CN1082947C - 己二腈起始同时制备己内酰胺和1,6－己二胺的方法 - Google Patents

己二腈起始同时制备己内酰胺和1,6－己二胺的方法 Download PDF

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Publication number
CN1082947C
CN1082947C CN96199220A CN96199220A CN1082947C CN 1082947 C CN1082947 C CN 1082947C CN 96199220 A CN96199220 A CN 96199220A CN 96199220 A CN96199220 A CN 96199220A CN 1082947 C CN1082947 C CN 1082947C
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CN
China
Prior art keywords
adiponitrile
aminocapronitrile
weight
hexanediamine
tower
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Expired - Lifetime
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CN96199220A
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English (en)
Chinese (zh)
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CN1205691A (zh
Inventor
G·阿哈梅
P·巴斯勒
R·菲舍
E·福赫斯
H·卢伊肯
W·施卢尔
G·沃伊特
L·希普雷赫特
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Polyamides (AREA)
  • Micro-Organisms Or Cultivation Processes Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
CN96199220A 1995-12-22 1996-12-11 己二腈起始同时制备己内酰胺和1,6－己二胺的方法 Expired - Lifetime CN1082947C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19548289.1 1995-12-22
DE19548289A DE19548289A1 (de) 1995-12-22 1995-12-22 Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CNB011326352A Division CN1237048C (zh) 1995-12-22 1996-12-11 蒸馏分离主要含6－氨基己腈和1,6－己二胺的混合物的方法

Publications (2)

Publication Number Publication Date
CN1205691A CN1205691A (zh) 1999-01-20
CN1082947C true CN1082947C (zh) 2002-04-17

Family

ID=7781117

Family Applications (2)

Application Number Title Priority Date Filing Date
CN96199220A Expired - Lifetime CN1082947C (zh) 1995-12-22 1996-12-11 己二腈起始同时制备己内酰胺和1,6－己二胺的方法
CNB011326352A Expired - Lifetime CN1237048C (zh) 1995-12-22 1996-12-11 蒸馏分离主要含6－氨基己腈和1,6－己二胺的混合物的方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
CNB011326352A Expired - Lifetime CN1237048C (zh) 1995-12-22 1996-12-11 蒸馏分离主要含6－氨基己腈和1,6－己二胺的混合物的方法

Country Status (15)

Country Link
US (1) US6147208A (enExample)
EP (1) EP0876341B1 (enExample)
JP (1) JP2000502660A (enExample)
KR (1) KR100453675B1 (enExample)
CN (2) CN1082947C (enExample)
AU (1) AU1369697A (enExample)
BR (1) BR9612107A (enExample)
CA (1) CA2237727C (enExample)
CZ (1) CZ184398A3 (enExample)
DE (2) DE19548289A1 (enExample)
ES (1) ES2149514T3 (enExample)
MX (1) MX9803952A (enExample)
MY (1) MY114039A (enExample)
TR (1) TR199801153T2 (enExample)
WO (1) WO1997023454A1 (enExample)

