CN115040461A - Moisturizing and hydrating fresh freeze-dried mask - Google Patents

Moisturizing and hydrating fresh freeze-dried mask Download PDF

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Publication number
CN115040461A
CN115040461A CN202210824536.XA CN202210824536A CN115040461A CN 115040461 A CN115040461 A CN 115040461A CN 202210824536 A CN202210824536 A CN 202210824536A CN 115040461 A CN115040461 A CN 115040461A
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freeze
dried
percent
extract
mask
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张晓敏
张岩
高春兰
殷刚
马燕红
刘丽娜
刘建岭
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Sino British Arnokang Ningxia Biological Technology Co ltd
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Sino British Arnokang Ningxia Biological Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/35Ketones, e.g. benzophenone
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645Proteins of vegetable origin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9722Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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    • A61Q19/00Preparations for care of the skin
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    • AHUMAN NECESSITIES
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    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
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    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/84Products or compounds obtained by lyophilisation, freeze-drying

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Abstract

The invention discloses a moisturizing, fresh and alive freeze-drying mask, and relates to the technical field of skin care products. The moisturizing, fresh-living and freeze-drying facial mask comprises mutually independent mask cloth and essence, wherein the mask cloth comprises base cloth and freeze-drying functional substances attached to the base cloth in a freeze-drying mode; the raw materials of the freeze-dried functional substance comprise a first humectant, a first skin conditioner, a preservative and the balance of water, and the raw materials of the essence comprise a second humectant, a thickening agent, a second skin conditioner, a pH regulator and the balance of water; the first skin conditioner comprises three to six of the following components in percentage by total mass of raw materials of the freeze-dried efficacy substance: dipotassium glycyrrhizinate, soybean polypeptide, aloe vera extract, centella asiatica extract, hydrolyzed rice protein, oligopeptide-3, snail secretion filtrate, fullerene, chamomile extract, yeast fermentation product filtrate, chlorella extract, rose petals and cherry blossom extract. It has effects of keeping moisture and supplementing water.

Description

Moisturizing and hydrating fresh freeze-dried mask
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to a moisturizing, fresh-keeping and alive-tonifying freeze-dried mask.
Background
At present, common facial masks are usually manufactured in a wet mode, each facial mask contains 20-30ml of water and is compounded with other various components, the preservative can ensure that the facial masks do not go bad for a long time, the activity of some components can be greatly reduced under a liquid environment, some components even can bring sensitization reaction to skin, the skin absorbs the preservative while absorbing nutrient components, facial mask cloth and facial mask bags are soaked in facial mask liquid for a long time, and the leaching of some harmful substances can also affect the health of the skin.
In view of this, the invention is particularly proposed.
Disclosure of Invention
The invention aims to provide a moisturizing, fresh-keeping and alive-tonifying freeze-dried mask.
The invention is realized by the following steps:
in a first aspect, the invention provides a moisturizing, fresh-keeping and live-freezing freeze-drying facial mask which comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-drying functional substances attached to the base cloth in a freeze-drying manner; the raw materials of the freeze-dried functional substance comprise, by mass, 7% -16% of a first moisturizing agent, 1.5% -11% of a first skin conditioning agent, 0.02% -0.5% of a preservative and the balance of water, and the raw materials of the essence comprise, by mass, 2% -10% of a second moisturizing agent, 0.1% -0.5% of a thickening agent, 0.05% -3% of a second skin conditioning agent, 0.05% -0.1% of a pH regulator and the balance of water;
wherein the first skin conditioner comprises three to six of the following components in percentage by total mass of the raw materials of the freeze-dried efficacy substance: 1.0-2.0% of dipotassium glycyrrhizinate, 0.5-1.0% of soybean polypeptide, 0.5-1.0% of aloe vera extract, 0.5-1.0% of centella extract, 0.5-1.0% of hydrolyzed rice protein, 30.1-0.5% of oligopeptide, 1.0-2.0% of snail secretion filtrate, 0.1-0.5% of fullerene, 1.0-2.0% of golden yellow chamomile extract, 1.0-2.0% of yeast fermentation product filtrate, 0.5-1.0% of chlorella extract, 0.5-1.0% of rose petal and 1.0-2.0% of oriental cherry flower extract.
