CN109700754B - Preparation method of face protection spray - Google Patents
Preparation method of face protection spray Download PDFInfo
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Abstract
The invention provides a face protection spray, which is prepared into an air pressure spray by respectively mixing, homogenizing, controlling the temperature and the like of the components through operations of mixing, homogenizing, and the like, and is convenient to use and convenient for outdoor use.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a preparation method of a face protection spray.
Background
The skin care and nursing is always the focus of attention of the vast females, and the pursuit goal of the vast females is to delay aging, whiten and beautify the skin without generating any side effect. In modern life, radiation from computers, televisions, and cell phones severely affects facial health, and the increasingly deteriorating environment further affects skin health. Professor Krutmann et al (Pollution and skin: From epidemic and structural students to clinical applications, Journal of biological Science, 2014 12, vol.76, No. 3: 163-168) found that ultraviolet rays, ozone, PM10, PM2.5 and other particulate matters in the air can act together to cause the skin barrier to change, the secretion of inflammatory factors and the activation of various aromatic hydrocarbon receptors, thereby causing various skin aging problems such as the loss of collagen and the formation of pigment of various skins. Since the particles of PM2.5 are small and can easily penetrate the skin, the carried free radicals can cause oxidative stress damage inside the skin, so that proteins, lipids and DNA in cells are oxidized, degraded or reduced in activity to different degrees. Therefore, skin care is not only the goal of beauty ladies, but also the problem that all people pay attention to.
The skin is the first barrier of the human body, protecting tissues and organs in the body from external mechanical, physical, chemical or biological attacks or irritations. The face is the most exposed to the air, and is the face of a person, and the face is most damaged, and is also the most protected part. Research shows that no matter which skin belongs to, 90% of the skin has water shortage, so that moisturizing and water replenishing are the basis of skin care, and elasticity and smoothness of the skin can be improved through water replenishing, so that the aim of preventing aging is fulfilled. On the other hand, even though moisturizing can prevent aging to some extent, with the increase of age, cellular and structural damage of the skin occurs, which is manifested by a decrease in collagen fibers, a loss of elastin fibers and an increase in unaligned elastin fibers, an increase in proteoglycan content, a low adipocyte density of the subcutaneous tissue, etc., resulting in the formation of wrinkles, brown spots, etc. Therefore, there is a need for further delaying skin aging, generally in three ways: first, photodamage is avoided with sunscreen products containing sunscreens of chemical or physical spectrum; secondly, performing daily care by using cosmetics containing anti-aging functional components so as to delay or eliminate aging marks; third, if the skin is severely aged, invasive means are required for treatment, such as laser assisted strong acid stripping, injection of botulinum toxin type A or a filler, etc.
It can be seen that there are various needs for facial skin care, and most of the skin care products on the market today have single efficacy and often contain some unsafe ingredients, for example, patent application CN103690428A discloses a moisturizing and repairing skin care lotion comprising the following ingredients in weight percentage: 80-90% of water, 0.5-2% of propylene glycol, 1-3.0% of PEG-40 hydrogenated castor oil, 0.5-2% of butanediol, 0.02-0.03% of sodium hyaluronate, 0.05-0.3% of dipotassium glycyrrhizinate, 2-5% of glycerol, 1-5% of lily bulb extract, 0.2-0.6% of methylparaben, 0.5-3% of chamomile extract, 0.05-0.3% of dicetyl phosphate, 0.2% of phospholipid and 0.1-0.2% of essence. The moisturizing and repairing skin moisturizer disclosed by the invention is suitable for the skin after being dried in the sun, can supplement the moisture required by the skin, can repair the skin which is sunburned, promotes the regeneration of new cells, makes the skin soft and tender, and moisturizes the skin. Patent application CN105520873A discloses a traditional Chinese medicine anti-aging skin cream, which takes scutellaria baicalensis extract and total salvianolic acid as main raw materials, and also comprises poria cocos, codonopsis pilosula, skin nutrients, chamomile essence, soybean extract, a thickening agent and an antioxidant. In addition, for example, the world famous brand of xinel, opal and some new domestic brands of skin care products contain acrylamide, and the raw materials have a virulent effect on the nervous system, are carcinogens and are accepted by the biological world for a long time.
