CN108902209A - A kind of vegetable cultivation vegetable insecticide and preparation method thereof - Google Patents
A kind of vegetable cultivation vegetable insecticide and preparation method thereof Download PDFInfo
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- CN108902209A CN108902209A CN201810658170.7A CN201810658170A CN108902209A CN 108902209 A CN108902209 A CN 108902209A CN 201810658170 A CN201810658170 A CN 201810658170A CN 108902209 A CN108902209 A CN 108902209A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/20—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom three- or four-membered rings
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/14—Celastraceae [Staff-tree or Bittersweet family], e.g. spindle tree, bittersweet or thunder god vine
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/002—Solid waste from mechanical processing of material, e.g. seed coats, olive pits, almond shells, fruit residue, rice hulls
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a kind of vegetable cultivation vegetable insecticides and preparation method thereof, are related to field of agricultural cultivation, the raw material including following parts by weight meter：20-26 parts of Celastrus angulatus, 4-9 parts of azedarach, 6-12 parts of radix tetrastigme, 3-8 parts of the fruit of Rangoon creeper, 6-12 parts of elm bark powder, 4-9 parts of fructus ulmi, 5-10 parts of Dysosma versipellis, 10-16 parts of derris root, 2-5 parts of granatum, 3-8 parts of rhizome of cyrtomium, 2-5 parts of orange peel, 5-10 parts of onion, 3-8 parts of Chinese gall, 1.1-1.6 parts of surfactant and 0.4-0.8 parts of preservative；Insecticide of the present invention is prepared as a raw material with natural plants, is acted on by the coordinated between raw material, insecticidal range is wide, and effect is good, and medicament noresidue is environmentally protective.
Description
Technical field
The present invention relates to field of agricultural cultivation, and in particular to a kind of vegetable cultivation vegetable insecticide and preparation method thereof.
Background technique
Insecticide is mainly used for preventing and treating the drug of agricultural pests and urban health insect.Usage history is long-range, dosage is big, product
Kind is more, and in twentieth century, agriculture rapid development, insecticide enables farm output rise higher.In agricultural and forestry pest control
Chemical insecticide is largely used in the process, high production cost, efficacy time is short, while soil and water resource being caused seriously to pollute,
Environmental pollution is serious.And the production method of these chemical pesticides is complicated, has serious environmental pollution in production process, uses
It is long in the surface detention time of grain, vegetables, melon and fruit, herbage etc., it is difficult to decompose after these insecticides.As people's environment is anticipated
The enhancing of knowledge and food-safe needs, the whole society especially agriculture, woods, the animal husbandry producer are badly in need of efficiently, low toxicity, environment friend
Good insecticide.
Chinese patent CN105638767B discloses a kind of high efficacy pesticide for plant and preparation method thereof, in raw material containing with
The bulk pharmaceutical chemicals of lower parts by weight：50-100 parts of chinaberry, 50-100 parts of granatum, 50-100 parts of the fruit of glossy privet, 40-80 parts of tripterygium wilfordii,
30-70 parts of capsicum annum fasciculatum, 10-60 parts of tobacco leaf.By above-mentioned raw materials by extracting, being concentrated, auxiliary agent is added, vegetable insecticide is made.Tool
Have simple production process, material source is extensive, to people, animal, harmless, crop using it is safe the advantages that；It is sprayed on crop and is easy
It decomposes, avoids retaining residual hazard, reduce environmental pollution, but material composition is few in the present invention, insecticidal spectrum is narrow.
Chinese patent CN102626116B discloses vegetative insecticide and preparation method thereof, each component and constituent mass
Percentage is：Eucalyptol mother liquor 1-30%, emulsifier 5-20%, surplus are dehydrated alcohol, and preparation method includes the following steps：Eucalyptus
The preparation and mixture of olein mother liquor, the present invention are matched using blue gum using Chinese herbal medicines such as rhizoma atractylodis as primary raw material, and mother liquor is processed into extraction,
The auxiliary agents such as emulsifier and dehydrated alcohol are added.The toxicity of agents useful for same is smaller, not only environmentally friendly but also safety when operating with, but this hair
The preventive effect of bright insecticide is lower.