The invention has the following beneficial effects:
the fresh and alive freeze-dried mask with multiple effects of repairing, tightening and moisturizing provided by the invention has a synergistic effect through the matching of a specific first skin conditioner (1.0% -2.0% of dipotassium glycyrrhizinate, 0.5% -1.0% of soybean polypeptide, 0.5% -1.0% of aloe vera extract, 0.5% -1.0% of centella asiatica extract, 0.5% -1.0% of hydrolyzed rice protein, 30.1% -0.5% of oligopeptide, 1.0% -2.0% of snail secretion filtrate, 0.1% -0.5% of fullerene, 1.0% -2.0% of chamomile extract, 1.0% -2.0% of yeast fermentation product filtrate, 0.5% -1.0% of chlorella extract, 0.5% -1.0% of rose petals and 1.0% -2.0% of oriental cherry flower extract), and can realize a good moisturizing effect. By continuously using the moisturizing fresh and alive freeze-dried mask provided by the invention for 4 weeks, a test subject feels that the product can moisturize and moisturize, improve the dry and itching phenomenon of skin, improve the coarse pores of the skin, improve the moisturizing degree of the skin, improve the skin firmness, enhance the skin elasticity, improve the skin roughness, enable the skin to be smoother, improve the dry lines and fine lines of the skin, improve the facial glossiness, is suitable for sensitive muscles, has good fitting property and air permeability, and is mild and non-irritant.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings needed to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present invention and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained according to the drawings without inventive efforts.
Fig. 1 is a schematic view of a method of using the mask provided herein.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
The application provides a moisturizing, fresh and alive freeze-drying facial mask which comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-drying functional substances attached to the base cloth in a freeze-drying mode; the raw materials of the freeze-dried functional substance comprise, by mass, 7% -16% of a first moisturizing agent, 1.5% -11% of a first skin conditioning agent, 0.02% -0.5% of a preservative and the balance of water.
The first humectant comprises three to six of the following components in percentage by total mass of raw materials of the freeze-dried functional substance: 2.0 to 3.0 percent of butanediol, 2.0 to 3.0 percent of mannitol, 2.0 to 3.0 percent of trehalose, 0.5 to 0.7 percent of sodium hyaluronate, 0.5 to 1.0 percent of cubilose extract, 2.0 to 3.0 percent of dendrobium officinale stem extract, 2.0 to 3.0 percent of hydrolyzed collagen and 0.5 to 1.0 percent of glycerol.
The first skin conditioner comprises three to six of the following components in percentage by total mass of the raw materials of the freeze-dried efficacy substance: 1.0-2.0% of dipotassium glycyrrhizinate, 0.5-1.0% of soybean polypeptide, 0.5-1.0% of aloe vera extract, 0.5-1.0% of centella extract, 0.5-1.0% of hydrolyzed rice protein, 30.1-0.5% of oligopeptide, 1.0-2.0% of snail secretion filtrate, 0.1-0.5% of fullerene, 1.0-2.0% of golden yellow chamomile extract, 1.0-2.0% of yeast fermentation product filtrate, 0.5-1.0% of chlorella extract, 0.5-1.0% of rose petal and 1.0-2.0% of oriental cherry flower extract.
In this application, through injecing multiple first skin conditioner, through selecting above-mentioned first skin conditioner, can obtain the freeze-drying effect thing composition of multiple fresh and alive freeze-drying facial mask that has moisturizing effect. Specifically, dipotassium glycyrrhizinate can accelerate skin absorption in cosmetics to enhance the effect, and can be used for sun protection and assisting whitening. The soybean polypeptide has strong permeability, and can activate epidermal cells of skin, so that more nutrients can be absorbed by the skin, and the protein synthesis speed can be increased quickly. The soybean polypeptide contains a large amount of natural moisturizing factor components, particularly hydrophilic factors, and has a great effect on locking and supplementing water. The soybean polypeptide can also increase the activity of collagen, so that the skin can obtain more nutrition, cells can be quickly updated, the elasticity of the skin can be recovered, the probability of wrinkle appearance can be reduced, and fine wrinkles can disappear. The Aloe Barbadensis Miller extract has effects of keeping moisture, replenishing water, whitening skin, resolving macula, resisting aging, repairing wound, and relieving inflammation. Herba Centellae extract has antibacterial, antiinflammatory, and healing effectsWound and scar, antioxidant, and skin whitening effects. The hydrolyzed rice protein is rich in amino acids, and can promote fibroblasts to produce collagen. The cosmetic composition can be applied to cosmetics, and has effects of enhancing skin defense function, keeping keratinization of keratinocyte normal, and inhibiting bacterial reproduction while exerting high-efficiency moisturizing effect. The oligopeptide-3 can be directly and effectively absorbed and utilized by cells, and can rapidly supplement collagen, thereby playing a good role in conditioning, such as promoting metabolism, stimulating cell regeneration, proliferating and regenerating collagen, and achieving the effect of skin renewal and anti-aging. The snail secretion filtrate has effects of nourishing skin, effectively preventing skin aging, and eliminating speckle, scar and acne on skin. Fullerene can effectively eliminate intracellular UVA irradiation and H 2 O 2 The generated free radicals can well protect cells. Inhibiting excessive production of active oxygen in cells, inhibiting PGE2 inflammatory factor, and reducing skin inflammation. The golden yellow chamomile extract has antibacterial and anti-inflammatory effects; can inhibit the activity of free radicals and has antioxidant effect; can also repair sensitive skin, reduce red blood streak and accelerate soothing of the reddish skin. Secondly, it has the application of increasing the moisture entering the skin so as to improve the moisturizing effect of the skin care product. The yeast fermentation product filtrate has excellent oil balancing, whitening and spot lightening, anti-aging, moisturizing and repairing functions. The chlorella extract has multiple effects of moisturizing, resisting aging, resisting wrinkles, repairing, improving skin immunity, refining pores, purifying skin and the like. The rose petals are added into the cosmetics to increase the artistic feeling of the product, endow the product with good taste and shape and bring people with beautiful feeling. The oriental cherry flower extract has the effects of resisting oxidation, whitening skin and removing freckles.