Disclosure of Invention
Based on the defects of the prior art, the anti-antagonism effect among different functional components is avoided through reasonable matching of various active components such as lactobacillus/soybean milk fermentation product filtrate, purslane extract, oat β -glucan, fullerene and perilla extract, the effect of the active components is fully exerted, water replenishing and moisture preserving can be realized, sun blocking and aging resistance can be realized, the repair function is realized, the facial skin is comprehensively protected, and the protective spray provided by the invention is mild in component and is particularly suitable for delicate sensitive facial skin.
The invention provides an ice muscle face protection spray which comprises the following components of lactobacillus/soybean milk fermentation product filtrate, purslane extract, hexapeptide-9, oat β -glucan, fullerene, perilla extract, allantoin, titanium dioxide, phenyl trimethicone, cyclopentadimethylsiloxane, butanediol, glycerol, C12-15 alcohol benzoate, cetyl PEG/PPG-10/1 polydimethylsiloxane, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, PEG-10 polydimethylsiloxane, sodium chloride, nicotinamide, silica, CI77492, disteardimonium hectorite, phenoxyethanol, CI77491, methylparaben, propylhydroxybenzoate, sodium polyglutamate, disodium EDTA, sodium hyaluronate and essence.
Further, the spray comprises the following components, by weight, 1-3 parts of lactobacillus/soybean milk fermentation product filtrate, 1-3 parts of purslane extract, 1-2 parts of hexapeptide-9, 1-2 parts of oat β -glucan, 0.1-1 part of fullerene, 0.1-1 part of perilla extract, 1-3 parts of allantoin, 100 parts of titanium dioxide, 100 parts of phenyl trimethicone, 100 parts of cyclopentadimethylsiloxane, 100 parts of butanediol, 80-100 parts of glycerol, 20-40 parts of C12-15 alcohol benzoate, 20-40 parts of cetyl PEG/PDMS-10/1 polydimethylsiloxane, 10-30 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 10-20 parts of PEG-10 polydimethylsiloxane, 10-20 parts of sodium chloride, 5-10 parts of nicotinamide, 5-10 parts of silica, 3-8 parts of CI77492, 3-6 parts of lithium stearate, 3-5 parts of dimethylammonium dimethyl benzoate, 77491-1.1-1 part of PEG-1 part of sodium hydroxybenzoate, 1-1.1-1 part of sodium glutamate, 1-1 part of sodium hyaluronate, 1.1-1 part of EDTA, 1 part of sodium hydroxide, 1 part of sodium benzoate and 1 part of sodium glutamate.
Furthermore, the spray comprises the following components, by weight, 1.5-2.5 parts of lactobacillus/soybean milk fermentation product filtrate, 1.5-2.5 parts of purslane extract, 1.2-1.8 parts of hexapeptide-9, 1.2-1.8 parts of oat β -glucan, 0.4-0.8 part of fullerene, 0.4-0.8 part of perilla extract, 1.5-2.5 parts of allantoin, 105-115 parts of titanium dioxide, 105-115 parts of phenyl trimethicone, 105-115 parts of cyclopentadimethylsiloxane, 105-115 parts of butanediol, 85-95 parts of glycerol, 25-35 parts of C12-15 alcohol benzoate, 25-35 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 15-25 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 12-18 parts of PEG-10 parts of polydimethylsiloxane, 12-18 parts of sodium chloride, 6-9 parts of silica, 6-9 parts of 7747-92 parts of silica, 4-7 parts of CI-4.8 parts of sodium hydroxybenzoate, 0.8-2 parts of sodium glutamate, 0.5-2 parts of CI-2-8 parts of sodium hydroxybenzoate, 0.8 parts of sodium glutamate, 0.8-2 parts of sodium benzoate, 0.8 parts of sodium hydroxybenzoate, 0-8 parts of sodium glutamate, 0.8 parts of sodium alginate, 0-8 parts of sodium alginate, 0-2 parts of sodium alginate, 1.
