CN109363040A - Folium cortex eucommiae compound beverage and preparation method thereof for conditioning subhealthy state - Google Patents
Folium cortex eucommiae compound beverage and preparation method thereof for conditioning subhealthy state Download PDFInfo
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- CN109363040A CN109363040A CN201811597168.XA CN201811597168A CN109363040A CN 109363040 A CN109363040 A CN 109363040A CN 201811597168 A CN201811597168 A CN 201811597168A CN 109363040 A CN109363040 A CN 109363040A
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- cortex eucommiae
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- 235000013402 health food Nutrition 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 201000005630 leukorrhea Diseases 0.000 description 1
- 230000003340 mental effect Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 235000020823 overnutrition Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 208000013220 shortness of breath Diseases 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 206010046901 vaginal discharge Diseases 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/44—Preservation of non-alcoholic beverages by adding preservatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/42—Preservation of non-alcoholic beverages
- A23L2/46—Preservation of non-alcoholic beverages by heating
- A23L2/48—Preservation of non-alcoholic beverages by heating by irradiation or electric treatment
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/15—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The folium cortex eucommiae compound beverage and preparation method thereof that the invention discloses a kind of for conditioning subhealthy state, compound beverage is proportionally formulated after pure water is added in (mass ratio) by following material: 20-30 parts of folium cortex eucommiae concentrate, 5-10 parts of Radix Astragali instant powder, 10-20 parts of root of kirilow rhodiola instant powder, 5-10 parts of rhizoma polygonati instant powder, 5-10 parts of dendrobium candidum instant powder, 5-10 parts of Fructus Corni instant powder, 4-8 parts of trehalose, 1-2 parts of honey, 0.05-0.08 parts of citric acid, 0.08-0.12 parts of sodium citrate, 0.01-0.02 parts of ethylmaltol, 0.05-0.08 parts of sodium dehydroacetate, 0.05-0.1 parts of calgon, 0.03-0.05 parts of gellan gum, 0.08-0.12 parts of xanthan gum, carboxymethyl cellulose Plain sodium 0.05-0.1 parts, 0.03-0.05 parts of fruity flavor.The folium cortex eucommiae compound beverage for conditioning subhealthy state prepared according to the present invention has the health-care efficacies such as good conditioning subhealthy state, strengthen immunity, is able to satisfy white collar, brain worker and special population demand, wide market.
Description
Technical field
The invention belongs to health food manufacture fields, are related to a kind of Du with conditioning subhealthy state, increase immunity function
Zhong Ye compound beverage and preparation method thereof.
Background technique
With the rapid development of Chinese national economy, numerous office workers due to work and life rhythm quickening, in addition strong
Kang Yishi and healthy self-management are insufficient, irregular and over fatigue of living, and generate the symptom of inferior health, and be gradually increased
Trend.Inferior health refers to a kind of state that human body is between health and disease.In sub-health state person, cannot reach strong
The standard of health shows as the symptom that the vigor in certain time reduces, function and adaptability decline, therefore researches and develops to have and improve
Inferior health, and have the compound functional beverage of extensive adaptability, there is reality and far-reaching social benefit.
Cortex Eucommiae is the distinctive rare tonic herb of China, and folium cortex eucommiae is rich in flavones, loose ester alcohol diglucoside, Geniposide
The various nutrient elements such as glycosides, chlorogenic acid, caffeic acid, aucubin, the minerals such as Yi Jitie, zinc, selenium have and clear liver and improve vision,
Tonify Qi of the kidney, regulating lipoid and reducing blood pressure, anti-inflammatory be antibacterial, strengthening the bones and muscles, anti-aging, it is antifatigue, increase many effects such as immunity, therefore Cortex Eucommiae
Leaf is a kind of comprehensive invigorant of conditioning subhealthy state.
It is more using folium cortex eucommiae as the functional beverage of primary raw material currently on the market, but lack a kind of for certain white collar ranks
Layer, brain worker and special population conditioning subhealthy state compound drink.In addition, in existing folium cortex eucommiae leach extraction method, all
The effective component of folium cortex eucommiae is not studied, and analysis measurement only is carried out to its effective component, can just produce health care
The good product of effect.
