A kind of degradable efficient greenbelt herbicide, including the following raw material formed by weight: 12 parts of kudzu, aqueous solution 50 parts, 16 parts of cottonseed oil, 12 parts of chrysanthemum peach root, fragrant small cup spend 9 parts, 6 parts of auxiliary agent and 26 parts of active biochemical bacteria solution.
Specifically, the auxiliary agent is specially phosphoric anhydride in the present embodiment.
Specifically, the aqueous solution is specially that mass fraction is 95wt% aqueous acetone solution in the present embodiment.
A kind of preparation method of degradable efficient greenbelt herbicide, which comprises the following steps:
1) kudzu after drying, is crushed to 20 mesh to obtain being added in aqueous solution after kudzu powder, be then added cottonseed oil and Auxiliary agent is ultrasonically treated after mixing, and is filtered, washed and obtains kudzu solution after being concentrated and obtain kudzu extract Solution for standby;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, i.e., The water that temperature is 45 DEG C, volume is 6 times of rumen fluid amounts, the active biochemical that 7 times of rumen fluid opportunistic pathogen amounts are made are put into seed cylinder Bacterium solution for standby;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 15wt%, then crushed, 180 meshes are crossed, it is dry After be uniformly mixed, then carry out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added in wall material solution after mixing After matter, spray drying, cooling degradable efficient greenbelt herbicide.
Specifically, the frequency of ultrasonic treatment is 55kHz in the present embodiment step 1), the power of ultrasonic treatment is 700W, is surpassed The time of sonication is 5min.
Embodiment 3
A kind of degradable efficient greenbelt herbicide, including the following raw material formed by weight: 8 parts of kudzu, aqueous solution 25 parts, 12 parts of cottonseed oil, 7 parts of chrysanthemum peach root, fragrant small cup spend 5 parts, 3 parts of auxiliary agent and 15 parts of active biochemical bacteria solution.
Specifically, the auxiliary agent is specially asparagine in the present embodiment.
Specifically, the aqueous solution is specially that mass fraction is 92wt% aqueous acetone solution in the present embodiment.
A kind of preparation method of degradable efficient greenbelt herbicide, which comprises the following steps:
1) kudzu after drying, is crushed to 10 mesh to obtain being added in aqueous solution after kudzu powder, be then added cottonseed oil and Auxiliary agent is ultrasonically treated after mixing, and is filtered, washed and obtains kudzu solution after being concentrated and obtain kudzu extract Solution for standby;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, i.e., The water that temperature is 45 DEG C, volume is 6 times of rumen fluid amounts, the active biochemical that 7 times of rumen fluid opportunistic pathogen amounts are made are put into seed cylinder Bacterium solution for standby;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 10wt%, then crushed, 150 meshes are crossed, it is dry After be uniformly mixed, then carry out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added in wall material solution after mixing After matter, spray drying, cooling degradable efficient greenbelt herbicide.
Specifically, the frequency of ultrasonic treatment is 52kHz in the present embodiment step 1), the power of ultrasonic treatment is 650W, is surpassed The time of sonication is 3min.
Embodiment 4
A kind of degradable efficient greenbelt herbicide, including the following raw material formed by weight: 11 parts of kudzu, aqueous solution 40 parts, 15 parts of cottonseed oil, 11 parts of chrysanthemum peach root, fragrant small cup spend 7 parts, 5 parts of auxiliary agent and 0 part of active biochemical bacteria solution.
Specifically, the auxiliary agent is specially malic acid in the present embodiment.
Specifically, the aqueous solution is specially that mass fraction is 95wt% aqueous acetone solution in the present embodiment.
A kind of preparation method of degradable efficient greenbelt herbicide, which comprises the following steps:
1) kudzu after drying, is crushed to 20 mesh to obtain being added in aqueous solution after kudzu powder, be then added cottonseed oil and Auxiliary agent is ultrasonically treated after mixing, and is filtered, washed and obtains kudzu solution after being concentrated and obtain kudzu extract Solution for standby;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, i.e., The water that temperature is 45 DEG C, volume is 6 times of rumen fluid amounts, the active biochemical that 7 times of rumen fluid opportunistic pathogen amounts are made are put into seed cylinder Bacterium solution for standby;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 15wt%, then crushed, 180 meshes are crossed, it is dry After be uniformly mixed, then carry out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added in wall material solution after mixing After matter, spray drying, cooling degradable efficient greenbelt herbicide.
