CN109363046A - Sugarless type folium cortex eucommiae compound solid beverage and preparation method for conditioning subhealthy state - Google Patents
Sugarless type folium cortex eucommiae compound solid beverage and preparation method for conditioning subhealthy state Download PDFInfo
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- CN109363046A CN109363046A CN201811597178.3A CN201811597178A CN109363046A CN 109363046 A CN109363046 A CN 109363046A CN 201811597178 A CN201811597178 A CN 201811597178A CN 109363046 A CN109363046 A CN 109363046A
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- cortex eucommiae
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- folium cortex
- extract powder
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- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 208000013220 shortness of breath Diseases 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 206010046901 vaginal discharge Diseases 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/44—Preservation of non-alcoholic beverages by adding preservatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/46—Preservation of non-alcoholic beverages by heating
- A23L2/48—Preservation of non-alcoholic beverages by heating by irradiation or electric treatment
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Mycology (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses a kind of Sugarless type folium cortex eucommiae compound solid beverages and preparation method for conditioning subhealthy state, solid granular beverage is mixed by the material of following ratio (weight ratio), wherein folium cortex eucommiae extract powder 3-5 parts, 1-2 parts of Extract of Huangqi, 2-3 parts of root of kirilow rhodiola extract powder, 1-2 parts of huang jing extract powder, 1-2 parts of dendrobium candidum extract powder, 1-2 parts of Fructus Corni extract powder, 3-5 parts of xylitol, 0.05-0.1 parts of citric acid, 0.075-0.12 parts of sodium citrate, 24-30 parts of pueraria starch, coffee or 0.5-1 parts of orange flavor.The folium cortex eucommiae compound recuperating inferior health solid particle beverage prepared according to the present invention is a kind of granular granule, with health-care efficacies such as good conditioning subhealthy state, strengthen immunities, it is suitable for white collar, brain worker and specific demand crowd, wide market.
Description
Technical field
The invention belongs to health food manufacture fields, and it is solid to be related to a kind of Sugarless type folium cortex eucommiae compound for conditioning subhealthy state
Body beverage and preparation method thereof.
Background technique
With the rapid development of Chinese national economy, numerous office workers due to work and life rhythm quickening, in addition strong
Kang Yishi and healthy self-management are insufficient, irregular and over fatigue of living, and generate the symptom of inferior health, and be gradually increased
Trend.Inferior health refers to a kind of state that human body is between health and disease.In sub-health state person, cannot reach strong
The standard of health shows as the symptom that the vigor in certain time reduces, function and adaptability decline, therefore researches and develops to have and improve
Inferior health, and have the compound functional beverage of extensive adaptability, there is reality and far-reaching social benefit.
Cortex Eucommiae is the distinctive rare tonic herb of China, and folium cortex eucommiae is rich in flavones, loose ester alcohol diglucoside, Geniposide
The various nutrient elements such as glycosides, chlorogenic acid, caffeic acid, aucubin, the minerals such as Yi Jitie, zinc, selenium have and clear liver and improve vision,
Tonify Qi of the kidney, regulating lipoid and reducing blood pressure, anti-inflammatory be antibacterial, strengthening the bones and muscles, anti-aging, it is antifatigue, increase many effects such as immunity, therefore Cortex Eucommiae
Leaf is a kind of comprehensive invigorant of conditioning subhealthy state.
More using folium cortex eucommiae as the functional beverage of core material at present, a variety of function of folium cortex eucommiae are often utilized in these
Effect, but it is a lack of the compound drink for white collar, brain worker and other special population conditioning subhealthy states.Furthermore it is shutting out
In the method that Zhong Ye is extracted, also the effective component of folium cortex eucommiae is not studied, to obtain the production of high nutritive value
Object, it is ensured that the health-care efficacy of beverage.
Inventor is engaged in the research of Cortex Eucommiae beverage for many years, for example " a kind of Cortex Eucommiae is multiple in the Chinese patent of my invention in 2013
Close the preparation method (application No. is 201310658168.7) of anti-fatigue functional beverage, a kind of removal folium cortex eucommiae extract liquor peculiar smell is matched
The method (application No. is 201310658201.6) of health drink processed, a kind of preparation method of Cortex Eucommiae appetite-stimulating health-care drink
(201310658256.7) " in, a kind of preparation method of Cortex Eucommiae drinks is related to, after folium cortex eucommiae is extracted, using ozone
The method of processing and bioencapsulation processing overcomes careless fishy smell, bitter taste and the astringent taste problem outstanding in Cortex Eucommiae extract liquor, and soaks
Take use by folium cortex eucommiae boiled at 100 DEG C and hot conditions under the critical process that carries out.The above patented technology focuses on solving
The problem that folium cortex eucommiae peculiar smell how is removed in the preparation of Cortex Eucommiae beverage, does not optimize adjustment to technique in practice, to prevent
Only or reduce process for preparation in effective ingredient (active material) loss, so that it is guaranteed that the health-care efficacy of beverage.
