CN109363045A - A kind of antifatigue solid health-care beverage of folium cortex eucommiae compound and preparation method thereof - Google Patents

A kind of antifatigue solid health-care beverage of folium cortex eucommiae compound and preparation method thereof Download PDF

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Publication number
CN109363045A
CN109363045A CN201811597177.9A CN201811597177A CN109363045A CN 109363045 A CN109363045 A CN 109363045A CN 201811597177 A CN201811597177 A CN 201811597177A CN 109363045 A CN109363045 A CN 109363045A
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parts
cortex eucommiae
folium cortex
antifatigue
preparation
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翟文俊
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Shaanxi Tiancheng Biological Polytron Technologies Inc
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Shaanxi Tiancheng Biological Polytron Technologies Inc
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/385Concentrates of non-alcoholic beverages
    • A23L2/39Dry compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/42Preservation of non-alcoholic beverages
    • A23L2/44Preservation of non-alcoholic beverages by adding preservatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/42Preservation of non-alcoholic beverages
    • A23L2/46Preservation of non-alcoholic beverages by heating
    • A23L2/48Preservation of non-alcoholic beverages by heating by irradiation or electric treatment
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention discloses a kind of antifatigue solid health-care beverages of folium cortex eucommiae compound and preparation method thereof, solid health-care beverage, it is mixed by the material of following ratio (mass ratio), wherein folium cortex eucommiae extract powder 3-5 parts, 1-2 parts of Passion Flower instant powder, 1-2 parts of fructus rosae instant powder, 1-2 parts of fructus lycii instant powder, 1-2 parts of wilsonii instant powder, 20-30 parts of vegetable fat powder, 0.01-0.02 parts of ethylmaltol, 40-45 parts of trehalose, 30-35 parts of xylitol, 0.3-0.5 parts of microcrystalline cellulose, 0.1-0.15 parts of xanthan gum, 0.5-1 parts of sodium carboxymethylcellulose, 2-3 parts of pueraria starch, 0.08-0.12 parts of sodium citrate, 0.05-0.08 parts of citric acid, 0.03-0.05 parts of coffee aroma.The antifatigue solid health-care beverage of folium cortex eucommiae compound prepared according to the present invention have it is good it is antifatigue, the health-care efficacies such as regain one's strength of body, be suitable for white collar, brain worker and other specific demands crowd, wide market.

Description

A kind of antifatigue solid health-care beverage of folium cortex eucommiae compound and preparation method thereof
Technical field
The invention belongs to health food manufacture field, it is related to a kind of antifatigue solid health-care beverage of folium cortex eucommiae compound and its system Preparation Method.
Background technique
Cortex Eucommiae is the distinctive rare tonic herb of China, and folium cortex eucommiae is rich in flavones, loose ester alcohol diglucoside, Geniposide The various nutrient elements such as glycosides, chlorogenic acid, caffeic acid, aucubin, the minerals such as Yi Jitie, zinc, selenium have and clear liver and improve vision, Tonify Qi of the kidney, regulating lipoid and reducing blood pressure, anti-inflammatory be antibacterial, strengthening the bones and muscles, anti-aging, it is antifatigue, increase many effects such as immunity.
More using folium cortex eucommiae as the functional beverage of core material at present, a variety of function of folium cortex eucommiae are often utilized in these Effect, but it is a lack of antifatigue, the compound drink that supplements and regain one's strength when continuously working overtime for white collar, brain worker. Furthermore in the method that folium cortex eucommiae is extracted, also the effective component of folium cortex eucommiae is not studied, to obtain high nutrition The product of value, it is ensured that the health-care efficacy of beverage.
Inventor is engaged in the research of Cortex Eucommiae beverage for many years, for example " a kind of Cortex Eucommiae is multiple in the Chinese patent of my invention in 2013 Close the preparation method (application No. is 201310658168.7) of anti-fatigue functional beverage, a kind of removal folium cortex eucommiae extract liquor peculiar smell is matched The method (application No. is 201310658201.6) of health drink processed, a kind of preparation method of Cortex Eucommiae appetite-stimulating health-care drink (201310658256.7) " in, a kind of preparation method of Cortex Eucommiae drinks is related to, after folium cortex eucommiae is extracted, using ozone The method of processing and bioencapsulation processing overcomes careless fishy smell, bitter taste and the astringent taste problem outstanding in Cortex Eucommiae extract liquor, and soaks Take use by folium cortex eucommiae boiled at 100 DEG C and hot conditions under the critical process that carries out.The above patented technology focuses on solving The problem that folium cortex eucommiae peculiar smell how is removed in the preparation of Cortex Eucommiae beverage, does not optimize adjustment to technique in practice, to prevent Only or reduce process for preparation in effective ingredient (active material) loss, so that it is guaranteed that the health-care efficacy of beverage.
