CN108417404A - 一种超级电容器电极材料的制备方法 - Google Patents
一种超级电容器电极材料的制备方法 Download PDFInfo
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- CN108417404A CN108417404A CN201810210915.3A CN201810210915A CN108417404A CN 108417404 A CN108417404 A CN 108417404A CN 201810210915 A CN201810210915 A CN 201810210915A CN 108417404 A CN108417404 A CN 108417404A
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- microsphere
- graphene
- molybdenum disulfide
- silica
- graphene oxide
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Links
- 239000007772 electrode material Substances 0.000 title claims abstract description 24
- 239000003990 capacitor Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 83
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims abstract description 73
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 72
- 239000004005 microsphere Substances 0.000 claims abstract description 70
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 69
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims abstract description 69
- 150000001875 compounds Chemical class 0.000 claims abstract description 36
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 33
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims abstract description 26
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 13
- 239000002131 composite material Substances 0.000 claims abstract description 12
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 11
- 238000001027 hydrothermal synthesis Methods 0.000 claims abstract description 11
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- 239000006260 foam Substances 0.000 claims abstract description 9
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 9
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical class CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims abstract description 4
- 125000002091 cationic group Chemical group 0.000 claims abstract description 4
- 239000004570 mortar (masonry) Substances 0.000 claims abstract description 4
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- 238000006243 chemical reaction Methods 0.000 claims description 15
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- UMGDCJDMYOKAJW-UHFFFAOYSA-N thiourea Chemical compound NC(N)=S UMGDCJDMYOKAJW-UHFFFAOYSA-N 0.000 claims description 8
- 230000005611 electricity Effects 0.000 claims description 7
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- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims description 6
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- 239000007864 aqueous solution Substances 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 5
- 239000011684 sodium molybdate Substances 0.000 claims description 5
- 235000015393 sodium molybdate Nutrition 0.000 claims description 5
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims description 5
- 239000011149 active material Substances 0.000 claims description 4
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- 239000013067 intermediate product Substances 0.000 claims description 4
- 238000001338 self-assembly Methods 0.000 claims description 4
- 241000790917 Dioxys <bee> Species 0.000 claims description 3
- 229910003978 SiClx Inorganic materials 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 230000009467 reduction Effects 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 2
- 239000005864 Sulphur Substances 0.000 claims description 2
- -1 alkyl dimethyl ammonium chloride Chemical compound 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims description 2
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- 239000013049 sediment Substances 0.000 claims description 2
- 238000003786 synthesis reaction Methods 0.000 claims description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims 1
- 239000004202 carbamide Substances 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 239000010703 silicon Substances 0.000 claims 1
- 239000004408 titanium dioxide Substances 0.000 claims 1
- 238000005253 cladding Methods 0.000 abstract description 2
- 230000008021 deposition Effects 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 238000001291 vacuum drying Methods 0.000 abstract description 2
- 238000000227 grinding Methods 0.000 abstract 1
- 239000000463 material Substances 0.000 description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 4
- 239000011733 molybdenum Substances 0.000 description 4
- 229910052750 molybdenum Inorganic materials 0.000 description 4
- 239000000084 colloidal system Substances 0.000 description 3
- 239000003792 electrolyte Substances 0.000 description 3
- 239000013078 crystal Substances 0.000 description 2
- 125000004122 cyclic group Chemical group 0.000 description 2
- 238000002484 cyclic voltammetry Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000000157 electrochemical-induced impedance spectroscopy Methods 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000002114 nanocomposite Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000000634 powder X-ray diffraction Methods 0.000 description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 2
- BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- NJSSICCENMLTKO-HRCBOCMUSA-N [(1r,2s,4r,5r)-3-hydroxy-4-(4-methylphenyl)sulfonyloxy-6,8-dioxabicyclo[3.2.1]octan-2-yl] 4-methylbenzenesulfonate Chemical compound C1=CC(C)=CC=C1S(=O)(=O)O[C@H]1C(O)[C@@H](OS(=O)(=O)C=2C=CC(C)=CC=2)[C@@H]2OC[C@H]1O2 NJSSICCENMLTKO-HRCBOCMUSA-N 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