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DE19704613A1 (de) 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronsäurenitril aus Mischungen, die 6-Aminocapronsäurenitril und ein Imin enthalten
DE19704620A1 (de) 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronitril aus Mischungen, die 6-Aminocapronitril und ein Imin enthalten
DE19704614A1 (de) 1997-02-07 1998-08-13 Basf Ag Verfahren zur Abtrennnung eines Imins aus einer Mischung enthaltend ein Amin und ein Imin
DE19704612A1 (de) * 1997-02-07 1998-08-13 Basf Ag Verfahren zur Gewinnung von Hexamethylendiamin aus Hexamethylendiamin enthaltenden Mischungen
DE19812427A1 (de) 1998-03-20 1999-09-23 Basf Ag Verfahren zur Abtrennung eines Azepin-Derivats aus einer Mischung enthaltend ein Amin und ein Azepin-Derivat
DE19831889A1 (de) * 1998-07-17 2000-01-27 Basf Ag Verbessertes Verfahren zur Herstellung von Hexamethylendiamin
US6346641B1 (en) 1998-07-20 2002-02-12 Basf Aktiengesellschaft Method for simultaneous production of 6-aminocapronitrile and hexamethylenediamine
DE19832529A1 (de) * 1998-07-20 2000-01-27 Basf Ag Verbessertes Verfahren zur gleichzeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin
FR2781476B1 (fr) 1998-07-22 2000-09-22 Rhone Poulenc Fibres Procede de distillation d'ammoniac contenu dans un melange comprenant du caprolactame
DE19839338A1 (de) * 1998-08-28 2000-03-02 Basf Ag Verbessertes Verfahren zur gleizeitigen Herstellung von 6-Aminocapronitril und Hexamethylendiamin
DE19923894A1 (de) * 1999-05-25 2000-11-30 Basf Ag Verfahren zur Herstellung von Polyamiden
US6627046B1 (en) * 2000-01-21 2003-09-30 E. I. Du Pont De Nemours And Company Separation of the products of polyamide ammonolysis
DE10021201A1 (de) 2000-05-03 2001-11-08 Basf Ag Verfahren zur Herstellung cyclischer Lactame
FR2809395B1 (fr) 2000-05-26 2002-07-19 Rhodia Polyamide Intermediates Procede de purification de lactames
MY127068A (en) * 2000-06-05 2006-11-30 Basf Ag Removal of ammonia from solutions including caprolactam and ammonia
DE10029187A1 (de) * 2000-06-19 2001-12-20 Basf Ag Verfahren zur Abtrennung von 6-Aminocapronitril aus Gemischen, die 6-Aminocapronitril, Adipodinitril und Hexamethylendiamin enthalten
DE10033544A1 (de) * 2000-07-11 2002-01-24 Basf Ag Kontinuierliches Verfahren zur Herstellung von Polyamiden aus Aminonitrilen
DE10033518A1 (de) * 2000-07-11 2002-01-24 Basf Ag Verfahren zur Abtrennung von Ammoniak
DE10059716A1 (de) 2000-11-30 2002-06-06 Basf Ag Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Amin und ein Nitril
JP2005509022A (ja) * 2001-11-16 2005-04-07 ビーエーエスエフ アクチェンゲゼルシャフト 水溶液からアミンを単離する方法
DE10223827A1 (de) * 2002-05-28 2003-12-11 Basf Ag Verfahren zur Reduzierung des Gehalts an einem ungesättigten Amin in einer Mischung enthaltend ein Aminonitril, ein Diamin, ein Dinitril oder deren Gemische
DE10319159A1 (de) * 2003-04-29 2004-11-18 Basf Ag Verfahren zur destillativen Gewinnung von hochreinem Triethylendiamin (TEDA)
FR2892118B1 (fr) 2005-10-18 2010-12-10 Rhodia Recherches & Tech Procede de fabrication d'hexamethylene diamine et d'aminocapronitrile.
FR2902425B1 (fr) * 2006-06-20 2008-07-18 Rhodia Recherches & Tech Procede de fabrication de diamines primaires
ATE459607T1 (de) * 2006-09-28 2010-03-15 Basf Se Verfahren zur kontinuierlichen destillativen auftrennung von gemischen enthaltend morpholin (mo), monoaminodiglykol (adg), ammoniak und wasser
US8669397B2 (en) 2009-06-13 2014-03-11 Rennovia, Inc. Production of adipic acid and derivatives from carbohydrate-containing materials
EP2440514B1 (en) 2009-06-13 2018-08-22 Archer-Daniels-Midland Company Production of adipic acid and derivatives from carbohydrate-containing materials
BRPI1010708B1 (pt) 2009-06-13 2018-04-03 Rennovia, Inc. "processos para preparar um produto de ácido adípico, e ácido adípico ou derivado do mesmo"
CN102803194B (zh) 2009-06-13 2016-01-20 莱诺维亚公司 由含碳水化合物的物质生产戊二酸和衍生物
US8669393B2 (en) * 2010-03-05 2014-03-11 Rennovia, Inc. Adipic acid compositions
WO2011109051A1 (en) 2010-03-05 2011-09-09 Rennovia, Inc. Adipic acid composition
US9770705B2 (en) 2010-06-11 2017-09-26 Rennovia Inc. Oxidation catalysts
WO2013090031A2 (en) 2011-12-14 2013-06-20 Rennovia, Inc. Water concentration reduction process
US8884036B2 (en) 2011-12-30 2014-11-11 E I Du Pont De Nemours And Company Production of hydroxymethylfurfural from levoglucosenone
US8962894B2 (en) 2011-12-30 2015-02-24 E I Du Pont De Nemours And Company Process for preparing 1, 6-hexanediol
US8865940B2 (en) 2011-12-30 2014-10-21 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
CN104024197A (zh) 2011-12-30 2014-09-03 纳幕尔杜邦公司 己二醇的制备方法
US8889912B2 (en) 2011-12-30 2014-11-18 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
BR112014015994A2 (pt) 2011-12-30 2018-05-22 Du Pont processo.
WO2013126250A1 (en) * 2012-02-23 2013-08-29 Rennovia, Inc. Production of caprolactam from adipic acid
DE102012006946A1 (de) 2012-04-10 2013-10-10 Stratley Ag Verfahren zur Herstellung von Caprolactam
US9018423B2 (en) 2012-04-27 2015-04-28 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US8846985B2 (en) 2012-04-27 2014-09-30 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US8859826B2 (en) 2012-04-27 2014-10-14 E I Du Pont De Nemours And Company Production of alpha, omega-diols
CN105658618A (zh) * 2013-09-13 2016-06-08 因温斯特技术公司 催化剂制备和氢化方法
KR20200128087A (ko) * 2018-02-27 2020-11-11 바스프 에스이 헥사메틸렌디아민의 정제 방법
CN113072463B (zh) * 2021-04-14 2023-11-28 江苏扬农化工集团有限公司 一种从己内酰胺氨化液的脱水物料中回收6-氨基己腈的方法
WO2025119889A1 (en) 2023-12-07 2025-06-12 Basf Se Process for manufacturing an aliphatic diamine
CN119241367B (zh) * 2024-10-14 2025-06-27 北京道思克能源设备有限公司 一种甲基戊二腈加氢生产甲基戊二胺及甲基哌啶的方法

