CN109589280A - A kind of moisturising preparations and preparation method thereof - Google Patents
A kind of moisturising preparations and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The present invention relates to cosmetic field, in particular to a kind of moisturising preparations and preparation method thereof.The moisturising preparations include acceptable auxiliary agent in extractive of flax seed and cosmetics；Extractive of flax seed includes flaxseed gum and linseed oil；Flaxseed gum the preparation method comprises the following steps: mechanical stirring after taking linseed to mix with water, is collected by filtration concentration, alcohol precipitation after filtrate, precipitating is collected after filtering, it is dry after dehydration；Linseed oil the preparation method comprises the following steps: linseed squeezing is taken to collect feedstock oil, mix with salt, degumming after sedimentation, cooling, filtering dewaxes.The moisturising preparations have effects that moist moisturizing, improve the colour of skin.
Description
Technical field
The present invention relates to cosmetic field, in particular to a kind of moisturising preparations and preparation method thereof.
Background technique
With the development of economy, rhythm of life is increasingly accelerated, the factors such as environmental degradation, skin nursing mistake cause skin
Injury, leads to more and more people's skin aging, shows as that dry skin, pore is coarse, the colour of skin is dim mute.Skin aging be by
Skin aging phenomenon caused by natural cause or non-natural factor.Skin histology is increasingly flourishing after people's birth, and function is gradually active,
It will start to degenerate when reaching certain age, it is that one kind continues gradually that this degeneration, which is often unconsciously slowly carried out in people,
Into the physiology course of property, the appearance and function of skin are directly affected.
Skin ageing phenomenon is mainly manifested in two aspects: first is that physiological function is low.Sebaceous glands, sweat gland deterioration,
Sweat and sebum exclude to reduce, and skin gradually loses gloss in the past and becomes drying.Blood circulation hypofunction is to supplement skin
Necessary nutrition, therefore the refractory conjunction of the elderly's skin wound.Second is that skin histology fails.The thickness of skin with the age increase
And it substantially change.Most thick at the epidermis of people 20 years old, later gradually thinning, atrophic to disappearing to senescence phase stratum granulosum, spine is thin
Born of the same parents' short survival.Epidermal cell nuclear fission increases, therefore melanin also increases, so that the colour of skin of the elderly is mostly brownish black.With
The raising of people's quality of life, anti-aging whitening return to the topic that the youth pays close attention at the majority of consumers.
Currently there are improvement skin quality cosmetics, majority is all engineer, although effect is preferable,
The ingredient being often harmful to the human body containing various heavy, hormone etc., long-time service can generate dependence and the damage to body.
Therefore it provides a kind of cosmetics of the improvement skin quality of safety, applicability extensively have realistic meaning.
Moisturiser can be obviously improved skin as a kind of common skin care item.But existing moisturiser function
It is single, exist and have the chemical substance centainly injured to skin, therefore it provides a kind of have both moist moisturizing, mention containing natural component
The moisturiser of skin lightening color has important practical significance.
Summary of the invention
In view of this, the present invention provides a kind of moisturising preparations and preparation method thereof.The moisturising preparations, which have, to be moistened moisturizing, mentions
The effect of high colour of skin.
In order to achieve the above-mentioned object of the invention, the present invention the following technical schemes are provided:
The present invention provides acceptable auxiliary agents in a kind of moisturising preparations, including extractive of flax seed and cosmetics；
The extractive of flax seed includes flaxseed gum and linseed oil；
The flaxseed gum the preparation method comprises the following steps: mechanical stirring after taking linseed to mix with water, be collected by filtration dense after filtrate
Precipitating is collected in contracting, alcohol precipitation after filtering, dry after dehydration；
The linseed oil the preparation method comprises the following steps: take linseed squeezing collect feedstock oil, mixed with salt, degumming after sedimentation,
It is cooling, it filters, dewaxing.
In some specific embodiments of the invention, the content of the flaxseed gum is 0.01w/w%~5w/w%；Institute
The content for stating linseed oil is 0.1w/w%~15w/w%.
In some specific embodiments of the invention, in the preparation method of the flaxseed gum, the matter of linseed and water
Amount is than being 1:(7~10)；The churned mechanically temperature be 95 DEG C~100 DEG C, the churned mechanically time be 20~
30min；The cocnentration factor is be concentrated into original volume 1/3~1/5；The alcohol precipitation be according to 1:(1.5~2) volume ratio and second
Alcohol precipitation is carried out after alcohol mixing；The temperature of the dehydration is 105 DEG C~115 DEG C；Moisture content < 12% after the drying.
In some specific embodiments of the invention, in the preparation method of the linseed oil, the temperature of the squeezing
It is 80~100 DEG C, the salt additional amount is the 0.1~0.5% of the quality of the feedstock oil；The time of the sedimentation is 3~8h；
The temperature of the cooling is 20~30 DEG C；It is described be filtered into filtering and impurity removing after, be cooled to 0-10 DEG C, the matter of the feedstock oil be added
The super-cell of the 1-3% of amount filters after stirring 15~20min；Linolenic acid content > 45% in the linseed oil.