Furthermore, the spray comprises the following components, by weight, 2 parts of lactobacillus/soybean milk fermentation product filtrate, 2 parts of purslane extract, 1.5 parts of hexapeptide-9, 1.5 parts of oat β -glucan, 0.5 part of fullerene, 0.5 part of perilla extract, 2 parts of allantoin, 110 parts of titanium dioxide, 110 parts of phenyl trimethicone, 110 parts of cyclopentadimethylsiloxane, 110 parts of butanediol, 90 parts of glycerol, 30 parts of C12-15 alcohol benzoate, 30 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 20 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 15 parts of PEG-10 polydimethylsiloxane, 15 parts of sodium chloride, 7 parts of nicotinamide, 7 parts of silica, 6 parts of CI77492, 5 parts of disteardimonium ammonium montmorillonite, 4 parts of phenoxyethanol, 3 parts of CI77491, 1.5 parts of methylparaben, 1.5 parts of propylhydroxybenzoate, 0.6 parts of sodium polyglutamate, 0.6 parts of disodium EDTA, 0.6 parts of sodium hyaluronate, and 0.6 parts of essence.
The invention also provides a preparation method of the ice muscle protection spray, which comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, and mixing to obtain a mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, dimethicone/vinyl dimethicone crosspolymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 dimethicone, PEG-10 dimethicone, silica, propyl hydroxybenzoate to obtain mixture 2;
(3) adding the mixture 2 into the mixture 1 for homogenizing to obtain mixed emulsion;
(4) adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, and mixing.
Further, heating the materials in the step (1) to 75-85 ℃ and uniformly stirring.
Further, the temperature of the material in the step (1) is increased to 82 ℃.
Further, heating the materials in the step (2) to 75-80 ℃, and uniformly stirring.
Further, the temperature of the material in the step (2) is increased to 76 ℃.
Further, the homogenization time in the step (3) is 5-15min, and the temperature is kept for 20-40min after homogenization.
Further, in the step (4), after the temperature is reduced to 40-45 ℃, adding the oat β -glucan, the fullerene, the phenoxyethanol, the hexapeptide-9, the lactobacillus/soybean milk fermentation product filtrate, the purslane extract, the perilla extract and the essence, mixing and stirring for 25-30min to obtain the product.
Further, the stirring time in the step (4) is 28 min.
And (3) further, filling the semi-finished product in the step (4) with air by using an aluminum can after the semi-finished product is qualified.
The invention has the beneficial effects that:
(1) according to the invention, by adding various active ingredients such as lactobacillus/soybean milk fermentation product filtrate, purslane extract, oat β -glucan, fullerene and perilla extract, through reasonable matching, antagonistic action among different functional ingredients is avoided, the effect of the active ingredients is fully exerted, water can be supplemented and moisture preserved, sun protection and anti-aging can be realized, meanwhile, the repair function is also provided, the facial skin is comprehensively protected, and damage to air pollution and the like is avoided.
(2) The body spray provided by the invention contains natural active ingredients, and titanium dioxide is added, so that the effects of physical isolation and protection are achieved, meanwhile, the effect of modifying facial skin muscles is achieved, internal conditioning and external protection are realized, and the body spray is particularly suitable for outdoor use.
(3) The invention is prepared in a mode of air pressure spraying, is convenient to use and is particularly suitable for outdoor use.
Detailed Description
Example 1 Ice skin facial protective spray and method of making same
The spray comprises the following components, by weight, 2 parts of lactobacillus/soybean milk fermentation product filtrate, 2 parts of purslane extract, 1.5 parts of hexapeptide-9, 1.5 parts of oat β -glucan, 0.5 part of fullerene, 0.5 part of perilla extract, 2 parts of allantoin, 110 parts of titanium dioxide, 110 parts of phenyl trimethicone, 110 parts of cyclopentadimethylsiloxane, 110 parts of butanediol, 90 parts of glycerol, 30 parts of C12-15 alcohol benzoate, 30 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 20 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 15 parts of PEG-10 polydimethylsiloxane, 15 parts of sodium chloride, 7 parts of nicotinamide, 7 parts of silica, 6 parts of CI77492, 5 parts of disteardimonium hectorite, 4 parts of phenoxyethanol, 3 parts of CI77491, 1.5 parts of methylparaben, 1.5 parts of propylhydroxybenzoate, 0.6 parts of sodium polyglutamate, 0.6 parts of disodium EDTA, 0.6 parts of sodium hyaluronate, and 0.6 parts of essence.
