CN109527000A - A kind of Frankliniella occidentalis plant-originated repellent and preparation method thereof - Google Patents

A kind of Frankliniella occidentalis plant-originated repellent and preparation method thereof Download PDF

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CN109527000A
CN109527000A CN201811428158.3A CN201811428158A CN109527000A CN 109527000 A CN109527000 A CN 109527000A CN 201811428158 A CN201811428158 A CN 201811428158A CN 109527000 A CN109527000 A CN 109527000A
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frankliniella occidentalis
leaf
plant
ageratum conyzoides
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曹宇
李�灿
王丽娟
杨红
李军
王春
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Guiyang University
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Guiyang University
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/22Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/34Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Agronomy & Crop Science (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of Frankliniella occidentalis plant-originated repellents, are made of raw material from the following weight: 55~95 parts of Radical Injury in Wampee Seeds, octagonal 65~105 parts of leaf, 50~80 parts of rosin, 50~80 parts of neem tree skin, golden 60~100 parts of waist arrow, 60~100 parts of white radishes, 45~95 parts of cherry leaf, 45~95 parts of tomato leaf, 35~85 parts of Alocasia ordora, 25~65 parts of Ageratum conyzoides, 25~65 parts of Ageratum conyzoides, 35~75 parts of peppermint, 40~90 parts of Jasmine, 500~600 parts of ethyl alcohol.The raw materials used present invention is pure natural substances, the active constituent of Frankliniella occidentalis repellant after processed is plant extracts, it is nontoxic to people and animals, no pollution to the environment, and there are stronger anti-repelling properties to Frankliniella occidentalis, the preparation and use of the Frankliniella occidentalis repellant are all more convenient, are a kind of safe and efficient, environmentally friendly Frankliniella occidentalis repellants.

Description

A kind of Frankliniella occidentalis plant-originated repellent and preparation method thereof
Technical field
The invention belongs to pest control pesticide producing processing technique field more particularly to a kind of Frankliniella occidentalis plant source repellents Agent and preparation method thereof.
Background technique
Frankliniella occidentalis is also known as alfalfa thrips, belongs to Thysanoptera Thysanoptera, Thripidae Thripidae is outside risk To invade pest.The worm originates in North America, and it was once that California, USA is most common that nineteen fifty-five finds in Hawaii Kauai first A kind of thrips.From after the 1980s, become surging type, varying environment and resistance to insecticides are enhanced.The pest can endanger 500 various plants of Hai60Duo Ge section, while a variety of virosis are also propagated, seriously affect crop yield and quality.2003 Nian Bei Capital is found for the first time, and potential suitable ecumene is distributed in national 28 provinces, autonomous regions and municipalities, in Yunnan Province, Zhejiang The ground such as river, Shandong are found and outburst is caused disaster in some areas.
Frankliniella occidentalis fertility is very strong, and individual is tiny, and great invisible, general field control is difficult to effectively control.? Under the indoor equilibrium temperature of temperature, it can recur 12-15 generation within 1 year, the bisexual reproduction of female adult row and single-female generation.At 15 DEG C -35 DEG C It can develop, only be needed from ovum to adult 14 days;27.2 DEG C of produce surviving of son are most, and a female adult can lay eggs 229, plant in common host On object, blastoprolepsis, and fertility is extremely strong.Frankliniella occidentalis is spread at a distance relies primarily on human factor.Seedling, flowers and its The allocation and transportation of its agricultural product, especially cut-flower transport and artificial carrying are the major ways of its long-distance communications.Its survival ability is strong, Frankliniella occidentalis remains to survive after tossing about transportation and sales to other cities.In addition, the pest be easy to drift with the wind, easily with clothes, fortune The carryings such as defeated tool are propagated.