In some specific embodiments of the invention, acceptable auxiliary agent includes moisturizer, antiallergic in the cosmetics
It is more than one or both of agent, chelating agent, thickener, emulsifier, cosolvent, antioxidant, acid-base modifier or preservative
Mixture.
In some specific embodiments of the invention, the moisturizer includes allantoin, glycerol, 1,3-PD, hydrogen
Change the mixture of one or both of jojoba oil, Butyrospermum parkii fruit fatty oil or Sodium Hyaluronate or more；
The chelating agent is EDETATE SODIUM；
The thickener is cetostearyl alcohol or Sodium Hyaluronate；
The emulsifier is spermaceti hard base glucoside；
The cosolvent is ring five dimethyl silicone polymer；
The antioxidant is tocopherol acetate；
The anti-sensitizer is allantoin；
The acid-base modifier is triethanolamine；
In terms of mass percentage, the moisturising preparations include following component:
The present invention also provides application of the moisturising preparations in skin moisture-keeping.
The present invention also provides the preparation methods of the moisturising preparations, take in extractive of flax seed and cosmetics and are subjected to
Auxiliary agent mixing；
The extractive of flax seed includes flaxseed gum and linseed oil；
The flaxseed gum the preparation method comprises the following steps: mechanical stirring after taking linseed to mix with water, be collected by filtration dense after filtrate
Precipitating is collected in contracting, alcohol precipitation after filtering, dry after dehydration；
The linseed oil the preparation method comprises the following steps: take linseed squeezing collect feedstock oil, mixed with salt, degumming after sedimentation,
It is cooling, it filters, dewaxing.
In some specific embodiments of the invention, in the preparation method of the flaxseed gum, the matter of linseed and water
Amount is than being 1:(7~10)；The churned mechanically temperature be 95 DEG C~100 DEG C, the churned mechanically time be 20~
30min；The cocnentration factor is be concentrated into original volume 1/3~1/5；The alcohol precipitation be according to 1:(1.5~2) volume ratio and second
Alcohol precipitation is carried out after alcohol mixing；The temperature of the dehydration is 105 DEG C~115 DEG C；Moisture content < 12% after the drying；
In the preparation method of the linseed oil, the temperature of the squeezing is 80~100 DEG C, and the salt additional amount is described
The 0.1~0.5% of the quality of feedstock oil；The time of the sedimentation is 3~8h；The temperature of the cooling is 20~30 DEG C；It is described
After being filtered into filtering and impurity removing, it is cooled to 0-10 DEG C, the super-cell of the 1-3% of the quality of the feedstock oil is added, is stirred
It is filtered after 15~20min；Linolenic acid content > 45% in the linseed oil.
The present invention also provides the preparation method of moisturising preparations,
In terms of mass percentage, the moisturising preparations include following component:
Include the following steps:
Step 1: mixing after 20~30 DEG C mix water with the flaxseed gum, then with B component, stirred in 85~90 DEG C
30min, under conditions of vacuum degree -0.2MPa after homogeneous, with the stirring of 60r/min revolving speed；Step 2: taking component C in 20~30 DEG C
It is mixed after being heated to 85 DEG C with the product of step 1, vacuum homogeneous is cooled to 50~55 DEG C, mixes with component D, in vacuum degree-
1-3min is emulsified with 6000rpm homogeneous speed matter under the conditions of 0.2MPa.
In some specific embodiments of the invention, the moisturising preparations are moisturiser.
Specifically, a kind of preparation method of linseed essence moisturiser provided by the invention, steps are as follows:
(1) flaxseed gum is prepared: the seed water ratio of 1:7-1:10 in mass ratio, 95 DEG C of mechanical stirrings after linseed is cleaned
30min.After being separated by solid-liquid separation, it is concentrated in vacuo filtrate, is concentrated into 1/3-the 1/5 of original volume.Concentrate is added by 1:1.5 volume ratio
Enter ethyl alcohol and carries out alcohol precipitating.Alcohol precipitation filiform precipitating 105 DEG C of heated-air drying to moisture contents after filtering, press dewatering are less than
12%, crushed after being dried obtains powdered product.
(2) it prepares linseed oil: after the selected dedusting of linseed, squeezing out feedstock oil at 80-100 DEG C.After being heated to 50 DEG C,
The edible iodizedsalt of raw material oil mass 0.1-0.5% is added, stirs 15-30min, settles degumming after 3-8h.Degummed oil is cooled to 20-
30 DEG C, impurity screening.It is cooled to 0-10 DEG C, the super-cell of oil weight 1-3% is added, is filtered after stirring 15min.It is repeatedly de-
After cured filtering, product is obtained.
(3) select linseed oil: linolenic acid content is greater than 45% and is prepared in selection linseed oil.