The preparation method comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, heating to 82 deg.C, and mixing to obtain mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 polydimethylsiloxane, PEG-10 polydimethylsiloxane, silica and propylhydroxybenzoate, heating to 76 ℃, and uniformly mixing to obtain a mixture 2;
(3) adding the mixture 2 into the mixture 1, homogenizing for 10min, and keeping the temperature for 30min to obtain mixed emulsion;
(4) cooling the mixed emulsion to 40 deg.C, adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, mixing, stirring for 28min, inspecting semi-product, and bottling with aluminum bottle.
Example 2 Ice skin facial protective spray and method of making same
The spray comprises the following components, by weight, 1 part of lactobacillus/soybean milk fermentation product filtrate, 1 part of purslane extract, 1 part of hexapeptide-9, 1 part of oat β -glucan, 0.1 part of fullerene, 0.1 part of perilla extract, 1 part of allantoin, 100 parts of titanium dioxide, 105 parts of phenyl trimethicone, 105 parts of cyclopentadimethylsiloxane, 105 parts of butanediol, 85 parts of glycerol, 25 parts of C12-15 alcohol benzoate, 25 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 15 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 12 parts of PEG-10 polydimethylsiloxane, 10 parts of sodium chloride, 5 parts of nicotinamide, 5 parts of silica, 3 parts of CI77492, 3 parts of disteardimonium hectorite, 3.5 parts of phenoxyethanol, 2 parts of CI77491, 1 part of methylparaben, 1 part of propylhydroxybenzoate, 0.2 part of sodium polyglutamate, 0.2 part of disodium EDTA, 0.2 part of sodium hyaluronate essence, and 0.2 part of essence.
The preparation method comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, heating to 85 ℃, and uniformly mixing to obtain a mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 polydimethylsiloxane, PEG-10 polydimethylsiloxane, silica and propylhydroxybenzoate, heating to 80 ℃, and uniformly mixing to obtain a mixture 2;
(3) adding the mixture 2 into the mixture 1, homogenizing for 15min, and keeping the temperature for 40min to obtain mixed emulsion;
(4) cooling the mixed emulsion to 40 deg.C, adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, mixing, stirring for 30min, inspecting semi-product, and bottling with aluminum bottle.
Example 3 Ice skin facial protective spray and method of making same
The spray comprises the following components, by weight, 3 parts of lactobacillus/soybean milk fermentation product filtrate, 2.5 parts of purslane extract, 1.8 parts of hexapeptide-9, 2 parts of oat β -glucan, 1 part of fullerene, 1 part of perilla extract, 2.5 parts of allantoin, 115 parts of titanium dioxide, 115 parts of phenyl trimethicone, 120 parts of cyclopentadimethylsiloxane, 120 parts of butanediol, 100 parts of glycerol, 40 parts of C12-15 alcohol benzoate, 40 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 30 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 20 parts of PEG-10 polydimethylsiloxane, 18 parts of sodium chloride, 9 parts of nicotinamide, 9 parts of silica, 7 parts of CI77492, 5 parts of disteardimonium hectorite, 1.5 parts of phenoxyethanol, 5 parts of CI77491, 2 parts of methylparaben, 2 parts of propylhydroxybenzoate, 1 part of sodium polyglutamate, 1 part of EDTA disodium, 1 part of sodium hyaluronate essence, and 1 part of essence.
The preparation method comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, heating to 82 deg.C, and mixing to obtain mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 polydimethylsiloxane, PEG-10 polydimethylsiloxane, silica and propylhydroxybenzoate, heating to 76 ℃, and uniformly mixing to obtain a mixture 2;
(3) adding the mixture 2 into the mixture 1, homogenizing for 10min, and keeping the temperature for 30min to obtain mixed emulsion;
(4) cooling the mixed emulsion to 40 deg.C, adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, mixing, stirring for 28min, inspecting semi-product, and bottling with aluminum bottle.