Frankliniella occidentalis has strong thigmotaxis since polypide is small, often moves in the shelters such as flower, bud, high reproductive ability, short life Phase, and lay eggs in plant tissue, so bringing very big difficulty to chemical prevention.A kind of medicament or primary spray be difficult by Its each worm state is wholly or largely killed, and repeatedly or high concentration medication is easy to that it is made to develop drug resistance.
Patent about prevention and treatment Frankliniella occidentalis has, such as: patent application CN201310299599.9 discloses one kind Insecticide is preventing and treating the application in Frankliniella occidentalis, contains multiple killing teichomycin and pymetrozine in the insecticide composition.Containing killing more The insecticide of mycin and pymetrozine is efficient, less toxic, and to the simple process of Frankliniella occidentalis, the raw material of investment is completely converted into product, High income, no three wastes solve the problems, such as that prevention and treatment Frankliniella occidentalis effect is undesirable in the prior art.But add in the patent drug Chemical raw material is added, when carrying out the prevention and treatment of Frankliniella occidentalis to crops, crops will cause with certain influence, it is also possible to can break Bad soil and environment.
Therefore, the Frankliniella occidentalis repellant for developing a kind of safety non-pollution is particularly important.
Summary of the invention
The present invention is in order to solve the above technical problems, provide a kind of Frankliniella occidentalis plant-originated repellent and preparation method thereof. The application Frankliniella occidentalis repellant is using plant as raw material, and raw material sources are abundant, and cost of material is lower, is matched by scientific and reasonable 5, so that the active constituent of each raw material is complemented each other, have cooperative synergism effect, can repellent Frankliniella occidentalis, influence its mating, Oviposition, to achieve the effect that pest control and protect crops from infringement, repellent effect is good, will not develop drug resistance, and has There is the features such as at low cost, high-efficient, environmentally friendly, safety of human and livestock, there are wide economy, society and ecological benefits.
In order to reach purpose described above, the invention adopts the following technical scheme:
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 55~95 parts of Radical Injury in Wampee Seeds, illiciumverum 65~105 parts of leaf, 50~80 parts of rosin, 50~80 parts of neem tree skin, golden 60~100 parts of waist arrow, 60~100 parts of white radishes, cherry It is 45~95 parts of peach leaves, 45~95 parts of tomato leaf, 35~85 parts of Alocasia ordora, 25~65 parts of Ageratum conyzoides, 25~65 parts of Ageratum conyzoides, thin 35~75 parts of lotus, 40~90 parts of Jasmine, 500~600 parts of ethyl alcohol.
Further, a kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: Calusena lansium kind 65~85 parts of son, octagonal 75~95 parts of leaf, 60~70 parts of rosin, 60~70 parts of neem tree skin, golden 70~90 parts of waist arrow, white radishes 70~90 parts, 55~85 parts of cherry leaf, 55~85 parts of tomato leaf, 45~75 parts of Alocasia ordora, 35~55 parts of Ageratum conyzoides, Ageratum conyzoides 35~55 parts, 45~65 parts of peppermint, 50~80 parts of Jasmine, 520~580 parts of ethyl alcohol.
Further, a kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: Calusena lansium kind 75 parts of son, octagonal 85 parts of leaf, 65 parts of rosin, 65 parts of neem tree skin, golden 80 parts of waist arrow, 80 parts of white radishes, 70 parts of cherry leaf, west 70 parts of red persimmon leaf, 60 parts of Alocasia ordora, 45 parts of Ageratum conyzoides, 45 parts of Ageratum conyzoides, 55 parts of peppermint, 65 parts of Jasmine, 550 parts of ethyl alcohol.
Further, the Alocasia ordora is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The volume of the ethyl alcohol Percentage is 95%.
