CN109730226A - A kind of folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing and preparation method thereof - Google Patents
A kind of folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing and preparation method thereof Download PDFInfo
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- CN109730226A CN109730226A CN201811597148.2A CN201811597148A CN109730226A CN 109730226 A CN109730226 A CN 109730226A CN 201811597148 A CN201811597148 A CN 201811597148A CN 109730226 A CN109730226 A CN 109730226A
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- cortex eucommiae
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Non-Alcoholic Beverages (AREA)
Abstract
The invention discloses a kind of folium cortex eucommiae compound solid particle beverages of blood activating and fat reducing, solid granular beverage is mixed by the material of following ratio (mass ratio), wherein folium cortex eucommiae extract powder 3-5 parts, 2-3 parts of moringa seeds Ultramicro-powder, burdock ultramicro powder or 2-3 parts of extract powder, 1-2 parts of mulberry extract powder, 1-2 parts of gynostemma pentaphyllum extract powder, 45-55 parts of xylitol, 25-35 parts of D-sorbite, 3-5 parts of maltodextrin, 3-5 parts of casein sodium, 0.3-0.5 parts of beta-cyclodextrin, 0.05-0.1 parts of citric acid, 0.075-0.15 parts of sodium citrate, 0.05-0.1 parts of calgon, 0.01-0.02 parts of ethylmaltol, 0.05-0.08 parts of sodium dehydroacetate.The folium cortex eucommiae compound solid particle beverage of the blood activating and fat reducing prepared according to the present invention is a kind of granular granule, with good promoting blood circulation, lipid-loweringing, remove the health-care efficacies such as blood rubbish, it is suitable for white collar, brain worker and sub-health population demand, wide market.
Description
Technical field
The invention belongs to health food manufacture field, be related to a kind of blood activating and fat reducing folium cortex eucommiae compound solid particle beverage and
Preparation method.
Background technique
Cortex Eucommiae is the distinctive rare tonic herb of China, and folium cortex eucommiae is rich in flavones, loose ester alcohol diglucoside, Geniposide
The various nutrient elements such as glycosides, chlorogenic acid, caffeic acid, aucubin, the minerals such as Yi Jitie, zinc, selenium have and clear liver and improve vision,
Tonify Qi of the kidney, regulating lipoid and reducing blood pressure, anti-inflammatory be antibacterial, strengthening the bones and muscles, anti-aging, it is antifatigue, increase many effects such as immunity.
More using folium cortex eucommiae as the functional beverage of core material at present, a variety of function of folium cortex eucommiae are often utilized in these
Effect, but be a lack of for certain white collars or sub-health population blood activating and fat reducing, the compound beverage for removing rubbish in blood.This
In the method that external folium cortex eucommiae is extracted, also the effective component of folium cortex eucommiae is not studied, to obtain high nutrition valence
The product of value, it is ensured that the health-care efficacy of product.
Inventor is engaged in the research of Cortex Eucommiae beverage for many years, for example " a kind of Cortex Eucommiae is multiple in the Chinese patent of my invention in 2013
Close the preparation method (application No. is 201310658168.7) of anti-fatigue functional beverage, a kind of removal folium cortex eucommiae extract liquor peculiar smell is matched
The method (application No. is 201310658201.6) of health drink processed, a kind of preparation method of Cortex Eucommiae appetite-stimulating health-care drink
(201310658256.7) " in, a kind of preparation method of Cortex Eucommiae drinks is related to, after folium cortex eucommiae is extracted, using ozone
The method of processing and bioencapsulation processing overcomes careless fishy smell, bitter taste and the astringent taste problem outstanding in Cortex Eucommiae extract liquor, and soaks
Take use by folium cortex eucommiae boiled at 100 DEG C and hot conditions under the critical process that carries out.The above patented technology focuses on solving
The problem that folium cortex eucommiae peculiar smell how is removed in the preparation of Cortex Eucommiae beverage, does not optimize adjustment to technique in practice, to prevent
Only or reduce process for preparation in effective ingredient (active material) loss, so that it is guaranteed that the health-care efficacy of beverage.
Summary of the invention
The invention proposes folium cortex eucommiae compound solid particle beverages of a kind of blood activating and fat reducing and preparation method thereof, with folium cortex eucommiae
Extract powder is basic raw material, and mixing is added to the extract powders such as moringa seeds, fructus arctii, mulberry leaf, gynostemma pentaphylla or Ultramicro-powder, and it is solid that compound is made
Body beverage, is a kind of blood activating and fat reducing, the health care product for removing blood rubbish, while it is excellent in folium cortex eucommiae extraction to have carried out link technique
Change, reduces the loss of effective component, it is ensured that the health-care efficacy of product.
