CN108677562A - 一种涤棉混纺纤维无前处理染色方法 - Google Patents

一种涤棉混纺纤维无前处理染色方法 Download PDF

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CN108677562A
CN108677562A CN201810452401.9A CN201810452401A CN108677562A CN 108677562 A CN108677562 A CN 108677562A CN 201810452401 A CN201810452401 A CN 201810452401A CN 108677562 A CN108677562 A CN 108677562A
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位东
边建伟
徐峰
丰硕
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Luthai Textile Co Ltd
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Abstract

本发明提供一种涤棉混纺纤维无前处理染色方法，采用以下步骤为：1)将涤棉混纺纤维入水，向主缸内加入去油灵1‐3g/L，90℃保温10min后排水，再水洗后又入温水，完后向主缸内加入分散剂RDT、AB酸和分散染料，135℃保温后降温至80℃，排水；2)入温水，向主缸内加入还原清洗液，深色品种清洗温度选择85℃，浅色品种清洗温度选择100℃，保温均为20min；完后入温水，向主缸内加入醋酸HACP85 2‐3g/L，50℃保温15min后排水，再温水洗涤；3)浴比为1：6～16，向主缸内加入水和元明粉，50℃保温20min，再向主缸内加入活性染料，升温至60℃，保温30min；向主缸内加入纯碱10‐30g/L，保温60min后排液；入热水进行皂洗后入温水，一次向主缸内加入醋酸HACP85、柔软剂PLS和固色剂，排液。