Inventor is engaged in the research of Cortex Eucommiae beverage for many years, for example " a kind of Cortex Eucommiae is multiple in the Chinese patent of my invention in 2013
Close the preparation method (application No. is 201310658168.7) of anti-fatigue functional beverage, a kind of removal folium cortex eucommiae extract liquor peculiar smell is matched
The method (application No. is 201310658201.6) of health drink processed, a kind of preparation method of Cortex Eucommiae appetite-stimulating health-care drink
(201310658256.7) " in, a kind of preparation method of Cortex Eucommiae drinks is related to, after folium cortex eucommiae is extracted, using ozone
The method of processing and bioencapsulation processing overcomes careless fishy smell, bitter taste and the astringent taste problem outstanding in Cortex Eucommiae extract liquor, and soaks
Take use by folium cortex eucommiae boiled at 100 DEG C and hot conditions under the critical process that carries out.The above patented technology focuses on solving
The problem that folium cortex eucommiae peculiar smell how is removed in the preparation of Cortex Eucommiae beverage, does not optimize adjustment to technique in practice, to prevent
Only or reduce process for preparation in effective ingredient (active material) loss, so that it is guaranteed that the health-care efficacy of beverage.
Summary of the invention
The folium cortex eucommiae compound beverage and preparation method thereof that the invention proposes a kind of for conditioning subhealthy state is dense with folium cortex eucommiae
Contracting liquid is basic raw material, and mixing is added to the instant powders such as Radix Astragali, root of kirilow rhodiola, rhizoma polygonati, dendrobium candidum, Fructus Corni, and it is solid that compound is made
Body beverage is a kind of conditioning subhealthy state health care product, while having carried out link process optimization in folium cortex eucommiae extraction, is reduced effectively
The loss of composition, it is ensured that the health-care efficacy of beverage.
The present invention is added to following auxiliary material on the basis of folium cortex eucommiae concentrate:
(1) Radix Astragali: there is enhancing body's immunity, liver protection, diuresis, anti-aging, resisting stress, decompression and wide anti-
Bacterium effect；(2) root of kirilow rhodiola: have effects that tonifying Qi clearing lung-heat, intelligence development nourishing heart, controlling of bleeding with astringents, eliminating stasis to subdue swelling, to deficiency of vital energy and physically weak, disease
Chilly, shortness of breath and fatigue, cough with lung heat, hemoptysis, leukorrhea diarrhea, traumatic injury etc. also have good effects afterwards；(3) rhizoma polygonati: have and mend
Gas invigorating the spleen, nourishing Yin and moistening lung, strengthening the bones and muscles, bacteriostasis antibiosis, lower hyperlipidemia, hypertension, hyperglycemia, strengthen immunity, anti-aging and other effects；(4) dendrobium candidum:
With promoting fluid production and nourishing stomach, nourishing Yin and clearing heat, moistening lung kidney-nourishing, the strong waist of improving eyesight, enhancing immunity of organisms and other effects；(5) Fructus Corni: have and grow
Benefit, stomach invigorating, diuresis, nourishing liver and kidney, replenishing qi and blood and other effects.Above-mentioned functional material is combined, the antifatigue solid particle of compound is made
Shape beverage.
Technical scheme is as follows:
A kind of folium cortex eucommiae compound beverage for conditioning subhealthy state, compound beverage by following material proportionally (mass ratio)
It is formulated after pure water is added: 20-30 parts of folium cortex eucommiae concentrate, 5-10 parts of Radix Astragali instant powder, root of kirilow rhodiola instant powder 10-20
Part, 5-10 parts of rhizoma polygonati instant powder, 5-10 parts of dendrobium candidum instant powder, 5-10 parts of Fructus Corni instant powder, 4-8 parts of trehalose, honey
1-2 parts, 0.05-0.08 parts of citric acid, 0.08-0.12 parts of sodium citrate, 0.01-0.02 parts of ethylmaltol, sodium dehydroacetate
0.05-0.08 parts, 0.05-0.1 parts of calgon, 0.03-0.05 parts of gellan gum, 0.08-0.12 parts of xanthan gum, carboxymethyl is fine
Plain 0.05-0.1 parts of the sodium of dimension, 0.03-0.05 parts of fruity flavor.
A kind of preparation method of the folium cortex eucommiae compound beverage for conditioning subhealthy state, comprising the following steps:
[1] prepared by folium cortex eucommiae concentrate
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation is stored in using black woven bag and is kept away
It is spare in the warehouse of light；
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction,
Temperature is 60-70 DEG C, and water logging extraction time is 3-4 hours；
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,；
[1.4] protective agent adds
Food acids are added in concentrated slurry, so that pH value is 3.5-4.0, add the edible of 20-30% (mass ratio)
Sugar is made folium cortex eucommiae concentration prime cement, is placed in sterile aluminum foil bag and stores, prepare for beverage.