Summary of the invention
The Sugarless type folium cortex eucommiae compound solid beverage and preparation method thereof that the invention proposes a kind of for conditioning subhealthy state,
It is basic raw material with folium cortex eucommiae extract powder, mixing is added to the extract powders such as Radix Astragali, root of kirilow rhodiola, rhizoma polygonati, dendrobium candidum, Fructus Corni,
Compound solid beverage is made, is a kind of conditioning subhealthy state health care product, while link is extracted to folium cortex eucommiae and has carried out process optimization, subtracts
The loss of effective ingredient is lacked, it is ensured that beverage the effect of property.
The present invention is added to following auxiliary material on the basis of folium cortex eucommiae extract powder:
(1) Radix Astragali: there is enhancing immunity of organisms, liver protection, diuresis, anti-aging, resisting stress, decompression and wide antibacterial
Effect；(2) root of kirilow rhodiola: have effects that tonifying Qi clearing lung-heat, intelligence development nourishing heart, controlling of bleeding with astringents, eliminating stasis to subdue swelling.Cure mainly deficiency of vital energy and physically weak, disease
Chilly, shortness of breath and fatigue, cough with lung heat, hemoptysis, leukorrhea diarrhea, traumatic injury and other effects afterwards；(3) rhizoma polygonati: there is air making-up and spleen enlivening, grow
Negative moistening lung, strengthening the bones and muscles, bacteriostasis antibiosis, lower hyperlipidemia, hypertension, hyperglycemia, strengthen immunity, anti-aging and other effects；(4) dendrobium candidum: have and promote the production of body fluid
Nourishing the stomach, nourishing Yin and clearing heat, moistening lung kidney-nourishing, the strong waist of improving eyesight, enhancing immunity of organisms and other effects；(5) Fructus Corni: have nourishing, stomach invigorating,
Diuresis, nourishing liver and kidney, replenishing qi and blood and other effects.Above-mentioned functional material is combined, compound recuperating inferior health solid granular drink is made
Material.
Technical scheme is as follows:
A kind of Sugarless type folium cortex eucommiae compound solid beverage for conditioning subhealthy state, by the material of following ratio (weight ratio)
It mixes, wherein folium cortex eucommiae extract powder 3-5 parts, 1-2 parts of Extract of Huangqi, 2-3 parts of root of kirilow rhodiola extract powder, huang jing extract powder 1-
2 parts, 1-2 parts of dendrobium candidum extract powder, 1-2 parts of Fructus Corni extract powder, 3-5 parts of xylitol, 0.05-0.1 parts of citric acid, citric acid
0.075-0.12 parts of sodium, 24-30 parts of pueraria starch, coffee or 0.5-1 parts of orange flavor.