Description

一种涤棉混纺纤维无前处理染色方法
本发明提供一种涤棉混纺纤维无前处理染色方法，属于纺织工业纱线染色技术领域。
技术背景
涤棉混纺纤维是涤纶纤维与棉纤维混合而成的纤维，织造而成的纺织品俗称的确良，具有优良的服用性能；涤棉织物是我国20世纪60年代初期开发的一个品种，其既突出了涤纶的风格，又有棉织物的长处，在干、湿情况下，弹性和耐磨性都较好，尺寸稳定，缩水率小，同时具有挺拔、不易皱折，易洗，快干的特点，深受消费者喜爱。现有涤棉混纺纤维生产工艺繁琐，首先需要对纤维进行前处理，提高白度，去除杂质；然后对涤组分进行染色，还原清洗，去除涤染料浮色；最后对棉组分进行染色，皂洗，去除浮色。
发明内容
本发明的目的是提供一种能克服上述缺陷、缩短涤棉品种染色流程、同时减少涤棉纱线强力降低的一种涤棉混纺纤维无前处理染色法。其技术方案为：
一种涤棉混纺纤维无前处理染色方法，其特征在于采用以下步骤为：
1)染涤：将涤棉混纺纤维入水，浴比为1：6～16，完后向主缸内加入去油灵，去油灵在主缸内的浓度为1-3g/L.，90℃保温10min，排水；再入热水，保温10min，水洗后排水；又入温水，完后向主缸内加入分散剂RDT、AB酸和分散染料，使分散剂RDT的浓度为1-2g/L，使AB酸的浓度1.5g/L，使分散染料的浓度为0-3％(o.w.f)(但不包括0)，135℃保温30min～50min，完后降温至80℃，排水；
2)还原清洗：入温水，向主缸内加入还原清洗液，还原清洗液中保险粉浓度3.5-5g/L、烧碱浓度3-4g/L、净洗剂WOLR浓度1-3g/L，深色品种清洗温度选择85℃，浅色品种清洗温度选择100℃，保温均为20min，排水后还原清洗；完后入温水，向主缸内加入醋酸HACP85使其浓度为2-3g/L，50℃保温15min，排水；完后入温水，10min水洗后排水；
3)染棉：浴比为1：6～16，向主缸内加入水，然后向主缸内加入元明粉，元明粉浓度在主缸内浓度为10-80g/L，50℃保温20min，再向主缸内加入活性染料浓度为为0-10％(o.w.f)(但不包括0)，以1℃/min的升温速率升温至60℃，保温30min；向主缸内加入纯碱，使纯碱浓度为10-30g/L，保温60min后排液；入热水，向主缸内加入皂洗剂WOLR，使皂洗剂WOLR浓度为1-2g/L，升温至98℃保温15min后排液，皂洗；入温水，一次向主缸内加入醋酸HACP85、柔软剂PLS和固色剂，三者的浓度分别为0.5-0.6g/L、2.5-3.5％和3-5％，55℃保温21min，排液。
所述一种涤棉混纺纤维无前处理染色方法，所染纤维为筒纱状态或经轴状态，筒纱要求个重为1±0.05kg，密度为0.36-0.4g/cm3，筒纱为规则圆柱体，单批筒纱密度一致，经轴密度为0.45-0.49g/cm3，经轴表面无明显凹凸不平现象。
所述一种涤棉混纺纤维无前处理染色方法，染涤过程中，分散染料为E型染料、SE型染料或者S型染料，其中E型染料包括Blue E-RPD、Red E-RPD和Yellow E-RP等的一种或几种的任意组合，SE型染料包括Blue SE-RPD、Red SE-RPD和Yellow SE-RPD等的一种或几种的任意组合，S型染料包括NavyBlue S-WF、Red S-WF和Yellow S-WF等的一种或几种的任意组合。
所述一种涤棉混纺纤维无前处理染色方法，染筒纱过程中，染机泵速为90％；染经轴过程中，泵速为95-99％。
所述一种涤棉混纺纤维无前处理染色方法，整个工艺过程中，分散染料及活性染料均为均匀10min加入，纯碱为均匀30min加入。
所述一种涤棉混纺纤维无前处理染色方法，整个工艺过程中，常温水为20-30℃、温水为50℃±2℃、热水为80-90℃。
本发明与现有技术相比，无前处理步骤，能够省略前处理过程，只用去油灵对涤棉混纺纤维进行10min水洗，直接染涤，然后利用还原清洗过程对棉组分进行漂白及精炼，直接染棉。该项生产技术可以缩短涤棉品种染色流程，节约用气、用电，减少助剂的消耗，提高劳动效率，同时减少涤棉纱线强力的降低。
具体实施方案：
下面结合实施例对本发明技术方案做进一步阐述，但本发明不局限于所列实例。
实施例一：筒纱个重为1kg，密度为0.36g/cm3，筒纱为规则圆柱体，纱密度一致，表面无明显凹凸不平现象。具体步骤如下：
1)染涤：放入涤棉混纺纤维，入水，浴比为1：6，完后向主缸内加入去油灵，使去油灵浓度为1g/L，90℃保温10min，排水；入热水，保温10min，水洗后排水；入温水，完后向主缸内加入分散剂RDT 1g/L、AB酸1.5g/L和E型分散染料，E型分散染料具体为Blue E-RPD0.036％、Red E-RPD 0.012％和Yellow E-RPD 0.001％，135℃保温30min，完后降温至80℃，排水；
2)还原清洗：入温水，向主缸内加入还原清洗液，其配方为保险粉3.5g/L、烧碱3g/L、净洗剂WOLR 1g/L，100℃保温20min，排水，选择一次还原清洗；完后入温水，向主缸内加入醋酸HACP85 2g/L，50℃保温15min，排水；完后入温水，10min水洗后排水；