[2] ingredient
According to 20-30 parts of folium cortex eucommiae concentrate, 5-10 parts of Radix Astragali instant powder, 10-20 parts of root of kirilow rhodiola instant powder, rhizoma polygonati is instant
5-10 parts of powder, 5-10 parts of dendrobium candidum instant powder, 5-10 parts of Fructus Corni instant powder, 4-8 parts of trehalose, 1-2 parts of honey, citric acid
0.05-0.08 parts, 0.08-0.12 parts of sodium citrate, 0.01-0.02 parts of ethylmaltol, 0.05-0.08 parts of sodium dehydroacetate,
0.05-0.1 parts of calgon, 0.03-0.05 parts of gellan gum, 0.08-0.12 parts of xanthan gum, sodium carboxymethylcellulose 0.05-
0.1 part, 0.03-0.05 parts of ingredients of fruity flavor, and pure water is added and sufficiently dissolves, wherein the weight of pure water is that folium cortex eucommiae is dense
90-100 times of contracting liquid weight；
[3] filtering, homogeneous, sterilizing, filling
Mother liquor after ingredient is pumped into high pressure homogenizer after the filtering of diatomite plate filter and carries out homogeneous, and using micro-
Wave sterilization machine is sterilized, and the temperature of beverage is controlled at 60-70 DEG C in sterilization process.
In the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state, folium cortex eucommiae contains in step [1.1]
Water rate is lower than 13%.
In the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state, the water for cleaning in step [1.2]
Tap water and pure water is respectively adopted, wherein folium cortex eucommiae is placed on conveyer belt after being cleaned in pond with tap water, use is pure
Water carries out spray cleaning.
It is inverse using ultrasound in step [1.2] in the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state
The continuous extract equipment that flows back extracts.
In the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state, step soaks folium cortex eucommiae in [1.3]
Extract is placed in dual-effect concentrator and is concentrated.
In the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state, food acids are lemon in step [1.5]
Lemon acid.
In the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state, table sugar is sugarcane in step [1.4]
Sugar or fructose.
In the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state, drink is passed through into pipe in step [4]
Road, which is delivered to after microwave sterilization machine sterilization, to carry out filling, and the frequency of microwave is 2450MHz.
It is in step [4] that drink is filling extremely in the above-mentioned preparation method for the folium cortex eucommiae compound beverage of conditioning subhealthy state
It after vial or plastic bottle, is delivered to microwave sterilization machine and is sterilized, the frequency of microwave is 2450MHz.
The advantageous effects that the present invention has are as follows:
1, for the present invention for groups such as current white collar, brain workers, operating pressure is big, is easy to appear inferior health etc.
Problem, preferably Cortex Eucommiae, Radix Astragali, root of kirilow rhodiola, rhizoma polygonati, dendrobium candidum, Fructus Corni a variety of tonic food, wherein Radix Astragali, red scape
It, rhizoma polygonati, dendrobium candidum, Fructus Corni deployed according to reasonable ratio, play invigorating the spleen clearing lung-heat, lower hyperlipidemia, hypertension, hyperglycemia, tonify Qi of the kidney, improve and exempt from
The effect of the comprehensive nourishings such as epidemic disease power, conditioning subhealthy state.Especially Cortex Eucommiae itself has liver heat removing and kidney replenishing, adjusts as rare invigorant
Lipoid and reducing blood pressure, strengthening the bones and muscles, anti-aging, the nourishing effects for improving immunity, at the same also have it is neutral mild, as ministerial drug when repellency
Small property feature can enhance effect with a variety of food medicinal material compatibilities such as Radix Astragali, root of kirilow rhodiola, rhizoma polygonati, dendrobium candidum, Fructus Corni.Drink
After material is taken for a long time, modern's inferior health illness can be improved, while also there are other composite efficacies, nourish, achieve many things at one stroke comprehensively.
2, the present invention is in the stabilization to nutritional ingredients such as Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves, flavones, Geniposidic acid, Aucubins
Property, on the basis of the characteristics such as anti-oxidant further investigation, in conjunction with the characteristic of institute's synthetic beverage, to the illumination influenced in raw material preparation,
The factors such as temperature, pH value have carried out accurate control, substantially increase product nutrient substances content.