Further, a kind of preparation method of Frankliniella occidentalis plant-originated repellent, comprising the following steps:
(1) golden waist arrow, white radishes, cherry leaf, tomato leaf, Alocasia ordora, Ageratum conyzoides, Ageratum conyzoides are weighed according to parts by weight And peppermint, it is cut into the segment of 2~3cm long, the clear water of golden 5~6 times of weight of waist arrow is added, turns small fire after high fire is boiled and continues to decoct 3~5h, decompression filter and obtain filtrate and filter residue;
(2) Radical Injury in Wampee Seeds, octagonal leaf, neem tree skin and Jasmine are sent into drying machine drying, the filter of step (1) is added Slag is stirring evenly and then adding into ethyl alcohol and impregnates 24~30h, first ultrasonic wave extraction, then 6~7h of refluxing extraction at 60~65 DEG C, It is re-fed into the mixed liquor that 200~300 meshes were ground into grinder;
(3) rosin is placed under 60~65 DEG C of environment and is placed up to being completely melt, under stirring, the rosin of fusing is delayed In the slow filtrate that step (1) is added, 2~4h is kept the temperature at 55~60 DEG C, and the mixed liquor of step (2) is then added, stirs evenly Afterwards, 60~65 DEG C and 3~5h of isothermal holding are warming up to, ultrasonication, cooled to room temperature is made the Frankliniella occidentalis and plants Material resource repellant.
Further, in step (2), the frequency of the ultrasonic wave extraction is 0.2~0.6MHz, and power is 600~700W, Time is 45~55min.
Further, in step (2), the temperature of the drying is 55~60 DEG C, and the time is 150~200min, is dried to Material moisture is 20~25%.
Further, in step (2), the pressure of the grinding is 0.3~0.7MPa, and the time is 35~45min.
Further, in step (2) and (3), the speed of the stirring is 200~250r/min.
Further, in step (3), the process conditions of the ultrasonication: frequency is 0.6~1.0MHz, and power is 800~900W, time are 30~40min.
The application gold waist arrow, white radishes, cherry leaf, tomato leaf, Alocasia ordora, Ageratum conyzoides, Ageratum conyzoides and peppermint are by decocting Odor compound rich in the filtrate obtained after boiling, can effective repellent Frankliniella occidentalis;Wherein Radical Injury in Wampee Seeds, octagonal leaf, The mixed liquor smell rich in that neem tree skin, Jasmine can obtain after ethyl alcohol immersion, ultrasonic extraction, refluxing extraction Object is closed, it can effective repellent Frankliniella occidentalis;And filtrate and mixed liquor are after mixing, isothermal holding, ultrasonic treatment, it is mutually auxiliary between substance It coordinates, mutually promotes, the abundant odor compound solubility for making it possible to repellent Frankliniella occidentalis is higher, volatility is stronger, lasting Property more preferably, to improve repellant to the repellent effect of Frankliniella occidentalis.
Application of the application Frankliniella occidentalis plant-originated repellent on repellent Frankliniella occidentalis, concrete application method are as follows: in west Flower thrips moves into initial stage, in morning before 9:00 of non-rainy day, by Frankliniella occidentalis repellant spray pesticide on crops, per acre Dosage is 12~18L.
The ethanol extract of octagonal leaf has stronger repellent action and fumigation action to Frankliniella occidentalis adult.
Turpentine oil and neem emulsifiable solution are preferable to Frankliniella occidentalis Adult worms producting eggs repellent action.
Neem emulsifiable solution, golden waist arrow and turpentine oil are preferable to adult Antifeeding Effects.
Neem emulsifiable solution, Alocasia ordora, eucalyptus oil and Ageratum conyzoides are preferable to Frankliniella occidentalis population control efficiency.
Cherry leaf, tomato leaf volatiles have some repellent actions to Frankliniella occidentalis adult.
There are extremely significant anti-repelling properties to Frankliniella occidentalis for white radishes;
The methanolic extract of Radical Injury in Wampee Seeds has stronger repellent activity and action of contace poison to Frankliniella occidentalis.