Specifically, the frequency of ultrasonic treatment is 55kHz in the present embodiment step 1), the power of ultrasonic treatment is 700W, is surpassed The time of sonication is 5min.
Embodiment 5
A kind of degradable efficient greenbelt herbicide, including the following raw material formed by weight: 10 parts of kudzu, aqueous solution 30 parts, 13 parts of cottonseed oil, 8 parts of chrysanthemum peach root, fragrant small cup spend 6 parts, 18 parts of 4 parts of auxiliary agent and activity biochemical bacteria solution.
Specifically, the auxiliary agent is specially alkyl polyglycoside in the present embodiment.
Specifically, the aqueous solution is specially that mass fraction is 95wt% aqueous acetone solution in the present embodiment.
A kind of preparation method of degradable efficient greenbelt herbicide, which comprises the following steps:
1) kudzu after drying, is crushed to 10 mesh to obtain being added in aqueous solution after kudzu powder, be then added cottonseed oil and Auxiliary agent is ultrasonically treated after mixing, and is filtered, washed and obtains kudzu solution after being concentrated and obtain kudzu extract Solution for standby;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, i.e., The water that temperature is 45 DEG C, volume is 6 times of rumen fluid amounts, the active biochemical that 7 times of rumen fluid opportunistic pathogen amounts are made are put into seed cylinder Bacterium solution for standby;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 15wt%, then crushed, 180 meshes are crossed, it is dry After be uniformly mixed, then carry out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added in wall material solution after mixing After matter, spray drying, cooling degradable efficient greenbelt herbicide.
Specifically, the frequency of ultrasonic treatment is 55kHz in the present embodiment step 1), the power of ultrasonic treatment is 650W, is surpassed The time of sonication is 3min.
Comparative example 1
Compared with Example 5, kudzu is free of, other are same as Example 5.
Comparative example 2
Compared with Example 5, without chrysanthemum peach root and fragrant small cup flower, other are same as Example 5.
Comparative example 3
Compared with Example 5, active biochemical bacteria solution is free of, other are same as Example 5.
Performance test
It makes a service test to the embodiment of the present invention 5, as a control group using comparative example 1-3, selects Euonymus japonicus greening Band is as experimental field, and under the identical amount of spraying, spraying time and field pipe measure, result is as shown in the table:
Test result table
As can be seen that degradable efficient greenbelt herbicide prepared by the present invention has efficient weeding from result above Ability, while can degrade sufficiently, environment is avoided pollution, can be seen that from the data comparison of embodiment 5 and comparative example 1-3 The chrysanthemum peach root and fragrant small cup flower that the present invention is added, can effectively improve the degradation capability of herbicide, the activity that the present invention is added Biochemical bacteria solution can significantly improve the weeding ability of herbicide, at the same time, drop of the kudzu that the present invention is added to herbicide Solution ability and weeding ability have a certain upgrade.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention Various changes can be made.

Claims (8)

1. a kind of degradable efficient greenbelt herbicide, which is characterized in that including the following raw material formed by weight: kudzu 5- 12 parts, 20-50 parts of aqueous solution, 10-16 parts of cottonseed oil, 6-12 parts of chrysanthemum peach root, fragrant 4-9 parts of small cup flower, 2-6 parts of auxiliary agent and activity 12-26 parts of biochemical bacteria solution.
2. degradable efficient greenbelt herbicide according to claim 1, which is characterized in that including following group by weight At raw material: 8-11 parts of kudzu, 25-40 parts of aqueous solution, 12-15 parts of cottonseed oil, 7-11 parts of chrysanthemum peach root, 5-7 parts of fragrant small cup flower, 3-5 parts and 15-20 parts of active biochemical bacteria solution of auxiliary agent.