(4) moisturiser stoste is prepared:
A, by each component precise in component C to containers for future use under the conditions of 25 DEG C ± 5 DEG C.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization under the conditions of 25 DEG C ± 5 DEG C, it is spare.By load weighted deionized water
It is put into emulsion pot, homogeneous speed is 3000rpm, and flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.It is stirred under room temperature
30min enables flaxseed gum to be sufficiently swollen.B component raw material, 85-90 DEG C of stirring 30min, in vacuum degree -0.2MPa condition is added
Lower homogeneous is stirred at low speed to exquisiteness with 60r/min revolving speed.
C, load weighted C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling water drop
Temperature stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Under the conditions of vacuum degree -0.2MPa with
6000rpm homogeneous speed matter emulsifies 1-3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, use
Product is made in 100 mesh screens.
(5) it prepares moisturiser: by the moisturiser stoste sealed package, moisturiser is made.
The present invention provides a kind of moisturising preparations, specially a kind of moisturiser, moisturiser, which has skin, to be moistened moisturizing, mentions
The effect of skin lightening color.
Specific embodiment
The invention discloses a kind of moisturiser and preparation method thereof, those skilled in the art can use for reference present disclosure, fit
When improvement realization of process parameters.In particular, it should be pointed out that all similar substitutions and modifications are for a person skilled in the art
It is it will be apparent that they are considered as being included in the present invention.Method of the invention and application passed through preferred embodiment into
Gone description, related personnel obviously can not depart from the content of present invention, in spirit and scope to method described herein and application
It is modified or appropriate changes and combinations, carrys out implementation and application the technology of the present invention.
Raw materials used and reagent is available on the market in moisturiser provided by the invention and preparation method thereof.
Below with reference to embodiment, the present invention is further explained:
The preparation of 1 linseed essence moisturiser of embodiment
S1. the preparation of linseed oil: after the selected dedusting of linseed, feedstock oil is squeezed out at 80 DEG C；Feedstock oil is heated to 50
DEG C, the edible iodizedsalt of 0.1% oil mass is added, stirs 15min, stops stirring, settles 3h degumming；Degummed oil is cooled to 20 DEG C,
Filter out impurity；10 DEG C are continued cool to, the super-cell that oil weighs 1%, stirring 15min filtering is added；Multiple dewaxing mistake
After filter, finished product linseed oil is obtained.
S2. the selection of linseed oil: selection linolenic acid content is greater than 45% linseed oil.
S3. the preparation of flaxseed gum: linseed clean after in 1:7 seed water ratio, under mechanical stirring 95 DEG C extraction
30min；It is separated by solid-liquid separation, filtrate is concentrated in vacuo, and the 1/3 of original volume is concentrated into；Ethyl alcohol is added by 1:1.5 volume ratio in concentrate
Carry out alcohol precipitation；Alcohol precipitation filiform precipitating through filtering, after press dewatering 105 DEG C of heated-air dryings to moisture content less than 12%；After drying
Crushing obtains powdery flaxseed gum.
S4. weigh each split-phase: A by following mass ratio: water is surplus, flaxseed gum 0.01%；B: allantoin 0.3%,
EDETATE SODIUM 0.05%, glycerol 2.0%, 1,3- propylene glycol 2.0%, carbomer 0.1%；C: linseed oil 0.1%, cetearyl alcohol
Pure and mild cetearyl glucoside 2.0%, cetostearyl alcohol 1.0%, hydrogenated jojoba oil 1.0%, five polydimethylsiloxanes of ring
Alkane 1.0%, Butyrospermum parkii fruit fatty oil 0.5%, tocopherol acetate 0.5%；D: Sodium Hyaluronate 0.01%, triethanolamine
0.1%, no added preservative 0.6%.
S5. above-mentioned substance is operated according to the following steps, prepares stoste:
A, at 20 °C by each component precise in component C to containers for future use.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization at 20 °C, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.30min is stirred under room temperature, makes Asia
Numb seed glue can be sufficiently swollen.B component raw material is added, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness, low speed stir under vacuum conditions
It mixes.
C, load weighted C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling water drop
Temperature stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying 1- under vacuum conditions
3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharging, inspection declaration.
S6. by above-mentioned 50g moisturiser stoste sealed package, moisturiser is made in sterilizing.
The preparation of 2 linseed essence moisturiser of embodiment
S1. the preparation of linseed oil: after the selected dedusting of linseed, feedstock oil is squeezed out at 85 DEG C；Feedstock oil is heated to 50
DEG C, the edible iodizedsalt of 0.3% oil mass is added, stirs 20min, stops stirring, settles 5h degumming；Degummed oil is cooled to 22 DEG C,
Filter out impurity；5 DEG C are continued cool to, the super-cell that oil weighs 2%, stirring 15min filtering is added；Multiple dewaxing filtering
Afterwards, finished product linseed oil is obtained.
S2. the selection of linseed oil: selection linolenic acid content is greater than 45% linseed oil.
S3. the preparation of flaxseed gum: linseed clean after in 1:8 seed water ratio, under mechanical stirring 95 DEG C extraction
30min；It is separated by solid-liquid separation, filtrate is concentrated in vacuo, and the 1/4 of original volume is concentrated into；Ethyl alcohol is added by 1:1.5 volume ratio in concentrate
Carry out alcohol precipitation；Alcohol precipitation filiform precipitating through filtering, after press dewatering 105 DEG C of heated-air dryings to moisture content less than 12%；After drying
Crushing obtains powdery flaxseed gum.