The present invention is added to following auxiliary material on the basis of folium cortex eucommiae extract powder: (1) moringa seeds: moringa seeds are reducing blood
Rouge, blood pressure, weight-reducing adjust stomach, and protect liver abstinence from alcohol, enhancing human immunity aspect has significant curative effect；(2) fructus arctii: tool
There is the effects for the treatment of diabetes, hypertension, hyperlipidemia, anticancer.Can hypoglycemic, blood pressure lowering, blood lipid, treatment insomnia, improve human body
Immunity and other effects；(3) mulberry leaf: there is lowering blood pressure and blood fat, hypoglycemic, norcholesterol, prevention myocardial infarction, cerebral hemorrhage, resist
Thrombosis and study of anti-atherogenic effect；(4) gynostemma pentaphylla: hypertension, hyperlipidemia, hyperglycemia, fatty liver can be treated by having
And other effects.Above-mentioned functional material is combined, compound promoting blood circulation solid granular beverage is made.
Technical scheme is as follows:
A kind of folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing, is mixed by the material of following ratio (mass ratio)
Solid granular beverage, wherein folium cortex eucommiae extract powder 3-5 parts, 2-3 parts of moringa seeds Ultramicro-powder, burdock ultramicro powder or extract powder 2-3
Part, 1-2 parts of mulberry extract powder, 1-2 parts of gynostemma pentaphyllum extract powder, 45-55 parts of xylitol, 25-35 parts of D-sorbite, maltodextrin 3-
5 parts, 3-5 parts of casein sodium, 0.3-0.5 parts of beta-cyclodextrin, 0.05-0.1 parts of citric acid, 0.075-0.15 parts of sodium citrate,
0.05-0.1 parts of calgon, 0.01-0.02 parts of ethylmaltol, 0.05-0.08 parts of sodium dehydroacetate.
A kind of preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation is stored in using black woven bag and is kept away
It is spare in the warehouse of light；
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction,
Temperature is 60-70 DEG C, and water logging extraction time is 3-4 hours；
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,；
[1.4] protective agent adds
Food acids are added in concentrated slurry, so that pH value is 3.5-4.0, add the table sugar of 5% (mass ratio), so
The beta-cyclodextrin of 5%-10% (mass ratio) is added afterwards, folium cortex eucommiae concentrate is made；
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, wherein shutting out
The moisture content of Zhong Ye extract powder is 5%-10%；The folium cortex eucommiae extract powder of preparation is placed in low-temperature storage in sterile aluminum foil bag, is used for
Beverage preparation；
[2] mixing granulation
According to 3-5 parts of folium cortex eucommiae extract powder, 2-3 parts of moringa seeds Ultramicro-powder, burdock ultramicro powder or 2-3 parts of extract powder, mulberry leaf
1-2 parts of extract powder, 1-2 parts of gynostemma pentaphyllum extract powder, 45-55 parts of xylitol, 25-35 parts of D-sorbite, 3-5 parts of maltodextrin, junket
3-5 parts of protein acid sodium, 0.3-0.5 parts of beta-cyclodextrin, 0.05-0.1 parts of citric acid, 0.075-0.15 parts of sodium citrate, six inclined phosphorus
Sour sodium 0.05-0.1 parts, 0.01-0.02 parts of ethylmaltol, the mass ratio that 0.05-0.08 parts of sodium dehydroacetate is weighed after mixing
The ethyl alcohol infiltration of 70-90% purity is added, is placed in pelletizer, it is that 10-12 purpose moistens particle that granularity, which is made, and sabot is sent into true
3-4 hours are dried at a temperature of 65-70 DEG C of empty drying box to get finished particle；
[3] it sterilizes
Microwave disinfection or radiation sterilizing will be carried out after finished particle quantitative package；Wherein in microwave disinfection beverage temperature control
System is at 60-70 DEG C；
[4] it is packed and stored
Vanning, coding, inspection, storage.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, folium cortex eucommiae in step [1.1]
Moisture content is lower than 13%.
Cleaning point in the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, in step [1.2]
Not Cai Yong tap water and pure water wherein folium cortex eucommiae is placed on conveyer belt after being cleaned in pond with tap water use pure water
Carry out spray cleaning.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, using ultrasound in step [1.2]
The continuous extract equipment of reverse back stream extracts.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, by folium cortex eucommiae in step [1.3]
Leaching liquor is placed in dual-effect concentrator and is concentrated.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, food acids are in step [1.4]
Citric acid.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, table sugar is in step [1.4]
Sucrose or fructose.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, spray drying in step [1.5]
The leaving air temp of tower is 50-60 DEG C.