The raw materials of the freeze-dried functional substance also comprise an antioxidant, and the antioxidant comprises at least one of the following components in percentage by total mass of the raw materials of the freeze-dried functional substance: 0.5-1.0% of hydrolyzed procyanidin, 0.5-1.0% of tocopherol acetate, 0.5-1% of haematococcus pluvialis extract, 0.1-0.5% of astaxanthin and 0.1-0.5% of tocopherol (vitamin E).
The raw material of the freeze-drying functional substance also comprises 0.1-0.5% of cyclodextrin.
The freeze-dried functional substance also comprises an emulsifier, and the emulsifier comprises at least two of the following components in percentage by total mass of the raw materials of the freeze-dried functional substance: 0.5 to 1 percent of PEG-40 hydrogenated castor oil, 0.1 to 0.5 percent of PPG-30 cetyl ether, 0.1 to 0.5 percent of polyglycerol-10 stearate and 0.1 to 0.5 percent of polyglycerol-10 laurate.
The antiseptic comprises at least one of 1, 2-hexanediol, caprylyl glycol and phenoxyethanol.
The essence comprises the following raw materials, by mass, 2-10% of a second humectant, 0.1-0.5% of a thickening agent, 0.05-3% of a second skin conditioner, 0.05-0.1% of a pH regulator and the balance of water;
the second humectant comprises at least two of the following components in percentage by mass of the total raw materials of the essence: 2-5% of glycerol, 1-2% of beta-glucan, 81-2% of acetyl hexapeptide, 1-3% of tranexamic acid and 1.0% -3.0% of sodium alginate.
The second skin conditioner comprises at least one of the following components in percentage by mass of the raw materials of the essence: tripeptide-1 copper 0.05-0.4%, palmitoyl pentapeptide-40.1-0.5% and nicotinamide 1-3%.
The thickener is carbomer.
The pH regulator is triethanolamine.
In addition, the invention also provides a preparation method of the moisturizing and hydrating fresh and alive freeze-dried mask, which comprises the following steps:
and S1, preparing the membrane cloth.
Specifically, the freeze-dried functional substance is dissolved in water to form functional liquid, the functional liquid is sprayed on a base fabric, the base fabric is spunlace non-woven fabric, the base fabric is soaked for 10-30min at a constant temperature of 50-60 ℃, and after the base fabric is fully soaked, the materials are pre-frozen: freezing the membrane cloth fiber with nutrient components in an ultra-low temperature freeze dryer at the low temperature of-40 to-50 ℃, wherein the freezing time is as follows: 2-4 h. Then, primary drying: the vacuum freeze dryer controls the temperature of primary drying at minus 45-20 ℃, performs slope temperature control, controls the vacuum to be 10PA-80PA, controls the primary drying time to be 8-15 hours, and dries 85-95% of water of the material. Finally, resolving and drying: the temperature for analysis and drying of the freeze dryer is 30-50 ℃, the slope temperature is controlled, the vacuum is controlled to be 10PA-80PA, the analysis and drying time is about 4-8h, and 5-15% of water is remained in the dried material.
S2, preparing essence.
Specifically, firstly, injecting water into a vacuum stirring homogenizing emulsifying machine, sequentially adding the weighed raw materials, stirring for 5-20 min, and finally adding triethanolamine to adjust the pH value to 4.0-8.0; discharging after the semi-finished product is detected to be qualified, and transferring the material body to a material storage tank.
And S3, partitioning the membrane bags, arranging mutually independent membrane cloth bags and essence bags, and respectively filling the membrane cloth and the essence into the membrane cloth bags and the essence bags.