S4. weigh each split-phase: A by following mass ratio: water is surplus, flaxseed gum 0.2%；B: allantoin 0.2%, EDTA
Disodium 0.1%, glycerol 3.0%, 1,3- propylene glycol 3.0%, carbomer 0.2%；C: the pure and mild whale of linseed oil 7%, cetearyl alcohol
Wax stearyl glucoside 2.0%, cetostearyl alcohol 3.0%, hydrogenated jojoba oil 3.0%, ring five dimethyl silicone polymer
3.0%, Butyrospermum parkii fruit fatty oil 0.1%, tocopherol acetate 1.0%；D: Sodium Hyaluronate 0.05%, triethanolamine 0.3%,
No added preservative 0.6%.
S5. above-mentioned substance is operated according to the following steps, prepares stoste:
A, by each component precise in component C to containers for future use under the conditions of 30 DEG C.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization under the conditions of 30 DEG C, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.30min is stirred under room temperature, makes Asia
Numb seed glue can be sufficiently swollen.B component raw material is added, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness, low speed stir under vacuum conditions
It mixes.
C, load weighted C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling water drop
Temperature stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying 1- under vacuum conditions
3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharging, inspection declaration.
S6. by above-mentioned 40g moisturiser stoste sealed package, moisturiser is made in sterilizing.
The preparation of 3 linseed essence moisturiser of embodiment
S1. the preparation of linseed oil: after the selected dedusting of linseed, feedstock oil is squeezed out at 90 DEG C；Feedstock oil is heated to 50
DEG C, the edible iodizedsalt of 0.2% oil mass is added, stirs 23min, stops stirring, settles 5h degumming；Degummed oil is cooled to 24 DEG C,
Filter out impurity；0 DEG C is continued cool to, the super-cell that oil weighs 2%, stirring 15min filtering is added；Multiple dewaxing filtering
Afterwards, finished product linseed oil is obtained.
S2. the selection of linseed oil: selection linolenic acid content is greater than 45% linseed oil.
S3. the preparation of flaxseed gum: linseed clean after in 1:9 seed water ratio, under mechanical stirring 95 DEG C extraction
30min；It is separated by solid-liquid separation, filtrate is concentrated in vacuo, and the 1/5 of original volume is concentrated into；Ethyl alcohol is added by 1:1.5 volume ratio in concentrate
Carry out alcohol precipitation；Alcohol precipitation filiform precipitating through filtering, after press dewatering 105 DEG C of heated-air dryings to moisture content less than 12%；After drying
Crushing obtains powdery flaxseed gum.
S4. weigh each split-phase: A by following mass ratio: water is surplus, flaxseed gum 2.0%；B: allantoin 0.3%, EDTA
Disodium 0.3%, glycerol 4.0%, 1,3- propylene glycol 2.0%, carbomer 0.3%；C: the pure and mild whale of linseed oil 10%, cetearyl alcohol
Wax stearyl glucoside 2.0%, cetostearyl alcohol 3.0%, hydrogenated jojoba oil 3.0%, ring five dimethyl silicone polymer
1.0%, Butyrospermum parkii fruit fatty oil 3.0%, tocopherol acetate 1.0%；D: Sodium Hyaluronate 0.05%, triethanolamine 0.2%,
No added preservative 0.6%.
S5. above-mentioned substance is operated according to the following steps, prepares stoste:
A, by each component precise in component C to containers for future use under the conditions of 25 DEG C.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization under the conditions of 25 DEG C, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.30min is stirred under room temperature, makes Asia
Numb seed glue can be sufficiently swollen.B component raw material is added, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness, low speed stir under vacuum conditions
It mixes.
C, load weighted C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling water drop
Temperature stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying 1- under vacuum conditions
3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharging, inspection declaration.
S6. by above-mentioned 35g moisturiser stoste sealed package, moisturiser is made in sterilizing.
The preparation of 4 linseed essence moisturiser of embodiment
S1. the preparation of linseed oil: after the selected dedusting of linseed, feedstock oil is squeezed out at 100 DEG C；Feedstock oil is heated to 50
DEG C, the edible iodizedsalt of 0.5% oil mass is added, stirs 30min, stops stirring, settles 8h degumming；Degummed oil is cooled to 30 DEG C,
Filter out impurity；6 DEG C are continued cool to, the super-cell that oil weighs 3%, stirring 15min filtering is added；Multiple dewaxing filtering
Afterwards, finished product linseed oil is obtained.
S2. the selection of linseed oil: selection linolenic acid content is greater than 45% linseed oil.
S3. the preparation of flaxseed gum: linseed clean after in 1:10 seed water ratio, under mechanical stirring 95 DEG C extraction
30min；It is separated by solid-liquid separation, filtrate is concentrated in vacuo, and the 1/5 of original volume is concentrated into；Ethyl alcohol is added by 1:1.5 volume ratio in concentrate
Carry out alcohol precipitation；Alcohol precipitation filiform precipitating through filtering, after press dewatering 105 DEG C of heated-air dryings to moisture content less than 12%；After drying
Crushing obtains powdery flaxseed gum.