In the preparation method of the folium cortex eucommiae compound solid particle beverage of above-mentioned blood activating and fat reducing, finished particle contains in step [2]
Water < 8%.
The advantageous effects that the present invention has are as follows:
1, the problems such as present invention is directed to current white collar, brain worker or sub-health population blood viscousness, blood lipid is high,
It is preferred that compound solid beverage is made in folium cortex eucommiae, moringa seeds, fructus arctii, mulberry leaf, gynostemma pentaphylla, wherein moringa seeds, fructus arctii, mulberry leaf, strand
Stock is blue to be deployed by reasonable component ratio, plays the role of blood activating and fat reducing, and folium cortex eucommiae itself has and adjusts as rare invigorant
The effect of lipoid and reducing blood pressure, at the same also have it is neutral mild, as ministerial drug when the small property feature of repellency, can with moringa seeds, fructus arctii,
A variety of food medicinal material compatibilities such as mulberry leaf, gynostemma pentaphylla enhance effect.Beverage take for a long time after, except meet sub-health population blood activating and fat reducing,
Outside the health-care efficacy for removing blood rubbish, moreover it is possible to it plays strengthening the bones and muscles, anti-aging, improve the composite efficacies such as immunity, nourish comprehensively,
It achieves many things at one stroke.
2, the present invention is in the stabilization to nutritional ingredients such as Chlorogenic Acid in Eucommia ulmoides Oliv. Leaves, flavones, Geniposidic acid, Aucubins
Property, on the basis of the characteristics such as anti-oxidant further investigation, in conjunction with the characteristic of institute's synthetic beverage, to the illumination influenced in raw material preparation,
The factors such as temperature, pH value have carried out accurate control, substantially increase product nutrient substances content.
3, intermediate products of the present invention in beverage --- in extract powder preparation, to the loss characteristic of folium cortex eucommiae nutritional ingredient into
Research of having gone, so that the PH that prime cement is concentrated is 3.5-4.0 or so, has by addition citric acid or the scheme of other food acid agent
Effect prevents the loss of the ingredients such as flavones, chlorogenic acid, Geniposidic acid, adjust again in beverage preparation in later use prime cement
To suitable pH value, the peculiar mouthfeel of Cortex Eucommiae beverage is maintained.The table sugar that joined 5% in concentration prime cement simultaneously, passes through increasing
Add sucrose concentration to reduce dissolved oxygen amount, effectively inhibits the oxygenolysis of the substances such as flavones, chlorogenic acid.Wherein selection 5% is sugared adds
Dosage be comprehensively consider sugared part ratio it is dry to subsequent spray to the degree of protection of nutritional ingredient and too low sugar in caused by
Agglomeration, viscous wall etc. influence, and carry out the result of parameter optimization.Furthermore it is added to the beta-cyclodextrin of 5%-10% before spray drying,
The characteristics of using its embedding effect and granular material, under the premise of not influencing drying process with atomizing, realize nutritional ingredient
Retain.
4, the raw material in the present invention takes shading treatment in storage and preparation process, and folium cortex eucommiae is stored up using black woven bag
It deposits, reducing illumination influences the brings oxygenolysis such as chlorogenic acid, Geniposidic acid, Aucubin；Simultaneously by picking
Fresh folium cortex eucommiae is processed in time is prepared into folium cortex eucommiae concentration prime cement or eucommia ulmoides extract product, and arranges through overnutrition protection
Long term storage is applied, and logistics deployment is carried out according to the progress demand of subsequent beverage preparation, is avoided in traditional Cortex Eucommiae beverage preparation
Because of the long term storage bring nutrient loss of folium cortex eucommiae, at the same also reduce storage area and strange land end product preparation plus
The transportation cost in working hour has adapted to the place of production in modern plants extraction product manufacturing and has carried out raw material roughing extraction, strange land completion eventually
Hold product manufacturing sale with the new model of save the cost.
5, the present invention has carried out accurate control to temperature in extract powder preparation, so that drying, water logging are extracted, concentration is dry
Temperature in dry controls within 70 DEG C, these measures effectively prevent the loss of effective component in folium cortex eucommiae.
6, the present invention uses microwave sterilization in beverage preparation link and replaces traditional TRANSIENT HIGH TEMPERATURE sterilization method, sterilizing
The temperature of drink is continued to monitor in the process, and by extending sterilization time, temperature is controlled 60-70 DEG C, utilizes microwave heating effect
With the collective effect of non-thermal effect, so that microbial body internal protein and physiological activator is morphed, develops and delay and dead,
Achieve the purpose that food sterilizing, fresh-keeping, simultaneously because temperature control is at 65 DEG C or so, to Huang when reducing conventional high temperature sterilizing
The decomposition of ketone, chlorogenic acid, Geniposidic acid, Aucubin and Pinoresinol diglucoside improves the holding of nutritional ingredient
Rate.Simultaneously in microwave sterilization, can by drink it is filling after reserve the air gap and be placed in microwave sterilization machine and carry out, facilitate existing
Field operation.
