CA2993712A1 - Organic aerogels based on isocyanate and cyclic ether polymer networks - Google Patents

Organic aerogels based on isocyanate and cyclic ether polymer networks Download PDF

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Publication number
CA2993712A1
CA2993712A1 CA2993712A CA2993712A CA2993712A1 CA 2993712 A1 CA2993712 A1 CA 2993712A1 CA 2993712 A CA2993712 A CA 2993712A CA 2993712 A CA2993712 A CA 2993712A CA 2993712 A1 CA2993712 A1 CA 2993712A1
Authority
CA
Canada
Prior art keywords
organic aerogel
gel
solvent
compound
isocyanate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2993712A
Other languages
English (en)
French (fr)
Inventor
Miquel LOMBA HUGUET
Joan Garduno Perez
Elisabet TORRES CANO
Fouad Salhi
Sergi BASSAGANAS TURON
Asta SAKALYTE
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Henkel IP and Holding GmbH
Original Assignee
Henkel AG and Co KGaA
Henkel IP and Holding GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henkel AG and Co KGaA, Henkel IP and Holding GmbH filed Critical Henkel AG and Co KGaA
Publication of CA2993712A1 publication Critical patent/CA2993712A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/003Polymeric products of isocyanates or isothiocyanates with epoxy compounds having no active hydrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/18Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1816Catalysts containing secondary or tertiary amines or salts thereof having carbocyclic groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/18Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1833Catalysts containing secondary or tertiary amines or salts thereof having ether, acetal, or orthoester groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08Processes
    • C08G18/16Catalysts
    • C08G18/18Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/1875Catalysts containing secondary or tertiary amines or salts thereof containing ammonium salts or mixtures of secondary of tertiary amines and acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805Compounds having only one group containing active hydrogen
    • C08G18/2815Monohydroxy compounds
    • C08G18/283Compounds containing ether groups, e.g. oxyalkylated monohydroxy compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72Polyisocyanates or polyisothiocyanates
    • C08G18/74Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7657Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C08J3/075Macromolecular gels
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00Foam properties
    • C08G2110/0091Aerogels; Xerogels
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00Thermal insulation material
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00Foams characterised by their properties
    • C08J2205/02Foams characterised by their properties the finished foam itself being a gel or a gel being temporarily formed when processing the foamable composition
    • C08J2205/026Aerogel, i.e. a supercritically dried gel
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L59/00Thermal insulation in general
    • F16L59/02Shape or form of insulating materials, with or without coverings integral with the insulating materials
    • F16L59/028Compositions for or methods of fixing a thermally insulating material
    • GPHYSICS
    • G10MUSICAL INSTRUMENTS; ACOUSTICS
    • G10KSOUND-PRODUCING DEVICES; METHODS OR DEVICES FOR PROTECTING AGAINST, OR FOR DAMPING, NOISE OR OTHER ACOUSTIC WAVES IN GENERAL; ACOUSTICS NOT OTHERWISE PROVIDED FOR
    • G10K11/00Methods or devices for transmitting, conducting or directing sound in general; Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/16Methods or devices for protecting against, or for damping, noise or other acoustic waves in general
    • G10K11/162Selection of materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Polyethers (AREA)
CA2993712A 2015-07-28 2016-06-20 Organic aerogels based on isocyanate and cyclic ether polymer networks Abandoned CA2993712A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP15178682.9 2015-07-28
EP15178682.9A EP3124516A1 (en) 2015-07-28 2015-07-28 Organic aerogels based on isocyanate and cyclic ether polymer networks
PCT/EP2016/064177 WO2017016755A1 (en) 2015-07-28 2016-06-20 Organic aerogels based on isocyanate and cyclic ether polymer networks

Publications (1)

Publication Number Publication Date
CA2993712A1 true CA2993712A1 (en) 2017-02-02

Family

ID=54035113

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2993712A Abandoned CA2993712A1 (en) 2015-07-28 2016-06-20 Organic aerogels based on isocyanate and cyclic ether polymer networks

Country Status (8)

Country Link
US (1) US20180258215A1 (https=)
EP (1) EP3124516A1 (https=)
JP (1) JP2018529797A (https=)
KR (1) KR20180035804A (https=)
CN (1) CN107922580A (https=)
CA (1) CA2993712A1 (https=)
MX (1) MX2018001138A (https=)
WO (1) WO2017016755A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110494478A (zh) * 2017-04-06 2019-11-22 汉高股份有限及两合公司 基于胺和环醚聚合物网络的有机气凝胶