3, intermediate products of the present invention in beverage --- in concentration prime cement preparation, to the loss characteristic of folium cortex eucommiae nutritional ingredient
It is studied, by addition citric acid or the scheme of other food acid agent, so that the PH of concentration prime cement is 3.5-4.0 or so,
The loss for effectively preventing the ingredients such as flavones, chlorogenic acid, Geniposidic acid adjust again in beverage preparation in later use prime cement
Whole to suitable pH value maintains the peculiar mouthfeel of Cortex Eucommiae beverage.It joined the table sugar of 20-30% in concentration prime cement simultaneously
(common beverages are about 8%) reduces dissolved oxygen amount by increasing sucrose concentration, effectively inhibits the oxygen of the substances such as flavones, chlorogenic acid
Change and decomposes.
4, the raw material in the present invention takes shading treatment in storage and preparation process, and folium cortex eucommiae is stored up using black woven bag
It deposits, reducing illumination influences the brings oxygenolysis such as chlorogenic acid, Geniposidic acid, Aucubin；Simultaneously by picking
Fresh folium cortex eucommiae is processed in time is prepared into folium cortex eucommiae concentration prime cement or eucommia ulmoides extract product, and arranges through overnutrition protection
Long term storage is applied, and logistics deployment is carried out according to the progress demand of subsequent beverage preparation, is avoided in traditional Cortex Eucommiae beverage preparation
Because of the long term storage bring nutrient loss of folium cortex eucommiae, at the same also reduce storage area and strange land end product preparation plus
The transportation cost in working hour has adapted to the place of production in modern plants extraction product manufacturing and has carried out raw material roughing extraction, strange land completion eventually
Hold product manufacturing sale with the new model of save the cost.
5, in the preparation of present invention concentration prime cement, accurate control has been carried out to temperature, so that drying, water logging are extracted, concentration is dry
Temperature in dry controls within 70 DEG C, these measures effectively prevent the loss of effective component in folium cortex eucommiae.
6, the present invention uses microwave sterilization in beverage preparation link and replaces traditional TRANSIENT HIGH TEMPERATURE sterilization method, sterilizing
Process continues to monitor the temperature of drink, and by extending sterilization time, and temperature is controlled 60-70 DEG C, using microwave heating effect with
The collective effect of non-thermal effect makes microbial body internal protein and physiological activator morph, develops and delay and dead, reaches
To food sterilizing, fresh-keeping purpose, simultaneously because temperature control at 65 DEG C or so, reduces conventional high temperature sterilizing to flavones, green
The decomposition of ortho acid, Geniposidic acid, Aucubin and Pinoresinol diglucoside improves the retention rate of nutritional ingredient.Together
When in microwave sterilization, can by drink it is filling after reserve the air gap and be placed in microwave sterilization machine and carry out, facilitate live behaviour
Make.
Specific embodiment
Inventor is studied for a long period of time discovery, either the storage of folium cortex eucommiae, water logging extract or beverage preparation link in,
The nutritional ingredients such as chlorogenic acid, flavones, Geniposidic acid, Aucubin, Pinoresinol diglucoside can all occur in various degree
It decomposes and is lost, major influence factors have:
(1) storage time and illumination effect
In traditional folium cortex eucommiae beverage processing, drying of being exposed to the sun in the sunlight after the picking of fresh folium cortex eucommiae, in the form of cured leaf into
Row long term storage carries out water logging extraction to Cortex Eucommiae leaf raw material again according to demand in beverage preparation.And inventor and other scholars
Research achievement show that raw material in prolonged storage, is influenced by extraneous factor, especially illumination is to yellow in folium cortex eucommiae
Ketone, chlorogenic acid, Geniposidic acid, Aucubin and Pinoresinol diglucoside have large effect effect, under light illumination
It easily causes oxygenolysis and causes nutrition loss.
For the influence of illumination factor in raw material long term storage, the present invention abandoned traditional folium cortex eucommiae drying and
Storing mode disposably dries storage using drying machine after feedstock capture in the fall, and carries out water to folium cortex eucommiae as early as possible
Extraction process is soaked, manufactured folium cortex eucommiae concentrate, which is placed in freezer, to be stored.In addition, taken in raw material storage and preparation process
Shading treatment, folium cortex eucommiae select the storage of black woven bag, and the folium cortex eucommiae concentration prime cement after preparation is then placed on the aluminium foil of shading
Bag stored for extended periods, this mode not only reduce the loss of nutritional ingredient, and by the side of folium cortex eucommiae at source long term storage
Formula be changed to folium cortex eucommiae concentration prime cement long term storage, greatly reduce storage area and strange land beverage preparation processing when transport at
This.