Specific embodiment
Inventor is studied for a long period of time discovery, either the storage of folium cortex eucommiae, water logging extract or beverage preparation link in,
The nutritional ingredients such as chlorogenic acid, flavones, Geniposidic acid, Aucubin, Pinoresinol diglucoside can all occur in various degree
It decomposes and is lost, major influence factors have:
(1) storage time and illumination effect
In traditional folium cortex eucommiae beverage processing, drying of being exposed to the sun in the sunlight after the picking of fresh folium cortex eucommiae, in the form of cured leaf into
Row long term storage carries out water logging extraction to Cortex Eucommiae leaf raw material again according to demand in beverage preparation.And inventor and other scholars
Research achievement show that raw material in prolonged storage, is influenced by extraneous factor, especially illumination is to yellow in folium cortex eucommiae
Ketone, chlorogenic acid, Geniposidic acid, Aucubin and Pinoresinol diglucoside have large effect effect, under light illumination
It easily causes oxygenolysis and causes nutrition loss.
For the influence of illumination factor in raw material long term storage, the present invention abandoned traditional folium cortex eucommiae drying and
Storing mode disposably dries storage using drying machine after feedstock capture in the fall, and carries out water to folium cortex eucommiae as early as possible
Extraction process is soaked, manufactured folium cortex eucommiae extract powder, which is placed in freezer, to be stored.In addition, taken in raw material storage and preparation process
Shading treatment, folium cortex eucommiae select the storage of black woven bag, and the folium cortex eucommiae concentration prime cement after preparation is then placed on the aluminium foil of shading
Bag stored for extended periods, this mode not only reduce the loss of nutritional ingredient, and by the side of folium cortex eucommiae at source long term storage
Formula is changed to the long term storage of folium cortex eucommiae extract powder, greatly reduce storage area and strange land beverage preparation processing when transport at
This.
(2) influence of temperature parameter
Traditional folium cortex eucommiae extracts usually leaches dozens of minutes in the boiled water boiled, and the newest result of study of inventor
During showing Cortex Eucommiae beverage preparation, high temperature is to flavones, chlorogenic acid, two grape of Geniposidic acid, Aucubin and rosin spirit
Glucoside has large effect, and chlorogenic acid therein is heat-sensitive substance, when heating temperature is more than 70 DEG C, green original in leaching liquid
The content meeting rapid decrease of acid, it is therefore desirable to water soaking temperature be controlled, the present invention is continuously extracted using ultrasonic reverse back stream and set
It is standby to be extracted in temperature for 60-70 DEG C, while taking into account extracting efficiency, reduce the loss of nutritional ingredient.
(3) influence of pH value and sugar
The research achievement of inventor shows the protection of sugar content and pH value appropriate in beverage to nutritional ingredient in folium cortex eucommiae
It acts on more significant.Within the scope of certain sucrose concentration, the loss late of the ingredients such as flavones, chlorogenic acid is with sucrose concentration in beverage
Increase and reduce, this is because the increase of sugared content, declines the oxygen content in solution, inhibits the oxidation of flavones, chlorogenic acid
It decomposes.Therefore concentration prime cement preparation in be purposefully added 5% sucrose, meet the requirement that extract powder product stores for a long time, and
The sugar of the ratio has no effect on subsequent spray drying process.In later period beverage preparation according to production need be diluted with water sugar it is dense
Degree, will not influence the mouthfeel of product.
By on pH value on nutritional ingredient influence studies have shown that for eucommia bark flavone, resist under acidic environment
Oxidability is stronger, and antioxidant activity significantly reduces under alkaline environment；And for chlorogenic acid, Geniposidic acid, peach jaurel
For glucoside and Pinoresinol diglucoside, under acidic environment, thermal stability is also at preferable states, comprehensively consider it is different at
Point different to the influence degree of pH value, and combine drink and production process and organoleptic requirements, final choice is by the soda acid of concentrate
Degree is 3.5-4.0 by increasing the scheme of the food acids such as citric acid to deploy to PH, realizes flavones and chlorogenic acid to the maximum extent
Etc. Different Nutritions ingredient balance retain.