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- 238000012512 characterization method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
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- 208000002925 dental caries Diseases 0.000 description 1
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- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
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- NASFKTWZWDYFER-UHFFFAOYSA-N sodium;hydrate Chemical compound O.[Na] NASFKTWZWDYFER-UHFFFAOYSA-N 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000002336 sorption--desorption measurement Methods 0.000 description 1
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Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/24—Electrodes characterised by structural features of the materials making up or comprised in the electrodes, e.g. form, surface area or porosity; characterised by the structural features of powders or particles used therefor
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/32—Carbon-based
- H01G11/36—Nanostructures, e.g. nanofibres, nanotubes or fullerenes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Nanotechnology (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
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CN201810210915.3A CN108417404B (zh) | 2016-08-26 | 2016-08-26 | 一种超级电容器电极材料的制备方法 |
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CN201810210915.3A CN108417404B (zh) | 2016-08-26 | 2016-08-26 | 一种超级电容器电极材料的制备方法 |
CN201610748848.1A CN106128784B (zh) | 2016-08-26 | 2016-08-26 | 一种二硫化钼/石墨烯空心复合微球及其制备方法 |
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Cited By (5)
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CN110061206A (zh) * | 2019-03-28 | 2019-07-26 | 华南师范大学 | 一种SiO基纳米复合材料、负极及其制备方法 |
CN112928289A (zh) * | 2021-01-26 | 2021-06-08 | 上海应用技术大学 | N杂三维泡沫石墨烯-二氧化钛微生物燃料电池电极材料及制备方法和应用 |
US20210319960A1 (en) * | 2020-04-14 | 2021-10-14 | National Chin-Yi University Of Technology | Supercapacitor electrode including silicon dioxide microsphere and fabrication method thereof |
CN113851664A (zh) * | 2021-10-28 | 2021-12-28 | 南京师范大学 | 一种制备含sp-氮掺杂石墨炔空心球电催化剂的方法及制得的材料和应用 |
CN114429865A (zh) * | 2022-01-10 | 2022-05-03 | 重庆文理学院 | 一种镍丝/三氧化二铁/二氧化锰复合纤维的制备方法 |
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CN106898759A (zh) * | 2017-04-25 | 2017-06-27 | 张廷祥 | 石墨烯锂离子电池负极极片的制备方法及石墨烯锂离子电池组 |
CN107161986A (zh) * | 2017-07-05 | 2017-09-15 | 哈尔滨理工大学 | 一种三维石墨烯空心球/ito玻璃电极的制备及应用 |
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CN108305789B (zh) * | 2017-12-29 | 2020-04-07 | 西安交通大学 | 一种用于超级电容器的聚丙烯腈/二硫化钼复合材料的制备方法 |
CN108545721A (zh) * | 2018-05-18 | 2018-09-18 | 南京师范大学 | 一种高稳态的三维石墨烯空心球的制备方法及其所得材料和应用 |
CN110600682B (zh) * | 2018-06-12 | 2022-03-01 | 天津大学 | 三明治形中空球形锂离子电池负极材料及其制备方法 |
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CN110853935A (zh) * | 2019-11-21 | 2020-02-28 | 北京协同创新研究院 | 一种硫化钼超级电容器电极及其制备方法 |
CN111106346B (zh) * | 2019-12-17 | 2022-03-11 | 合肥国轩高科动力能源有限公司 | 一种SnS2/rGO改性硫正极材料及其制备方法和应用 |
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EP2280095A2 (de) * | 2009-07-30 | 2011-02-02 | Ewald Dörken Ag | Verfahren zur elektrochemischen Beschichtung eines Werkstücks |
CN102796590A (zh) * | 2012-08-24 | 2012-11-28 | 江苏大学 | 一种管状石墨烯/MoS2纳米复合材料的制备方法 |
CN105098151A (zh) * | 2015-06-19 | 2015-11-25 | 上海交通大学 | 一种二硫化钼-碳空心球杂化材料及其制备方法 |
CN105609737A (zh) * | 2016-02-21 | 2016-05-25 | 钟玲珑 | 一种石墨烯/二氧化硅空心球/硫复合材料的制备工艺 |
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CN102142541B (zh) * | 2011-02-25 | 2014-08-13 | 浙江大学 | 一种高容量和循环性能稳定的锂离子电池电极及制备方法 |
CN102142551B (zh) * | 2011-02-25 | 2014-02-19 | 浙江大学 | 一种石墨烯纳米片/MoS2复合纳米材料及其合成方法 |
JP6164695B2 (ja) * | 2012-07-30 | 2017-07-19 | 国立大学法人信州大学 | 複合フィルムの製造方法 |
CN104934602B (zh) * | 2015-06-19 | 2017-03-08 | 上海交通大学 | 一种二硫化钼/碳复合材料及其制备方法 |
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- 2016-08-26 CN CN201810210915.3A patent/CN108417404B/zh active Active
Patent Citations (4)
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EP2280095A2 (de) * | 2009-07-30 | 2011-02-02 | Ewald Dörken Ag | Verfahren zur elektrochemischen Beschichtung eines Werkstücks |
CN102796590A (zh) * | 2012-08-24 | 2012-11-28 | 江苏大学 | 一种管状石墨烯/MoS2纳米复合材料的制备方法 |
CN105098151A (zh) * | 2015-06-19 | 2015-11-25 | 上海交通大学 | 一种二硫化钼-碳空心球杂化材料及其制备方法 |
CN105609737A (zh) * | 2016-02-21 | 2016-05-25 | 钟玲珑 | 一种石墨烯/二氧化硅空心球/硫复合材料的制备工艺 |
Cited By (8)
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---|---|---|---|---|
CN110061206A (zh) * | 2019-03-28 | 2019-07-26 | 华南师范大学 | 一种SiO基纳米复合材料、负极及其制备方法 |
CN110061206B (zh) * | 2019-03-28 | 2021-01-15 | 华南师范大学 | 一种SiO基纳米复合材料、负极及其制备方法 |
US20210319960A1 (en) * | 2020-04-14 | 2021-10-14 | National Chin-Yi University Of Technology | Supercapacitor electrode including silicon dioxide microsphere and fabrication method thereof |
US11776767B2 (en) * | 2020-04-14 | 2023-10-03 | National Chin-Yi University Of Technology | Fabrication methods for supercapacitor electrode including silicon dioxide microsphere |
CN112928289A (zh) * | 2021-01-26 | 2021-06-08 | 上海应用技术大学 | N杂三维泡沫石墨烯-二氧化钛微生物燃料电池电极材料及制备方法和应用 |
CN113851664A (zh) * | 2021-10-28 | 2021-12-28 | 南京师范大学 | 一种制备含sp-氮掺杂石墨炔空心球电催化剂的方法及制得的材料和应用 |
CN114429865A (zh) * | 2022-01-10 | 2022-05-03 | 重庆文理学院 | 一种镍丝/三氧化二铁/二氧化锰复合纤维的制备方法 |
CN114429865B (zh) * | 2022-01-10 | 2023-10-13 | 重庆文理学院 | 一种镍丝/三氧化二铁/二氧化锰复合纤维的制备方法 |
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CN106128784B (zh) | 2018-03-30 |
CN108417404B (zh) | 2019-03-15 |
CN106128784A (zh) | 2016-11-16 |
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