(2) influence of temperature parameter
Traditional folium cortex eucommiae extracts usually leaches dozens of minutes in the boiled water boiled, and the newest result of study of inventor
During showing Cortex Eucommiae beverage preparation, high temperature is to flavones, chlorogenic acid, two grape of Geniposidic acid, Aucubin and rosin spirit
Glucoside has large effect, and chlorogenic acid therein is heat-sensitive substance, when heating temperature is more than 70 DEG C, green original in leaching liquid
The content meeting rapid decrease of acid, it is therefore desirable to water soaking temperature be controlled, the present invention is continuously extracted using ultrasonic reverse back stream and set
It is standby to be extracted in temperature for 60-70 DEG C, while taking into account extracting efficiency, reduce the loss of nutritional ingredient.
(3) influence of pH value and sugar
The research achievement of inventor shows the protection of sugar content and pH value appropriate in beverage to nutritional ingredient in folium cortex eucommiae
It acts on more significant.Within the scope of certain sucrose concentration, the loss late of the ingredients such as flavones, chlorogenic acid is with sucrose concentration in beverage
Increase and reduce, this is because the increase of sugared content, declines the oxygen content in solution, inhibits the oxidation of flavones, chlorogenic acid
It decomposes.Therefore, the sucrose of 20%-30% has been especially added in concentration prime cement preparation (sugar content is about in common Sugared beverages
8%), to meet the requirement stored for a long time.It needs to be diluted with water sugared concentration according to production in later period beverage preparation, will not influence
The mouthfeel of product.
By on pH value on nutritional ingredient influence studies have shown that for eucommia bark flavone, resist under acidic environment
Oxidability is stronger, and antioxidant activity significantly reduces under alkaline environment；And for chlorogenic acid, Geniposidic acid, peach jaurel
For glucoside and Pinoresinol diglucoside, under acidic environment, thermal stability is also at preferable states, comprehensively consider it is different at
Point different to the influence degree of pH value, and combine drink and production process and organoleptic requirements, final choice is by the soda acid of concentrate
Degree is 3.5-4.0 by increasing the scheme of the food acids such as citric acid to deploy to PH, realizes flavones and chlorogenic acid to the maximum extent
Etc. Different Nutritions ingredient balance retain.
Embodiment one:
A kind of preparation method of the folium cortex eucommiae compound beverage for conditioning subhealthy state, comprising the following steps:
[1] preparation of folium cortex eucommiae concentrate:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 60 DEG C, so that folium cortex eucommiae contains
Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag；
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step,
Wash off the dust on blade face；Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water
It is dry；
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:10 (mass ratio) is placed in ultrasonic reverse back
It flows continuous extract equipment to extract, temperature is 60 DEG C, and water logging extraction time is 3 hours；The work of the ultrasonic continuous extract equipment of reverse back stream
It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle
Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted
Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real
Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 20% or so.Inspissator is preferably double
Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter
The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 3.5 are added in concentrated slurry；
Sucrose is added according still further to the ratio of 20% (mass ratio), is finally made folium cortex eucommiae concentrate；
The purpose of addition food acids and table sugar is to prevent the oxidational losses of nutritional ingredient in folium cortex eucommiae in concentrate, prolongs
Long shelf lives, and have no effect on subsequent drink mouthfeel.
[1.5] it stores
Manufactured folium cortex eucommiae concentrate is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer
It is stored, is prepared for beverage, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] ingredient
According to 20 parts of folium cortex eucommiae concentrate, 5 parts of Radix Astragali instant powder, 10 parts of root of kirilow rhodiola instant powder, 5 parts of rhizoma polygonati instant powder, iron
5 parts of skin dendrobium nobile instant powder, 5 parts of Fructus Corni instant powder, 4 parts of trehalose, 1 part of honey, 0.05 part of citric acid, sodium citrate 0.08
Part, 0.01 part of ethylmaltol, 0.05 part of sodium dehydroacetate, 0.05 part of calgon, 0.03 part of gellan gum, xanthan gum 0.08
Part, 0.05 part of sodium carboxymethylcellulose, the quality that 0.03 part of fruity flavor is added pure water and sufficiently dissolves than ingredient, wherein
The weight of pure water is 90 times of folium cortex eucommiae concentrate weight；
[3] filtering, homogeneous, sterilizing, filling
Mother liquor after ingredient is pumped into high pressure homogenizer after the filtering of diatomite plate filter and carries out homogeneous, after homogeneous
It is then filling into metal top pop tank after drink is by Pipeline transport to microwave sterilization machine sterilization, wherein diatomite plate filter
Filtering accuracy be 200 mesh, the homogenization pressure of high pressure homogenizer is 50kPa；The frequency of microwave is 2450MHz, sterilization in sterilizing
The temperature control of beverage is at 60 DEG C in the process, the time of sterilizing depending on drink flow and microwave power, drink after sterilizing
Total plate count and yeast bacterial content are no more than national regulations.