Summary of the invention
Aiming at the problems existing in the prior art, the present invention provides a kind of vegetable cultivation vegetable insecticide and its preparations
Method, insecticide of the present invention are prepared as a raw material with natural plants, are acted on by the coordinated between raw material, insecticidal range
Extensively, effect is good, medicament noresidue, environmentally protective.
In order to achieve the above object, the present invention is achieved through the following technical solutions：
A kind of vegetable cultivation vegetable insecticide, the raw material including following parts by weight meter；
20-26 parts of Celastrus angulatus, 4-9 parts of azedarach, 6-12 parts of radix tetrastigme, 3-8 parts of the fruit of Rangoon creeper, 6-12 parts of elm bark powder, grassland
Sprout 4-9 parts, 5-10 parts of Dysosma versipellis, 10-16 parts of derris root, 2-5 parts of granatum, 3-8 parts of rhizome of cyrtomium, 2-5 parts of orange peel, onion 5-10
Part, 3-8 parts of Chinese gall, 1.1-1.6 parts of surfactant and 0.4-0.8 parts of preservative.
Preferably, the raw material including following parts by weight meter：22-24 parts of Celastrus angulatus, 5-8 parts of azedarach, 8-10 parts of radix tetrastigme,
4-7 parts of the fruit of Rangoon creeper, 5-8 parts of fructus ulmi, 6-9 parts of Dysosma versipellis, 12-14 parts of derris root, 3-4 parts of granatum, is passed through 8-10 parts of elm bark powder
4-7 parts many, 3-4 parts of orange peel, 6-9 parts of onion, 4-7 parts of Chinese gall, 1.2-1.5 parts of surfactant and preservative 0.5-0.7
Part.
Preferably, the raw material including following parts by weight meter：23 parts of Celastrus angulatus, 7 parts of azedarach, 9 parts of radix tetrastigme, the fruit of Rangoon creeper 6
Part, 9 parts of elm bark powder, 6 parts of fructus ulmi, 8 parts of Dysosma versipellis, 13 parts of derris root, 3.5 parts of granatum, 6 parts of rhizome of cyrtomium, 3.5 parts of orange peel,
8 parts of onion, 6 parts of Chinese gall, 1.4 parts of surfactant and 0.6 part of preservative.
Preferably, the surfactant is fatty alcohol polyethenoxy ether class, alkylphenol glymes, sulfonate
At least one of class, hard acid esters, amides and organic silicon.
Preferably, the organosilicone surfactants are dimethyl polysiloxane, methyl phenyl silicone, silicon containing chlorine
One or more of oil, ring dress polysiloxanes, Organosilicon wax and methyl polysiloxane combine.
Preferably, the preservative is one in sodium benzoate, potassium sorbate, p-hydroxybenzoate and sodium dehydroacetate
Kind or several combinations.
A kind of preparation method of above-mentioned vegetable cultivation vegetable insecticide is also disclosed in the present invention, specifically, including with
Lower step：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum,
Grain diameter is crushed to less than 2 millimeters in rhizome of cyrtomium, orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) it after organic solvent immersion being added 5 hours in the mixed powder in step (2), is placed in water bath sonicator pot and heats
3-5 hours, 70-75 degrees Celsius of water bath sonicator pot temperature, filtering obtained filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried,
With surplus stock mixed grinding 30-60 minutes, packaging envelope modeling to get the vegetable cultivation vegetable insecticide.
Preferably, the ethanol water that the organic solvent in the step (3) is 78%-85%
Preferably, the dosage of the ethanol water is mixed powder 15-20 times of weight.
Preferably, spray drying to moisture content is lower than 3% in the step (5).
The present invention has following beneficial effect：
(1) insecticide of the present invention is prepared as a raw material with natural plants, is acted on by the coordinated between raw material, desinsection
Range is wide, and effect is good, and medicament noresidue is environmentally protective.