Summary of the invention
The invention proposes a kind of antifatigue solid health-care beverages of folium cortex eucommiae compound and preparation method thereof, with folium cortex eucommiae medicinal extract Powder is basic raw material, and mixing is added to the instant powders such as Passion Flower, fructus rosae, wilsonii, fructus lycii, compound solid beverage is made, With antifatigue health-care efficacy, while link is extracted to folium cortex eucommiae and has carried out process optimization, reduces the loss of effective ingredient, The effect of ensuring beverage property.
The present invention is added to following auxiliary material on the basis of folium cortex eucommiae extract powder:
(1) passionflower: natural tranquillizer, relaxation, calming nerves effect are particularly good, can treat insomnia, induction sleep naturally with Deep sleep alleviates sense of discomfort caused by nervous and extremely anxious, and having improves depressed, spiritual overanxiexty etc. Effect;(2) fructus rosae: have the function of significant anti-aging, antifatigue, anti-radiation, brain, promote longevity, can be used for Indigestion, the treatment of loss of appetite;(3) fructus lycii: having tonifying kidney and benefiting sperm, and nourishing blood for improving eyesight improves immune, anti-aging, drop blood The excellent efficacies such as sugar;(4) wilsonii: having antifatigue effect, enhances endurance and ability, increases alert and resourceful and learning ability, is The self-medication drug of rehabilitation after being ill.Above-mentioned functional material is combined, compound anti-fatigue solid beverage is made.
Technical scheme is as follows:
A kind of antifatigue solid health-care beverage of folium cortex eucommiae compound, is mixed by the material of following ratio (mass ratio), 3-5 parts of middle folium cortex eucommiae extract powder, 1-2 parts of Passion Flower instant powder, 1-2 parts of fructus rosae instant powder, 1-2 parts of fructus lycii instant powder, thorn 1-2 parts of slender acanthopanax instant powder, 20-30 parts of vegetable fat powder, 0.01-0.02 parts of ethylmaltol, 40-45 parts of trehalose, xylitol 30-35 Part, 0.3-0.5 parts of microcrystalline cellulose, 0.1-0.15 parts of xanthan gum, 0.5-1 parts of sodium carboxymethylcellulose, 2-3 parts of pueraria starch, 0.08-0.12 parts of sodium citrate, 0.05-0.08 parts of citric acid, 0.03-0.05 parts of coffee aroma.
A kind of antifatigue solid health-care beverage of folium cortex eucommiae compound, is mixed by the material of following ratio (mass ratio), 3-5 parts of middle folium cortex eucommiae extract powder, 1-2 parts of Passion Flower instant powder, 1-2 parts of fructus rosae instant powder, 1-2 parts of fructus lycii instant powder, thorn 1-2 parts of slender acanthopanax instant powder, 20-30 parts of vegetable fat powder, 0.01-0.02 parts of ethylmaltol, 40-45 parts of trehalose, xylitol 30-35 Part, 0.3-0.5 parts of microcrystalline cellulose, 0.1-0.15 parts of xanthan gum, 0.5-1 parts of sodium carboxymethylcellulose, 2-3 parts of pueraria starch, 0.08-0.12 parts of sodium citrate, 0.05-0.08 parts of citric acid, 0.03-0.05 parts of coffee aroma.