A kind of preparation method of the Sugarless type folium cortex eucommiae compound solid beverage for conditioning subhealthy state, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation is stored in using black woven bag and is kept away
It is spare in the warehouse of light；
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction,
Temperature is 60-70 DEG C, and water logging extraction time is 3-4 hours；
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,；
[1.4] protective agent adds
Food acids are added in concentrated slurry, so that pH value is 3.5-4.0, add the table sugar of 5% (mass ratio), so
The beta-cyclodextrin of 5%-10% (mass ratio) is added afterwards, folium cortex eucommiae concentrate is made；
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, wherein shutting out
The moisture content of Zhong Ye extract powder is 5%-10%；It is stand-by that the folium cortex eucommiae extract powder of preparation is placed in low-temperature storage in sterile aluminum foil bag；
[2] mixing granulation
According to 3-5 parts of folium cortex eucommiae extract powder, 1-2 parts of Extract of Huangqi, 2-3 parts of root of kirilow rhodiola extract powder, huang jing extract powder 1-2
Part, 1-2 parts of dendrobium candidum extract powder, 1-2 parts of Fructus Corni extract powder, 3-5 parts of xylitol, 0.05-0.1 parts of citric acid, citric acid
0.075-0.12 parts of sodium, 24-30 parts of pueraria starch, 70- is added after the weight ratio weighing mixing of coffee or 0.5-1 parts of orange flavor
The ethyl alcohol of 90% purity infiltrates, and is placed in pelletizer, and it is that 10-12 purpose moistens particle that granularity, which is made, and vacuum drying is sent into sabot
3-4 hours are dried at a temperature of 65-70 DEG C of case to get finished particle；
[3] it sterilizes
Microwave disinfection or radiation sterilizing will be carried out after finished particle quantitative package；Wherein the temperature control of microwave disinfection exists
60-70℃；
[4] it is packed and stored
Vanning, coding, inspection, storage.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.1]
The moisture content of folium cortex eucommiae is lower than 13%.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.2]
Cleaning tap water and pure water is respectively adopted, wherein folium cortex eucommiae is placed on conveyer belt after being cleaned in pond with tap water,
Spray is carried out with pure water to clean.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.2]
It is extracted using the ultrasonic continuous extract equipment of reverse back stream.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.3]
Folium cortex eucommiae leaching liquor is placed in dual-effect concentrator and is concentrated.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.5]
Food acids are citric acid.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.4]
Table sugar is sucrose or fructose.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [1.5]
The leaving air temp of spray drying tower is 50-60 DEG C.
In the above-mentioned preparation method for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, in step [2] at
Product particle water content < 8%.
The advantageous effects that the present invention has are as follows:
1, for the present invention for groups such as current white collar, brain workers, operating pressure is big, is easy to appear inferior health etc.
Problem, preferably Cortex Eucommiae, Radix Astragali, root of kirilow rhodiola, rhizoma polygonati, dendrobium candidum, Fructus Corni a variety of tonic food, wherein Radix Astragali, red scape
It, rhizoma polygonati, dendrobium candidum, Fructus Corni deployed according to reasonable ratio, play invigorating the spleen clearing lung-heat, lower hyperlipidemia, hypertension, hyperglycemia, tonify Qi of the kidney, improve and exempt from
The effect of the comprehensive nourishings such as epidemic disease power, conditioning subhealthy state.Especially Cortex Eucommiae itself has liver heat removing and kidney replenishing, adjusts as rare invigorant
Lipoid and reducing blood pressure, strengthening the bones and muscles, anti-aging, the nourishing effects for improving immunity, at the same also have it is neutral mild, as ministerial drug when repellency
Small property feature can enhance effect with a variety of food medicinal material compatibilities such as Radix Astragali, root of kirilow rhodiola, rhizoma polygonati, dendrobium candidum, Fructus Corni.Drink
After material is taken for a long time, modern's inferior health illness can be improved, while also there are other composite efficacies, nourish, achieve many things at one stroke comprehensively.
Furthermore in order to expand its adaptation range, make various crowds, including patients with diabetes mellitus, no cane sugar type is made in drink, more
Universal meaning.
2, the present invention is in the stabilization to nutritional ingredients such as Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves, flavones, Geniposidic acid, Aucubins
Property, on the basis of the characteristics such as anti-oxidant further investigation, in conjunction with the characteristic of institute's synthetic beverage, to the illumination influenced in raw material preparation,
The factors such as temperature, pH value have carried out accurate control, substantially increase product nutrient substances content.
3, intermediate products of the present invention in beverage --- in extract powder preparation, to the loss characteristic of folium cortex eucommiae nutritional ingredient into
Research of having gone, so that the PH that prime cement is concentrated is 3.5-4.0 or so, has by addition citric acid or the scheme of other food acid agent
Effect prevents the loss of the ingredients such as flavones, chlorogenic acid, Geniposidic acid, adjust again in beverage preparation in later use prime cement
To suitable pH value, the peculiar mouthfeel of Cortex Eucommiae beverage is maintained.The table sugar that joined 5% in concentration prime cement simultaneously, passes through increasing
Add sucrose concentration to reduce dissolved oxygen amount, effectively inhibits the oxygenolysis of the substances such as flavones, chlorogenic acid.Wherein selection 5% is sugared adds
Dosage be comprehensively consider sugared part ratio it is dry to subsequent spray to the degree of protection of nutritional ingredient and too low sugar in caused by
Agglomeration, viscous wall etc. influence, and carry out the result of parameter optimization.Furthermore it is added to the beta-cyclodextrin of 5%-10% before spray drying,
The characteristics of using its embedding effect and granular material, under the premise of not influencing drying process with atomizing, realize nutritional ingredient
Retain.