Since present invention employs above technical schemes, have the advantages that
(1) the raw materials used present invention is pure natural substance, it is processed after Frankliniella occidentalis repellant active constituent it is equal It is nontoxic to people and animals for plant extracts, no pollution to the environment, and there is stronger anti-repelling properties, west flower to Frankliniella occidentalis The preparation and use of thrips repellant are all more convenient, are a kind of safe and efficient, environmentally friendly Frankliniella occidentalis repellants.
(2) the Frankliniella occidentalis repellant of the application interferes or inhibits and acting on the peripheral neverous system of Frankliniella occidentalis The behavior of Frankliniella occidentalis, reaches repellent action, so that harm and population quantity of the Frankliniella occidentalis to crops is effectively reduced, and Do not have anti-repelling properties for the natural enemy of field predatism, this is entirely different with the mechanism of action of insecticide.
(3) the application Frankliniella occidentalis repellant is using plant as raw material, and raw material sources are abundant, and cost of material is lower, passes through section Learn reasonable compatibility, the active constituent of each raw material made to complement each other, have cooperative synergism effect, can repellent Frankliniella occidentalis, Its mating, oviposition are influenced, to achieve the effect that pest control and protect crops from infringement, repellent effect is good, will not produce Raw drug resistance, has the characteristics that at low cost, high-efficient, environmentally friendly, safety of human and livestock, has wide economy, society and life State benefit.
Specific embodiment
Specific embodiments of the present invention will be described in further detail below, but the invention is not limited to these realities Mode is applied, it is claimed to still fall within the claims in the present invention for any improvement or replacement on the present embodiment essence spirit Range.
Embodiment 1
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 55 parts of Radical Injury in Wampee Seeds, octagonal leaf 65 Part, 50 parts of rosin, 50 parts of neem tree skin, golden 60 parts of waist arrow, 60 parts of white radishes, 45 parts of cherry leaf, 45 parts of tomato leaf, Alocasia ordora 35 parts, 25 parts of Ageratum conyzoides, 25 parts of Ageratum conyzoides, 35 parts of peppermint, 40 parts of Jasmine, 500 parts of ethyl alcohol.
Further, the Alocasia ordora is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The volume of the ethyl alcohol Percentage is 95%.
A kind of preparation method of Frankliniella occidentalis plant-originated repellent as described above, comprising the following steps:
(1) golden waist arrow, white radishes, cherry leaf, tomato leaf, Alocasia ordora, Ageratum conyzoides, Ageratum conyzoides are weighed according to parts by weight And peppermint, it is cut into the segment of 2~3cm long, the clear water of golden 5~6 times of weight of waist arrow is added, turns small fire after high fire is boiled and continues to decoct 3~5h, decompression filter and obtain filtrate and filter residue;
(2) Radical Injury in Wampee Seeds, octagonal leaf, neem tree skin and Jasmine are sent into drying machine drying, the filter of step (1) is added Slag is stirring evenly and then adding into ethyl alcohol and impregnates 24~30h, first ultrasonic wave extraction, then 6~7h of refluxing extraction at 60~65 DEG C, It is re-fed into the mixed liquor that 200~300 meshes were ground into grinder;The frequency of the ultrasonic wave extraction is 0.2~0.6MHz, Power is 600~700W, and the time is 45~55min;The temperature of the drying is 55~60 DEG C, and the time is 150~200min, is dried Doing to material moisture is 20~25%;The pressure of the grinding is 0.3~0.7MPa, and the time is 35~45min;
(3) rosin is placed under 60~65 DEG C of environment and is placed up to being completely melt, under stirring, the rosin of fusing is delayed In the slow filtrate that step (1) is added, 2~4h is kept the temperature at 55~60 DEG C, and the mixed liquor of step (2) is then added, stirs evenly Afterwards, 60~65 DEG C and 3~5h of isothermal holding are warming up to, ultrasonication, cooled to room temperature is made the Frankliniella occidentalis and plants Material resource repellant;The process conditions of the ultrasonication: frequency is 0.6~1.0MHz, and power is 800~900W, and the time is 30~40min.