A kind of preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation is stored in using black woven bag and is kept away It is spare in the warehouse of light;
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction, Temperature is 60-70 DEG C, and water logging extraction time is 3-4 hours;
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,;
[1.4] protective agent adds
Food acids are added in concentrated slurry, so that pH value is 3.5-4.0, add the table sugar of 5% (mass ratio), so The beta-cyclodextrin of 5%-10% (mass ratio) is added afterwards, folium cortex eucommiae concentrate is made;
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, wherein shutting out The moisture content of Zhong Ye extract powder is 5%-10%;It is stand-by that the folium cortex eucommiae extract powder of preparation is placed in low-temperature storage in sterile aluminum foil bag;
[2] mixing is sterilized
According to 3-5 parts of folium cortex eucommiae extract powder, 1-2 parts of Passion Flower instant powder, 1-2 parts of fructus rosae instant powder, fructus lycii is instant 1-2 parts of powder, 1-2 parts of wilsonii instant powder, 20-30 parts of vegetable fat powder, 0.01-0.02 parts of ethylmaltol, 40-45 parts of trehalose, 30-35 parts of xylitol, 0.3-0.5 parts of microcrystalline cellulose, 0.1-0.15 parts of xanthan gum, 0.5-1 parts of sodium carboxymethylcellulose, pueraria lobata 2-3 parts of starch, 0.08-0.12 parts of sodium citrate, 0.05-0.08 parts of citric acid, the mass ratio that 0.03-0.05 parts of coffee aroma claims Mixing after weight, stirs evenly, and carries out microwave disinfection or radiation sterilizing after carrying out quantitative package;The wherein temperature control of microwave disinfection At 60-70 DEG C;
[3] it is packed and stored
Vanning, coding, inspection, storage.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, folium cortex eucommiae is aqueous in step [1.1] Rate is lower than 13%.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, the cleaning in step [1.2] is adopted respectively It is carried out wherein folium cortex eucommiae is placed on conveyer belt after being cleaned in pond with tap water with pure water with tap water and pure water Spray cleaning.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, using ultrasonic reverse back in step [1.2] Continuous extract equipment is flowed to extract.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, step extracts folium cortex eucommiae in [1.3] Liquid is placed in dual-effect concentrator and is concentrated.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, food acids are lemon in step [1.4] Acid.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, table sugar is sucrose in step [1.4] Or fructose.
In the preparation method of the above-mentioned antifatigue solid health-care beverage of folium cortex eucommiae compound, spray drying tower in step [1.5] Leaving air temp is 50-60 DEG C.
The advantageous effects that the present invention has are as follows:
1, the present invention is big for special populations operating pressures such as white collar, brain workers, continuously needs when overtime work anti- Fatigue the demands such as supplements and regains one's strength, preferably Cortex Eucommiae, Passion Flower, fructus rosae, fructus lycii, wilsonii combine be made it is multiple Square solid beverage, wherein Passion Flower, fructus rosae, fructus lycii, wilsonii are deployed by rational proportion, play antifatigue, restoring consciouness, increasing The effects of adding alert and resourceful and endurance, and Cortex Eucommiae itself has antifatigue effect as rare invigorant, while also having neutrality Mildly, repellency small property feature when as ministerial drug, can be with a variety of food medicinal materials such as Passion Flower, fructus rosae, fructus lycii, wilsonii Compatibility enhances effect.After beverage is taken for a long time, wanted meeting the health care that brain worker is antifatigue, supplements and regains one's strength Other than asking comprehensively, moreover it is possible to play strengthening the bones and muscles, anti-aging, improve the composite efficacies such as immunity, nourish, achieve many things at one stroke.
2, the present invention is in the stabilization to nutritional ingredients such as Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves, flavones, Geniposidic acid, Aucubins Property, on the basis of the characteristics such as anti-oxidant further investigation, in conjunction with the characteristic of institute's synthetic beverage, to the illumination influenced in raw material preparation, The factors such as temperature, pH value have carried out accurate control, substantially increase product nutrient substances content.
3, intermediate products of the present invention in beverage --- in extract powder preparation, to the loss characteristic of folium cortex eucommiae nutritional ingredient into Research of having gone, so that the PH that prime cement is concentrated is 3.5-4.0 or so, has by addition citric acid or the scheme of other food acid agent Effect prevents the loss of the ingredients such as flavones, chlorogenic acid, Geniposidic acid, adjust again in beverage preparation in later use prime cement To suitable pH value, the peculiar mouthfeel of Cortex Eucommiae beverage is maintained.The table sugar that joined 5% in concentration prime cement simultaneously, passes through increasing Add sucrose concentration to reduce dissolved oxygen amount, effectively inhibits the oxygenolysis of the substances such as flavones, chlorogenic acid.Wherein selection 5% is sugared adds Dosage be comprehensively consider sugared part ratio it is dry to subsequent spray to the degree of protection of nutritional ingredient and too low sugar in caused by Agglomeration, viscous wall etc. influence, and carry out the result of parameter optimization.Furthermore it is added to the beta-cyclodextrin of 5%-10% before spray drying, The characteristics of using its embedding effect and granular material, under the premise of not influencing drying process with atomizing, realize nutritional ingredient Retain.