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US2257814A (en) * 1940-05-02 1941-10-07 Du Pont Preparation of omega-amino nitriles
JPS4919250A (enExample) * 1972-06-16 1974-02-20
WO1992021650A1 (en) * 1991-05-31 1992-12-10 E.I. Du Pont De Nemours And Company Selective low pressure hydrogenation of a dinitrile to an aminonitrile

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US2208598A (en) * 1938-09-24 1940-07-23 Du Pont Aliphatic amino-nitriles and process of producing them
US2357484A (en) * 1941-09-12 1944-09-05 Du Pont Process for producing compounds containing an n-substituted amide group
US2301964A (en) * 1941-09-12 1942-11-17 Du Pont Method of preparing lactams
DE848654C (de) * 1950-08-19 1952-09-08 Basf Ag Verfahren zur Herstellung von partiellen Hydrierungsprodukten des Adipinsaeuredinitrils
DE954416C (de) * 1952-11-04 1956-12-20 Basf Ag Verfahren zur Herstellung von Aminonitrilen und Diaminen
US2762835A (en) * 1953-03-12 1956-09-11 Celanese Corp Preparation of amino nitriles
JPS4821958B1 (enExample) * 1969-01-28 1973-07-02
BE792649A (fr) * 1971-12-13 1973-06-12 Rhone Poulenc Sa Catalyseur a base de nickel raney au fer
EP0150295A3 (en) * 1983-12-19 1988-03-30 Allied Corporation Selective production of n-substituted amides by use of cu(o)/metallic oxides catalyst compositions
US4601859A (en) * 1984-05-04 1986-07-22 Allied Corporation Selective hydrogenation of aliphatic dinitriles to omega-aminonitriles in ammonia with supported, finely dispersed rhodium-containing catalyst
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Patent Citations (3)

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US2257814A (en) * 1940-05-02 1941-10-07 Du Pont Preparation of omega-amino nitriles
JPS4919250A (enExample) * 1972-06-16 1974-02-20
WO1992021650A1 (en) * 1991-05-31 1992-12-10 E.I. Du Pont De Nemours And Company Selective low pressure hydrogenation of a dinitrile to an aminonitrile

Also Published As

Publication number Publication date
BR9612107A (pt) 1999-02-23
WO1997023454A1 (de) 1997-07-03
EP0876341A1 (de) 1998-11-11
CA2237727A1 (en) 1997-07-03
MX9803952A (es) 1998-09-30
DE19548289A1 (de) 1997-06-26
DE59605731D1 (de) 2000-09-14
MY114039A (en) 2002-07-31
KR100453675B1 (ko) 2005-01-15
ES2149514T3 (es) 2000-11-01
JP2000502660A (ja) 2000-03-07
TR199801153T2 (xx) 1998-10-21
KR19990076645A (ko) 1999-10-15
CN1375489A (zh) 2002-10-23
CA2237727C (en) 2004-02-24
CZ184398A3 (cs) 1998-09-16
CN1237048C (zh) 2006-01-18
AU1369697A (en) 1997-07-17
CN1205691A (zh) 1999-01-20
EP0876341B1 (de) 2000-08-09
US6147208A (en) 2000-11-14

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