CN104739716A - Toning lotion with flaxseed gum extract and preparation method of toning lotion with flaxseed gum extract - Google Patents
Toning lotion with flaxseed gum extract and preparation method of toning lotion with flaxseed gum extract Download PDFInfo
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- CN104739716A CN104739716A CN201510096496.1A CN201510096496A CN104739716A CN 104739716 A CN104739716 A CN 104739716A CN 201510096496 A CN201510096496 A CN 201510096496A CN 104739716 A CN104739716 A CN 104739716A
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- semen lini
- extracting solution
- lini glue
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Abstract
The invention discloses toning lotion with flaxseed gum extract and a preparation method of the toning lotion with flaxseed gum extract. The toning lotion with flaxseed gum extract comprises the following raw materials in percentages by weight: 68.00-94.90% of flaxseed gum extract, 5-25.02% of moisturizing agent, 0-3% of rheological adjusting agent, 0-3% of solubilizer and 0.1-1% of preservative. The preparation method comprises the following steps: adding sodium hyaluronate in the moisturizing agent and the rheological adjusting agent of transparent xanthan gum into the flaxseed gum extract under the condition of stirring; uniformly stirring the mixture until complete dissolution is realized; adding the rest components in the moisturizing agent into the mixture and uniformly stirring until complete dissolution is realized; then adding the preservative and the solubilizer into the mixture and uniformly stirring until complete dissolution is realized, so that the toning lotion with flaxseed gum extract is obtained. The toning lotion has the advantages of low excitability and good moisture retention and is capable of improving skin elasticity and permeability; moreover, the toning lotion also has good anti-inflammatory performance. The preparation technology of the toning lotion is simple and feasible.
Description
Technical field
The present invention relates to a kind of astringent containing Semen Lini glue extracting solution and preparation method thereof, belong to cosmetic technical field.
Background technology
Linum flax family (Linaceae), be one of the most ancient crop, mainly originate in Canada, India, the U.S., Argentina and the former Soviet Union, China is also one of main product state of Caulis et Folium Lini.Semen Lini by seed coat, endosperm and embryo three part form, Semen Lini glue is just mainly distributed in the kind Intradermal accounting for Semen Lini full weight 39.Semen Lini glue is a kind of plant gum based on polysaccharide, and contains the natural polymer compound adhesive of a small amount of protein and mineral element.
Semen Lini glue has that composition is high, viscosity is large, water absorption is strong, emulsify well, and heavy metal has the features such as adsorpting detoxication effect, also has effect of skin protection, beauty treatment, health care.Semen Lini glue is applied in cosmetics and has that zest is low, moisture retention good, improve skin elasticity and permeability, and there is antiphlogistic effects simultaneously.At present, the research about astringent has had a lot, but there is not yet open containing the astringent of Semen Lini glue extracting solution.
Summary of the invention
The object of the present invention is to provide a kind of astringent containing Semen Lini glue extracting solution and preparation method thereof.
Technical scheme of the present invention
Containing the astringent of Semen Lini glue extracting solution, calculate by mass percentage, its raw material composition and content as follows:
Described Semen Lini glue extracting solution, calculating by volume and Semen Lini: water is the ratio of 1-10:30, after Semen Lini and deionized water Homogeneous phase mixing, controlling bath temperature scope is 50-90 DEG C of lixiviate 5-90min, after filtering, supernatant is Semen Lini glue extracting solution to the lixiviating solution of gained;
Described wetting agent is the mixture of at least one composition in hyaluronate sodium and glycerol, 1,3 butylene glycol, 1,2-PD, dipropylene glycol, PEG-26 glycerin ether, Polyethylene Glycol-32, Polyethylene Glycol-1540, betanin;
Described rheology control agent is one or more mixture in acrylic compounds/C10-30 alkylol acrylamide acid esters cross linked polymer, acrylic compounds/acrylamide copolymer/white mineral oil/polysorbate 85, PEG-120 methyl dioleate, PEG-120 methyl trioleate, transparent xanthan gum, acrylate copolymer, polyacrylate-1 cross linked polymer, carbomer-U10, carbomer-ETD 2050, carbomer-934;
Described solubilizing agent is one or more mixture in PEG-20 castor oil hydrogenated, Cremophor RH40, PRG-60 castor oil hydrogenated;
Described antiseptic is methyl hydroxybenzoate, ethyl hydroxybenzoate, phenoxyethanol, germall class, Kazon class and dihydroxymethyl glycolylurea, 1, 2-benzisothiazole-3-ketone, essence of Niobe, Methylisothiazolinone, trichloro-symmetrical diphenyl urea, the bromo-2-nitro of 2--1.3-propylene glycol (Bronopol), glyceryl monolaurate, diazonium ureine, bromo-5 nitros-1 of propylene glycol-5-, 3-bis-Evil alkane, dehydroacetic acid, bromo-5 nitros-1 of propylene glycol-5-, 3-bis-Evil alkane, one or more mixture in propylene glycol-bis-imidazolidinyl urea iodo propinyl butyl carbamate.