S4, arranging an inlet at the middle part of the membrane bag, wherein the inlet is positioned between the membrane cloth bag and the essence bag, and the inlet can be extruded by external force to communicate the membrane cloth bag and the essence bag.
The application method of the moisturizing, fresh-keeping and live-freezing facial mask comprises the following steps: because the moisturizing fresh-living freeze-drying facial mask is produced by adopting a membrane-liquid separation process technology, essence needs to be introduced into one side of the freeze-drying facial mask cloth in an extrusion mode before use.
1. Folding the membrane bag along the middle (see the figure 1), folding from bottom to top again, collecting the essence around the corrugated inlet (see the figure 1), pressing the essence to completely inject the essence into the membrane cloth (see the figure 1), kneading fully, and absorbing the essence by the freeze-dried mask cloth uniformly.
2. After cleansing, tearing the mouth, taking out, spreading on the face, peeling off the omentum cover, gently pressing and smoothing the mask to make it fit completely (e.g., (r), and (l) in fig. 1). Removing after 15-25 min, gently massaging until the essence is absorbed (shown in fig. 1).
The features and properties of the present invention are described in further detail below with reference to examples.
Example 1
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the hyaluronic acid polypeptide water fresh and alive freeze-dried mask comprises mutually independent mask cloth and essence, wherein the mask cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
The freeze-drying functional substance comprises the following raw materials in percentage by mass: butanediol 2.5% (humectant), mannitol 2.5% (humectant), trehalose 2.5% (humectant), dipotassium glycyrrhizinate 1.5% (skin conditioner), sodium hyaluronate 0.6% (humectant), soybean (GLYCINE MAX) polypeptide 0.8% (skin conditioner), ALOE vera (ALOE BARBADENSIS) extract 0.8% (skin conditioner), centella asiatica (CENTELLA ASIATICA) extract 0.8% (skin conditioner), bird's nest extract 0.8% (humectant), hydrolyzed rice protein, 0.8% (skin conditioner), oligopeptide-30.3% (skin conditioner), phenoxyethanol 0.05% (preservative), and balance water.
The essence comprises the following raw materials in percentage by mass: glycerin 3.0% (humectant), beta-glucan 1.5% (humectant), carbomer 0.3% (thickener), palmitoyl pentapeptide-40.2% (skin conditioner), acetyl hexapeptide-80.2% (antioxidant), triethanolamine 0.07% (pH regulator) and the balance water.
Example 2
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the dendrobium officinale planting, moistening, fresh and alive freeze-dried mask comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
The freeze-drying functional substance comprises the following raw materials in percentage by mass: 2.5 percent of butanediol (humectant), 2.5 percent of mannitol (humectant), 2.5 percent of trehalose (humectant), 2.5 percent of DENDROBIUM OFFICINALE (DENDROBIUM OFFICINALE) stem extract (humectant), 1.5 percent of ALOE BARBADENSIS (ALOE BARBADENSIS) extract (skin conditioner), 1.5 percent of hydrolyzed rice protein (skin conditioner), 1.5 percent of snail secretion filtrate (skin conditioner), 0.8 percent of sodium hyaluronate (humectant), 30.3 percent of oligopeptide-fullerene (skin conditioner), 0.3 percent of fullerene (skin conditioner), 0.08 percent of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 4.0% (humectant), niacinamide 1.5% (humectant/skin conditioner), carbomer 0.3% (thickener), palmitoyl pentapeptide-40.3% (skin conditioner) triethanolamine 0.08% (pH adjuster), and balance water.
Example 3
The embodiment provides a moisturizing, fresh-keeping and live-freezing facial mask which is named as follows: the chamomile plant extract moisturizing, fresh and alive freeze-dried mask comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
Wherein, the raw materials of the freeze-dried functional substance comprise, by mass percentage, 2.5 percent of butanediol (humectant), 2.5 percent of hydrolyzed collagen (humectant), 1.5 percent of chamomile (Chrysanthemum INDICUM) extract (skin conditioner), 1.5 percent of yeast fermentation product filtrate (skin conditioner), 1.5 percent of soybean (Glycine MAX) polypeptide (skin conditioner), 0.7 percent of hydrolyzed procyanidin (antioxidant), 0.7 percent of sodium hyaluronate (humectant), 0.7 percent of tocopherol acetate (antioxidant), 0.7 percent of PEG-40 hydrogenated castor oil (emulsifier), 30.3 percent of oligopeptide (skin conditioner), 0.3 percent of PPG-30 cetyl ether (emulsifier), 0.06 percent of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 3.0% (humectant), tranexamic acid 2.0% (humectant), carbomer 0.3% (thickener), tripeptide-1 copper 0.3% (skin conditioner), triethanolamine 0.06% (pH regulator), and balance water.