(4) embedding effect of beta-cyclodextrin
Inventor it has been investigated that, a certain proportion of beta-cyclodextrin is added in folium cortex eucommiae concentrate, can effectively inhibit
The loss of the nutritional ingredients such as flavones and chlorogenic acid, this is because beta-cyclodextrin main component is stable oligosaccharide, embedding is made
With the oxygenolysis for inhibiting the nutritional ingredients such as chlorogenic acid, flavones, thermal stability is improved.And suitable beta-cyclodextrin will not be right
The mouthfeel of product has an impact, and will not also impact to the process that Cortex Eucommiae concentrate spray drying prepares extract powder.
Embodiment one:
A kind of preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 60 DEG C, so that folium cortex eucommiae contains
Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag；
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step,
Wash off the dust on blade face；Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water
It is dry；
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:10 (mass ratio) is placed in ultrasonic reverse back
It flows continuous extract equipment to extract, temperature is 60 DEG C, and water logging extraction time is 3 hours；The work of the ultrasonic continuous extract equipment of reverse back stream
It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle
Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted
Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real
Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 20% or so.Inspissator is preferably double
Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter
The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 3.5 are added in concentrated slurry；
Sucrose is added according still further to the ratio of 5% (mass ratio), the beta-cyclodextrin of 10% (mass ratio) is then added, folium cortex eucommiae concentration is made
Liquid；
The purpose that food acids, table sugar and beta-cyclodextrin is added is to prevent the oxygen of nutritional ingredient in folium cortex eucommiae in concentrate
Change loss, extends shelf lives, and have no effect on subsequent drink mouthfeel.
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, control into
Air temperature is 100 DEG C, and leaving air temp is 50 DEG C, and the moisture content for the folium cortex eucommiae extract powder being prepared is 5%-10%；
Material enters the hot wind progress that drying tower is atomization, sends with air inlet fan in dryer section through centrifugal spraying disk in implementation
Heat exchange, surface of material moisture evaporate rapidly, are landed the cone below equipment by dry extract powder, humid air is by arranging in tower
Blower is discharged, and institute's band particle is down in cone through Bag filter recycling and is mixed with extract powder in exhaust gas, automatic through rotating blanking valve
It flows out in tower.
[1.6] it stores
Manufactured folium cortex eucommiae extract powder is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer
It is stored, is prepared for beverage and other products, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] mixing granulation
According to 3 parts of folium cortex eucommiae extract powder, 2 parts of moringa seeds Ultramicro-powder, 2 parts of burdock ultramicro powder, 1 part of mulberry extract powder, strand
1 part of blue extract powder, 45 parts of xylitol, 25 parts of D-sorbite, 3 parts of maltodextrin, 3 parts of casein sodium, 0.3 part of beta-cyclodextrin,
0.05 part of citric acid, 0.075 part of sodium citrate, 0.05 part of calgon, 0.01 part of ethylmaltol, sodium dehydroacetate 0.05
The ratio weighing, mixing and uniform stirring of part.Wherein folium cortex eucommiae extract powder is according to the homemade product of previous process, remaining object
Material is commercially available up-to-standard products.
According to the ethyl alcohol infiltration that 90% purity is added after above-mentioned formula weighing mixing, it is placed in pelletizer, granularity, which is made, is
10-12 purpose moistens particle, and sabot is 4 hours dry at a temperature of being sent into 70 DEG C of vacuum oven, when particle water content < 8% to get
Finished particle.
[3] it sterilizes
By the material stirred evenly according to progress microwave disinfection or radiation sterilizing after every bag of 20g quantitative package；Wherein microwave
The frequency of microwave is 2450MHz in sterilization, and the temperature of solid beverage is controlled at 60 DEG C in sterilization process, and the time of sterilizing is according to drink
Depending on product flow and microwave power, the total plate count of drink and yeast bacterial content are no more than national regulations after sterilizing.
[4] it is packed and stored
Vanning, coding, inspection, storage.
Embodiment two:
A kind of preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing, comprising the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
The fresh folium cortex eucommiae for harvesting the current year 6-9 month is placed in circulation drying tunnel and is dried at 70 DEG C, so that folium cortex eucommiae contains
Water rate is lower than 13%, and cured leaf is stored in spare in the warehouse of ventilation lucifugal using black woven bag；
[1.2] water logging is extracted
Folium cortex eucommiae to be cleaned, cleaning is divided into two steps: folium cortex eucommiae is placed in pond and is cleaned using tap water by the first step,
Wash off the dust on blade face；Folium cortex eucommiae after cleaning is placed on conveyer belt by second step, is dripped after carrying out spray cleaning using pure water
It is dry；
By the folium cortex eucommiae after cleaning according to dry Cortex Eucommiae leaf raw material: the ratio of water=1:30 (mass ratio) is placed in ultrasonic reverse back
It flows continuous extract equipment to extract, temperature is 70 DEG C, and water logging extraction time is 4 hours；The work of the ultrasonic continuous extract equipment of reverse back stream
It is that the high-frequency signal issued by ultrasonic wave is converted into the cell that mechanical oscillating wave destroys extract by energy converter as principle
Wall dissolves in effective component with free state and completes extraction process in water, and ensures that the effective component of water and extract is quickly melted
Dissolution is closed, while effective component is not destroyed, extraction time and efficiency are significantly improved.The equipment can be automatic at low temperature real
Existing continuous feed and continuous discharge, have the characteristics that water-saving, energy conservation, recovery rate are high.