Further, in step (2) and (3), the speed of the stirring is 200~250r/min.
Embodiment 2
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 95 parts of Radical Injury in Wampee Seeds, octagonal leaf 105 parts, 80 parts of rosin, 80 parts of neem tree skin, golden 100 parts of waist arrow, 100 parts of white radishes, 95 parts of cherry leaf, tomato leaf 95 Part, 85 parts of Alocasia ordora, 65 parts of Ageratum conyzoides, 65 parts of Ageratum conyzoides, 75 parts of peppermint, 90 parts of Jasmine, 600 parts of ethyl alcohol.
Further, the Alocasia ordora is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The volume of the ethyl alcohol Percentage is 95%.Preparation method is same as Example 1.
Embodiment 3
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 65 parts of Radical Injury in Wampee Seeds, octagonal leaf 75 Part, 60 parts of rosin, 60 parts of neem tree skin, golden 70 parts of waist arrow, 70 parts of white radishes, 55 parts of cherry leaf, 55 parts of tomato leaf, Alocasia ordora 45 parts, 35 parts of Ageratum conyzoides, 35 parts of Ageratum conyzoides, 45 parts of peppermint, 50 parts of Jasmine, 520 parts of ethyl alcohol.
Further, the Alocasia ordora is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The volume of the ethyl alcohol Percentage is 95%.Preparation method is same as Example 1.
Embodiment 4
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 85 parts of Radical Injury in Wampee Seeds, octagonal leaf 95 Part, 70 parts of rosin, 70 parts of neem tree skin, golden 90 parts of waist arrow, 90 parts of white radishes, 85 parts of cherry leaf, 85 parts of tomato leaf, Alocasia ordora 75 parts, 55 parts of Ageratum conyzoides, 55 parts of Ageratum conyzoides, 65 parts of peppermint, 80 parts of Jasmine, 580 parts of ethyl alcohol.
Further, the Alocasia ordora is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The volume of the ethyl alcohol Percentage is 95%.Preparation method is same as Example 1.
Embodiment 5
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 75 parts of Radical Injury in Wampee Seeds, octagonal leaf 85 Part, 65 parts of rosin, 65 parts of neem tree skin, golden 80 parts of waist arrow, 80 parts of white radishes, 70 parts of cherry leaf, 70 parts of tomato leaf, Alocasia ordora 60 parts, 45 parts of Ageratum conyzoides, 45 parts of Ageratum conyzoides, 55 parts of peppermint, 65 parts of Jasmine, 550 parts of ethyl alcohol.
Further, the Alocasia ordora is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The volume of the ethyl alcohol Percentage is 95%.Preparation method is same as Example 1.
Comparative example 1
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 50 parts of Radical Injury in Wampee Seeds, octagonal leaf 45,40 parts of rosin, 35 parts of neem tree skin, golden 55 parts of waist arrow, 50 parts of white radishes, 35 parts of cherry leaf, 40 parts of tomato leaf, Alocasia ordora 30 parts, 15 parts of Ageratum conyzoides, 15 parts of Ageratum conyzoides, 25 parts of peppermint, 30 parts of Jasmine, 450 parts of ethyl alcohol.Preparation method and embodiment 1 It is identical.
Comparative example 2
A kind of Frankliniella occidentalis plant-originated repellent, is made of raw material from the following weight: 105 parts of Radical Injury in Wampee Seeds, octagonal leaf 125 parts, 95 parts of rosin, 100 parts of neem tree skin, golden 115 parts of waist arrow, 120 parts of white radishes, 105 parts of cherry leaf, tomato leaf 100 parts, 90 parts of Alocasia ordora, 75 parts of Ageratum conyzoides, 70 parts of Ageratum conyzoides, 85 parts of peppermint, 100 parts of Jasmine, 615 parts of ethyl alcohol.Its preparation side Method is same as Example 1.