Example 4
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the aloe plant extract polypeptide beauty and freshness-retaining freeze-dried mask comprises mutually independent mask cloth and essence, wherein the mask cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
Wherein, the raw materials of the freeze-dried efficacy substance comprise, by mass percentage, 2.5 percent of butanediol (humectant), 2.5 percent of PEG-40 hydrogenated castor oil (emulsifier), 2.5 percent of hydrolyzed procyanidin (antioxidant), 1.5 percent of tocopherol acetate (antioxidant), 1.5 percent of hydrolyzed collagen (humectant), 1.0 percent of ALOE vera (ALOE BARBADENSIS) extract (skin conditioner), 2.0 percent of centella asiatica (CENTELLA ASIATICA) extract (skin conditioner/antioxidant), 0.7 percent of sodium hyaluronate (humectant), 0.7 percent of PPG-30 cetyl ether (emulsifier), 30.3 percent of oligopeptide (skin conditioner), 0.02 percent of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 3.0% (humectant), beta-glucan 1.5%, carbomer 0.3% (thickener), palmitoyl pentapeptide-40.2% (skin conditioner), acetyl hexapeptide-80.2% (antioxidant/humectant), triethanolamine 0.06% (pH regulator) and balance water.
Example 5
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the fresh-keeping freeze-dried seaweed mask comprises mutually independent mask cloth and essence, wherein the mask cloth comprises base cloth and freeze-dried functional substances which are attached to the base cloth in a freeze-dried mode.
Wherein, the raw materials of the freeze-drying functional substance comprise, by mass percentage, 3.0 percent of mannitol (humectant), 3.0 percent of trehalose (humectant), 3.0 percent of butanediol (humectant), 0.5 percent of PEG-40 hydrogenated castor oil (emulsifier), 0.5 percent of dipotassium glycyrrhizinate (skin conditioner), 0.5 percent of tocopherol acetate (antioxidant), 0.9 percent of sodium hyaluronate (humectant), 0.9 percent of CHLORELLA (Chlorella VULGARIS) extract (humectant), 0.9 percent of ALOE vera (ALOE BARBADENSIS) extract (skin conditioner), 30.2 percent of oligopeptide-30 (skin conditioner), 0.09 percent of PPG-30 cetyl ether (emulsifier), 0.09 percent of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 3.0% (humectant), sodium alginate 2.0% (humectant), niacinamide 2% (skin conditioner), carbomer 0.4% (thickener), palmitoyl pentapeptide-40.2% -0.5% (skin conditioner), triethanolamine 0.09% (pH regulator) and balance water.
Example 6
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the rose flower cyanine extract fresh-living freeze-dried mask comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
The raw materials of the freeze-dried functional substance comprise, by mass percentage, 2.8% of butanediol (humectant), 2.8% of centella asiatica (CENTELLA ASIATICA) extract (skin conditioner/antioxidant), 2.8% of hydrolyzed collagen (humectant), 1.8% of hydrolyzed procyanidin (antioxidant), 1.8% of tocopherol acetate (antioxidant), 0.7% of sodium hyaluronate (humectant), 0.7% of PEG-40 hydrogenated castor oil (emulsifier), 0.7% of rose petals (skin conditioner), 0.3% of PPG-30 cetyl ether (emulsifier), 30.3% of oligopeptide-skin conditioner, 0.07% of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 4% (humectant), tranexamic acid 2% (humectant), carbomer 0.4% (thickener), tripeptide-1 copper 0.4% (skin conditioner), triethanolamine 0.07% (pH regulator) and balance water.
Example 7
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the rose gold foil fresh and alive freeze-dried mask comprises mutually independent mask cloth and essence, wherein the mask cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
The raw materials of the freeze-dried efficacy substance comprise, by mass, 12% of ROSA DAMASCENA (ROSA DAMASCENA) flower water, 2.5% of butanediol (humectant), 2.50% of mannitol (humectant), 2.5% of trehalose (humectant), 2.5% of dipotassium glycyrrhizinate (skin conditioner), 2.5% of soybean (GLYCINE MAX) polypeptide (skin conditioner), 2.5% of ALOE vera (ALOE BARBADENSIS) extract (skin conditioner), 1.5% of bird's nest extract (humectant), 0.8% of sodium hyaluronate (humectant), 30.3% of oligopeptide-skin conditioner, 0.3% of fullerene (skin conditioner), 0.08% of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 3.0% (humectant), niacinamide 2.0% (skin conditioner), carbomer 0.3% (thickener), palmitoyl pentapeptide-40.3% (skin conditioner), triethanolamine 0.08% (pH regulator), and water in balance.