[1.3] filtering and concentrating
Leaching liquor is placed in inspissator and is concentrated, being concentrated into solid content is 30% or so.Inspissator is preferably double
Inspissator is imitated, which can be had using external heat Natural Circulation and negative pressure of vacuum mode according to enrichment factor come selection parameter
The features such as evaporation rate is fast, and cocnentration factor is great, pollution-free, easy to clean.
[1.4] protective agent adds
Citric acid, uniform and monitoring potential stirring while adding, until pH value is 4.0 are added in concentrated slurry；
Sucrose is added according still further to the ratio of 5% (mass ratio), the beta-cyclodextrin of 5% (mass ratio) is then added, folium cortex eucommiae concentration is made
Liquid；
The purpose that food acids, table sugar and beta-cyclodextrin is added is to prevent the oxygen of nutritional ingredient in folium cortex eucommiae in concentrate
Change loss, extend shelf lives, and since concentrate and extract powder are beverage and the intermediate product of other product configurations, and simultaneously
Subsequent drink mouthfeel is not influenced.
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, control into
Air temperature is 120 DEG C, and leaving air temp is 60 DEG C, and the moisture content for the folium cortex eucommiae extract powder being prepared is 5%-10%；
[1.6] it stores
Manufactured folium cortex eucommiae extract powder is canned into sterile aluminum foil bag in clean workplace, and in air-conditioned cold store or freezer
It is stored, is prepared for beverage and other products, wherein the storage temperature of freezer is -10~-5 DEG C.
[2] mixing granulation
According to 5 parts of folium cortex eucommiae extract powder, 3 parts of moringa seeds Ultramicro-powder, 3 parts of fructus arctii extract powder, 2 parts of mulberry extract powder, strand
2 parts of blue extract powder, 55 parts of xylitol, 35 parts of D-sorbite, 5 parts of maltodextrin, 5 parts of casein sodium, 0.5 part of beta-cyclodextrin,
0.1 part of citric acid, 0.15 part of sodium citrate, 0.1 part of calgon, 0.02 part of ethylmaltol, 0.08 part of sodium dehydroacetate
Ratio weighing, mixing and uniform stirring.Wherein folium cortex eucommiae extract powder is according to the homemade product of previous process, remaining material
For commercially available up-to-standard products.
According to the ethyl alcohol infiltration that 70% purity is added after above-mentioned formula weighing mixing, it is placed in pelletizer, granularity, which is made, is
10-12 purpose moistens particle, and sabot is 3 hours dry at a temperature of being sent into 65 DEG C of vacuum oven, when particle water content < 8% to get
Finished particle.
[3] it sterilizes
By the material stirred evenly according to progress microwave disinfection or radiation sterilizing after every bag of 20g quantitative package；Wherein microwave
The frequency of microwave is 2450MHz in sterilization, and the temperature of solid beverage is controlled at 70 DEG C in sterilization process, and the time of sterilizing is according to drink
Depending on product flow and microwave power, the total plate count of drink and yeast bacterial content are no more than national regulations after sterilizing.
[4] it is packed and stored
Vanning, coding, inspection, storage.
In order to be verified to above-mentioned technical effect, the present invention carried out respectively folium cortex eucommiae drying sunning comparative experiments,
Extraction temperature comparative experiments, pH value comparative experiments, pol comparative experiments, beta-cyclodextrin embedding experiment, and chromatographic column is used, according to
National standard measurement method determines the content of the nutritional ingredients such as flavones, chlorogenic acid, Pinoresinol diglucoside.Experimental result
It is as follows:
(1) drying sunning comparative experiments
The fresh folium cortex eucommiae of picking is divided into three parts of phase homogenous quantities, carried out respectively fresh leaf directly extract, the sun
Under dry with the drying experiment of 60-70 DEG C of machine, wherein dried under the sun and continue one week under ventilated environment in the fall, use is identical
Process conditions are completed water logging and are extracted.Every group is tested in triplicate, takes its average value, measures the relative amount of its nutritional ingredient.Knot
Fruit is as shown in table 1.