Example 4 Ice skin facial protective spray and method of making same
The spray comprises the following components, by weight, 1.5 parts of lactobacillus/soybean milk fermentation product filtrate, 1.5 parts of purslane extract, 1.2 parts of hexapeptide-9, 1.2 parts of oat β -glucan, 0.4 part of fullerene, 0.4 part of perilla extract, 1.5 parts of allantoin, 105 parts of titanium dioxide, 100 parts of phenyl trimethicone, 100 parts of cyclopentadimethylsiloxane, 100 parts of butanediol, 80 parts of glycerol, 20 parts of C12-15 alcohol benzoate, 20 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 10 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 10 parts of PEG-10 polydimethylsiloxane, 12 parts of sodium chloride, 6 parts of nicotinamide, 6 parts of silica, 4 parts of CI77492, 4 parts of disteardimonium lithium hectorite, 3 parts of phenoxyethanol, 1 part of CI77491, 1 part of methylparaben, 1 part of hydroxypropyl hydroxybenzoate, 0.1 part of sodium polyglutamate, 0.1 part of disodium EDTA, 0.1 part of hyaluronic acid, and 0.1 part of essence.
The preparation method comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, heating to 75 ℃, and uniformly mixing to obtain a mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 polydimethylsiloxane, PEG-10 polydimethylsiloxane, silica and propylhydroxybenzoate, heating to 75 ℃, and uniformly mixing to obtain a mixture 2;
(3) adding the mixture 2 into the mixture 1, homogenizing for 5min, and keeping the temperature for 20min to obtain mixed emulsion;
(4) cooling the mixed emulsion to 42 deg.C, adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, mixing, stirring for 25min, inspecting semi-product, and bottling with aluminum bottle.
Example 5 Ice skin facial protective spray and method of making same
The spray comprises the following components, by weight, 2.5 parts of lactobacillus/soybean milk fermentation product filtrate, 3 parts of purslane extract, 2 parts of hexapeptide-9, 1.8 parts of oat β -glucan, 0.8 part of fullerene, 0.8 part of perilla extract, 3 parts of allantoin, 120 parts of titanium dioxide, 120 parts of phenyl trimethicone, 115 parts of cyclopentadimethylsiloxane, 115 parts of butanediol, 95 parts of glycerol, 35 parts of C12-15 alcohol benzoate, 35 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 25 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 18 parts of PEG-10 polydimethylsiloxane, 20 parts of sodium chloride, 10 parts of nicotinamide, 10 parts of silica, 8 parts of CI77492, 6 parts of disteardimonium montmorillonite, 5 parts of phenoxyethanol, 4 parts of CI77491, 2 parts of methylparaben, 2 parts of propylhydroxybenzoate, 0.8 parts of sodium polyglutamate, 0.8 parts of disodium EDTA, 0.8 parts of sodium hectorite, and 0.8 parts of essence.
The preparation method comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, heating to 82 deg.C, and mixing to obtain mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 polydimethylsiloxane, PEG-10 polydimethylsiloxane, silica and propylhydroxybenzoate, heating to 76 ℃, and uniformly mixing to obtain a mixture 2;
(3) adding the mixture 2 into the mixture 1, homogenizing for 10min, and keeping the temperature for 30min to obtain mixed emulsion;
(4) cooling the mixed emulsion to 40 deg.C, adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, mixing, stirring for 28min, inspecting semi-product, and bottling with aluminum bottle.
Comparative example 1 face protection spray without lactobacillus/soymilk fermentation product filtrate and method for preparing the same
The same procedure as in example 1 was repeated, except that the filtrate was not containing lactobacillus/soybean milk fermentation product.
Comparative example 2 facial protection spray without purslane extract and method of preparing the same
The same as example 1 except that the purslane extract was not contained.
Comparative example 3 face-protecting spray containing no hexapeptide-9 and method for preparing the same
The procedure is as in example 1 except that hexapeptide-9 is not included.
Comparative example 4 oat β -glucan free face-protective spray and method of making same
The same procedure as in example 1 was repeated, except that the oat β -glucan was not included.
Comparative example 5 face protection spray containing no titanium dioxide and method for preparing the same
The procedure is as in example 1 except that titanium dioxide is not contained.