Example 8
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the fullerene black crystal fresh freeze-dried facial mask comprises mutually independent mask cloth and essence, wherein the mask cloth comprises base cloth and freeze-dried functional substances which are attached to the base cloth in a freeze-dried mode.
The raw materials of the freeze-dried efficacy substance comprise, by mass, 2.0% of butanediol (humectant), 2.0% of trehalose (humectant), 2.0% of mannitol (humectant), 2.0% of dipotassium glycyrrhizinate (skin conditioner), 2.0% of cubilose extract (humectant), 1.0% of centella asiatica (CENTELLA ASIATICA) extract (skin conditioner), 1.0% of ALOE BARBADENSIS (ALOE BARBADENSIS) extract (skin conditioner), 1.0% of soybean (GLYCINE MAX) polypeptide (skin conditioner), 0.5% of sodium hyaluronate (humectant), 30.2% of oligopeptide-skin conditioner, 0.2% of fullerene (skin conditioner), 0.05% of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 2.0% (humectant), niacinamide 1.0% (skin conditioner), carbomer 0.2% (thickener), palmitoyl pentapeptide-40.2% (skin conditioner), triethanolamine 0.05% (pH regulator), and water in balance.
Example 9
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the centella asiatica plant extract polypeptide tender and fresh freeze-dried mask comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode.
Wherein the raw materials of the freeze-drying functional substance comprise the following components in percentage by mass
Butanediol 2.0% (humectant), mannitol 2.0% (humectant), trehalose 2.0% (humectant), centella asiatica (CENTELLA ASIATICA) extract 2.0% (skin conditioner), Aloe BARBADENSIS (Aloe BARBADENSIS) extract 1.0% (skin conditioner), hydrolyzed rice protein 1.0% (skin conditioner), snail secretion filtrate 1.0% (skin conditioner), sodium hyaluronate 0.5% (humectant), oligopeptide-30.1% (skin conditioner), fullerene 0.1% -0.5% (skin conditioner), phenoxyethanol 0.02 (preservative), and balance water.
The essence comprises the following raw materials in percentage by mass: 2.0% of glycerin (humectant), 1.0% of beta-glucan, 0.2% of carbomer (thickener), 80.1% of acetyl hexapeptide (antioxidant), 40.1% of palmitoyl pentapeptide (skin conditioner), 0.05% of triethanolamine (pH regulator) and the balance of water.
Example 10
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the astaxanthin tranexamic acid fresh and alive freeze-dried facial mask comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises a base cloth and freeze-dried functional substances which are attached to the base cloth in a freeze-dried mode.
Wherein, the raw materials of the freeze-dried efficacy substance comprise 3.0 percent of butanediol (humectant), 3.0 percent of dipotassium glycyrrhizinate (skin conditioner), 3.0 percent of mannitol (humectant), 2.0 percent of trehalose (humectant), 2.0 percent of ALOE BARBADENSIS (ALOE BARBADENSIS) extract (skin conditioner), 2.0 percent of oriental cherry (PRUNUS SPECIOSA) flower extract (skin conditioner), 2.0 percent of cubilose extract (humectant), 1.0 percent of sodium hyaluronate (humectant), 1.0 percent of glycerol (humectant), 31.0 percent of oligopeptide-31.0 percent of skin conditioner, 1.0 percent of HAEMATOCOCCUS PLUVIALIS (HAEMATOUS PLUVIALIS) extract (antioxidant), 0.5 percent of polyglycerol-10 stearate (emulsifier), 0.5 percent of polyglycerol-10 lauric acid (emulsifier), 0.5 percent of astaxanthin (antioxidant), 0.5 percent of cyclodextrin (adsorbent), 0.5 percent of tocopherol (vitamin E) and/or vitamin E (antioxidant), 0.5% of 1, 2-hexanediol (preservative), 0.1% of caprylyl glycol (preservative), and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 5.0% (humectant), tranexamic acid 2.0% (humectant), carbomer 0.5% (thickener), tripeptide-1 copper 0.4% (skin conditioner), triethanolamine 0.1% (pH regulator), and water in balance.
Example 11
The embodiment provides a moisturizing, fresh and alive freeze-drying mask which is named as: the fullerene glittering and translucent elastic fresh and alive freeze-dried facial mask comprises mutually independent membrane cloth and essence, wherein the membrane cloth comprises base cloth and freeze-dried functional substances which are attached to the base cloth in a freeze-dried mode.