The preparation method of above-mentioned a kind of astringent containing Semen Lini glue extracting solution, step is as follows:
Semen Lini glue extracting solution is accurately taken in beaker, under agitation the hyaluronate sodium in wetting agent and rheology control agent are joined in Semen Lini glue extracting solution, stir and completely dissolve after, add remaining wetting agent component, continue to stir and completely dissolve after, add antiseptic and solubilizing agent, then after continuing to stir, namely obtain a kind of astringent containing Semen Lini glue extract.
Beneficial effect of the present invention
A kind of astringent containing Semen Lini glue extracting solution of the present invention, owing to being obtained the main component containing Semen Lini glue in the aqueous solution containing Semen Lini glue extracting solution by restricted-access media, as polysaccharide material, protein, lignan etc.Polysaccharide material and protein are natural moisturizing ingredient, have well lock water moisturizing, emulsifying, stablize thickening efficiency, therefore compared with tradition cosmetic water, the astringent containing Semen Lini glue extracting solution has effect of better lock water moisturizing; Lignan is vehicle natural in cosmetics or anti-aging actives, therefore compared with traditional astringent, astringent containing Semen Lini glue extracting solution is preventing or is treating skin ageing, particularly skin relaxes, lack flexibility, reduce wrinkle and formed, make skin more full of elasticity and prevent or treat scaly dry skin have significant effect, skin can be kept to moisten, improve skin appearance, preparation technology's simple possible of this astringent.
Accompanying drawing explanation
The moistening effect figure of Fig. 1, variable concentrations Semen Lini glue extracting solution aqueous solution 48h.
Detailed description of the invention
Below in conjunction with instantiation, the present invention is described further, but protection scope of the present invention is not limited in this:
Specification and manufacturer's information of raw material used in various embodiments of the present invention are as follows:
embodiment 1
Containing the astringent of Semen Lini glue extracting solution, calculate by mass percentage, its raw material composition and content as follows:
Described Semen Lini glue extracting solution, calculates, i.e. Semen Lini by volume: water is the ratio of 1:30, after Semen Lini and deionized water Homogeneous phase mixing, controlling bath temperature scope is 60 DEG C of lixiviate 30min, and after filtering, supernatant is Semen Lini glue extracting solution to the lixiviating solution of gained;
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, PEG-26 glycerin ether and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32:PEG-26 glycerin ether: hyaluronate sodium is 10:5:5:5:0.02;
Described rheology control agent is transparent xanthan gum;
Described solubilizing agent is Cremophor RH40;
Described antiseptic is methyl hydroxybenzoate.
The preparation method of above-mentioned a kind of astringent containing Semen Lini glue extracting solution, step is as follows:
72.83g Semen Lini glue extracting solution is placed in beaker, under agitation the 0.02g hyaluronate sodium in wetting agent and 0.05g rheology control agent transparent xanthan gum are joined in Semen Lini glue extracting solution, stir and completely dissolve after, add 10g glycerol, 5g1 successively, 3-butanediol, 5g Polyethylene Glycol-32 and 5gPEG-26 glycerin ether, continue to stir and completely dissolve after, add 0.1g antiseptic methyl hydroxybenzoate and 2g solubilizing agent Cremophor RH40, then after continuing to stir, namely obtain a kind of astringent containing Semen Lini glue extract.。
embodiment 2
Containing the astringent of Semen Lini glue extracting solution, calculate by mass percentage, its raw material composition and content as follows:
Described Semen Lini glue extracting solution, calculates, i.e. Semen Lini by volume: water is the ratio of 1:30, after Semen Lini and deionized water Homogeneous phase mixing, controlling bath temperature scope is 60 DEG C of lixiviate 30min, and after filtering, supernatant is Semen Lini glue extracting solution to the lixiviating solution of gained;
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, dipropylene glycol and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32: dipropylene glycol: hyaluronate sodium is 10:6:1:2:0.01;
Described solubilizing agent is Cremophor RH40;
Described antiseptic is methyl hydroxybenzoate.