Comparative example 6 Fullerene-free face-protective spray and method of making same
The procedure is as in example 1 except that the fullerene is not contained.
Comparative example 7 face protection spray containing no perilla extract and preparation method thereof
The same procedure as in example 1 was repeated, except that the perilla extract was not contained.
Comparative example 8 face protection spray prepared by different preparation methods and preparation method thereof
The formula is as follows: same as example 1
The preparation method comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, and mixing to obtain a mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, dimethicone/vinyl dimethicone crosspolymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 dimethicone, PEG-10 dimethicone, silica, propyl hydroxybenzoate are mixed uniformly to obtain mixture 2;
(3) adding the mixture 2 into the mixture 1, homogenizing for 10min, and keeping the temperature for 30min to obtain mixed emulsion;
(4) adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, mixing, stirring for 28min, inspecting semi-product, and bottling with aluminum bottle.
Test example 1 ultraviolet ray protection effect test
For the S plate (5 × 5cm V groove PMMA plate, SPFMASTER-PA01) at 2mg/cm2The spray prepared in examples 1 to 5 and comparative examples 1 to 8 was added dropwise, and after drying for 15 minutes, the absorbance was measured using a spectrophotometer. The absorbance (Abs) was calculated by the following formula using glycerol having no ultraviolet absorption as a control.
Abs＝-log(T/T0)
T: the transmittance of the sample;
T0: transmittance of Glycerol
The measured plate was immersed in water having a hardness of 50 to 500 for 30 minutes, dried, and then the absorbance was measured again to calculate the Abs change rate (the following formula) and the Abs change rate was used as the ultraviolet ray protection performance improving effect.
Ultraviolet ray protection performance improving effect:
abs Change (%). Abs after Water bath/Abs before Water bath × 100%
The samples with Abs change rate over 100% showed higher UV protection, and the specific results are shown in the following table
Table 1 uv protection test of different face protection sprays
| Abs Change Rate (%) | |
| Example 1 | 121 |
| Example 2 | 117 |
| Example 3 | 114 |
| Example 4 | 119 |
| Example 5 | 108 |
| Comparative example 1 | 98 |
| Comparative example 2 | 101 |
| Comparative example 3 | 99 |
| Comparative example 4 | 93 |
| Comparative example 5 | 66 |
| Comparative example 6 | 87 |
| Comparative example 7 | 88 |
| Comparative example 8 | 101 |
As can be seen from the data in Table 1, the protective spray for the ice skin face provided by the invention has the best effect on ultraviolet protection, and the ultraviolet protection effect can be obviously reduced by the synergistic effect and the mutual matching of the components due to the lack of any one component.
Test example 2 moisturizing effect and skin elasticity test
The sprays of examples 1 to 5 and comparative examples 1 to 8 were used as test samples, 65 volunteers were selected, and the moisturizing effect test was conducted on square regions of 4cm long and wide marks on the left and right cheeks in accordance with the standard of 3.0. + -. 0.1mg/cm2The test sample was uniformly applied to the square area, and the skin moisture content was measured at 1h, 4h in the square area and the control area not coated with the test sample by using a skin moisture meter model CM825, and the skin moisture content increase rate was calculated by the following formula, and the results are shown in table 2:
φ=
where φ is the skin moisture growth rate;
MMV0 — moisture content of skin before application;
MMVt-moisture content of the skin at the time of application t.
The skin elasticity test adopts a suction method for testing. Applying negative pressure (2000-5000 Pa) to the tested skin to suck the skin into a probe (MPA 580, the diameter of a probe test hole is phi 4 mm), measuring the skin depth of the sucked probe by a non-contact optical tester, wherein a light transmitter and a light receiver are arranged in the probe, and obtaining the parameter reflecting the skin elasticity by calculating the relation between the proportion of transmitted light and received light and the sucked skin depth. When constant negative pressure is applied, U is used for maximum skin lifting amountfIndicates that U is the value of skin recovery from the removal of the test negative pressure to the next application of negative pressureaIt is shown that,
R2=Ua/Uf，R2i.e. the skin elasticity parameter, the higher the value, the better the skin elasticity, measured 1 month after using the protective spray according to the invention, and the results are given in table 3.