4, the raw material in the present invention takes shading treatment in storage and preparation process, and folium cortex eucommiae is stored up using black woven bag
It deposits, reducing illumination influences the brings oxygenolysis such as chlorogenic acid, Geniposidic acid, Aucubin；Simultaneously by picking
Fresh folium cortex eucommiae is processed in time is prepared into folium cortex eucommiae concentration prime cement or eucommia ulmoides extract product, and arranges through overnutrition protection
Long term storage is applied, and logistics deployment is carried out according to the progress demand of subsequent beverage preparation, is avoided in traditional Cortex Eucommiae beverage preparation
Because of the long term storage bring nutrient loss of folium cortex eucommiae, at the same also reduce storage area and strange land end product preparation plus
The transportation cost in working hour has adapted to the place of production in modern plants extraction product manufacturing and has carried out raw material roughing extraction, strange land completion eventually
Hold product manufacturing sale with the new model of save the cost.
5, the present invention has carried out accurate control to temperature in product preparation, so that drying, water logging are extracted, are concentrated and dried
In temperature control within 70 DEG C, these measures effectively prevent the loss of effective component in folium cortex eucommiae.
6, present invention employs microwave sterilization mode, temperature is continued to monitor in sterilization process, and by extending sterilization time,
Temperature is controlled 60-70 DEG C, using the collective effect of microwave heating effect and non-thermal effect, makes microbial body internal protein and physiology
Movable substance morphs, develops and delays and dead, achievees the purpose that food sterilizing, fresh-keeping, simultaneously because temperature control is 65
DEG C or so, to flavones, chlorogenic acid, two grape of Geniposidic acid, Aucubin and rosin spirit when reducing conventional high temperature sterilizing
The decomposition of glucoside improves the conservation rate of nutritional ingredient.Simultaneously in microwave sterilization, the product after packaging can be placed directly within micro-
It is carried out in wave sterilizer, facilitates execute-in-place.
Specific embodiment
Inventor is studied for a long period of time discovery, either the storage of folium cortex eucommiae, water logging extract or beverage preparation link in,
The nutritional ingredients such as chlorogenic acid, flavones, Geniposidic acid, Aucubin, Pinoresinol diglucoside can all occur in various degree
It decomposes and is lost, major influence factors have:
(1) storage time and illumination effect
In traditional folium cortex eucommiae beverage processing, drying of being exposed to the sun in the sunlight after the picking of fresh folium cortex eucommiae, in the form of cured leaf into
Row long term storage carries out water logging extraction to Cortex Eucommiae leaf raw material again according to demand in beverage preparation.And inventor and other scholars
Research achievement show that raw material in prolonged storage, is influenced by extraneous factor, especially illumination is to yellow in folium cortex eucommiae
Ketone, chlorogenic acid, Geniposidic acid, Aucubin and Pinoresinol diglucoside have large effect effect, under light illumination
It easily causes oxygenolysis and causes nutrition loss.
For the influence of illumination factor in raw material long term storage, the present invention abandoned traditional folium cortex eucommiae drying and
Storing mode disposably dries storage using drying machine after feedstock capture in the fall, and carries out water to folium cortex eucommiae as early as possible
Extraction process is soaked, manufactured folium cortex eucommiae extract powder, which is placed in freezer, to be stored.In addition, taken in raw material storage and preparation process
Shading treatment, folium cortex eucommiae select the storage of black woven bag, and the folium cortex eucommiae concentration prime cement after preparation is then placed on the aluminium foil of shading
Bag stored for extended periods, this mode not only reduce the loss of nutritional ingredient, and by the side of folium cortex eucommiae at source long term storage
Formula is changed to the long term storage of folium cortex eucommiae extract powder, greatly reduce storage area and strange land beverage preparation processing when transport at
This.
(2) influence of temperature parameter
Traditional folium cortex eucommiae extracts usually leaches dozens of minutes in the boiled water boiled, and the newest result of study of inventor
During showing Cortex Eucommiae beverage preparation, high temperature is to flavones, chlorogenic acid, two grape of Geniposidic acid, Aucubin and rosin spirit
Glucoside has large effect, and chlorogenic acid therein is heat-sensitive substance, when heating temperature is more than 70 DEG C, green original in leaching liquid
The content meeting rapid decrease of acid, it is therefore desirable to water soaking temperature be controlled, the present invention is continuously extracted using ultrasonic reverse back stream and set
It is standby to be extracted in temperature for 60-70 DEG C, while taking into account extracting efficiency, reduce the loss of nutritional ingredient.
