CN107922580A - 基于异氰酸酯和环醚聚合物网络的有机气凝胶 - Google Patents

基于异氰酸酯和环醚聚合物网络的有机气凝胶 Download PDF

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Publication number
CN107922580A
CN107922580A CN201680043940.6A CN201680043940A CN107922580A CN 107922580 A CN107922580 A CN 107922580A CN 201680043940 A CN201680043940 A CN 201680043940A CN 107922580 A CN107922580 A CN 107922580A
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CN
China
Prior art keywords
organic
gel
solvent
isocyanate
compound
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Pending
Application number
CN201680043940.6A
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English (en)
Chinese (zh)
Inventor
M·隆巴乌格特
J·加杜尼奥佩雷斯
E·托里斯卡诺
F·萨尔希
S·巴萨格纳斯图龙
A·萨卡里特
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Henkel IP and Holding GmbH
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Henkel AG and Co KGaA
Henkel IP and Holding GmbH
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Publication of CN107922580A publication Critical patent/CN107922580A/zh
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/003Polymeric products of isocyanates or isothiocyanates with epoxy compounds having no active hydrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/74Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7657Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/18Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1816Catalysts containing secondary or tertiary amines or salts thereof having carbocyclic groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/18Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1833Catalysts containing secondary or tertiary amines or salts thereof having ether, acetal, or orthoester groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/18Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1875Catalysts containing secondary or tertiary amines or salts thereof containing ammonium salts or mixtures of secondary of tertiary amines and acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805Compounds having only one group containing active hydrogen
    • C08G18/2815Monohydroxy compounds
    • C08G18/283Compounds containing ether groups, e.g. oxyalkylated monohydroxy compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C08J3/075Macromolecular gels
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00Foam properties
    • C08G2110/0091Aerogels; Xerogels
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00Thermal insulation material
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00Foams characterised by their properties
    • C08J2205/02Foams characterised by their properties the finished foam itself being a gel or a gel being temporarily formed when processing the foamable composition
    • C08J2205/026Aerogel, i.e. a supercritically dried gel
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L59/00Thermal insulation in general
    • F16L59/02Shape or form of insulating materials, with or without coverings integral with the insulating materials
    • F16L59/028Compositions for or methods of fixing a thermally insulating material
    • GPHYSICS
    • G10MUSICAL INSTRUMENTS; ACOUSTICS
    • G10KSOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
    • G10K11/00Methods or devices for transmitting, conducting or directing sound in general; Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/16Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/162Selection of materials

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Polyethers (AREA)
CN201680043940.6A 2015-07-28 2016-06-20 基于异氰酸酯和环醚聚合物网络的有机气凝胶 Pending CN107922580A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP15178682.9 2015-07-28
EP15178682.9A EP3124516A1 (en) 2015-07-28 2015-07-28 Organic aerogels based on isocyanate and cyclic ether polymer networks
PCT/EP2016/064177 WO2017016755A1 (en) 2015-07-28 2016-06-20 Organic aerogels based on isocyanate and cyclic ether polymer networks

Publications (1)

Publication Number Publication Date
CN107922580A true CN107922580A (zh) 2018-04-17

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Family Applications (1)

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CN201680043940.6A Pending CN107922580A (zh) 2015-07-28 2016-06-20 基于异氰酸酯和环醚聚合物网络的有机气凝胶

Country Status (8)

Country Link
US (1) US20180258215A1 (https=)
EP (1) EP3124516A1 (https=)
JP (1) JP2018529797A (https=)
KR (1) KR20180035804A (https=)
CN (1) CN107922580A (https=)
CA (1) CA2993712A1 (https=)
MX (1) MX2018001138A (https=)
WO (1) WO2017016755A1 (https=)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL2018589B1 (nl) 2017-03-28 2018-03-09 Turtle B V An insulated shipping container for works of art
JP2020516710A (ja) * 2017-04-06 2020-06-11 ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェンHenkel AG & Co. KGaA アミンおよび環状エーテルポリマーネットワークに基づく有機エアロゲル
EP3727671A1 (en) * 2017-12-19 2020-10-28 Henkel AG & Co. KGaA Thiol-epoxy based aerogels
CN108212032B (zh) * 2018-01-18 2020-05-08 航天特种材料及工艺技术研究所 一种形状记忆气凝胶材料及其制备方法
WO2019185207A1 (en) 2018-03-28 2019-10-03 Henkel Ag & Co. Kgaa Hydrophobic organic aerogels based on epoxy-isocyanate polymer network
WO2020173911A1 (en) 2019-02-25 2020-09-03 Henkel Ag & Co. Kgaa Composite aerogel material
US11135556B2 (en) 2019-03-04 2021-10-05 Saudi Arabian Oil Company Crosslinked polyethylene glycol polymer membranes for gas separation
CN115304739A (zh) * 2022-08-29 2022-11-08 山东北理华海复合材料有限公司 一种气凝胶聚氨酯复合保温材料的制备方法