S4. weigh each split-phase A by following mass ratio: water is surplus, flaxseed gum 5.0%；B: allantoin 0.3%, EDTA
Disodium 0.3%, glycerol 5.0%, 1,3- propylene glycol 5.0%, carbomer 0.1%；C: the pure and mild whale of linseed oil 15%, cetearyl alcohol
Wax stearyl glucoside 3.0%, cetostearyl alcohol 1.0%, hydrogenated jojoba oil 2.0%, ring five dimethyl silicone polymer
3.0%, Butyrospermum parkii fruit fatty oil 2.0%, tocopherol acetate 1.0%；D: Sodium Hyaluronate 0.1%, triethanolamine 0.3%,
No added preservative 0.6%.
S5. above-mentioned substance is operated according to the following steps, prepares stoste:
A, by each component precise in component C to containers for future use under the conditions of 28 DEG C.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization under the conditions of 28 DEG C, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.30min is stirred under room temperature, makes Asia
Numb seed glue can be sufficiently swollen.B component raw material is added, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness, low speed stir under vacuum conditions
It mixes.
C, load weighted component C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling
Water cooling, stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying under vacuum conditions
1-3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharge, report
Inspection.
S6. by above-mentioned 30g moisturiser stoste sealed package, moisturiser is made in sterilizing.
Embodiment 5
The detection that physical and chemical index and microbiological indicator are carried out to moisturiser prepared by embodiment 1 to 4, the results are shown in Table 1, table 2.
1 physical and chemical index of table
2 microbiological indicator of table
Testing result is shown, in the moisturising preparations provided through the invention, reduces the heavy metals such as lead, total arsenic, total mercury
Content controls the content of lead within 1.3mg/kg, and the content of total arsenic controls within 1.1mg/kg, and the content of total mercury controls
It within 0.25mg/kg, has no toxic and side effect to human body, and microorganism indices reach criterion of acceptability.
Comparative example 1
Weigh each split-phase: A by following mass ratio: water is surplus；B: allantoin 0.3%, EDETATE SODIUM 0.3%, glycerol
5.0%, 1,3- propylene glycol 2.0%, carbomer 0.1%；C: the pure and mild cetearyl glucoside 3.0% of cetearyl alcohol, spermaceti are hard
Lipidol 1%, hydrogenated jojoba oil 1%, ring five dimethyl silicone polymer 1%, Butyrospermum parkii fruit fatty oil 3%, tocopherol acetate
1.0%；D: Sodium Hyaluronate 0.1%, triethanolamine 0.1%, no added preservative 0.6%.
Above-mentioned substance is operated according to the following steps, prepares stoste:
A, at room temperature by each component precise in component C to containers for future use.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization at room temperature, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, is added B component raw material, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness under vacuum conditions,
It stirs at low speed.
C, load weighted component C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling
Water cooling, stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying under vacuum conditions
1-3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharge, report
Inspection.
By above-mentioned 35g moisturiser stoste sealed package, moisturiser is made in sterilizing.
Comparative example 2
Weigh each split-phase: A by following mass ratio: water is surplus, flaxseed gum 0.5%；B: allantoin 0.3%, EDTA bis-
Sodium 0.3%, glycerol 5.0%, 1,3- propylene glycol 2.0%, carbomer 0.1%；C: the pure and mild cetearyl glucoside of cetearyl alcohol
3.0%, cetostearyl alcohol 1%, hydrogenated jojoba oil 1%, ring five dimethyl silicone polymer 1%, Butyrospermum parkii fruit fatty oil 3%,
Tocopherol acetate 1.0%；D: Sodium Hyaluronate 0.1%, triethanolamine 0.1%, no added preservative 0.6%.
S5. above-mentioned substance is operated according to the following steps, prepares stoste:
A, at room temperature by each component precise in component C to containers for future use.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization at room temperature, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.30min is stirred under room temperature, makes Asia
Numb seed glue can be sufficiently swollen.B component raw material is added, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness, low speed stir under vacuum conditions
It mixes.
C, load weighted component C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling
Water cooling, stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying under vacuum conditions
1-3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharge, report
Inspection.
S6. by above-mentioned 35g moisturiser stoste sealed package, moisturiser is made in sterilizing.
Comparative example 3
Weigh each split-phase: A by following mass ratio: water is surplus；B: allantoin 0.3%, EDETATE SODIUM 0.3%, glycerol
5.0%, 1,3- propylene glycol 2.0%, carbomer 0.1%；C: the pure and mild cetearyl glucoside of linseed oil 10%, cetearyl alcohol
3.0%, cetostearyl alcohol 1%, hydrogenated jojoba oil 1%, ring five dimethyl silicone polymer 1%, Butyrospermum parkii fruit fatty oil 3%,
Tocopherol acetate 1.0%；D: Sodium Hyaluronate 0.1%, triethanolamine 0.1%, no added preservative 0.6%.