(3) influence of pH value and sugar
The research achievement of inventor shows the protection of sugar content and pH value appropriate in beverage to nutritional ingredient in folium cortex eucommiae
It acts on more significant.Within the scope of certain sucrose concentration, the loss late of the ingredients such as flavones, chlorogenic acid is with sucrose concentration in beverage
Increase and reduce, this is because the increase of sugared content, declines the oxygen content in solution, inhibits the oxidation of flavones, chlorogenic acid
It decomposes.Therefore concentration prime cement preparation in be purposefully added 5% sucrose, meet the requirement that extract powder product stores for a long time, and
The sugar of the ratio has no effect on subsequent spray drying process.In later period beverage preparation according to production need be diluted with water sugar it is dense
Degree, will not influence the mouthfeel of product.
By on pH value on nutritional ingredient influence studies have shown that for eucommia bark flavone, resist under acidic environment
Oxidability is stronger, and antioxidant activity significantly reduces under alkaline environment；And for chlorogenic acid, Geniposidic acid, peach jaurel
For glucoside and Pinoresinol diglucoside, under acidic environment, thermal stability is also at preferable states, comprehensively consider it is different at
Point different to the influence degree of pH value, and combine drink and production process and organoleptic requirements, final choice is by the soda acid of concentrate
Degree is 3.5-4.0 by increasing the scheme of the food acids such as citric acid to deploy to PH, realizes flavones and chlorogenic acid to the maximum extent
Etc. Different Nutritions ingredient balance retain.
(4) embedding effect of beta-cyclodextrin
Inventor it has been investigated that, a certain proportion of beta-cyclodextrin is added in folium cortex eucommiae concentrate, can effectively inhibit
The loss of the nutritional ingredients such as flavones and chlorogenic acid, this is because beta-cyclodextrin main component is stable oligosaccharide, embedding is made
With the oxygenolysis for inhibiting the nutritional ingredients such as chlorogenic acid, flavones, thermal stability is improved.And suitable beta-cyclodextrin will not be right
The mouthfeel of product has an impact, and will not also impact to the process that Cortex Eucommiae concentrate spray drying prepares extract powder.
Embodiment one:
The preparation method of Sugarless type folium cortex eucommiae compound solid beverage for conditioning subhealthy state, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 60 DEG C, so that folium cortex eucommiae contains
Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag；
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step,
Wash off the dust on blade face；Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water
It is dry；
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:10 (mass ratio) is placed in ultrasonic reverse back
It flows continuous extract equipment to extract, temperature is 60 DEG C, and water logging extraction time is 3 hours；The work of the ultrasonic continuous extract equipment of reverse back stream
It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle
Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted
Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real
Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 20% or so.Inspissator is preferably double
Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter
The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 3.5 are added in concentrated slurry；
Sucrose is added according still further to the ratio of 5% (mass ratio), the beta-cyclodextrin of 10% (mass ratio) is then added, folium cortex eucommiae concentration is made
Liquid；
The purpose that food acids, table sugar and beta-cyclodextrin is added is to prevent the oxygen of nutritional ingredient in folium cortex eucommiae in concentrate
Change loss, extends shelf lives, and have no effect on subsequent drink mouthfeel.
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, control into
Air temperature is 100 DEG C, and leaving air temp is 50 DEG C, and the moisture content for the folium cortex eucommiae extract powder being prepared is 5%-10%；
Material enters the hot wind progress that drying tower is atomization, sends with air inlet fan in dryer section through centrifugal spraying disk in implementation
Heat exchange, surface of material moisture evaporate rapidly, are landed the cone below equipment by dry extract powder, humid air is by arranging in tower
Blower is discharged, and institute's band particle is down in cone through Bag filter recycling and is mixed with extract powder in exhaust gas, automatic through rotating blanking valve
It flows out in tower.