(2) it is added with derris root in raw material of the present invention, contains active principle rotenone in derris root, rotenone has insect
Action of contace poison, insecticidal spectrum is wide, and rotenone gradually decomposes at ambient, does not stay residual.
(3) it is added with onion in the present invention, a kind of oil volatile substances of allyl sulfides are contained in onion, are distributed pungent
Simple pungent has the function of antibacterial expelling parasite, and in onion needed for the crops such as riboflavin rich in, calcium, phosphorus, iron, selenium
Nutriment can promote the growth of crop.
(4) Celastrus angulatus is added in raw material of the present invention, the insecticidal active ingredient contained in Celastrus angulatus is mainly with β-dihydro
Agarofuran is the polyol ester of skeleton, comprehensive to insect tool there are three types of activity, i.e. antifeedant activity, narcotic activity and cytotoxicity
Cooperation is with good insecticidal effect.
(5) vegetable insecticide of the present invention not only can be with sterilization and disinfestation, simultaneously containing organic matter rich in insecticide
It can promote plant growth for plant absorption with nutrient, waste plant medicine dregs produced during the preparation process can be used as agriculture
Crop-planting fertilizer, raw material utilize abundant, energy conservation and environmental protection.
Specific embodiment
Below with reference to embodiment, further description of the specific embodiments of the present invention, and following embodiment is only used for more
Technical solution of the present invention is clearly demonstrated, and not intended to limit the protection scope of the present invention.
Embodiment 1
A kind of vegetable cultivation vegetable insecticide, the raw material including following parts by weight meter；
20 parts of Celastrus angulatus, 4 parts of azedarach, 6 parts of radix tetrastigme, 3 parts of the fruit of Rangoon creeper, 6 parts of elm bark powder, 4 parts of fructus ulmi, Dysosma versipellis 5
Part, 10 parts of derris root, 2 parts of granatum, 3 parts of rhizome of cyrtomium, 2 parts of orange peel, 5 parts of onion, 3 parts of Chinese gall, 1.1 parts of surfactant and
0.4 part of preservative.
Surfactant is fatty alcohol polyethenoxy ether class.
Preservative is sodium benzoate.
The preparation method of vegetable cultivation vegetable insecticide in the present embodiment specifically includes the following steps：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum,
Grain diameter is crushed to less than 2 millimeters in rhizome of cyrtomium, orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) it after organic solvent immersion being added 5 hours in the mixed powder in step (2), is placed in water bath sonicator pot and heats 3
Hour, 70 degrees Celsius of water bath sonicator pot temperature, filtering obtains filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried,
With surplus stock mixed grinding 30 minutes, packaging envelope modeling to get the vegetable cultivation vegetable insecticide.
The ethanol water that organic solvent in step (3) is 78%
The dosage of ethanol water is 15 times of weight of mixed powder.
Spray drying to moisture content is lower than 3% in step (5).
Embodiment 2
A kind of vegetable cultivation vegetable insecticide, the raw material including following parts by weight meter；
26 parts of Celastrus angulatus, 9 parts of azedarach, 12 parts of radix tetrastigme, 8 parts of the fruit of Rangoon creeper, 12 parts of elm bark powder, 9 parts of fructus ulmi, Dysosma versipellis
10 parts, 16 parts of derris root, 5 parts of granatum, 8 parts of rhizome of cyrtomium, 5 parts of orange peel, 10 parts of onion, 8 parts of Chinese gall, surfactant 1.6
Part and 0.8 part of preservative.
Surfactant is Sulfonates and hard acid esters according to mass ratio 1:1 mixing composition.
Preservative is potassium sorbate.
The preparation method of vegetable cultivation vegetable insecticide in the present embodiment specifically includes the following steps：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum,
Grain diameter is crushed to less than 2 millimeters in rhizome of cyrtomium, orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) it after organic solvent immersion being added 5 hours in the mixed powder in step (2), is placed in water bath sonicator pot and heats
3-5 hours, 73 degrees Celsius of water bath sonicator pot temperature, filtering obtained filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried,
With surplus stock mixed grinding 40 minutes, packaging envelope modeling to get the vegetable cultivation vegetable insecticide.