The drying sunning control experiment result of table 1
| Flavones retention rate | Chlorogenic acid retention rate | |
| Fresh folium cortex eucommiae water logging is extracted | 100% | 100% |
| Sun sunning | 86.7% | 83.5% |
| Machine drying | 95.2% | 94.4% |
1 experimental data of table explanation, using 60-70 DEG C of machine drying technology, than being dried under traditional sun to flavones and green
10% or so reserved can be improved in ortho acid.
(2) extraction temperature control experiment
The Folium Eucommiae of equal mass is placed in water logging in extractor to extract, only changes water soaking temperature, other parameters are identical,
Setting at a temperature of heat 30 minutes, then kept for 3 hours at 60 DEG C, measure the relative amount of its nutritional ingredient.Every group
It tests in triplicate, takes its average value, the results are shown in Table 2.
2 extraction temperature control experiment of table
| Extraction temperature | 100℃ | 90℃ | 80℃ | 70℃ | 60℃ | 50℃ |
| Chlorogenic acid | 75.2% | 80.4% | 88.5% | 96.8% | 105.3% | 100% |
| Pinoresinol diglucoside | 73.3% | 79.1% | 85.5% | 92.2% | 98.2% | 100% |
2 experimental data of table explanation, extraction temperature are most important to the reservation of nutritional ingredient.
(3) pH value control experiment
Appropriate citric acid is added in leaching liquor, is adjusted pH to setting value, is kept in dark place 3 months at room temperature, measures its battalion
The relative amount formed point, every group is tested in triplicate, takes its average value, the results are shown in Table 3.
3 pH value control experiment of table
| PH value | 3.0 | 4.0 | 5.0 | 6.0 |
| Chlorogenic acid | 110.3% | 104.6% | 103.5% | 100% |
| Flavones | 114.3% | 109.1% | 102.8% | 100% |
3 experimental data of table explanation, leaching liquor is under acidic environment, conducive to the long-term preservation of nutriment.
(4) pol control experiment
Suitable amount of sucrose is added in leaching liquor, is adjusted sugar content, is kept in dark place 3 months at room temperature, measures its nutritional ingredient
Relative amount, every group is tested in triplicate, takes its average value, the results are shown in Table 4.
4 pol control experiment of table
4 experimental data of table explanation, addition sucrose facilitate the long-term preservation of leaching liquor nutriment.
(5) beta-cyclodextrin embedding experiment
Suitable beta-cyclodextrin is added in leaching liquor, is adjusted adding proportion, is kept in dark place 3 months at room temperature, measures it
The relative amount of nutritional ingredient, every group is tested in triplicate, takes its average value, the results are shown in Table 5.
The embedding experiment of 5 beta-cyclodextrin of table
| Beta-cyclodextrin amount | 0% | 2% | 4% | 6% | 8% | 10% |
| Chlorogenic acid | 88.2% | 90.4% | 90.4% | 93.0% | 94.6% | 100% |
| Pinoresinol diglucoside | 90.2% | 93.6% | 93.0% | 95.6% | 97.8% | 100% |
5 experimental data of table explanation is added beta-cyclodextrin to folium cortex eucommiae leaching liquor, facilitates the long-term preservation of nutriment.
The present invention on influenced in beverage and other product configurations the temperature of folium cortex eucommiae nutritional ingredient, illumination, pH value, containing sugar
Amount etc. has carried out parameter optimization and accurate control, is used successfully in the preparation of extract powder, and further experiment shows this hair
It is bright that the retention rate of the nutritional ingredients such as flavones, chlorogenic acid improves 20%-30% compared with traditional folium cortex eucommiae extractive technique,
Effectively reduce the loss of nutritional ingredient in product, it is ensured that the health-care efficacy of Cortex Eucommiae leaf beverage.
Color is reddish brown bright after the folium cortex eucommiae compound solid particle beverage bath of the blood activating and fat reducing prepared according to the present invention, does not have
There is apparent precipitating, and have the weak coffee fragrance of Cortex Eucommiae, there is good blood activating and fat reducing, remove the health-care efficacies such as blood rubbish,
It is suitable for white collar, brain worker and sub-health population demand, wide market.
Claims (10)
1. a kind of folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing, it is characterised in that: by the object of following ratio (mass ratio)
Material be mixed and made into solid granular beverage, wherein folium cortex eucommiae extract powder 3-5 parts, 2-3 parts of moringa seeds Ultramicro-powder, burdock ultramicro powder or
2-3 parts of extract powder, 1-2 parts of mulberry extract powder, 1-2 parts of gynostemma pentaphyllum extract powder, 45-55 parts of xylitol, 25-35 parts of D-sorbite,
3-5 parts of maltodextrin, 3-5 parts of casein sodium, 0.3-0.5 parts of beta-cyclodextrin, 0.05-0.1 parts of citric acid, sodium citrate
0.075-0.15 parts, 0.05-0.1 parts of calgon, 0.01-0.02 parts of ethylmaltol, sodium dehydroacetate 0.05-0.08
Part.