4, the raw material in the present invention takes shading treatment in storage and preparation process, and folium cortex eucommiae is stored up using black woven bag It deposits, reducing illumination influences the brings oxygenolysis such as chlorogenic acid, Geniposidic acid, Aucubin;Simultaneously by picking Fresh folium cortex eucommiae is processed in time is prepared into folium cortex eucommiae concentration prime cement or eucommia ulmoides extract product, and arranges through overnutrition protection Long term storage is applied, and logistics deployment is carried out according to the progress demand of subsequent beverage preparation, is avoided in traditional Cortex Eucommiae beverage preparation Because of the long term storage bring nutrient loss of folium cortex eucommiae, at the same also reduce storage area and strange land end product preparation plus The transportation cost in working hour has adapted to the place of production in modern plants extraction product manufacturing and has carried out raw material roughing extraction, strange land completion eventually Hold product manufacturing sale with the new model of save the cost.
5, the present invention has carried out accurate control to temperature in product preparation, so that drying, water logging are extracted, are concentrated and dried In temperature control within 70 DEG C, these measures effectively prevent the loss of effective component in folium cortex eucommiae.
6, present invention employs microwave sterilization mode, temperature is continued to monitor in sterilization process, and by extending sterilization time, Temperature is controlled 60-70 DEG C, using the collective effect of microwave heating effect and non-thermal effect, makes microbial body internal protein and physiology Movable substance morphs, develops and delays and dead, achievees the purpose that food sterilizing, fresh-keeping, simultaneously because temperature control is 65 DEG C or so, to flavones, chlorogenic acid, two grape of Geniposidic acid, Aucubin and rosin spirit when reducing conventional high temperature sterilizing The decomposition of glucoside improves the conservation rate of nutritional ingredient.Simultaneously in microwave sterilization, the product after packaging can be placed directly within micro- It is carried out in wave sterilizer, facilitates execute-in-place.
Specific embodiment
Inventor is studied for a long period of time discovery, either the storage of folium cortex eucommiae, water logging extract or beverage preparation link in, The nutritional ingredients such as chlorogenic acid, flavones, Geniposidic acid, Aucubin, Pinoresinol diglucoside can all occur in various degree It decomposes and is lost, major influence factors have:
(1) storage time and illumination effect
In traditional folium cortex eucommiae beverage processing, drying of being exposed to the sun in the sunlight after the picking of fresh folium cortex eucommiae, in the form of cured leaf into Row long term storage carries out water logging extraction to Cortex Eucommiae leaf raw material again according to demand in beverage preparation.And inventor and other scholars Research achievement show that raw material in prolonged storage, is influenced by extraneous factor, especially illumination is to yellow in folium cortex eucommiae Ketone, chlorogenic acid, Geniposidic acid, Aucubin and Pinoresinol diglucoside have large effect effect, under light illumination It easily causes oxygenolysis and causes nutrition loss.
For the influence of illumination factor in raw material long term storage, the present invention abandoned traditional folium cortex eucommiae drying and Storing mode disposably dries storage using drying machine after feedstock capture in the fall, and carries out water to folium cortex eucommiae as early as possible Extraction process is soaked, manufactured folium cortex eucommiae extract powder, which is placed in freezer, to be stored.In addition, taken in raw material storage and preparation process Shading treatment, folium cortex eucommiae select the storage of black woven bag, and the folium cortex eucommiae concentration prime cement after preparation is then placed on the aluminium foil of shading Bag stored for extended periods, this mode not only reduce the loss of nutritional ingredient, and by the side of folium cortex eucommiae at source long term storage Formula is changed to the long term storage of folium cortex eucommiae extract powder, greatly reduce storage area and strange land beverage preparation processing when transport at This.