The preparation method of above-mentioned a kind of astringent containing Semen Lini glue extracting solution, step is as follows:
Semen Lini glue extracting solution is placed in beaker, under agitation the 0.01g hyaluronate sodium in wetting agent is joined in Semen Lini glue extracting solution, stir and completely dissolve after, add 10g glycerol, 6g1 successively, 3-butanediol, 1g Polyethylene Glycol-32 and 2g dipropylene glycol, continue to stir and completely dissolve after, add 0.1g antiseptic methyl hydroxybenzoate and 0.15g solubilizing agent Cremophor RH40, then after continuing to stir, namely obtain a kind of astringent containing Semen Lini glue extract.
embodiment 3
Containing the astringent of Semen Lini glue extracting solution, calculate by mass percentage, its raw material composition and content as follows:
Described Semen Lini glue extracting solution, calculates, i.e. Semen Lini by volume: water is the ratio of 1:30, after Semen Lini and deionized water Homogeneous phase mixing, controlling bath temperature scope is 60 DEG C of lixiviate 30min, and after filtering, supernatant is Semen Lini glue extracting solution to the lixiviating solution of gained;
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, dipropylene glycol and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32: dipropylene glycol: hyaluronate sodium is 5:3:1:2:0.01;
Described solubilizing agent is Cremophor RH40;
Described antiseptic is methyl hydroxybenzoate.
The preparation method of above-mentioned a kind of astringent containing Semen Lini glue extracting solution, step is as follows:
90.74g Semen Lini glue extracting solution is placed in beaker, under agitation the 0.01g hyaluronate sodium in wetting agent is joined in Semen Lini glue extracting solution, stir and completely dissolve after, add 5g glycerol, 3g1 successively, 3-butanediol, 1g Polyethylene Glycol-32 and 2g dipropylene glycol, continue to stir and completely dissolve after, add 0.1g antiseptic methyl hydroxybenzoate and 0.15g solubilizing agent Cremophor RH40, then after continuing to stir, namely obtain a kind of astringent containing Semen Lini glue extract.
application Example
The test of Semen Lini glue extracting solution performance of keeping humidity
It is 2 that Semen Lini glue extracting solution deionized water used for above-described embodiment 1 is mixed with concentration, 5, 8, the Semen Lini glue extracting solution aqueous solution of 12g/ml, not add the deionized water of Semen Lini glue extracting solution for blank, be 35 at relative humidity RH, temperature is test the performance of keeping humidity of Semen Lini glue extracting solution in the enclosed environment of 35 DEG C, concentration is 0, 2, 5, 8, the moistening effect of the Semen Lini glue extracting solution aqueous solution 48h of 12g/ml as shown in Figure 1, as can be seen from Figure 1 concentration is 5, 8, the deionized water moisturizing rate that the moisturizing rate of the Semen Lini glue extracting solution of 12g/ml is more used than contrast is high, the astringent indicated thus containing Semen Lini glue extracting solution is better than the astringent moistening effect not adding Semen Lini glue extracting solution.
In sum, a kind of astringent containing Semen Lini glue extract of the present invention has effect of well lock water moisturizing.
The above is only the citing of embodiments of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvement and modification, these improve and modification also should be considered as protection scope of the present invention.
Claims (6)
1., containing the astringent of Semen Lini glue extract, it is characterized in that the described astringent containing Semen Lini glue extract is calculated by mass percentage, its raw material composition and content as follows:
Semen Lini glue extracting solution 67.98-94.90%
Wetting agent 5.00-25.02%
Rheology control agent 0-3%
Solubilizing agent 0-3%
Antiseptic 0.1-1%;
Described Semen Lini glue extracting solution, calculating by volume and Semen Lini: water is the ratio of 1-10:30, after Semen Lini and deionized water Homogeneous phase mixing, controlling bath temperature scope is 50-90 DEG C of lixiviate 5-90min, after filtering, supernatant is Semen Lini glue extracting solution to the lixiviating solution of gained;
Described wetting agent is the mixture of at least one composition in hyaluronate sodium and glycerol, 1,3 butylene glycol, 1,2-PD, dipropylene glycol, PEG-26 glycerin ether, Polyethylene Glycol-32, Polyethylene Glycol-1540, betanin;
Described rheology control agent is one or more mixture in acrylic compounds/C10-30 alkylol acrylamide acid esters cross linked polymer, acrylic compounds/acrylamide copolymer/white mineral oil/polysorbate 85, PEG-120 methyl dioleate, PEG-120 methyl trioleate, transparent xanthan gum, acrylate copolymer, polyacrylate-1 cross linked polymer, carbomer-U10, carbomer-ETD 2050, carbomer-934;
Described solubilizing agent is one or more mixture in PEG-20 castor oil hydrogenated, Cremophor RH40, PRG-60 castor oil hydrogenated;
Described antiseptic is methyl hydroxybenzoate, ethyl hydroxybenzoate, phenoxyethanol, germall class, Kazon class and dihydroxymethyl glycolylurea, 1, bromo-5 nitros-1 of 2-benzisothiazole-3-ketone, essence of Niobe, Methylisothiazolinone, trichloro-symmetrical diphenyl urea, 2-bromo-2-nitro-1.3-propylene glycol (Bronopol), glyceryl monolaurate, diazonium ureine, propylene glycol-5-, one or more mixture in bromo-5 nitro-1, the 3-bis-Evil alkane of 3-bis-Evil alkane, dehydroacetic acid, propylene glycol-5-, propylene glycol-bis-imidazolidinyl urea iodo propinyl butyl carbamate.