3)染棉：浴比为1：6，向主缸内加入水，然后向主缸内加入元明粉，元明粉浓度为10g/L，50℃保温20min，再向主缸内加入活性染料B4R 0.04％、BLUE HL 0.06％和RK3BS0.01％，以1℃/min的升温速率升温至60℃，保温30min；向主缸内加入纯碱，使纯碱的浓度为10g/L，保温60min后排液；入热水，向主缸内加入皂洗剂WOLR 1g/L，升温至98℃保温15min后排液，皂洗；入温水，一次向主缸内加入醋酸HACP85 0.5g/L、柔软剂PLS 2.5％和固色剂FARLR 3％，55℃保温21min，排液。
上述步骤中，染机泵速为90％；染经轴过程中泵速为95％；分散染料及活性染料均为均匀10min加入，纯碱为均匀30min加入；常温水为20℃，温水为50℃，热水为80℃。
对该工艺涤完后纱线的毛效，进行测试，并对通过该工艺染色后纱线的干摩擦牢度、湿摩擦牢度、皂洗牢度、日晒牢度及最终强力损失进行测试，测试结果如下：
实施例二：所染纤维为经轴状态，个重为1.05kg，密度为0.4g/cm3，经轴密度为0.49g/cm3，经轴表面无明显凹凸不平现象。具体步骤为
1)染涤：放涤棉混纺纤维入水，浴比为1：10，完后向主缸内加入去油灵2g/L，90℃保温10min，排水；入热水，保温10min，水洗后排水；入温水，完后向主缸内加入分散剂RDT1.5g/L，AB酸1.5g/L及分散染料，分散染料具体为Blue SE-RPD 0.56％，Red SE-RPD0.01％，Yellow SE-RPD 0.02％，135℃保温50min，完后降温至80℃，排水；
2)还原清洗过程为：入温水，向主缸内加入还原清洗液，其配方为保险粉4g/L、烧碱3.5g/L、净洗剂WOLR 2g/L，85℃保温20min，排水，两次还原清洗；完后入温水，向主缸内加入醋酸HACP85 2.5g/L，50℃保温15min，排水；完后入温水，10min水洗后排水；
3)染棉过程浴比为1：10，向主缸内加入水，然后向主缸内加入元明粉，元明粉浓度为60g/L，50℃保温20min，再向主缸内加入活性染料，活性染料具体为B4R 0.286％、BLUEHL 0.22％、RK3BS 0.03％，以1℃/min的升温速率升温至60℃，保温30min；向主缸内加入纯碱，纯碱的浓度为15g/L，保温60min后排液；入热水，向主缸内加入皂洗剂WOLR 1g/L，升温至98℃保温15min后排液，1次皂洗；入温水，一次向主缸内加入醋酸HACP85 0.5g/L、柔软剂PLS 3.0％和固色剂FARLR 4％，55℃保温21min，排液；
上述步骤中，染机泵速为90％；染经轴过程中泵速为95％；分散染料及活性染料均为均匀10min加入，纯碱为均匀30min加入；常温水为20℃，温水为50℃，热水为80℃。
对该工艺涤完后纱线的毛效，进行测试，并对通过该工艺染色后纱线的干摩擦牢度、湿摩擦牢度、皂洗牢度、日晒牢度及最终强力损失进行测试，测试结果如下：
实施例三：所染纤维为筒纱状态，筒纱个重为1.05kg，密度为0.4g/cm3，筒纱为规则圆柱体，密度一致。具体步骤为
1)染涤：放入涤棉混纺纤维入水，浴比为1：16，完后向主缸内加入去油灵3g/L，90℃保温10min，排水；入热水，保温10min，水洗后排水；入温水，完后向主缸内加入分散剂RDT2g/L，AB酸1.5g/L及分散染料，分散染料具体为BKSWF 2.5％、RSWF 0.1％和YSWF0.8％，135℃保温50min，完后降温至80℃，排水；
2)还原清洗：入温水，向主缸内加入还原清洗液，其配方为保险粉5g/L、烧碱4g/L、净洗剂WOLR 3g/L，85℃保温20min，排水，两次还原清洗；完后入温水，向主缸内加入醋酸HACP85 3g/L，50℃保温15min，排水；完后入温水，10min水洗后排水；
3)染棉：浴比为1：16，向主缸内加入水，然后向主缸内加入元明粉，元明粉浓度为80g/L，50℃保温20min，再向主缸内加入活性染料BKDYA6.0％、R3BF 1.4％Y3R和F 1.6％，以1℃/min的升温速率升温至60℃，保温30min；向主缸内加入纯碱，纯碱的浓度为30g/L，保温60min后排液；入热水，向主缸内加入皂洗剂WOLR 2g/L，升温至98℃保温15min后排液；入热水，向主缸内加入皂洗剂WOLR 1g/L，升温至98℃保温15min后排液，重复两次；入温水，一次向主缸内加入醋酸HACP85 0.6g/L、柔软剂PLS 3.5％和固色剂FARLR5％，55℃保温21min，排液
上述步骤中，染机泵速为90％；染经轴过程中泵速为99％；分散染料及活性染料均为均匀10min加入，纯碱为均匀30min加入；常温水为30℃，温水为52℃，热水为90℃。
对该工艺涤完后纱线的毛效，进行测试，并对通过该工艺染色后纱线的干摩擦牢度、湿摩擦牢度、皂洗牢度、日晒牢度及最终强力损失进行测试，测试结果如下：