(2) influence of temperature parameter
Traditional folium cortex eucommiae extracts usually leaches dozens of minutes in the boiled water boiled, and the newest result of study of inventor During showing Cortex Eucommiae beverage preparation, high temperature is to flavones, chlorogenic acid, two grape of Geniposidic acid, Aucubin and rosin spirit Glucoside has large effect, and chlorogenic acid therein is heat-sensitive substance, when heating temperature is more than 70 DEG C, green original in leaching liquid The content meeting rapid decrease of acid, it is therefore desirable to water soaking temperature be controlled, the present invention is continuously extracted using ultrasonic reverse back stream and set It is standby to be extracted in temperature for 60-70 DEG C, while taking into account extracting efficiency, reduce the loss of nutritional ingredient.
(3) influence of pH value and sugar
The research achievement of inventor shows the protection of sugar content and pH value appropriate in beverage to nutritional ingredient in folium cortex eucommiae It acts on more significant.Within the scope of certain sucrose concentration, the loss late of the ingredients such as flavones, chlorogenic acid is with sucrose concentration in beverage Increase and reduce, this is because the increase of sugared content, declines the oxygen content in solution, inhibits the oxidation of flavones, chlorogenic acid It decomposes.Therefore concentration prime cement preparation in be purposefully added 5% sucrose, meet the requirement that extract powder product stores for a long time, and The sugar of the ratio has no effect on subsequent spray drying process.In later period beverage preparation according to production need be diluted with water sugar it is dense Degree, will not influence the mouthfeel of product.
By on pH value on nutritional ingredient influence studies have shown that for eucommia bark flavone, resist under acidic environment Oxidability is stronger, and antioxidant activity significantly reduces under alkaline environment;And for chlorogenic acid, Geniposidic acid, peach jaurel For glucoside and Pinoresinol diglucoside, under acidic environment, thermal stability is also at preferable states, comprehensively consider it is different at Point different to the influence degree of pH value, and combine drink and production process and organoleptic requirements, final choice is by the soda acid of concentrate Degree is 3.5-4.0 by increasing the scheme of the food acids such as citric acid to deploy to PH, realizes flavones and chlorogenic acid to the maximum extent Etc. Different Nutritions ingredient balance retain.
(4) embedding effect of beta-cyclodextrin
Inventor it has been investigated that, a certain proportion of beta-cyclodextrin is added in folium cortex eucommiae concentrate, can effectively inhibit The loss of the nutritional ingredients such as flavones and chlorogenic acid, this is because beta-cyclodextrin main component is stable oligosaccharide, embedding is made With the oxygenolysis for inhibiting the nutritional ingredients such as chlorogenic acid, flavones, thermal stability is improved.And suitable beta-cyclodextrin will not be right The mouthfeel of product has an impact, and will not also impact to the process that Cortex Eucommiae concentrate spray drying prepares extract powder.
Embodiment one:
The preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 60 DEG C, so that folium cortex eucommiae contains Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag;
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step, Wash off the dust on blade face;Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water It is dry;
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:10 (mass ratio) is placed in ultrasonic reverse back It flows continuous extract equipment to extract, temperature is 60 DEG C, and water logging extraction time is 3 hours;The work of the ultrasonic continuous extract equipment of reverse back stream It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 20% or so.Inspissator is preferably double Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 3.5 are added in concentrated slurry; Sucrose is added according still further to the ratio of 5% (mass ratio), the beta-cyclodextrin of 10% (mass ratio) is then added, folium cortex eucommiae concentration is made Liquid;
The purpose that food acids, table sugar and beta-cyclodextrin is added is to prevent the oxygen of nutritional ingredient in folium cortex eucommiae in concentrate Change loss, extends shelf lives, and have no effect on subsequent drink mouthfeel.
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, control into Air temperature is 100 DEG C, and leaving air temp is 50 DEG C, and the moisture content for the folium cortex eucommiae extract powder being prepared is 5%-10%;
Material enters the hot wind progress that drying tower is atomization, sends with air inlet fan in dryer section through centrifugal spraying disk in implementation Heat exchange, surface of material moisture evaporate rapidly, are landed the cone below equipment by dry extract powder, humid air is by arranging in tower Blower is discharged, and institute's band particle is down in cone through Bag filter recycling and is mixed with extract powder in exhaust gas, automatic through rotating blanking valve It flows out in tower.