[1.6] it stores
Manufactured folium cortex eucommiae extract powder is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer
It is stored, is prepared for beverage and other products, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] mixing granulation
According to 3 parts of folium cortex eucommiae extract powder, 1 part of Extract of Huangqi, 2 parts of root of kirilow rhodiola extract powder, 1 part of huang jing extract powder, iron sheet
1 part of dendrobium nobile extract powder, 1 part of Fructus Corni extract powder, 3 parts of xylitol, 0.05 part of citric acid, 0.075 part of sodium citrate, pueraria starch
24 parts, ratio weighing, mixing and the uniform stirring of coffee or 0.5 part of orange flavor.Wherein folium cortex eucommiae extract powder is according to front
The homemade product of technique, remaining material are commercially available up-to-standard products.
According to the ethyl alcohol infiltration that 90% purity is added after above-mentioned formula weighing mixing, it is placed in pelletizer, granularity, which is made, is
10-12 purpose moistens particle, and sabot dries 4 hours to get finished particle at a temperature of being sent into 70 DEG C of vacuum oven.
[3] it sterilizes
Microwave disinfection or radiation sterilizing will be carried out after the material dosing stirred evenly packaging；Wherein microwave in microwave disinfection
Frequency is 2450MHz, and the temperature of beverage is controlled at 60 DEG C in sterilization process, and the time of sterilizing is according to drink flow and microwave power
Depending on, the total plate count of drink and yeast bacterial content are no more than national regulations after sterilizing.
[4] it is packed and stored
Vanning, coding, inspection, storage.
Embodiment two:
The preparation method of Sugarless type folium cortex eucommiae compound solid beverage for conditioning subhealthy state, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 70 DEG C, so that folium cortex eucommiae contains
Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag；
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step,
Wash off the dust on blade face；Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water
It is dry；
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:30 (mass ratio) is placed in ultrasonic reverse back
It flows continuous extract equipment to extract, temperature is 70 DEG C, and water logging extraction time is 4 hours；The work of the ultrasonic continuous extract equipment of reverse back stream
It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle
Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted
Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real
Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 30% or so.Inspissator is preferably double
Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter
The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 4.0 are added in concentrated slurry；
Sucrose is added according still further to the ratio of 5% (mass ratio), the beta-cyclodextrin of 5% (mass ratio) is then added, folium cortex eucommiae concentration is made
Liquid；
The purpose that food acids, table sugar and beta-cyclodextrin is added is to prevent the oxygen of nutritional ingredient in folium cortex eucommiae in concentrate
Change loss, extend shelf lives, and since concentrate and extract powder are beverage and the intermediate product of other product configurations, and simultaneously
Subsequent drink mouthfeel is not influenced.
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, control into
Air temperature is 120 DEG C, and leaving air temp is 60 DEG C, and the moisture content for the folium cortex eucommiae extract powder being prepared is 5%-10%；
[1.6] it stores
Manufactured folium cortex eucommiae extract powder is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer
It is stored, is prepared for beverage and other products, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] mixing granulation
According to 5 parts of folium cortex eucommiae extract powder, 2 parts of Extract of Huangqi, 3 parts of root of kirilow rhodiola extract powder, 2 parts of huang jing extract powder, iron sheet
2 parts of dendrobium nobile extract powder, 2 parts of Fructus Corni extract powder, 5 parts of xylitol, 0.1 part of citric acid, 0.12 part of sodium citrate, pueraria starch 30
Part, coffee or the weighing of 1 part of orange flavor of ratio, mixing and uniform stirring.Wherein folium cortex eucommiae extract powder is according to previous process
Homemade product, remaining material are commercially available up-to-standard products.
According to the ethyl alcohol infiltration that 70% purity is added after above-mentioned formula weighing mixing, it is placed in pelletizer, granularity, which is made, is
10-12 purpose moistens particle, and sabot dries 3 hours to get finished particle at a temperature of being sent into 65 DEG C of vacuum oven.
[3] it sterilizes
Microwave disinfection or radiation sterilizing will be carried out after the material dosing stirred evenly packaging；Wherein microwave in microwave disinfection
Frequency is 2450MHz, and the temperature of beverage is controlled at 70 DEG C in sterilization process, and the time of sterilizing is according to drink flow and microwave power
Depending on, the total plate count of drink and yeast bacterial content are no more than national regulations after sterilizing.
[4] it is packed and stored
Vanning, coding, inspection, storage.