Table 2 skin moisture content testing of different face protection sprays
| Skin moisture growth rate (%) | 4h skin moisture growth rate (%) | |
| Example 1 | 72 | 66 |
| Example 2 | 69 | 60 |
| Example 3 | 67 | 60 |
| Example 4 | 70 | 63 |
| Example 5 | 67 | 59 |
| Comparative example 1 | 31 | 25 |
| Comparative example 2 | 46 | 33 |
| Comparative example 3 | 37 | 29 |
| Comparative example 4 | 39 | 30 |
| Comparative example 5 | 52 | 41 |
| Comparative example 6 | 48 | 32 |
| Comparative example 7 | 49 | 23 |
| Comparative example 8 | 52 | 40 |
Table 3 skin elasticity test of different face protection sprays
| At 0 time R2 | R after 1 month2 | |
| Example 1 | 0.41 | 0.75 |
| Example 2 | 0.38 | 0.69 |
| Example 3 | 0.40 | 0.69 |
| Example 4 | 0.39 | 0.71 |
| Example 5 | 0.41 | 0.70 |
| Comparative example 1 | 0.41 | 0.60 |
| Comparative example 2 | 0.39 | 0.60 |
| Comparative example 3 | 0.37 | 0.49 |
| Comparative example 4 | 0.40 | 0.52 |
| Comparative example 5 | 0.41 | 0.65 |
| Comparative example 6 | 0.37 | 0.47 |
| Comparative example 7 | 0.38 | 0.53 |
| Comparative example 8 | 0.40 | 0.53 |
As can be seen from the data in table 2, the ice muscle body sunscreen spray provided by the present application has a good skin moisturizing effect within 4 hours, the skin still has high moisture, the run-off rate is significantly reduced, and if any one of the components is absent, the moisturizing effect of the spray is significantly reduced. The data in table 3 show that the spray provided by the invention has a significant anti-aging effect, and can smooth fine wrinkles and maintain skin elasticity.
Test example 3 study on the use effect of ice skin facial protective spray
Wangzhi, female, 37 years old, Shizhi, male, 40 years old, using the spray provided in example 1 of the present invention, no sticky feeling was experienced with use, and no sunburn was experienced. The product has certain whitening effect on skin after one month use.
The above detailed description is specific to one possible embodiment of the present invention, and the embodiment is not intended to limit the scope of the present invention, and all equivalent implementations or modifications without departing from the scope of the present invention should be included in the technical scope of the present invention.
Claims (4)
1. A preparation method of a face protection spray is characterized in that the ice muscle face protection spray comprises the following components, by weight, 1.5-2.5 parts of lactobacillus/soybean milk fermentation product filtrate, 1.5-2.5 parts of purslane extract, 1.2-1.8 parts of hexapeptide-9, 1.2-1.8 parts of oat β -glucan, 0.4-0.8 part of fullerene, 0.4-0.8 part of perilla extract, 1.5-2.5 parts of allantoin, 105-115 parts of titanium dioxide, 105-115 parts of phenyl trimethicone, 105-115 parts of cyclopentadimethylsiloxane, 105-115 parts of butanediol, 85-95 parts of glycerol, 25-35 parts of C12-15 alcohol benzoate, 25-35 parts of cetyl PEG/10/1 polydimethylsiloxane, 15-25 parts of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 12-18 parts of PEG-10 parts of polydimethylsiloxane, 12-18 parts of sodium hyaluronate, 12-6-18 parts of sodium hyaluronate, 0.6-9 parts of sodium benzoate, 0.2-4 parts of sodium benzoate, 0.5-2.8 parts of sodium benzoate, 0.5-2 parts of sodium benzoate, 0.8-2-4 parts of sodium benzoate, 0.8 parts of ethylene diamine, 0.8 parts of sodium benzoate, 0-4 parts of sodium benzoate, 0-4 parts of sodium benzoate, 0.8 parts of sodium benzoate, 0-4 parts of sodium benzoate, 0;
the preparation method of the protective spray comprises the following steps:
(1) adding butanediol, glycerol, EDTA disodium, sodium chloride, sodium hyaluronate, allantoin, sodium polyglutamate, methylparaben and nicotinamide into water, and mixing to obtain a mixture 1;
(2) phenyl trimethicone, cyclopentadimethylsiloxane, C12-15 alcohol benzoate, titanium dioxide, CI77492, CI77491, dimethicone/vinyl dimethicone crosspolymer, disteardimonium hectorite, cetyl PEG/PPG-10/1 dimethicone, PEG-10 dimethicone, silica, propyl hydroxybenzoate to obtain mixture 2;
(3) adding the mixture 2 into the mixture 1 for homogenizing to obtain mixed emulsion;
(4) adding oat β -dextran, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, herba Portulacae extract, Perillae herba extract, and essence, and mixing;
heating the materials in the step (1) to 75-85 ℃, and uniformly stirring;
heating the materials in the step (2) to 75-80 ℃, and uniformly stirring;
in the step (4), after the temperature is reduced to 40-45 ℃, adding β -glucan of oat, fullerene, phenoxyethanol, hexapeptide-9, lactobacillus/soybean milk fermentation product filtrate, purslane extract, perilla extract and essence, mixing and stirring for 25-30min to obtain the product.