S5. above-mentioned substance is operated according to the following steps, prepares stoste:
A, at room temperature by each component precise in component C to containers for future use.
B, emulsion pot is cleaned up into simultaneously high-temperature sterilization at room temperature, it is spare.Load weighted deionized water is put into
In emulsion pot, low speed homogeneous is opened, flaxseed gum is added, guarantees that flaxseed gum is unable to conglomeration.30min is stirred under room temperature, makes Asia
Numb seed glue can be sufficiently swollen.B component raw material is added, 85-90 DEG C of stirring 30min, homogeneous to exquisiteness, low speed stir under vacuum conditions
It mixes.
C, load weighted component C is heated in 85 DEG C of addition component B, under vacuum conditions homogeneous to exquisiteness, leads to cooling
Water cooling, stirs at low speed；When being cooled to 50-55 DEG C, component D raw material is added and stirs to dissolution.Emulsifying under vacuum conditions
1-3min.After sampling, detection emulsification sophistication and consistency, appearance and physical and chemical inspection qualification, with 100 mesh screens, discharge, report
Inspection.
S6. by above-mentioned 35g moisturiser stoste sealed package, moisturiser is made in sterilizing.
9 measure of merit of embodiment
240 ages (20-45 one full year of life) of volunteer, are randomly divided into 8 groups, every group of 30 people, try out respectively commercially available moisturizing face cream,
The moisturizing face cream that the moisturizing face cream and comparative example 1~3 that embodiment 1-4 is provided provide.Application method are as follows: daily sooner or later close to same
Time smears face, persistently uses 28 day time, then collects as a result, summarize test data, is shown in Table 3.
Table 3
Note:*Show compared with commercially available moisturizing face cream have significant difference (P < 0.05)；**Show compared with commercially available moisturizing face cream,
With extremely significant difference (P < 0.01)；
#Show compared with comparative example 1~3 have significant difference (P < 0.05)；##Show that compared with comparative example 1~3, there is pole
Significant difference (P < 0.01)；
Compared with control group 1~3, the whitening effect and moistening effect of experimental group 1~4 are significantly better than that pair experimental group 1~4
According to group 1~3, in irritant experiment, the nonirritant situation of all raw materials.
Illustrate the moisturizing face cream of the offer of the embodiment of the present invention 1~4 while with good performance of keeping humidity, it may have
Low irritant and good whitening performance.
The test of 10 anti-oxidation efficacy of embodiment
The anti-of Examples 1 to 4 and the obtained moisturizing face cream of comparative example 1~3 is measured by DPPH free radical scavenging ability
Oxidation efficiency.
Experimental group: product made from Examples 1 to 4；
Control group: product made from comparative example 1~3；
Commercially available moisturizing face cream；
Positive controls: reference substance VC。
0.02604gDPPH (percentage composition 96%) is accurately weighed, is that 95% ethyl alcohol dissolution constant volume arrives with volumetric concentration
100mL, DPPH concentration store for future use for 0.25gL-1.95% ethyl alcohol of the DPPH solution of 12mL0.25gL-1 is taken when experiment
Constant volume 100mL, DPPH concentration is 0.03gL-1.It is reference solution, timebase with 95% ethyl alcohol.Measure 0.03gL-1's
DPPH solution scans a length of 518nm of maximum absorption wave at 400-600nm.
The measurement of blank control absorbance: taking the DPPH solution of 5mL0.03gL-1 into the EP pipe of 10mL specification, then plus
Enter the ethanol solution that 0.1mL volumetric concentration is 95%, mixing.Its absorbance is measured at 518nm, is denoted as A0。
The measurement of prepare liquid absorbance: it takes the DPPH solution of 5mL0.03gL-1 into EP pipe, it is to be measured to add 0.1mL
Liquid mixes.Its absorbance is measured at 518nm, is denoted as Ai。
Data achieved above are calculated clearance rate E, E=1-Ai/A0 × 100% by data processing as follows.
Obtained free radical scavenging activity result is measured referring to table 4:
Table 4: Solution Free Radical clearance rate
Note:*Show compared with commercially available moisturizing face cream have significant difference (P < 0.05)；**Show compared with commercially available moisturizing face cream,
With extremely significant difference (P < 0.01)；
#Show compared with control group 2~3 have significant difference (P < 0.05)；##Show that compared with control group 2~3, there is pole
Significant difference (P < 0.01)；
As can be drawn from Table 4, the DPPH free radical scavenging activity Yu control group 1~3, commercially available moisturizing face cream of experimental group 1~4 and
Positive controls VCIt compares, Yao Mingxian (P < 0.05) is higher than positive controls, commercially available moisturizing face cream and control group 1~3, it was demonstrated that
The DPPH radicals scavenging effect of moisturizing face cream produced by the present invention obviously (P < 0.05) will be better than reference substance VC, therefore, this hair
Bright pack preparation obtained has good oxidation resistant effect, plays the effect of bright color.