2. a kind of astringent containing Semen Lini glue extracting solution as claimed in claim 1, calculates by mass percentage, its raw material composition and content as follows:
Semen Lini glue extracting solution 72.83-90.74%
Wetting agent 9.01-25.02%
Rheology control agent 0-0.05%
Solubilizing agent 0.15-2.00%
Antiseptic 0.1%;
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, PEG-26 glycerin ether and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32:PEG-26 glycerin ether: hyaluronate sodium is 10:5-6:1-5:2-5:0.01-0.02;
Described rheology control agent is transparent xanthan gum;
Described solubilizing agent is Cremophor RH40;
Described antiseptic is methyl hydroxybenzoate.
3. a kind of astringent containing Semen Lini glue extracting solution as claimed in claim 2, is characterized in that calculating by mass percentage, its raw material composition and content as follows:
Semen Lini glue extracting solution 80.74%
Wetting agent 19.01%
Solubilizing agent 0.15%
Antiseptic 0.1%;
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, dipropylene glycol and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32: dipropylene glycol: hyaluronate sodium is 10:6:1:2:0.01.
4. a kind of astringent containing Semen Lini glue extracting solution as claimed in claim 2, is characterized in that calculating by mass percentage, its raw material composition and content as follows:
Semen Lini glue extracting solution 90.74%
Wetting agent 9.01%
Solubilizing agent 0.15%
Antiseptic 0.1%
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, dipropylene glycol and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32: dipropylene glycol: hyaluronate sodium is 5:3:1:2:0.01.
5. a kind of astringent containing Semen Lini glue extracting solution as claimed in claim 2, is characterized in that calculating by mass percentage, its raw material composition and content as follows:
Semen Lini glue extracting solution 72.83%
Wetting agent 25.02%
Rheology control agent 0.05%
Solubilizing agent 2%
Antiseptic 0.1%;
Described wetting agent is glycerol, 1, the mixture of 3-butanediol, Polyethylene Glycol-32, PEG-26 glycerin ether and hyaluronate sodium composition, calculate in mass ratio, glycerol: 1,3 butylene glycol: Polyethylene Glycol-32:PEG-26 glycerin ether: hyaluronate sodium is 10:5:5:5:0.02.
6. the preparation method of the astringent containing Semen Lini glue extract as described in as arbitrary in claim 1-5, is characterized in that step is as follows:
Semen Lini glue extracting solution is accurately taken in beaker, under agitation the hyaluronate sodium in wetting agent and rheology control agent are joined in Semen Lini glue extracting solution, stir and completely dissolve after, add remaining wetting agent component, continue to stir and completely dissolve after, add antiseptic and solubilizing agent, then after continuing to stir, namely obtain a kind of astringent containing Semen Lini glue extract.
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| CN201510096496.1A CN104739716A (en) | 2015-03-04 | 2015-03-04 | Toning lotion with flaxseed gum extract and preparation method of toning lotion with flaxseed gum extract |
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| CN201510096496.1A CN104739716A (en) | 2015-03-04 | 2015-03-04 | Toning lotion with flaxseed gum extract and preparation method of toning lotion with flaxseed gum extract |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107485585A (en) * | 2017-08-17 | 2017-12-19 | 成都新柯力化工科技有限公司 | A kind of biomass cosmetic skin-care water with isolating function |
| CN109350569A (en) * | 2018-10-26 | 2019-02-19 | 浙江树人学院 | A kind of sun-proof walnut cosmetic skin-care water of natural whiting and preparation method thereof |
| CN109589280A (en) * | 2017-09-30 | 2019-04-09 | 新疆利世得生物科技有限公司 | A kind of moisturising preparations and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107485585A (en) * | 2017-08-17 | 2017-12-19 | 成都新柯力化工科技有限公司 | A kind of biomass cosmetic skin-care water with isolating function |
| CN109589280A (en) * | 2017-09-30 | 2019-04-09 | 新疆利世得生物科技有限公司 | A kind of moisturising preparations and preparation method thereof |
| CN109350569A (en) * | 2018-10-26 | 2019-02-19 | 浙江树人学院 | A kind of sun-proof walnut cosmetic skin-care water of natural whiting and preparation method thereof |
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