[1.6] it stores
Manufactured folium cortex eucommiae extract powder is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer It is stored, is prepared for beverage and other products, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] mixing is sterilized
According to 3 parts of folium cortex eucommiae extract powder, 1 part of Passion Flower instant powder, 1 part of fructus rosae instant powder, 1 part of fructus lycii instant powder, 1 part of wilsonii instant powder, 20 parts of vegetable fat powder, 0.01 part of ethylmaltol, 40 parts of trehalose, 30 parts of xylitol, microcrystalline cellulose 0.3 part, 0.1 part of xanthan gum, 0.5 part of sodium carboxymethylcellulose, 2 parts of pueraria starch, 0.08 part of sodium citrate, citric acid 0.05 Part, ratio weighing, mixing and the uniform stirring that 0.03 part of coffee aroma.Wherein folium cortex eucommiae extract powder is to make by oneself according to previous process Product, remaining material be commercially available up-to-standard products.
Microwave disinfection or radiation sterilizing will be carried out after the material dosing stirred evenly packaging;Wherein microwave in microwave disinfection Frequency is 2450MHz, and the temperature of beverage is controlled at 60 DEG C in sterilization process, and the time of sterilizing is according to drink flow and microwave power Depending on, the total plate count of drink and yeast bacterial content are no more than national regulations after sterilizing.
[3] it is packed and stored
Vanning, coding, inspection, storage.
Embodiment two:
The preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 70 DEG C, so that folium cortex eucommiae contains Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag;
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step, Wash off the dust on blade face;Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water It is dry;
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:30 (mass ratio) is placed in ultrasonic reverse back It flows continuous extract equipment to extract, temperature is 70 DEG C, and water logging extraction time is 4 hours;The work of the ultrasonic continuous extract equipment of reverse back stream It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 30% or so.Inspissator is preferably double Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 4.0 are added in concentrated slurry; Sucrose is added according still further to the ratio of 5% (mass ratio), the beta-cyclodextrin of 5% (mass ratio) is then added, folium cortex eucommiae concentration is made Liquid;
The purpose that food acids, table sugar and beta-cyclodextrin is added is to prevent the oxygen of nutritional ingredient in folium cortex eucommiae in concentrate Change loss, extend shelf lives, and since concentrate and extract powder are beverage and the intermediate product of other product configurations, and simultaneously Subsequent drink mouthfeel is not influenced.
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, control into Air temperature is 120 DEG C, and leaving air temp is 60 DEG C, and the moisture content for the folium cortex eucommiae extract powder being prepared is 5%-10%;
[1.6] it stores
Manufactured folium cortex eucommiae extract powder is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer It is stored, is prepared for beverage and other products, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] mixing is sterilized
According to 5 parts of folium cortex eucommiae extract powder, 2 parts of Passion Flower instant powder, 2 parts of fructus rosae instant powder, 2 parts of fructus lycii instant powder, 2 parts of wilsonii instant powder, 30 parts of vegetable fat powder, 0.02 part of ethylmaltol, 45 parts of trehalose, 33 parts of xylitol, microcrystalline cellulose 0.5 part, 0.15 part of xanthan gum, 1 part of sodium carboxymethylcellulose, 3 parts of pueraria starch, 0.12 part of sodium citrate, 0.08 part of citric acid, Ratio weighing, mixing and the uniform stirring that 0.05 part of coffee aroma.Wherein folium cortex eucommiae extract powder is homemade according to previous process Product, remaining material are commercially available up-to-standard products.
Microwave disinfection or radiation sterilizing will be carried out after the material dosing stirred evenly packaging;Wherein microwave in microwave disinfection Frequency is 2450MHz, and the temperature of beverage is controlled at 70 DEG C in sterilization process, and the time of sterilizing is according to drink flow and microwave power Depending on, the total plate count of drink and yeast bacterial content are no more than national regulations after sterilizing.
[3] it is packed and stored
Vanning, coding, inspection, storage.
