CN107693433A - A kind of moisturizing elite and preparation method thereof - Google Patents
A kind of moisturizing elite and preparation method thereof Download PDFInfo
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- CN107693433A CN107693433A CN201711113266.7A CN201711113266A CN107693433A CN 107693433 A CN107693433 A CN 107693433A CN 201711113266 A CN201711113266 A CN 201711113266A CN 107693433 A CN107693433 A CN 107693433A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of moisturizing elite and preparation method thereof, comprising：0.5 15 parts of polyalcohol NMF, 0.01 5 parts of thickener, 1 16 parts of humectants and emollientses, 0.01 10 parts of oily gel composition, 2 30 parts of functional component, 0.001 1 parts of essence and flavoring agent, 0.01 0.5 parts of preservative, surplus is deionized water.The present invention uses non-traditional emulsion process, emulsifying elite is can be prepared by by simply adding oily gel composition, the salubrious use feeling of skin sense is good, oily gel composition can also solubilized essence and flavoring agent simultaneously, so as to avoid use of the solubilizer in formula, final products will not bear without any harmful additive to skin tape.Its preparation technology is simple, and without high temperature and high pressure homogeneous, energy consumption is low, and financial cost is low, green safe, has good prospects for commercial application.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of moisturizing elite and preparation method thereof.
Background technology
With the improvement of living standards, nursing consciousness of the people for skin also gradually steps up.Pass through major survey institute
Analysis to Cosmetic Market, replenishing water and preserving moisture, skin are releived the primary demand for being still consumer to cosmetics.And elite is each
One of leading category of big skin care brand, while requirement of the consumer to elite also more and more higher, therefore develop good use feeling
Having the elite of effect concurrently turns into the emphasis of engineer.
Elite class product is mainly prepared using conventional emulsification methods at present, but more due to needing to add in preparation process
Emulsifying agent, emulsifying agent belong to surfactant and different degrees of stimulation are had to skin.Therefore, Cosmetic Market is for developing nothing
The skin-protection product of emulsifying agent or low emulsifying agent has put on schedule.Also, conventional emulsification methods technics comparing complexity is, it is necessary to high pressure
Homogeneous, energy consumption are higher.
The content of the invention
In view of this, primary and foremost purpose of the invention is to overcome above-mentioned the shortcomings of the prior art, there is provided a kind of moisturizing
Elite, the salubrious use feeling of skin sense of the moisturizing elite is good, to skin without any burden.
Another object of the present invention is to provide the preparation method of above-mentioned moisturizing elite, the technique is simple, without high temperature and
High-pressure homogeneous, energy consumption is low.
The technical solution adopted by the present invention is as follows：
A kind of moisturizing elite, is counted in parts by weight, includes following component：
Polyalcohol NMF 0.5-15 parts, thickener 0.01-5 parts, humectants and emollientses 1-16 parts, oily gel composition 0.01-10
Part, functional component 2-30 parts, essence and flavoring agent 0.001-1 parts, preservative 0.01-0.5 parts, surplus is deionized water.
As further preferred technical scheme of the invention, described moisturizing elite is counted in parts by weight, includes such as the following group
Point：
Polyalcohol NMF 3-8 parts, thickener 1-2 parts, humectants and emollientses 5-10 parts, oily gel composition 0.5-3 parts, effect into
Divide 10-20 parts, essence and flavoring agent 0.01-0.3 parts, preservative 0.05-0.3 parts, surplus is deionized water.
Wherein, the oily gel composition, by weight percentage, following component is included：Nonionic surfactant 2-
30%；Grease 20-60%；Polyalcohol 20-40%；Water surplus.Wherein, described nonionic surfactant is the table of polyol type
Face activating agent, preferably PEG-60 rilanit specials, PEG-20 iso stearic acid of glycerine ester, Natrulon H-10 isostearate or poly-
One or more of mixing in the dioleate of glycerine -10；The polyalcohol be glycerine, 1,3 butylene glycol, 1,2- propane diols, 1,
One or more of mixing, preferably glycerine or diglycerol in ammediol or diglycerol；The grease is artificial oil, mineral
Oil, silicone oil, hydrocarbon ils or plant origin oil in one or more of mixing, preferably nonpolar, density is close to 1 grease, example
Such as glycerine three（Thylhexoic acid）One or more of mixing in ester or caprylic/capric triglyceride.
Its particle diameter of the oily gel composition is less than 200nm, viscosity 1000mpas- through the test of Malvern particle instrument
500000mpas, preferable particle size 100-150nm, preferred viscosities 150000mpas-250000mpas.
The preparation method of the oily gel composition, comprises the following steps：
（1）By nonionic surfactant, polyalcohol, water, low-grade fever dissolving is well mixed in proportion, is designated as A, wherein nonionic table
Face activating agent：Polyalcohol：Water=1 ~ 2:1~2：（0~4）, the low-grade fever is the temperature not higher than 45 °C；
（2）Under A stirring conditions, grease is slowly added into, is designated as B；
（3）Under B stirring conditions, it will be slowly added into after remaining polynary alcohol and water premix, stir evenly and produce.
The polyalcohol NMF is glycerine, 1,3 butylene glycol, 1,2- propane diols, 1,3- propane diols, diglycerol, double third sweet
One or more of mixing in alcohol, 1,2- hexylene glycols or 1,2- pentanediols.
The thickener is ammonium acryloyldime-thyltaurate/VP copolymers, acrylic acid（Ester）Class/C10-30 alkanols third
Olefin(e) acid ester cross-linked polymer, hydroxyethyl cellulose, carbomer, polyacrylic acid, Scleroglucan, Sodium Polyacrylate graft starch, third
Olefin(e) acid（Ester）One or more of mixing in analog copolymer sodium, PAA/sodium acryloyldimethyl taurate copolymers.