2. The method of claim 1, wherein the spray comprises, in parts by weight, 2 parts of lactobacillus/soy milk fermentation product filtrate, 2 parts of purslane extract, 1.5 parts of hexapeptide-9, 1.5 parts of oat β -glucan, 0.5 parts of fullerene, 0.5 parts of perilla extract, 2 parts of allantoin, 110 parts of titanium dioxide, 110 parts of phenyl trimethicone, 110 parts of cyclopentadimethicone, 110 parts of butanediol, 90 parts of glycerol, 30 parts of C12-15 alcohol benzoate, 30 parts of cetyl PEG/PPG-10/1 dimethicone, 20 parts of dimethicone/vinyl dimethicone crosspolymer, 15 parts of PEG-10 dimethicone, 15 parts of sodium chloride, 7 parts of nicotinamide, 7 parts of silica, 6 parts of CI77492, 5 parts of disteardimonium hectorite, 4 parts of phenoxyethanol, 3 parts of CI77491, 1.5 parts of methylparaben, 1.5 parts of propylhydroxybenzoate, 0.6 parts of sodium hyaluronate, 0.6 parts of sodium glutamate, and 0.6 parts of essence.
3. The preparation method according to claim 1, wherein the homogenization time in the step (3) is 5-15min, and the temperature is kept for 20-40min after homogenization.
4. The method of claim 1, wherein the semi-product of step (4) is air-filled with aluminum bottles after passing the semi-product inspection.
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| CN106562913A (en) * | 2015-10-10 | 2017-04-19 | 孟宏 | An externally applied composition and cosmetic preparation having whitening effects and preparing methods thereof |
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| US6589541B2 (en) * | 2001-05-18 | 2003-07-08 | Classified Cosmetics, Inc. | Sprayable beautifying composition |
| JP6588345B2 (en) * | 2016-01-18 | 2019-10-09 | 株式会社 資生堂 | Water-in-oil emulsified cosmetic |
| CN106361684A (en) * | 2016-08-31 | 2017-02-01 | 广东芭薇生物科技股份有限公司 | Active composition for adjusting microorganism ecological balance of skin surface |
| CN107737027A (en) * | 2017-11-06 | 2018-02-27 | 诺斯贝尔化妆品股份有限公司 | A kind of moisturizing sun screen of high stability |
| CN108524382A (en) * | 2018-07-25 | 2018-09-14 | 周恒� | A kind of sunscreen spray and preparation method thereof |
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| CN105250148A (en) * | 2014-07-11 | 2016-01-20 | 玫琳凯有限公司 | Sunscreen compositions and methods of their use |
| CN108366916A (en) * | 2015-10-09 | 2018-08-03 | 株式会社资生堂 | Aerosol type sun care preparations |
| CN106562913A (en) * | 2015-10-10 | 2017-04-19 | 孟宏 | An externally applied composition and cosmetic preparation having whitening effects and preparing methods thereof |
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