In order to be verified to above-mentioned technical effect, the present invention carried out respectively folium cortex eucommiae drying sunning comparative experiments, Extraction temperature comparative experiments, pH value comparative experiments, pol comparative experiments, beta-cyclodextrin embedding experiment, and chromatographic column is used, according to National standard measurement method determines the content of the nutritional ingredients such as flavones, chlorogenic acid, Pinoresinol diglucoside.Experimental result It is as follows:
(1) drying sunning comparative experiments
The fresh folium cortex eucommiae of picking is divided into three parts of phase homogenous quantities, carried out respectively fresh leaf directly extract, the sun Under dry with the drying experiment of 60-70 DEG C of machine, wherein dried under the sun and continue one week under ventilated environment in the fall, use is identical Process conditions are completed water logging and are extracted.Every group is tested in triplicate, takes its average value, measures the relative amount of its nutritional ingredient.Knot Fruit is as shown in table 1.
The drying sunning control experiment result of table 1
Flavones retention rate Chlorogenic acid retention rate
Fresh folium cortex eucommiae water logging is extracted 100% 100%
Sun sunning 86.7% 83.5%
Machine drying 95.2% 94.4%
1 experimental data of table explanation, using 60-70 DEG C of machine drying technology, than being dried under traditional sun to flavones and green 10% or so reserved can be improved in ortho acid.
(2) extraction temperature control experiment
The Folium Eucommiae of equal mass is placed in water logging in extractor to extract, only changes water soaking temperature, other parameters are identical, Setting at a temperature of heat 30 minutes, then kept for 3 hours at 60 DEG C, measure the relative amount of its nutritional ingredient.Every group It tests in triplicate, takes its average value, the results are shown in Table 2.
2 extraction temperature control experiment of table
Extraction temperature 100℃ 90℃ 80℃ 70℃ 60℃ 50℃
Chlorogenic acid 75.2% 80.4% 88.5% 96.8% 105.3% 100%
Pinoresinol diglucoside 73.3% 79.1% 85.5% 92.2% 98.2% 100%
2 experimental data of table explanation, extraction temperature are most important to the reservation of nutritional ingredient.
(3) pH value control experiment
Appropriate citric acid is added in leaching liquor, is adjusted pH to setting value, is kept in dark place 3 months at room temperature, measures its battalion The relative amount formed point, every group is tested in triplicate, takes its average value, the results are shown in Table 3.
Table 3PH value control experiment
PH value 3.0 4.0 5.0 6.0
Chlorogenic acid 110.3% 104.6% 103.5% 100%
Flavones 114.3% 109.1% 102.8% 100%
3 experimental data of table explanation, leaching liquor is under acidic environment, conducive to the long-term preservation of nutriment.
(4) pol control experiment
Suitable amount of sucrose is added in leaching liquor, is adjusted sugar content, is kept in dark place 3 months at room temperature, measures its nutritional ingredient Relative amount, every group is tested in triplicate, takes its average value, the results are shown in Table 4.
4 pol control experiment of table
Sugar content 0% 5% 10% 15% 20% 25% 30%
Chlorogenic acid 83.4% 92.0% 94.6% 97.1% 97.2% 97.9% 100%
Flavones 84.3% 91.9% 95.2% 96.5% 97.2% 98.0% 100%
4 experimental data of table explanation, addition sucrose facilitate the long-term preservation of leaching liquor nutriment.
(5) beta-cyclodextrin embedding experiment
Suitable beta-cyclodextrin is added in leaching liquor, is adjusted adding proportion, is kept in dark place 3 months at room temperature, measures it The relative amount of nutritional ingredient, every group is tested in triplicate, takes its average value, the results are shown in Table 5.
The embedding experiment of 5 beta-cyclodextrin of table
Beta-cyclodextrin amount 0% 2% 4% 6% 8% 10%
Chlorogenic acid 88.2% 90.4% 90.4% 93.0% 94.6% 100%
Pinoresinol diglucoside 90.2% 93.6% 93.0% 95.6% 97.8% 100%
5 experimental data of table explanation is added beta-cyclodextrin to folium cortex eucommiae leaching liquor, facilitates the long-term preservation of nutriment.
The present invention carries out temperature, illumination, pH value, sugar content etc. that folium cortex eucommiae nutritional ingredient is influenced in beverage preparation Parameter optimization and accurate control, are used successfully in the preparation of extract powder, and further experiment shows the present invention and traditional Folium cortex eucommiae extractive technique is compared, and the retention rate of the nutritional ingredients such as flavones, chlorogenic acid improves 20%-30%, is effectively reduced The loss of nutritional ingredient in product, it is ensured that the health-care efficacy of Cortex Eucommiae leaf beverage.