[5] it is packed and stored
Packaging, labeling, vanning and coding storage.
Embodiment two:
A kind of preparation method of the folium cortex eucommiae compound beverage for conditioning subhealthy state, comprising the following steps:
[1] preparation of Cortex Eucommiae concentrate:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 70 DEG C, so that folium cortex eucommiae contains
Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag；
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step,
Wash off the dust on blade face；Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water
It is dry；
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:30 (mass ratio) is placed in ultrasonic reverse back
It flows continuous extract equipment to extract, temperature is 70 DEG C, and water logging extraction time is 4 hours；The work of the ultrasonic continuous extract equipment of reverse back stream
It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle
Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted
Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real
Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 30% or so.Inspissator is preferably double
Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter
The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 4.0 are added in concentrated slurry；
Sucrose is added according still further to the ratio of 30% (mass ratio), is finally made folium cortex eucommiae concentrate；
The purpose of addition food acids and table sugar is to prevent the oxidational losses of nutritional ingredient in folium cortex eucommiae in concentrate, prolongs
Long shelf lives, and have no effect on subsequent drink mouthfeel.
[1.5] it stores
Manufactured folium cortex eucommiae concentrate is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer
It is stored, is prepared for beverage, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] ingredient
According to 30 parts of folium cortex eucommiae concentrate, 10 parts of Radix Astragali instant powder, 20 parts of root of kirilow rhodiola instant powder, 10 parts of rhizoma polygonati instant powder,
10 parts of dendrobium candidum instant powder, 10 parts of Fructus Corni instant powder, 8 parts of trehalose, 2 parts of honey, 0.08 part of citric acid, sodium citrate
0.12 part, 0.02 part of ethylmaltol, 0.08 part of sodium dehydroacetate, 0.1 part of calgon, 0.05 part of gellan gum, xanthan gum
0.12 part, 0.1 part of sodium carboxymethylcellulose, the quality that 0.05 part of fruity flavor is added pure water and sufficiently dissolves than ingredient,
The weight of middle pure water is 100 times of folium cortex eucommiae concentrate weight；
[4] filtering, homogeneous, sterilizing, filling
Mother liquor after ingredient is pumped into high pressure homogenizer after the filtering of diatomite plate filter and carries out homogeneous, after homogeneous
Drink is filling to after vial or plastic bottle, is delivered to microwave sterilization machine and is sterilized；The wherein mistake of diatomite plate filter
Filter precision is 400 mesh, and the homogenization pressure of high pressure homogenizer is 60kPa；The frequency of microwave is 2450MHz, sterilization process in sterilizing
The temperature control of middle beverage at 70 DEG C, the time of sterilizing depending on drink flow and microwave power, the bacterium colony of drink after sterilizing
Sum and yeast bacterial content are no more than national regulations.
[5] it is packed and stored
Packaging, labeling, vanning and coding storage.
In order to be verified to above-mentioned technical effect, the present invention carried out respectively folium cortex eucommiae drying sunning comparative experiments,
Extraction temperature comparative experiments, pH value comparative experiments, pol comparative experiments, and chromatographic column and standard method of measurement are used, it determines
The content of the nutritional ingredients such as flavones, chlorogenic acid, Pinoresinol diglucoside.Experimental result is as follows:
(1) drying sunning comparative experiments
The fresh folium cortex eucommiae of picking is divided into three parts of phase homogenous quantities, carried out respectively fresh leaf directly extract, the sun
Under dry with the drying experiment of 60-70 DEG C of machine, wherein dried under the sun and continue one week under ventilated environment in the fall, use is identical
Process conditions are completed water logging and are extracted.Every group is tested in triplicate, takes its average value, measures the relative amount of its nutritional ingredient.Knot
Fruit is as shown in table 1.
The drying sunning control experiment result of table 1
| Flavones retention rate | Chlorogenic acid retention rate | |
| Fresh folium cortex eucommiae water logging is extracted | 100% | 100% |
| Sun sunning | 86.7% | 83.5% |
| Machine drying | 95.2% | 94.4% |
1 experimental data of table explanation, using 60-70 DEG C of machine drying technology, than being dried under traditional sun to flavones and green
10% or so reserved can be improved in ortho acid.
(2) extraction temperature control experiment
The Folium Eucommiae of equal mass is placed in water logging in extractor to extract, only changes water soaking temperature, other parameters are identical,
Setting at a temperature of heat 30 minutes, then kept for 3 hours at 60 DEG C, measure the relative amount of its nutritional ingredient.Every group
It tests in triplicate, takes its average value, the results are shown in Table 2.