3. degradable efficient greenbelt herbicide according to claim 1, which is characterized in that including following group by weight At raw material: 10 parts of kudzu, 30 parts of aqueous solution, 13 parts of cottonseed oil, 8 parts of chrysanthemum peach root, fragrant small cup spend 6 parts, 4 parts of auxiliary agent and while still alive 18 parts of solution of biochemical bacteria of property.
4. degradable efficient greenbelt herbicide according to claim 1 to 3, which is characterized in that the auxiliary agent is specific For one of alkenyl succinic anhydride, phosphoric anhydride, asparagine, malic acid or alkyl polyglycoside.
5. degradable efficient greenbelt herbicide according to claim 1 to 3, which is characterized in that the aqueous solution tool Body is that mass fraction is 92-95wt% aqueous acetone solution.
6. a kind of preparation method of degradable efficient greenbelt herbicide a method according to any one of claims 1-3, which is characterized in that The following steps are included:
1), kudzu after drying is crushed to after 10-20 mesh obtains kudzu powder and is added in aqueous solution, cottonseed oil is then added and helps Agent is ultrasonically treated after mixing, and is filtered, washed and obtains kudzu solution after being concentrated to obtain kudzu extract molten Liquid is spare;
2) rumen fluid, is sucked out out of health is ruminated Rumen of livestock with conduit, carries out level-one biochemistry opportunistic pathogen and expands culture, that is, planting Be put into sub- cylinder temperature be 45 DEG C, volume be 6 times of rumen fluid amount water, be made 7 times of rumen fluid opportunistic pathogen amount active biochemical bacteria it is molten Liquid is spare;
3) chrysanthemum peach root and fragrant small cup flower, are dried to that moisture content is 10-15wt%, then crushes, crosses 150-180 mesh, It is uniformly mixed after drying, then carries out mechanical shaking extraction, then filter, be concentrated to get extract;
4), kudzu extract solution, active biochemical bacteria solution and extract are added after mixing in wall material solution after homogeneous, Spray drying, cooling degradable efficient greenbelt herbicide.
7. the preparation method of degradable efficient greenbelt herbicide according to claim 6, which is characterized in that step 1) In, the frequency of ultrasonic treatment is 52-55kHz, and the power of ultrasonic treatment is 650-700W, and the time of ultrasonic treatment is 3-5min.
8. a kind of degradable efficient greenbelt herbicide a method according to any one of claims 1-3 is preparing answering in herbicidal product With.
CN201910146193.4A 2019-02-27 2019-02-27 Degradable efficient greenbelt herbicide of one kind and preparation method thereof Pending CN109805034A (en)

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Publication number Priority date Publication date Assignee Title
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CN104542730A (en) * 2015-01-06 2015-04-29 曹明军 Multifunctional active bioinsecticide and preparation method thereof
CN105028497A (en) * 2015-07-24 2015-11-11 安徽省圣丹生物化工有限公司 Preparation method of efficient herbicide micro-capsule
CN105028529A (en) * 2015-07-23 2015-11-11 安徽省圣丹生物化工有限公司 Environment-friendly herbicide and preparation method thereof
CN108112622A (en) * 2016-11-29 2018-06-05 山东润博生物科技有限公司 Good herbicide of a kind of bactericidal effect and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1944624A (en) * 2006-10-31 2007-04-11 南阳兴农生物技术开发有限公司 Method for cultivating and preparing active biochemical bacteria
CN104542730A (en) * 2015-01-06 2015-04-29 曹明军 Multifunctional active bioinsecticide and preparation method thereof
CN105028529A (en) * 2015-07-23 2015-11-11 安徽省圣丹生物化工有限公司 Environment-friendly herbicide and preparation method thereof
CN105028497A (en) * 2015-07-24 2015-11-11 安徽省圣丹生物化工有限公司 Preparation method of efficient herbicide micro-capsule
CN108112622A (en) * 2016-11-29 2018-06-05 山东润博生物科技有限公司 Good herbicide of a kind of bactericidal effect and preparation method thereof

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Application publication date: 20190528