The drink color of the antifatigue solid health-care beverage punching of the folium cortex eucommiae compound prepared according to the present invention is reddish brown bright, does not have There is apparent precipitating, and have the weak coffee fragrance of Cortex Eucommiae, there is good antifatigue, supplement the health-care efficacies such as to regain one's strength, fit Together in white collar, brain worker and other specific demands crowd, wide market.

Claims (9)

1. a kind of antifatigue solid health-care beverage of folium cortex eucommiae compound, it is characterised in that: mixed by the material of following ratio (mass ratio) It closes, wherein folium cortex eucommiae extract powder 3-5 parts, 1-2 parts of Passion Flower instant powder, 1-2 parts of fructus rosae instant powder, fructus lycii instant powder 1-2 parts, 1-2 parts of wilsonii instant powder, 20-30 parts of vegetable fat powder, 0.01-0.02 parts of ethylmaltol, 40-45 parts of trehalose, wood 30-35 parts of sugar alcohol, 0.3-0.5 parts of microcrystalline cellulose, 0.1-0.15 parts of xanthan gum, 0.5-1 parts of sodium carboxymethylcellulose, pueraria lobata forms sediment 2-3 parts of powder, 0.08-0.12 parts of sodium citrate, 0.05-0.08 parts of citric acid, 0.03-0.05 parts of coffee aroma.
2. a kind of preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound, which comprises the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation lucifugal is stored in using black woven bag It is spare in warehouse;
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction, temperature It is 60-70 DEG C, water logging extraction time is 3-4 hours;
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,;
[1.4] protective agent adds
Food acids are added in concentrated slurry so that pH value be 3.5-4.0, add the table sugar of 5% (mass ratio), then plus Folium cortex eucommiae concentrate is made in the beta-cyclodextrin for entering 5%-10% (mass ratio);
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, wherein folium cortex eucommiae The moisture content of extract powder is 5%-10%;It is stand-by that the folium cortex eucommiae extract powder of preparation is placed in low-temperature storage in sterile aluminum foil bag;
[2] mixing is sterilized
According to 3-5 parts of folium cortex eucommiae extract powder, 1-2 parts of Passion Flower instant powder, 1-2 parts of fructus rosae instant powder, fructus lycii instant powder 1-2 Part, 1-2 parts of wilsonii instant powder, 20-30 parts of vegetable fat powder, 0.01-0.02 parts of ethylmaltol, 40-45 parts of trehalose, xylitol 30-35 parts, 0.3-0.5 parts of microcrystalline cellulose, 0.1-0.15 parts of xanthan gum, 0.5-1 parts of sodium carboxymethylcellulose, pueraria starch 2- It 3 parts, 0.08-0.12 parts of sodium citrate, 0.05-0.08 parts of citric acid, is mixed after the mass ratio weighing that 0.03-0.05 parts of coffee aroma Material, stirs evenly, and carries out microwave disinfection or radiation sterilizing after carrying out quantitative package;Wherein the temperature of microwave disinfection is controlled in 60- 70℃;
[3] it is packed and stored
Vanning, coding, inspection, storage.
3. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly the moisture content of folium cortex eucommiae is lower than 13% in [1.1].
4. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly tap water and pure water is respectively adopted in the cleaning in [1.2], wherein being placed in folium cortex eucommiae after being cleaned in pond with tap water On conveyer belt, spray is carried out with pure water and is cleaned.
5. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly it is extracted in [1.2] using the ultrasonic continuous extract equipment of reverse back stream.
6. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly folium cortex eucommiae leaching liquor is placed in dual-effect concentrator in [1.3] and is concentrated.
7. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly food acids are citric acid in [1.4].
8. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly table sugar is sucrose or fructose in [1.4].
9. the preparation method of the antifatigue solid health-care beverage of folium cortex eucommiae compound according to claim 2, it is characterised in that: step Suddenly the leaving air temp of spray drying tower is 50-60 DEG C in [1.5].
CN201811597177.9A 2018-12-26 2018-12-26 A kind of antifatigue solid health-care beverage of folium cortex eucommiae compound and preparation method thereof Pending CN109363045A (en)

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Application publication date: 20190222