The ethanol water that organic solvent in step (3) is 85%
The dosage of ethanol water is 20 times of weight of mixed powder.
Spray drying to moisture content is lower than 3% in step (5).
Embodiment 3
A kind of vegetable cultivation vegetable insecticide, the raw material including following parts by weight meter；
22 parts of Celastrus angulatus, 5 parts of azedarach, 8 parts of radix tetrastigme, 4 parts of the fruit of Rangoon creeper, 8 parts of elm bark powder, 5 parts of fructus ulmi, Dysosma versipellis 6
Part, 12 parts of derris root, 3 parts of granatum, 4 parts of rhizome of cyrtomium, 3 parts of orange peel, 6 parts of onion, 4 parts of Chinese gall, 1.2 parts of surfactant and
0.5 part of preservative.
Surfactant is dimethyl polysiloxane.
Preservative is p-hydroxybenzoate.
The preparation method of vegetable cultivation vegetable insecticide in the present embodiment specifically includes the following steps：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum,
Grain diameter is crushed to less than 2 millimeters in rhizome of cyrtomium, orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) it after organic solvent immersion being added 5 hours in the mixed powder in step (2), is placed in water bath sonicator pot and heats
3-5 hours, 73 degrees Celsius of water bath sonicator pot temperature, filtering obtained filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried,
With surplus stock mixed grinding 50 minutes, packaging envelope modeling to get the vegetable cultivation vegetable insecticide.
The ethanol water that organic solvent in step (3) is 83%
The dosage of ethanol water is 18 times of weight of mixed powder.
Spray drying to moisture content is lower than 3% in step (5).
Embodiment 4
A kind of vegetable cultivation vegetable insecticide, the raw material including following parts by weight meter；
24 parts of Celastrus angulatus, 8 parts of azedarach, 10 parts of radix tetrastigme, 7 parts of the fruit of Rangoon creeper, 10 parts of elm bark powder, 8 parts of fructus ulmi, Dysosma versipellis
9 parts, 14 parts of derris root, 4 parts of granatum, 7 parts of rhizome of cyrtomium, 4 parts of orange peel, 9 parts of onion, 7 parts of Chinese gall, 1.5 parts of surfactant
With 0.7 part of preservative.
Surfactant is methyl phenyl silicone and silicone oil containing chlorine according to mass ratio 1:1 mixing composition.
Preservative is sodium dehydroacetate.
The preparation method of vegetable cultivation vegetable insecticide in the present embodiment specifically includes the following steps：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum,
Grain diameter is crushed to less than 2 millimeters in rhizome of cyrtomium, orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) it after organic solvent immersion being added 5 hours in the mixed powder in step (2), is placed in water bath sonicator pot and heats 4
Hour, 70-75 degrees Celsius of water bath sonicator pot temperature, filtering obtains filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried,
With surplus stock mixed grinding 45 minutes, packaging envelope modeling to get the vegetable cultivation vegetable insecticide.
The ethanol water that organic solvent in step (3) is 83%
The dosage of ethanol water is 19 times of weight of mixed powder.
Spray drying to moisture content is lower than 3% in step (5).
Embodiment 5
A kind of vegetable cultivation vegetable insecticide, the raw material including following parts by weight meter；
23 parts of Celastrus angulatus, 7 parts of azedarach, 9 parts of radix tetrastigme, 6 parts of the fruit of Rangoon creeper, 9 parts of elm bark powder, 6 parts of fructus ulmi, Dysosma versipellis 8
Part, 13 parts of derris root, 3.5 parts of granatum, 6 parts of rhizome of cyrtomium, 3.5 parts of orange peel, 8 parts of onion, 6 parts of Chinese gall, surfactant 1.4
Part and 0.6 part of preservative.
Surfactant is that ring fills polysiloxanes.
Preservative is p-hydroxybenzoate.