2 extraction temperature control experiment of table
| Extraction temperature | 100℃ | 90℃ | 80℃ | 70℃ | 60℃ | 50℃ |
| Chlorogenic acid | 75.2% | 80.4% | 88.5% | 96.8% | 105.3% | 100% |
| Pinoresinol diglucoside | 73.3% | 79.1% | 85.5% | 92.2% | 98.2% | 100% |
2 experimental data of table explanation, extraction temperature are most important to the reservation of nutritional ingredient.
(3) pH value control experiment
Appropriate citric acid is added in leaching liquor, is adjusted pH to setting value, is kept in dark place 3 months at room temperature, measures its battalion
The relative amount formed point, every group is tested in triplicate, takes its average value, the results are shown in Table 3.
3 pH value control experiment of table
| PH value | 3.0 | 4.0 | 5.0 | 6.0 |
| Chlorogenic acid | 110.3% | 104.6% | 103.5% | 100% |
| Flavones | 114.3% | 109.1% | 102.8% | 100% |
3 experimental data of table explanation, leaching liquor is under acidic environment, conducive to the long-term preservation of nutriment.
(4) pol control experiment
Suitable amount of sucrose is added in leaching liquor, is adjusted sugar content, is kept in dark place 3 months at room temperature, measures its nutritional ingredient
Relative amount, every group is tested in triplicate, takes its average value, the results are shown in Table 4.
4 pol control experiment of table
| Sugar content | 0% | 5% | 10% | 15% | 20% | 25% | 30% |
| Chlorogenic acid | 83.4% | 92.0% | 94.6% | 97.1% | 97.2% | 97.9% | 100% |
| Flavones | 84.3% | 91.9% | 95.2% | 96.5% | 97.2% | 98.0% | 100% |
4 experimental data of table explanation, addition sucrose facilitate the long-term preservation of leaching liquor nutriment.
The present invention is on the factor for influencing folium cortex eucommiae nutritional ingredient in beverage and other product configurations, such as temperature, illumination, soda acid
Degree, sugar content etc. have carried out parameter optimization and control, are used successfully in the preparation of concentrate, and further experiment shows
For the present invention compared with traditional folium cortex eucommiae extractive technique, the ratio of the nutritional ingredients such as flavones, chlorogenic acid improves about 20%-30%,
To effectively reduce product nutrient component damages produced during the preparation process, it is ensured that Cortex Eucommiae leaf beverage and other products are good
Health-care efficacy.
The folium cortex eucommiae compound beverage prepared according to the present invention, color is reddish brown bright, does not precipitate significantly, and have Cortex Eucommiae
Weak coffee fragrance has the health-care efficacies such as good conditioning subhealthy state, strengthen immunity, is able to satisfy white collar, mental labour
Person and special population demand, wide market.
Claims (10)
1. a kind of folium cortex eucommiae compound beverage for conditioning subhealthy state, which is characterized in that compound beverage by following material according to than
Example (mass ratio) is formulated after pure water is added: 20-30 parts of folium cortex eucommiae concentrate, 5-10 parts of Radix Astragali instant powder, and root of kirilow rhodiola speed
Molten powder 10-20 parts, 5-10 parts of rhizoma polygonati instant powder, 5-10 parts of dendrobium candidum instant powder, 5-10 parts of Fructus Corni instant powder, trehalose 4-
It 8 parts, 1-2 parts of honey, 0.05-0.08 parts of citric acid, 0.08-0.12 parts of sodium citrate, 0.01-0.02 parts of ethylmaltol, takes off
0.05-0.08 parts of acetate hydrogen sodium, 0.05-0.1 parts of calgon, 0.03-0.05 parts of gellan gum, 0.08-0.12 parts of xanthan gum,
0.05-0.1 parts of sodium carboxymethylcellulose, 0.03-0.05 parts of fruity flavor.
2. a kind of preparation method of the folium cortex eucommiae compound beverage for conditioning subhealthy state, which comprises the following steps:
[1] prepared by folium cortex eucommiae concentrate
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation lucifugal is stored in using black woven bag
It is spare in warehouse；
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction, temperature
It is 60-70 DEG C, water logging extraction time is 3-4 hours；
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,；
[1.4] protective agent adds
Food acids are added in concentrated slurry, so that pH value is 3.5-4.0, add the table sugar of 20-30% (mass ratio), make
Prime cement is concentrated at folium cortex eucommiae, is placed in sterile aluminum foil bag and stores, is prepared for beverage.