2. a kind of preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing, which comprises the following steps:
[1] preparation of folium cortex eucommiae extract powder:
[1.1] feedstock capture
After the fresh folium cortex eucommiae of acquisition is dried in 60-70 DEG C of drying tunnel, ventilation lucifugal is stored in using black woven bag
It is spare in warehouse；
[1.2] water logging is extracted
By the folium cortex eucommiae after cleaning according to dry folium cortex eucommiae: the ratio of water=1:10-30 (mass ratio) carries out flooding extraction, temperature
It is 60-70 DEG C, water logging extraction time is 3-4 hours；
[1.3] filtering and concentrating
It is 20-30% (mass ratio) that leaching liquor, which is concentrated into solid content,；
[1.4] protective agent adds
Food acids are added in concentrated slurry so that pH value be 3.5-4.0, add the table sugar of 5% (mass ratio), then plus
Folium cortex eucommiae concentrate is made in the beta-cyclodextrin for entering 5%-10% (mass ratio)；
[1.5] it is spray-dried
Cortex Eucommiae concentrate is placed in spray drying tower and is spray-dried, folium cortex eucommiae extract powder is prepared, wherein folium cortex eucommiae
The moisture content of extract powder is 5%-10%；The folium cortex eucommiae extract powder of preparation is placed in low-temperature storage in sterile aluminum foil bag, is used for beverage
Preparation；
[2] mixing granulation
According to 3-5 parts of folium cortex eucommiae extract powder, 2-3 parts of moringa seeds Ultramicro-powder, burdock ultramicro powder or 2-3 parts of extract powder, mulberry extract
1-2 parts of powder, 1-2 parts of gynostemma pentaphyllum extract powder, 45-55 parts of xylitol, 25-35 parts of D-sorbite, 3-5 parts of maltodextrin, casein
Sour sodium 3-5 parts, 0.3-0.5 parts of beta-cyclodextrin, 0.05-0.1 parts of citric acid, 0.075-0.15 parts of sodium citrate, calgon
It 0.05-0.1 parts, 0.01-0.02 parts of ethylmaltol, is added after the mass ratio that 0.05-0.08 part of sodium dehydroacetate weighing mixing
The ethyl alcohol of 70-90% purity infiltrates, and is placed in pelletizer, and it is that 10-12 purpose moistens particle that granularity, which is made, and it is dry that vacuum is sent into sabot
3-4 hours are dried at a temperature of 65-70 DEG C of dry case to get finished particle；
[3] it sterilizes
Microwave disinfection or radiation sterilizing will be carried out after finished particle quantitative package；Wherein the temperature control of beverage exists in microwave disinfection
60-70℃；
[4] it is packed and stored
Vanning, coding, inspection, storage.
3. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: the moisture content of folium cortex eucommiae is lower than 13% in step [1.1].
4. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: tap water and pure water is respectively adopted in the cleaning in step [1.2], wherein after being cleaned in pond with tap water, by Cortex Eucommiae
Leaf is placed on conveyer belt, is carried out spray with pure water and is cleaned.
5. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: it is extracted in step [1.2] using the ultrasonic continuous extract equipment of reverse back stream.
6. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: folium cortex eucommiae leaching liquor is placed in dual-effect concentrator in step [1.3] and is concentrated.
7. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: food acids are citric acid in step [1.4].
8. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: table sugar is sucrose or fructose in step [1.4].
9. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: the leaving air temp of spray drying tower is 50-60 DEG C in step [1.5].
10. the preparation method of the folium cortex eucommiae compound solid particle beverage of blood activating and fat reducing according to claim 2, feature exist
In: finished particle water content < 8% in step [2].
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Cited By (2)
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| CN112205559A (en) * | 2020-10-20 | 2021-01-12 | 山东贝隆杜仲生物工程有限公司 | Composition containing eucommia ulmoides and mulberry leaves and application |
| CN114668092A (en) * | 2022-04-14 | 2022-06-28 | 江苏天美健大自然生物工程有限公司 | Fish collagen dipeptide fruit-flavored drink and preparation method thereof |
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| CN1081826A (en) * | 1993-05-31 | 1994-02-16 | 赵岁元 | Health-care tea |
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| CN114668092A (en) * | 2022-04-14 | 2022-06-28 | 江苏天美健大自然生物工程有限公司 | Fish collagen dipeptide fruit-flavored drink and preparation method thereof |
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