Citations (7)

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US5342881A (en) * 1992-05-27 1994-08-30 Bayer Aktiengesellschaft Process for the standardization and stabilization of organic polyisocyanates and the stable products of this process
CN1127513A (zh) * 1993-07-22 1996-07-24 帝国化学工业公司 有机气凝胶
CN1258306A (zh) * 1997-04-01 2000-06-28 亨茨曼Ici化学品有限公司 多异氰酸酯基气凝胶
CN101815734A (zh) * 2007-10-05 2010-08-25 陶氏环球技术公司 异氰酸酯改性环氧树脂及其环氧粉末涂料组合物
CN101910230A (zh) * 2007-10-26 2010-12-08 陶氏环球技术公司 用于电层合体中的含有异氰脲酸酯的环氧树脂组合物
CN102363669A (zh) * 2010-06-21 2012-02-29 三星电子株式会社 气凝胶-泡沫体复合材料
CN103391954A (zh) * 2010-12-15 2013-11-13 拜耳知识产权有限责任公司 耐高温泡沫材料

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JPS5174095A (en) * 1974-12-25 1976-06-26 Mitsubishi Chem Ind Okisazoridon isoshianureetofuoomuno seizoho
DE68921092T2 (de) * 1988-05-13 1995-08-03 Nippon Paint Co Ltd Hitzehärtende Harzzusammensetzung und Herstellung von hitzebeständigen Überzügen und Gegenständen auf der Basis dieser Zusammensetzung.
JP2604201B2 (ja) * 1988-05-13 1997-04-30 日本ペイント株式会社 熱硬化性の反応性樹脂組成物ならびに耐熱性成形品の製造方法
US5430122A (en) * 1994-02-17 1995-07-04 E. I. Du Pont De Nemours And Company Preparation of poly(ether-urethanes) from cyclic ethers and organic isocyanates
KR20010005841A (ko) * 1997-04-01 2001-01-15 스윈넨 앤 마리 폴리이소시아네이트 기재 에어로겔
JP4107732B2 (ja) * 1998-10-20 2008-06-25 松下電器産業株式会社 有機多孔体の製造方法
US20100160472A1 (en) * 2005-11-28 2010-06-24 Aspen Aerogels, Inc. Polyolefin aerogels and composites
US8927079B2 (en) 2012-11-28 2015-01-06 Aerogel Technologies, Llc Porous polyurethane networks and methods of preparation

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5342881A (en) * 1992-05-27 1994-08-30 Bayer Aktiengesellschaft Process for the standardization and stabilization of organic polyisocyanates and the stable products of this process
CN1127513A (zh) * 1993-07-22 1996-07-24 帝国化学工业公司 有机气凝胶
CN1258306A (zh) * 1997-04-01 2000-06-28 亨茨曼Ici化学品有限公司 多异氰酸酯基气凝胶
CN101815734A (zh) * 2007-10-05 2010-08-25 陶氏环球技术公司 异氰酸酯改性环氧树脂及其环氧粉末涂料组合物
CN101910230A (zh) * 2007-10-26 2010-12-08 陶氏环球技术公司 用于电层合体中的含有异氰脲酸酯的环氧树脂组合物
CN102363669A (zh) * 2010-06-21 2012-02-29 三星电子株式会社 气凝胶-泡沫体复合材料
CN103391954A (zh) * 2010-12-15 2013-11-13 拜耳知识产权有限责任公司 耐高温泡沫材料

Also Published As

Publication number Publication date
EP3124516A1 (en) 2017-02-01
KR20180035804A (ko) 2018-04-06
CA2993712A1 (en) 2017-02-02
US20180258215A1 (en) 2018-09-13
JP2018529797A (ja) 2018-10-11
WO2017016755A1 (en) 2017-02-02
MX2018001138A (es) 2018-04-20

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Application publication date: 20180417