[2] ingredient
According to 20-30 parts of folium cortex eucommiae concentrate, 5-10 parts of Radix Astragali instant powder, 10-20 parts of root of kirilow rhodiola instant powder, rhizoma polygonati instant powder 5-
10 parts, 5-10 parts of dendrobium candidum instant powder, 5-10 parts of Fructus Corni instant powder, 4-8 parts of trehalose, 1-2 parts of honey, citric acid
0.05-0.08 parts, 0.08-0.12 parts of sodium citrate, 0.01-0.02 parts of ethylmaltol, 0.05-0.08 parts of sodium dehydroacetate,
0.05-0.1 parts of calgon, 0.03-0.05 parts of gellan gum, 0.08-0.12 parts of xanthan gum, sodium carboxymethylcellulose 0.05-
0.1 part, 0.03-0.05 parts of ingredients of fruity flavor, and pure water is added and sufficiently dissolves, wherein the weight of pure water is that folium cortex eucommiae is dense
90-100 times of contracting liquid weight；
[3] filtering, homogeneous, sterilizing, filling
Mother liquor after ingredient is pumped into high pressure homogenizer after the filtering of diatomite plate filter and carries out homogeneous, and is killed using microwave
Bacterium machine is sterilized, and the temperature of beverage is controlled at 60-70 DEG C in sterilization process.
3. the preparation method of the folium cortex eucommiae compound beverage according to claim 2 for conditioning subhealthy state, it is characterised in that:
The moisture content of folium cortex eucommiae is lower than 13% in step [1.1].
4. the preparation method of the folium cortex eucommiae compound beverage according to claim 2 for conditioning subhealthy state, it is characterised in that:
Tap water and pure water is respectively adopted in water for cleaning in step [1.2], wherein after being cleaned in pond with tap water, by Cortex Eucommiae
Leaf is placed on conveyer belt, is carried out spray with pure water and is cleaned.
5. the preparation method of the folium cortex eucommiae compound beverage according to claim 2 for conditioning subhealthy state, it is characterised in that:
It is extracted in step [1.2] using the ultrasonic continuous extract equipment of reverse back stream.
6. the preparation method of the folium cortex eucommiae compound beverage according to claim 2 for conditioning subhealthy state, it is characterised in that:
Folium cortex eucommiae leaching liquor is placed in dual-effect concentrator in step [1.3] and is concentrated.
7. the preparation method of the folium cortex eucommiae compound beverage according to claim 2 for conditioning subhealthy state, it is characterised in that:
Food acids are citric acid in step [1.5].
8. the preparation method of the folium cortex eucommiae compound beverage according to claim 2 for conditioning subhealthy state, it is characterised in that:
Table sugar is sucrose or fructose in step [1.4].
9. the preparation method of the folium cortex eucommiae compound beverage according to claim 1 for conditioning subhealthy state, it is characterised in that:
In step [4] that drink is filling by carrying out after Pipeline transport to microwave sterilization machine sterilization, the frequency of microwave is 2450MHz.
10. the preparation method of the folium cortex eucommiae compound beverage according to claim 1 for conditioning subhealthy state, feature exist
In: in step [4] that drink is filling to be delivered to microwave sterilization machine to after vial or plastic bottle and sterilized, the frequency of microwave
For 2450MHz.
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Citations (3)
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|---|---|---|---|---|
| CN103704801A (en) * | 2013-12-09 | 2014-04-09 | 陕西云智知识产权运营管理有限公司 | Preparation method of eucommia composite anti-fatigue functional beverage |
| CN108850319A (en) * | 2018-07-17 | 2018-11-23 | 陕西省安康市圣泰生物科技有限责任公司 | A kind of preparation method with health functions instant tea powder |
| CN108902417A (en) * | 2018-09-21 | 2018-11-30 | 苏州经贸职业技术学院 | A kind of health protection tea of antifatigue and increasing immune power and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103704801A (en) * | 2013-12-09 | 2014-04-09 | 陕西云智知识产权运营管理有限公司 | Preparation method of eucommia composite anti-fatigue functional beverage |
| CN108850319A (en) * | 2018-07-17 | 2018-11-23 | 陕西省安康市圣泰生物科技有限责任公司 | A kind of preparation method with health functions instant tea powder |
| CN108902417A (en) * | 2018-09-21 | 2018-11-30 | 苏州经贸职业技术学院 | A kind of health protection tea of antifatigue and increasing immune power and preparation method thereof |
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