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL2018589B1 (nl) 2017-03-28 2018-03-09 Turtle B V An insulated shipping container for works of art
EP3727671A1 (en) * 2017-12-19 2020-10-28 Henkel AG & Co. KGaA Thiol-epoxy based aerogels
CN108212032B (zh) * 2018-01-18 2020-05-08 航天特种材料及工艺技术研究所 一种形状记忆气凝胶材料及其制备方法
WO2019185207A1 (en) 2018-03-28 2019-10-03 Henkel Ag & Co. Kgaa Hydrophobic organic aerogels based on epoxy-isocyanate polymer network
WO2020173911A1 (en) 2019-02-25 2020-09-03 Henkel Ag & Co. Kgaa Composite aerogel material
US11135556B2 (en) 2019-03-04 2021-10-05 Saudi Arabian Oil Company Crosslinked polyethylene glycol polymer membranes for gas separation
CN115304739A (zh) * 2022-08-29 2022-11-08 山东北理华海复合材料有限公司 一种气凝胶聚氨酯复合保温材料的制备方法

Family Cites Families (15)

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Publication number Priority date Publication date Assignee Title
JPS5174095A (en) * 1974-12-25 1976-06-26 Mitsubishi Chem Ind Okisazoridon isoshianureetofuoomuno seizoho
DE68921092T2 (de) * 1988-05-13 1995-08-03 Nippon Paint Co Ltd Hitzehärtende Harzzusammensetzung und Herstellung von hitzebeständigen Überzügen und Gegenständen auf der Basis dieser Zusammensetzung.
JP2604201B2 (ja) * 1988-05-13 1997-04-30 日本ペイント株式会社 熱硬化性の反応性樹脂組成物ならびに耐熱性成形品の製造方法
DE4217525A1 (de) * 1992-05-27 1993-12-02 Bayer Ag Verfahren zur Standardisierung und Stabilisierung von organischen Polyisocyanaten und ihre Verwendung
WO1995003358A1 (en) * 1993-07-22 1995-02-02 Imperial Chemical Industries Plc Organic aerogels
US5430122A (en) * 1994-02-17 1995-07-04 E. I. Du Pont De Nemours And Company Preparation of poly(ether-urethanes) from cyclic ethers and organic isocyanates
KR20010005841A (ko) * 1997-04-01 2001-01-15 스윈넨 앤 마리 폴리이소시아네이트 기재 에어로겔
JP2001516393A (ja) * 1997-04-01 2001-09-25 ハンツマン・アイシーアイ・ケミカルズ・エルエルシー ポリイソシアネートベースのエーロゲル
JP4107732B2 (ja) * 1998-10-20 2008-06-25 松下電器産業株式会社 有機多孔体の製造方法
US20100160472A1 (en) * 2005-11-28 2010-06-24 Aspen Aerogels, Inc. Polyolefin aerogels and composites
US20100237292A1 (en) * 2007-10-05 2010-09-23 Joseph Gan Isocyanate modified epoxy resin and epoxy powder coating composition thereof
US20100240816A1 (en) * 2007-10-26 2010-09-23 Dow Global Technologies Inc. Epoxy resin composition containing isocyanurates for use in electrical laminates
KR20110139152A (ko) * 2010-06-21 2011-12-28 삼성전자주식회사 에어로젤-폼 복합체
EP2651997B1 (de) * 2010-12-15 2015-08-12 Bayer Intellectual Property GmbH Hochtemperaturbeständige schaumstoffe
US8927079B2 (en) 2012-11-28 2015-01-06 Aerogel Technologies, Llc Porous polyurethane networks and methods of preparation

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110494478A (zh) * 2017-04-06 2019-11-22 汉高股份有限及两合公司 基于胺和环醚聚合物网络的有机气凝胶

Also Published As

Publication number Publication date
EP3124516A1 (en) 2017-02-01
KR20180035804A (ko) 2018-04-06
US20180258215A1 (en) 2018-09-13
CN107922580A (zh) 2018-04-17
JP2018529797A (ja) 2018-10-11
WO2017016755A1 (en) 2017-02-02
MX2018001138A (es) 2018-04-20

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Legal Events

Date Code Title Description
FZDE Discontinued

Effective date: 20220913