In order to be verified to above-mentioned technical effect, the present invention carried out respectively folium cortex eucommiae drying sunning comparative experiments,
Extraction temperature comparative experiments, pH value comparative experiments, pol comparative experiments, beta-cyclodextrin embedding experiment, and chromatographic column is used, according to
National standard measurement method determines the content of the nutritional ingredients such as flavones, chlorogenic acid, Pinoresinol diglucoside.Experimental result
It is as follows:
(1) drying sunning comparative experiments
The fresh folium cortex eucommiae of picking is divided into three parts of phase homogenous quantities, carried out respectively fresh leaf directly extract, the sun
Under dry with the drying experiment of 60-70 DEG C of machine, wherein dried under the sun and continue one week under ventilated environment in the fall, use is identical
Process conditions are completed water logging and are extracted.Every group is tested in triplicate, takes its average value, measures the relative amount of its nutritional ingredient.Knot
Fruit is as shown in table 1.
The drying sunning control experiment result of table 1
| Flavones retention rate | Chlorogenic acid retention rate | |
| Fresh folium cortex eucommiae water logging is extracted | 100% | 100% |
| Sun sunning | 86.7% | 83.5% |
| Machine drying | 95.2% | 94.4% |
1 experimental data of table explanation, using 60-70 DEG C of machine drying technology, than being dried under traditional sun to flavones and green
10% or so reserved can be improved in ortho acid.
(2) extraction temperature control experiment
The Folium Eucommiae of equal mass is placed in water logging in extractor to extract, only changes water soaking temperature, other parameters are identical,
Setting at a temperature of heat 30 minutes, then kept for 3 hours at 60 DEG C, measure the relative amount of its nutritional ingredient.Every group
It tests in triplicate, takes its average value, the results are shown in Table 2.
2 extraction temperature control experiment of table
| Extraction temperature | 100℃ | 90℃ | 80℃ | 70℃ | 60℃ | 50℃ |
| Chlorogenic acid | 75.2% | 80.4% | 88.5% | 96.8% | 105.3% | 100% |
| Pinoresinol diglucoside | 73.3% | 79.1% | 85.5% | 92.2% | 98.2% | 100% |
2 experimental data of table explanation, extraction temperature are most important to the reservation of nutritional ingredient.
(3) pH value control experiment
Appropriate citric acid is added in leaching liquor, is adjusted pH to setting value, is kept in dark place 3 months at room temperature, measures its battalion
The relative amount formed point, every group is tested in triplicate, takes its average value, the results are shown in Table 3.
Table 3PH value control experiment
| PH value | 3.0 | 4.0 | 5.0 | 6.0 |
| Chlorogenic acid | 110.3% | 104.6% | 103.5% | 100% |
| Flavones | 114.3% | 109.1% | 102.8% | 100% |
3 experimental data of table explanation, leaching liquor is under acidic environment, conducive to the long-term preservation of nutriment.
(4) pol control experiment
Suitable amount of sucrose is added in leaching liquor, is adjusted sugar content, is kept in dark place 3 months at room temperature, measures its nutritional ingredient
Relative amount, every group is tested in triplicate, takes its average value, the results are shown in Table 4.
4 pol control experiment of table
| Sugar content | 0% | 5% | 10% | 15% | 20% | 25% | 30% |
| Chlorogenic acid | 83.4% | 92.0% | 94.6% | 97.1% | 97.2% | 97.9% | 100% |
| Flavones | 84.3% | 91.9% | 95.2% | 96.5% | 97.2% | 98.0% | 100% |
4 experimental data of table explanation, addition sucrose facilitate the long-term preservation of leaching liquor nutriment.
(5) beta-cyclodextrin embedding experiment
Suitable beta-cyclodextrin is added in leaching liquor, is adjusted adding proportion, is kept in dark place 3 months at room temperature, measures it
The relative amount of nutritional ingredient, every group is tested in triplicate, takes its average value, the results are shown in Table 5.
The embedding experiment of 5 beta-cyclodextrin of table
| Beta-cyclodextrin amount | 0% | 2% | 4% | 6% | 8% | 10% |
| Chlorogenic acid | 88.2% | 90.4% | 90.4% | 93.0% | 94.6% | 100% |
| Pinoresinol diglucoside | 90.2% | 93.6% | 93.0% | 95.6% | 97.8% | 100% |
5 experimental data of table explanation is added beta-cyclodextrin to folium cortex eucommiae leaching liquor, facilitates the long-term preservation of nutriment.
The present invention carries out temperature, illumination, pH value, sugar content etc. that folium cortex eucommiae nutritional ingredient is influenced in beverage preparation
Parameter optimization and accurate control, are used successfully in the preparation of extract powder, and further experiment shows the present invention and traditional
Folium cortex eucommiae extractive technique is compared, and the retention rate of the nutritional ingredients such as flavones, chlorogenic acid improves 20%-30%, is effectively reduced
The loss of nutritional ingredient in product, it is ensured that the health-care efficacy of Cortex Eucommiae leaf beverage.