Repellent effect experiment
1, experimental method
8 cells will be divided into the long bean field of one piece of unified management, test is arranged 8 processing altogether, each processing it is small Area's area is 100m2, repellant made from Examples 1 to 5 and comparative example 1~2 is tested, another set is as blank Group, sprays the clear water of equivalent, does not apply any drug.Spray is made in Frankliniella occidentalis repellant to handle, is being located respectively Before reason, 3 after processing, in 6,9 days investigation cells Frankliniella occidentalis adult quantity, each processing 3 repetitions of setting.
2, repellent effect
Revision insect recluced rate (%)=[(worm amount after worm amount-processing before handling)/worm amount before handling] × 100%
Repellent effect (%)=[(treatment region Revision insect recluced rate-check plot Revision insect recluced rate)/(check plot 1- insect population decline Rate)] × 100%.Repellent effect is as shown in 1 under table.
Repellent effect of 1 repellant of table to Frankliniella occidentalis
Shown compared with blank control group by 1 experimental data of table, made from the embodiment of the present application 1~5 and comparative example 1~2 Repellant is significant to the repellent effect of Frankliniella occidentalis;Repellent effect of the Frankliniella occidentalis repellant to Frankliniella occidentalis made from the application Quite, repellent effect gradually decreases as time increases after spraying, compared with comparative example 1 and comparative example 2, to Frankliniella occidentalis Repellent effect it is significant, and the repellent action time is longer.
In conclusion the raw materials used present invention is pure natural substance, it is processed after Frankliniella occidentalis repellant activity Ingredient is plant extracts, nontoxic to people and animals, no pollution to the environment, and has stronger anti-repelling properties to Frankliniella occidentalis, The preparation and use of the Frankliniella occidentalis repellant are all more convenient, are a kind of safe and efficient, environmentally friendly Frankliniella occidentalis repellants.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie In the case where without departing from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, nothing By from the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended Claim rather than above description limit, it is intended that by the institute in the meaning and scope for the equivalent loins for falling in claim It changes and includes within protection scope of the present invention.

Claims (10)

1. a kind of Frankliniella occidentalis plant-originated repellent, which is characterized in that be made of raw material from the following weight: Radical Injury in Wampee Seeds 55~ 95 parts, octagonal 65~105 parts of leaf, 50~80 parts of rosin, 50~80 parts of neem tree skin, golden 60~100 parts of waist arrow, white radishes 60~ 100 parts, 45~95 parts of cherry leaf, 45~95 parts of tomato leaf, 35~85 parts of Alocasia ordora, 25~65 parts of Ageratum conyzoides, Ageratum conyzoides 25 ~65 parts, 35~75 parts of peppermint, 40~90 parts of Jasmine, 500~600 parts of ethyl alcohol.
2. a kind of Frankliniella occidentalis plant-originated repellent according to claim 1, which is characterized in that by the original of following parts by weight Material is made: 65~85 parts of Radical Injury in Wampee Seeds, octagonal 75~95 parts of leaf, 60~70 parts of rosin, 60~70 parts of neem tree skin, golden waist arrow 70 ~90 parts, 70~90 parts of white radishes, 55~85 parts of cherry leaf, 55~85 parts of tomato leaf, 45~75 parts of Alocasia ordora, Ageratum conyzoides 35 ~55 parts, 35~55 parts of Ageratum conyzoides, 45~65 parts of peppermint, 50~80 parts of Jasmine, 520~580 parts of ethyl alcohol.
3. a kind of Frankliniella occidentalis plant-originated repellent according to claim 1, which is characterized in that by the original of following parts by weight Material is made: 75 parts of Radical Injury in Wampee Seeds, octagonal 85 parts of leaf, 65 parts of rosin, 65 parts of neem tree skin, golden 80 parts of waist arrow, 80 parts of white radishes, cherry 70 parts of peach leaves, 70 parts of tomato leaf, 60 parts of Alocasia ordora, 45 parts of Ageratum conyzoides, 45 parts of Ageratum conyzoides, 55 parts of peppermint, 65 parts of Jasmine, second 550 parts of alcohol.