Embodiment 11
The moistening effect of skin all has direct relation with moisture content of skin, so test moisture content of skin is also the one of evaluation
A important indicator.
Selection volunteer 240, women, the age 29-45 years old.It is divided into experimental group 1~4 and control group 1~3, commercially available moisturizing
Face cream, every group 30.
Experimental group includes experimental group 1~4, smears an embodiment of the present invention 1 to 4 before canthus is slept daily on the left of volunteer
The pack preparation of offer, right side canthus smears glycerol, continues 1 month, behind 2 weeks and 4 weeks, carries out skin to canthus skin and contains
Water testing.
Control group includes control group 1~3 and commercially available moisturizing face cream group, and canthus is slept daily on the left of the volunteer of control group 1~3
The pack preparation that a control group 1 to 3 provides is smeared before feeling, right side canthus smears glycerol, continues 1 month, use 2 weeks and 4 weeks
Afterwards, moisture content of skin test is carried out to canthus skin.
Primary commercially available moisturizing face cream, right side canthus are smeared before sleeping daily in commercially available moisturizing face cream group, volunteer left side canthus
Glycerol is smeared, continues 1 month, behind 2 weeks and 4 weeks, moisture content of skin test is carried out to canthus skin.
Moisture of skin tester (Courage+Khazaka CM825, Germany) can reflect skin keratin according to capacitance
Water content in layer, water content of stratum corneum is higher, and capacitance is also higher；Vice versa.The instrument is believed to accurately examine
Survey keratoderma water content.The aqueous level of application area skin around volunteer canthus is tested with moisture of skin tester,
It is measured in parallel 3 times when measurement in test zone, takes its average value, the results are shown in Table 5.
The moistening effect of 5 moisturizing face cream of table is analyzed
Note: every group of left eye with right eye compare compared with,*P < 0.05 has significant difference,**P < 0.01 has extremely significant difference
It is different；
Experimental group compared with the control group,#P < 0.05 has significant difference,##P < 0.01 has extremely significant difference.
The result shows that the moisturizing face cream that experimental group left eye compared with right eye compares, is provided through the embodiment of the present invention 1 to 4 applies
After smearing, moisture content of skin significant (P < 0.05) increases.Compared with the control group, experimental group is apparently higher than control group skin to experimental group
Water content.
Embodiment 12
Respectively in Xi'an, Zhengzhou, Shenyang, 500 people of each random investigation in Jinan and 5, Kweiyang city, respectively to of the invention real
The moisturizing face cream for applying the preparation of example 1 to 4 is tested and assessed, and the index of quality is the improvement, right of irritation, fragrance, Huang dim to the colour of skin
The improvement of pachylosis, to cutis laxa and to the improvement of skin lines, evaluation criterion is shown in Table 6, and evaluating result is shown in
Table 7.
6 sense evaluation standard of table
7 evaluating result of table
The masses are investigated in 500 participation, and the irritation satisfaction rate to moisturizing face cream made from the embodiment of the present invention 1 to 4 is
94.6%, fragrance satisfaction rate is 93.0%, and the satisfaction rate of Huang improvement dim to skin is 90.2%, improves to pachylosis and imitates
The satisfaction rate of fruit is 87.2%, and the satisfaction rate to cutis laxa improvement is 93.8%, to the satisfaction rate of microgroove improvement
It is 95.8%, is approved and like by the majority of consumers.
13 Detection of Stability of embodiment
According to embodiments of the present invention 1 places 24 months to moisturizing face cream prepared by embodiment 4 under normal temperature stock condition, respectively
Item Testing index all meets statutory standards, illustrates that this quality is stablized.
The above is only a preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, various improvements and modifications may be made without departing from the principle of the present invention, these improvements and modifications are also answered
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of moisturising preparations, which is characterized in that including acceptable auxiliary agent in extractive of flax seed and cosmetics；
The extractive of flax seed includes flaxseed gum and linseed oil；
The flaxseed gum the preparation method comprises the following steps: mechanical stirring after taking linseed to mix with water, is collected by filtration concentration, alcohol after filtrate
It is heavy, precipitating is collected after filtering, it is dry after dehydration；
The linseed oil the preparation method comprises the following steps: take linseed squeezing collect feedstock oil, mix with salt, degumming after sedimentation, cool down,
Filtering, dewaxing.
2. moisturising preparations according to claim 1, which is characterized in that the content of the flaxseed gum be 0.01w/w%~
5w/w%；The content of the linseed oil is 0.1w/w%~15w/w%.
3. moisturising preparations according to claim 1 or 2, which is characterized in that in the preparation method of the flaxseed gum, flax
The mass ratio of seed and water is 1:(7~10)；The churned mechanically temperature is 95 DEG C~100 DEG C, the churned mechanically time
For 20~30min；The cocnentration factor is be concentrated into original volume 1/3~1/5；The alcohol precipitation be according to 1:(1.5~2) volume
Than carrying out alcohol precipitation after mixing with ethyl alcohol；The temperature of the dehydration is 105 DEG C~115 DEG C；Moisture content < 12% after the drying.