The preparation method of vegetable cultivation vegetable insecticide in the present embodiment specifically includes the following steps：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum,
Grain diameter is crushed to less than 2 millimeters in rhizome of cyrtomium, orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) it after organic solvent immersion being added 5 hours in the mixed powder in step (2), is placed in water bath sonicator pot and heats
4.5 hours, 73 degrees Celsius of water bath sonicator pot temperature, filtering obtained filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried,
With surplus stock mixed grinding 50 minutes, packaging envelope modeling to get the vegetable cultivation vegetable insecticide.
The ethanol water that organic solvent in step (3) is 84%
The dosage of ethanol water is 17 times of weight of mixed powder.
Spray drying to moisture content is lower than 3% in step (5).
By vegetable cultivation vegetable insecticide made from embodiment 1-5 and city head with chemical insecticide according to 1:800
It is tested for the property after dilution proportion, test result is as follows：
| Test group | Prevention and control of aphids rate | Red spider control rate | Leaf miner control rate | Swallowtail butterfly caterpillar control rate |
| Embodiment 1 | 78 | 81 | 86 | 80 |
| Embodiment 2 | 82 | 76 | 81 | 79 |
| Embodiment 3 | 85 | 80 | 85 | 81 |
| Embodiment 4 | 87 | 82 | 84 | 82 |
| Embodiment 5 | 90 | 85 | 88 | 83 |
| Control group | 76 | 81 | 80 | 73 |
In conclusion the present invention has the following advantages that：
(1) insecticide of the present invention is prepared as a raw material with natural plants, is acted on by the coordinated between raw material, desinsection
Range is wide, and effect is good, and medicament noresidue is environmentally protective.
(2) it is added with derris root in raw material of the present invention, contains active principle rotenone in derris root, rotenone has insect
Action of contace poison, insecticidal spectrum is wide, and rotenone gradually decomposes at ambient, does not stay residual.
(3) it is added with onion in the present invention, a kind of oil volatile substances of allyl sulfides are contained in onion, are distributed pungent
Simple pungent has the function of antibacterial expelling parasite, and in onion needed for the crops such as riboflavin rich in, calcium, phosphorus, iron, selenium
Nutriment can promote the growth of crop.
(4) Celastrus angulatus is added in raw material of the present invention, the insecticidal active ingredient contained in Celastrus angulatus is mainly with β-dihydro
Agarofuran is the polyol ester of skeleton, comprehensive to insect tool there are three types of activity, i.e. antifeedant activity, narcotic activity and cytotoxicity
Cooperation is with good insecticidal effect.
(5) vegetable insecticide of the present invention not only can be with sterilization and disinfestation, simultaneously containing organic matter rich in insecticide
It can promote plant growth for plant absorption with nutrient, waste plant medicine dregs produced during the preparation process can be used as agriculture
Crop-planting fertilizer, raw material utilize abundant, energy conservation and environmental protection.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of vegetable cultivation vegetable insecticide, which is characterized in that the raw material including following parts by weight meter：Celastrus angulatus 20-26
Part, 4-9 parts of azedarach, 6-12 parts of radix tetrastigme, 3-8 parts of the fruit of Rangoon creeper, 6-12 parts of elm bark powder, 4-9 parts of fructus ulmi, Dysosma versipellis 5-10
Part, 10-16 parts of derris root, 2-5 parts of granatum, 3-8 parts of rhizome of cyrtomium, 2-5 parts of orange peel, 5-10 parts of onion, 3-8 parts of Chinese gall, table
Activating agent 1.1-1.6 parts and preservative 0.4-0.8 parts of face.
2. vegetable cultivation vegetable insecticide according to claim 1, which is characterized in that the original including following parts by weight meter
Material：22-24 parts of Celastrus angulatus, 5-8 parts of azedarach, 8-10 parts of radix tetrastigme, 4-7 parts of the fruit of Rangoon creeper, 8-10 parts of elm bark powder, fructus ulmi 5-8
Part, 6-9 parts of Dysosma versipellis, 12-14 parts of derris root, 3-4 parts of granatum, 4-7 parts of rhizome of cyrtomium, 3-4 parts of orange peel, 6-9 parts, five times of onion
4-7 parts sub-, 1.2-1.5 parts of surfactant and 0.5-0.7 parts of preservative.