4. described in any item a kind of Frankliniella occidentalis plant-originated repellents according to claim 1~3, it is characterised in that: the sea Taro is root, stem, the leaf for being grown in the nonirrigated farmland Alocasia ordora having abundant water resources;The percent by volume of the ethyl alcohol is 95%.
5. a kind of preparation method of Frankliniella occidentalis plant-originated repellent according to claim 4, which is characterized in that including with Lower step:
(1) golden waist arrow, white radishes, cherry leaf, tomato leaf, Alocasia ordora, Ageratum conyzoides, Ageratum conyzoides and thin are weighed according to parts by weight Lotus, is cut into the segment of 2~3cm long, and the clear water of golden 5~6 times of weight of waist arrow is added, turn after high fire is boiled small fire continue decoction 3~ 5h, decompression filter and obtain filtrate and filter residue;
(2) Radical Injury in Wampee Seeds, octagonal leaf, neem tree skin and Jasmine are sent into drying machine drying, the filter residue of step (1) is added, stirs Ethyl alcohol is added after mixing uniformly and impregnates 24~30h, first ultrasonic wave extraction, then 6~7h of refluxing extraction at 60~65 DEG C, is re-fed into The mixed liquor of 200~300 meshes was ground into grinder;
(3) rosin is placed under 60~65 DEG C of environment and is placed up to being completely melt, under stirring, the rosin of fusing is slowly added In the filtrate for entering step (1), 2~4h is kept the temperature at 55~60 DEG C, the mixed liquor of step (2) is then added, and after mixing evenly, is risen For temperature to 60~65 DEG C and 3~5h of isothermal holding, the Frankliniella occidentalis plant source is made in ultrasonication, cooled to room temperature Repellant.
6. a kind of preparation method of Frankliniella occidentalis plant-originated repellent according to claim 1, it is characterised in that: in step (2), the frequency of the ultrasonic wave extraction is 0.2~0.6MHz, and power is 600~700W, and the time is 45~55min.
7. a kind of preparation method of Frankliniella occidentalis plant-originated repellent according to claim 1, it is characterised in that: in step (2), the temperature of the drying is 55~60 DEG C, and the time is 150~200min, and being dried to material moisture is 20~25%.
8. a kind of preparation method of Frankliniella occidentalis plant-originated repellent according to claim 1, it is characterised in that: in step (2), the pressure of the grinding is 0.3~0.7MPa, and the time is 35~45min.
9. a kind of preparation method of Frankliniella occidentalis plant-originated repellent according to claim 1, it is characterised in that: in step (2) and (3), the speed of the stirring are 200~250r/min.
10. a kind of preparation method of Frankliniella occidentalis plant-originated repellent according to claim 1, it is characterised in that: in step Suddenly (3), the process conditions of the ultrasonication: frequency be 0.6~1.0MHz, power be 800~900W, the time be 30~ 40min。
CN201811428158.3A 2018-11-27 2018-11-27 A kind of Frankliniella occidentalis plant-originated repellent and preparation method thereof Pending CN109527000A (en)

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CN111296437A (en) * 2020-04-01 2020-06-19 浙江省农业科学院 Repellent for frankliniella occidentalis and application of active ingredients of repellent
CN113661986A (en) * 2021-09-03 2021-11-19 福建省农业科学院植物保护研究所 Specific repellent for preventing and controlling insect gall thrips on ficus plants

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CN111296437A (en) * 2020-04-01 2020-06-19 浙江省农业科学院 Repellent for frankliniella occidentalis and application of active ingredients of repellent
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Application publication date: 20190329