4. moisturising preparations according to any one of claims 1 to 3, which is characterized in that the preparation method of the linseed oil
In, the temperature of the squeezing is 80~100 DEG C, and the salt additional amount is the 0.1~0.5% of the quality of the feedstock oil；It is described
The time of sedimentation is 3~8h；The temperature of the cooling is 20~30 DEG C；It is described be filtered into filtering and impurity removing after, be cooled to 0-10 DEG C,
The super-cell of the 1-3% of the quality of the feedstock oil is added, is filtered after stirring 15~20min；In the linseed oil
Linolenic acid content > 45%.
5. moisturising preparations according to any one of claims 1 to 4, which is characterized in that acceptable in the cosmetics to help
Agent includes in moisturizer, anti-sensitizer, chelating agent, thickener, emulsifier, cosolvent, antioxidant, acid-base modifier or preservative
One or both more than mixture.
6. moisturising preparations according to claim 5, which is characterized in that the moisturizer includes allantoin, glycerol, 1,3- third
Mixture more than one or both of glycol, hydrogenated jojoba oil, Butyrospermum parkii fruit fatty oil or Sodium Hyaluronate；
The chelating agent is EDETATE SODIUM；
The thickener is cetostearyl alcohol or Sodium Hyaluronate；
The emulsifier is spermaceti hard base glucoside；
The cosolvent is ring five dimethyl silicone polymer；
The antioxidant is tocopherol acetate；
The anti-sensitizer is allantoin；
The acid-base modifier is triethanolamine；
In terms of mass percentage, the moisturising preparations include following component:
7. application of the moisturising preparations according to any one of claims 1 to 6 in skin moisture-keeping.
8. the preparation method of moisturising preparations according to any one of claims 1 to 6, which is characterized in that linseed is taken to extract
Object is mixed with auxiliary agent acceptable in cosmetics；
The extractive of flax seed includes flaxseed gum and linseed oil；
The flaxseed gum the preparation method comprises the following steps: mechanical stirring after taking linseed to mix with water, is collected by filtration concentration, alcohol after filtrate
It is heavy, precipitating is collected after filtering, it is dry after dehydration；
The linseed oil the preparation method comprises the following steps: take linseed squeezing collect feedstock oil, mix with salt, degumming after sedimentation, cool down,
Filtering, dewaxing.
9. preparation method according to claim 8, which is characterized in that in the preparation method of the flaxseed gum, linseed
Mass ratio with water is 1:(7~10)；The churned mechanically temperature is 95 DEG C~100 DEG C, and the churned mechanically time is
20~30min；The cocnentration factor is be concentrated into original volume 1/3~1/5；The alcohol precipitation be according to 1:(1.5~2) volume ratio
Alcohol precipitation is carried out after mixing with ethyl alcohol；The temperature of the dehydration is 105 DEG C~115 DEG C；Moisture content < 12% after the drying；
In the preparation method of the linseed oil, the temperature of the squeezing is 80~100 DEG C, and the salt additional amount is the raw material
The 0.1~0.5% of the quality of oil；The time of the sedimentation is 3~8h；The temperature of the cooling is 20~30 DEG C；The filtering
After filtering and impurity removing, it is cooled to 0-10 DEG C, is added the super-cell of the 1-3% of the quality of the feedstock oil, stirring 15~
It is filtered after 20min；Linolenic acid content > 45% in the linseed oil.
10. the preparation method of moisturising preparations according to claim 6, which comprises the steps of:
Step 1: mixing after 20~30 DEG C mix water with the flaxseed gum, then with B component, stirred in 85~90 DEG C
30min, under conditions of vacuum degree -0.2MPa after homogeneous, with the stirring of 60r/min revolving speed；
Step 2: it is mixed after taking component C to be heated to 85 DEG C in 20~30 DEG C with the product of step 1, vacuum homogeneous, it is cooled to 50~
It 55 DEG C, is mixed with component D, 1-3min is emulsified with 6000rpm homogeneous speed matter under the conditions of vacuum degree -0.2MPa.
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| CN109966182A (en) * | 2019-04-30 | 2019-07-05 | 莱博药妆技术（上海）股份有限公司 | A kind of cosmetics and preparation method thereof containing linseed oil |
| CN110090181A (en) * | 2019-04-16 | 2019-08-06 | 上海悦目化妆品有限公司 | A kind of preparation method and applications of linseed emulsifier |
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| CN104739716A (en) * | 2015-03-04 | 2015-07-01 | 上海应用技术学院 | Toning lotion with flaxseed gum extract and preparation method of toning lotion with flaxseed gum extract |
| CN106619268A (en) * | 2016-10-13 | 2017-05-10 | 姚晓宁 | Linseed moisture mask and preparation method |
| CN108685756A (en) * | 2017-04-06 | 2018-10-23 | 姚晓宁 | Natural and multi-functional facial mask and preparation method thereof |
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| CN104739716A (en) * | 2015-03-04 | 2015-07-01 | 上海应用技术学院 | Toning lotion with flaxseed gum extract and preparation method of toning lotion with flaxseed gum extract |
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