Claims (6)

1.一种涤棉混纺纤维无前处理染色方法，其特征在于采用以下步骤为：
1)染涤：将涤棉混纺纤维入水，浴比为1：6～16，完后向主缸内加入去油灵，去油灵在主缸内的浓度为1-3g/L.，90℃保温10min，排水；再入热水，保温10min，水洗后排水；又入温水，完后向主缸内加入分散剂RDT、AB酸和分散染料，使分散剂RDT的浓度为1-2g/L，使AB酸的浓度1.5g/L，使分散染料的浓度为0-3％(o.w.f)(不包括0)，135℃保温30～50min，完后降温至80℃，排水；
2)还原清洗：入温水，向主缸内加入还原清洗液，还原清洗液中保险粉浓度3.5-5g/L、烧碱浓度3-4g/L、净洗剂WOLR浓度1-3g/L，深色品种清洗温度选择85℃，浅色品种清洗温度选择100℃，保温均为20min，排水后还原清洗；完后入温水，向主缸内加入醋酸HACP85使其浓度为2-3g/L，50℃保温15min，排水；完后入温水，10min水洗后排水；
3)染棉：浴比为1：6～16，向主缸内加入水，然后向主缸内加入元明粉，元明粉浓度在主缸内浓度为10-80g/L，50℃保温20min，再向主缸内加入活性染料浓度为为0-10％(o.w.f)(但不包括0)，以1℃/min的升温速率升温至60℃，保温30min；向主缸内加入纯碱，使纯碱浓度为10-30g/L，保温60min后排液；入热水，向主缸内加入皂洗剂WOLR，使皂洗剂WOLR浓度为1-2g/L，升温至98℃保温15min后排液，皂洗；入温水，一次向主缸内加入醋酸HACP85、柔软剂PLS和固色剂，三者的浓度分别为0.5-0.6g/L、2.5-3.5％和3-5％，55℃保温21min，排液。
2.根据权利要求1所述一种涤棉混纺纤维无前处理染色方法，其特征在于：所染纤维为筒纱状态或经轴状态，筒纱要求个重为1±0.05kg，密度为0.36-0.4g/cm3，筒纱为规则圆柱体，单批筒纱密度一致，经轴密度为0.45-0.49g/cm3，经轴表面无明显凹凸不平现象。
3.根据权利要求1所述一种涤棉混纺纤维无前处理染色方法，其特征在于：染涤过程中，分散染料为E型染料、SE型染料或者S型染料，其中E型染料包括Blue E-RPD、Red E-RPD和Yellow E-RPD的一种或几种的任意组合，SE型染料包括Blue SE-RPD、Red SE-RPD和Yellow SE-RPD等的一种或几种的任意组合，S型染料包括NavyBlue S-WF、Red S-WF和Yellow S-WF等的一种或几种的任意组合。
4.根据权利要求1所述一种涤棉混纺纤维无前处理染色方法，其特征在于：染筒纱过程中，染机泵速为90％；染经轴过程中，泵速为95-99％。
5.根据权利要求1所述一种涤棉混纺纤维无前处理染色方法，其特征在于：整个工艺过程中，分散染料及活性染料均为均匀10min加入，纯碱为均匀30min加入。
6.根据权利要求1所述一种涤棉混纺纤维无前处理染色染色方法，其特征在于：整个工艺过程中，常温水为20-30℃、温水为50℃±2℃、热水为80-90℃。
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