The raw materials of the freeze-dried efficacy substance comprise, by mass, 3.0% of butanediol (humectant), 3.0% of trehalose (humectant), 3.0% of mannitol (humectant), 2.0% of dipotassium glycyrrhizinate (skin conditioner) bird's nest extract (humectant), 2.0% of centella asiatica (CENTELLA ASIATICA) extract (skin conditioner), 2.0% of ALOE BARBADENSIS (ALOE BARBADENSIS) extract (skin conditioner), 2.0% of soybean (GLYCINE MAX) polypeptide (skin conditioner), 1.0% of sodium hyaluronate (humectant), 31.0% of oligopeptide-31.0% (skin conditioner), 0.5% of fullerene (skin conditioner), 0.1% of phenoxyethanol (preservative) and the balance of water.
The essence comprises the following raw materials in percentage by mass: glycerin 5.0% (humectant), tranexamic acid 2.0% (humectant), carbomer 0.5% (thickener), tripeptide-1 copper 0.1% (skin conditioner), triethanolamine 0.4% (pH regulator), and water in balance.
Experimental example: efficacy test
1. Detection method
25 healthy Chinese male/female subjects with stratum corneum moisture content between 15-45 (comeometer Unit, C.U.) in arm test sites were selected, and aged 18-65 years. The water content of the stratum corneum of the inner side of the arm is measured by a method of self front-back control and parallel blank control before using the test product and after using the test product for 2 hours, 4 hours and 8 hours respectively. The evaluation results before and after the product is used are compared by a statistical test method to judge whether the product has statistical difference.
25 subjects were enrolled and 25 subjects were finally counted, with 15 males and 10 females aged 18 to 48 years, with a mean age of 27.60 ± 1.87 years. The using method comprises the following steps: laboratory technicians select 2 areas on the inner sides of the two arms, the area of each area is 3cm multiplied by 3cm, the intervals of the areas of the same arm are at least more than 1cm, and the usage amount of fresh and alive freeze-dried mask (liquid and film cloth are mixed and then extruded out) and blank control group (without product) liquid outlet of the tested product of the ryegrass rose cyanine extract is used in the product area according to the product usage requirements and is 2.0 +/-0.1 mg/cm 2
2. Detection site
(1) Water content of skin stratum corneum-inside of arm
3. Detecting the index
Figure BDA0003743521200000131
Figure BDA0003743521200000141
The result of the detection
Figure BDA0003743521200000142
Figure BDA0003743521200000151
Figure BDA0003743521200000152
And (4) a statistical method, namely analyzing by adopting a t test and a rank test method, wherein the test level alpha is 0.05.
The significance labeling method comprises the following steps: n.s means no statistical difference, p is not less than 0.05; p < 0.05 indicates significant differences (×) 0.01 ≦ p < 0.05, × 0.001 ≦ p < 0.01, and ≦ p < 0.001).
As can be seen from the above table, the moisture content of stratum corneum in the single-use product area was increased and significant (p < 0.001) compared to the blank control area at 2 hours, 4 hours, and 8 hours.
In addition, the moisturizing, fresh and alive freeze-dried masks provided in the above examples 1 to 11 of the present application are subjected to multiple skin irritation tests, microbial detection and heavy metal detection. The detection results show that the freeze-dried mask cloth and the essence of the moisturizing fresh and alive freeze-dried mask provided by the embodiments 1 to 11 are non-irritant, and the content of microorganisms and the content of heavy metals meet the detection requirements.
In conclusion, the fresh and alive freeze-dried mask with multiple effects of repairing, tightening and moisturizing provided by the invention has a synergistic effect through the cooperation of the specific first skin conditioner (1.0% -2.0% of dipotassium glycyrrhizinate, 0.5% -1.0% of soybean polypeptide, 0.5% -1.0% of aloe vera extract, 0.5% -1.0% of centella asiatica extract, 0.5% -1.0% of hydrolyzed rice protein, 30.1% -0.5% of oligopeptide, 1.0% -2.0% of snail secretion filtrate, 0.1% -0% of fullerene, 1.0% -2.0% of chamomile extract, 1.0% -2.0% of yeast fermentation product filtrate, 0.5% -1.0% of chlorella extract, 0.5% -1.0% of rose petal and 1.0% -2.0% of oriental cherry flower extract), and can realize a good moisturizing effect. By continuously using the moisturizing fresh and alive freeze-dried mask provided by the invention for 4 weeks, a test subject feels that the product can moisturize and moisturize, improve the dry and itching phenomenon of skin, improve the coarse pores of the skin, improve the moisturizing degree of the skin, improve the skin firmness, enhance the skin elasticity, improve the skin roughness, enable the skin to be smoother, improve the dry lines and fine lines of the skin, improve the facial glossiness, is suitable for sensitive muscles, has good fitting property and air permeability, and is mild and non-irritant.