3. vegetable cultivation vegetable insecticide according to claim 1, which is characterized in that the original including following parts by weight meter
Material：23 parts of Celastrus angulatus, 7 parts of azedarach, 9 parts of radix tetrastigme, 6 parts of the fruit of Rangoon creeper, 9 parts of elm bark powder, 6 parts of fructus ulmi, 8 parts of Dysosma versipellis, fish
13 parts of rattan root, 3.5 parts of granatum, 6 parts of rhizome of cyrtomium, 3.5 parts of orange peel, 8 parts of onion, 6 parts of Chinese gall, 1.4 parts of surfactant and
0.6 part of preservative.
4. vegetable cultivation vegetable insecticide according to claim 1, which is characterized in that the surfactant is fat
In alcohol polyethenoxy ether class, alkylphenol glymes, Sulfonates, hard acid esters, amides and organic silicon at least
It is a kind of.
5. according to regard to vegetable cultivation vegetable insecticide described in claim 1, which is characterized in that the organic silicon surface is living
Property agent be dimethyl polysiloxane, methyl phenyl silicone, silicone oil containing chlorine, ring fills polysiloxanes, Organosilicon wax and methyl gather
One or more of siloxanes combines.
6. vegetable cultivation vegetable insecticide according to claim 1, which is characterized in that the preservative is benzoic acid
One or more of sodium, potassium sorbate, p-hydroxybenzoate and sodium dehydroacetate combine.
7. a kind of preparation method of vegetable cultivation vegetable insecticide as claimed in any one of claims 1 to 6, which is characterized in that
Include the following steps：
(1) each raw material is weighed according to the raw material weight number of above-mentioned vegetable cultivation vegetable insecticide；
(2) by Celastrus angulatus, azedarach, radix tetrastigme, the fruit of Rangoon creeper, elm bark powder, fructus ulmi, Dysosma versipellis, derris root, granatum, rhizome of cyrtomium,
Grain diameter is crushed to less than 2 millimeters in orange peel and Chinese gall mixing investment pulverizer, obtains mixed powder；
(3) after organic solvent immersion being added 5 hours in the mixed powder in step (2), it is small to be placed in heating 3-5 in water bath sonicator pot
When, 70-75 degrees Celsius of water bath sonicator pot temperature, filtering obtains filtrate；
(4) onion is dialled skin to go in root addition pulverizer to crush, filtering squeezes, and obtains Conditions of Onion Juice；
(5) after mixing by Conditions of Onion Juice made from filtrate made from step (3) and step (4), it is concentrated, is spray-dried, and is surplus
Remaining raw material mixed grinding 30-60 minutes, packaging envelope modeling is to get the vegetable cultivation vegetable insecticide.
8. the preparation method of vegetable cultivation vegetable insecticide according to claim 7, which is characterized in that the step
(3) ethanol water that the organic solvent in is 78%-85%.
9. the preparation method of vegetable cultivation vegetable insecticide according to claim 8, which is characterized in that the ethanol water
The dosage of solution is mixed powder 15-20 times of weight.
10. the preparation method of vegetable cultivation vegetable insecticide according to claim 7, which is characterized in that the step
(5) spray drying to moisture content is lower than 3% in.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111133947A (en) * | 2020-02-07 | 2020-05-12 | 海南煊烨生物科技有限公司 | Cultivation method for promoting growth of machilus |
| CN114009429A (en) * | 2021-11-25 | 2022-02-08 | 张艳华 | Plant protective agent and preparation method and application thereof |
-
2018
- 2018-06-25 CN CN201810658170.7A patent/CN108902209A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111133947A (en) * | 2020-02-07 | 2020-05-12 | 海南煊烨生物科技有限公司 | Cultivation method for promoting growth of machilus |
| CN114009429A (en) * | 2021-11-25 | 2022-02-08 | 张艳华 | Plant protective agent and preparation method and application thereof |
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