Beverage color after the folium cortex eucommiae compound recuperating inferior health solid particle prepared according to the present invention brews is reddish brown bright,
It does not precipitate significantly, and has the weak coffee fragrance of Cortex Eucommiae, there is the health cares function such as good conditioning subhealthy state, strengthen immunity
Effect, is suitable for white collar, brain worker and other specific demands crowd, wide market.
Claims (10)
1. being used for the Sugarless type folium cortex eucommiae compound solid beverage of conditioning subhealthy state, it is characterised in that: by following ratio (weight ratio)
Material mix, wherein folium cortex eucommiae extract powder 3-5 parts, 1-2 parts of Extract of Huangqi, 2-3 parts of root of kirilow rhodiola extract powder, rhizoma polygonati leaching
1-2 parts of cream powder, 1-2 parts of dendrobium candidum extract powder, 1-2 parts of Fructus Corni extract powder, 3-5 parts of xylitol, 0.05-0.1 parts of citric acid,
0.075-0.12 parts of sodium citrate, 24-30 parts of pueraria starch, coffee or 0.5-1 parts of orange flavor.
2. a kind of preparation method of the Sugarless type folium cortex eucommiae compound solid beverage for conditioning subhealthy state, which is characterized in that including
Following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation lucifugal is stored in using black woven bag
It is spare in warehouse；
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction, temperature
It is 60-70 DEG C, water logging extraction time is 3-4 hours；
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,；
[1.4] protective agent adds
Food acids are added in concentrated slurry so that pH value be 3.5-4.0, add the table sugar of 5% (mass ratio), then plus
Folium cortex eucommiae concentrate is made in the beta-cyclodextrin for entering 5%-10% (mass ratio)；
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, wherein folium cortex eucommiae
The moisture content of extract powder is 5%-10%；It is stand-by that the folium cortex eucommiae extract powder of preparation is placed in low-temperature storage in sterile aluminum foil bag；
[2] mixing granulation
According to 3-5 parts of folium cortex eucommiae extract powder, 1-2 parts of Extract of Huangqi, 2-3 parts of root of kirilow rhodiola extract powder, 1-2 parts of huang jing extract powder,
1-2 parts of dendrobium candidum extract powder, 1-2 parts of Fructus Corni extract powder, 3-5 parts of xylitol, 0.05-0.1 parts of citric acid, sodium citrate
0.075-0.12 parts, 24-30 parts of pueraria starch, 70- is added after the weight ratio weighing mixing of coffee or 0.5-1 parts of orange flavor
The ethyl alcohol of 90% purity infiltrates, and is placed in pelletizer, and it is that 10-12 purpose moistens particle that granularity, which is made, and vacuum drying is sent into sabot
3-4 hours are dried at a temperature of 65-70 DEG C of case to get finished particle；
[3] it sterilizes
Microwave disinfection or radiation sterilizing will be carried out after finished particle quantitative package；Wherein the temperature of microwave disinfection is controlled in 60-70
℃；
[4] it is packed and stored
Vanning, coding, inspection, storage.
3. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: the moisture content of folium cortex eucommiae is lower than 13% in step [1.1].
4. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: tap water and pure water is respectively adopted in the cleaning in step [1.2], wherein being cleaned in pond with tap water
Afterwards, folium cortex eucommiae is placed on conveyer belt, carries out spray with pure water and cleans.
5. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: being extracted in step [1.2] using the ultrasonic continuous extract equipment of reverse back stream.
6. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is concentrated it is characterized by: folium cortex eucommiae leaching liquor is placed in dual-effect concentrator in step [1.3].
7. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: food acids are citric acid in step [1.5].
8. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: table sugar is sucrose or fructose in step [1.4].
9. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: the leaving air temp of spray drying tower is 50-60 DEG C in step [1.5].
10. the preparation method of the Sugarless type folium cortex eucommiae compound solid beverage according to claim 2 for conditioning subhealthy state,
It is characterized by: finished particle water content < 8% in step [2].
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| CN111264736A (en) * | 2020-03-13 | 2020-06-12 | 云南植虫药生物科技有限公司 | Instant solid beverage containing rhizoma polygonati and dendrobium |
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