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (10)

1. The moisture-preserving moisturizing fresh-living freeze-dried mask is characterized by comprising mutually independent mask cloth and essence, wherein the mask cloth comprises a base cloth and freeze-dried functional substances attached to the base cloth in a freeze-dried mode; the raw materials of the freeze-dried functional substance comprise, by mass, 7% -16% of a first moisturizing agent, 1.5% -11% of a first skin conditioning agent, 0.02% -0.5% of a preservative and the balance of water, and the raw materials of the essence comprise, by mass, 2% -10% of a second moisturizing agent, 0.1% -0.5% of a thickening agent, 0.05% -3% of a second skin conditioning agent, 0.05% -0.1% of a pH regulator and the balance of water;
wherein the first skin conditioner comprises three to six of the following components in percentage by total mass of the raw materials of the freeze-dried efficacy substance: 1.0-2.0% of dipotassium glycyrrhizinate, 0.5-1.0% of soybean polypeptide, 0.5-1.0% of aloe vera extract, 0.5-1.0% of centella extract, 0.5-1.0% of hydrolyzed rice protein, 30.1-0.5% of oligopeptide, 1.0-2.0% of snail secretion filtrate, 0.1-0.5% of fullerene, 1.0-2.0% of golden yellow chamomile extract, 1.0-2.0% of yeast fermentation product filtrate, 0.5-1.0% of chlorella extract, 0.5-1.0% of rose petal and 1.0-2.0% of oriental cherry flower extract.
2. The moisture-preserving fresh-living freeze-dried mask as claimed in claim 1, wherein the first moisture-preserving agent comprises three to six of the following components in percentage by total mass of raw materials of the freeze-dried functional substance: 2.0 to 3.0 percent of butanediol, 2.0 to 3.0 percent of mannitol, 2.0 to 3.0 percent of trehalose, 0.5 to 0.7 percent of sodium hyaluronate, 0.5 to 1.0 percent of cubilose extract, 2.0 to 3.0 percent of dendrobium officinale stem extract, 2.0 to 3.0 percent of hydrolyzed collagen and 0.5 to 1.0 percent of glycerol.
3. The moisture-preserving moisture-supplementing fresh-alive freeze-dried mask as claimed in claim 1, wherein the raw materials of the freeze-dried efficacy substances further comprise an antioxidant, and the antioxidant comprises at least one of the following components in percentage by mass of the total mass of the raw materials of the freeze-dried efficacy substances: 0.5-1.0% of hydrolyzed procyanidin, 0.5-1.0% of tocopherol acetate, 0.5-1% of haematococcus pluvialis extract, 0.1-0.5% of astaxanthin and 0.1-0.5% of tocopherol (vitamin E).
4. The moisture-preserving, water-replenishing, fresh-living and freeze-dried mask as claimed in claim 1, wherein the raw material of the freeze-dried efficacy substance further comprises 0.1% -0.5% of cyclodextrin.
5. The moisture-preserving fresh-living freeze-dried mask as claimed in claim 1, wherein the freeze-dried efficacy substance further comprises an emulsifier, and the emulsifier comprises at least two of the following components in percentage by mass of the total mass of the raw materials of the freeze-dried efficacy substance: 0.5 to 1 percent of PEG-40 hydrogenated castor oil, 0.1 to 0.5 percent of PPG-30 cetyl ether, 0.1 to 0.5 percent of polyglycerol-10 stearate and 0.1 to 0.5 percent of polyglycerol-10 laurate.
6. The moisture-preserving fresh-living freeze-dried mask as claimed in claim 1, wherein the preservative comprises at least one of 1, 2-hexanediol, caprylyl glycol and phenoxyethanol.
7. The moisturizing fresh-living freeze-dried mask as claimed in any one of claims 1 to 6, wherein the second moisturizer comprises at least two of the following components in percentage by mass of the total raw materials of the essence: 2-5% of glycerol, 1-2% of beta-glucan, 81-2% of acetyl hexapeptide, 1-3% of tranexamic acid and 1.0% -3.0% of sodium alginate.
8. The moisturizing fresh-living freeze-dried mask as claimed in any one of claims 1 to 6, wherein the second skin conditioner comprises at least one of the following components in percentage by mass of the raw materials of the essence: tripeptide-1 copper 0.05-0.4%, palmitoyl pentapeptide-40.1-0.5% and nicotinamide 1-3%.
9. The moisture-retentive, fresh-living, freeze-dried mask according to any one of claims 1 to 6, wherein the thickener is carbomer.
10. The moisture-retaining, moisturizing, fresh-living and freeze-dried mask according to any one of claims 1 to 6, wherein the pH regulator is triethanolamine.
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