The humectants and emollientses are polyethylene glycol -32, PEG-8, glycine betaine, trehalose, double-PEG-18 methyl ethers
Dimethylsilane, saualane, water-soluble olive oil, entire leaf Queensland nut seed oil tocopherol, Butyrospermum parkii fruit fat, olea europaea fruit
Shell oil, phytosterol Tower rape oil glyceride type, white pond flower seed oil, glycerine three（Thylhexoic acid）Ester or cetanol ethyl hexyl
One or more of mixing in acid esters, preferably polyethylene glycol -32, PEG-8, trehalose or double-PEG-18 methyl
One or more of mixing in ether dimethylsilane.
Functional component can be properly added according to the actual requirements, the amount of addition is the conventional amount used in the industry, described effect
It is at least a kind of in class, whitening class, moisturizing class, the anti-ageing class of smoothing wrinkle or equilibrium oil lipid functional component that composition is that antiallergic is releived.
Antiallergic class functional component of releiving includes such as dipotassium glycyrrhizinate, bisabolol, purslane extract, allantoin, dish
At least one of artichoke leaf extract, tuckahoe extracts, hamamelis extract, camomile extract but it is not limited to listed kind
Class.
Whitening class functional component include such as ursin, niacinamide, fructus crataegi cuneatae berry extract, wineberry berry extract,
At least one of Echinacea angustifolia extract but it is not limited to listed species.
Moisturizing class functional component includes such as hyaluronic acid, dried tremella extract, glucan（Such as glucan MC-Glucan NP
（EF））At least one of but be not limited to listed species.
The anti-ageing class functional component of smoothing wrinkle include such as adenosine, sugar Thallus Laminariae (Thallus Eckloniae) extract, palmitoyl oligopeptide, Matrixyl -4,
At least one of Argireline but it is not limited to listed species.
Equilibrium oil lipid functional component includes such as at least one of tartaric acid, ZnG, Folium Aloe extract but not
It is limited to listed species.
The preparation method of the above-mentioned moisturizing elite of the present invention, comprises the following steps：
(1), polyalcohol NMF, thickener, humectants and emollientses are added in deionized water, are heated to 50-60 °C of stirring or low
Fast homogeneous to solid material all it is scattered it is homogeneous after start to cool；
(2), oily gel composition, essence and flavoring agent are well mixed standby；
(3) 45 °C or so, are cooled to, sequentially adds functional component and preservative；
(4), mixed system obtained by step (3) is stirred continuously, step（2）Gained mixed system is slowly added into, then with suitable
Container is rinsed clean and washing lotion is poured into mixed system obtained by step (3) by amount deionized water；
(5), mixed system obtained by step (4) is stirred, stops stirring；
(6), mixture obtained by step (5) is sampled, micro- inspection is qualified, goes out sample.
The present invention compared with prior art, has the advantages that：
（1）The present invention uses non-traditional emulsion process, and emulsifying elite, skin sense are can be prepared by by simply adding oily gel composition
Salubrious use feeling is good, at the same oily gel composition can also solubilized essence and flavoring agent, so as to avoid use of the solubilizer in formula；
（2）Gained moisturizing elite of the invention is good using skin sense, and final products will not come without any harmful additive to skin tape
Burden；
（3）The preparation technology of the present invention is simple, and without high temperature and high pressure homogeneous, energy consumption is low, and financial cost is low, green safe, tool
There is good prospects for commercial application.
Brief description of the drawings
Fig. 1 is subject's self-test assessment design sketch.
Embodiment
The present invention is further illustrated below by embodiment, but embodiments of the present invention are not by following realities
Apply the limitation of example.
Raw material used in the embodiment of the present invention and comparative example derives from purchased in market.
Oily gel composition particle diameter method of testing:Using Malvern laser particle analyzer Mastersizer 3000, oleogel
Composition is diluted to 2% solution with deionized water in advance, then is with the measure of Malvern laser particle analyzer Mastersizer 3000
Can.
Oily gel composition viscosity determining procedure：Tested using model DV-C digital displays viscosimeter, select suitable rotor
And rotating speed（4#1r）Afterwards, directly rotor is inserted in the oily gel composition without any processing and determined, treat that numerical value is basicly stable
Reading.
The preparation of oily gel composition：
It is formulated by table 1 Suo Shi, nonionic surfactant, polyalcohol, water is well mixed in 40 °C of dissolvings in proportion, A is designated as,
Wherein nonionic surfactant：Polyalcohol：Water=1-2:1-2：（0~4）；Under A stirring conditions, grease is slowly added into, remembered
For B；Under B stirring conditions, it will be slowly added into after remaining polynary alcohol and water premix, stir evenly and produce oily gel composition, test
Results of property is as shown in table 1.
Wherein, in embodiment 1, nonionic surfactant：Polyalcohol：Water=1:1：0.05；
In embodiment 2, nonionic surfactant：Polyalcohol：Water=1:1：0.1；
In embodiment 3, nonionic surfactant：Polyalcohol：Water=1:1：0；
In embodiment 4, nonionic surfactant：Polyalcohol：Water=1:1：0.15；
In embodiment 5, nonionic surfactant：Polyalcohol：Water=1:1：0；
The oily gel composition of table 1 matches somebody with somebody when results of property (percentage by weight)
The preparation of moisturizing elite：
Embodiment 1-3：
(1), as shown in table 2, load weighted polyalcohol NMF, thickener, humectants and emollientses are added in deionized water, heating
To 50-60 °C of stirring or low speed homogeneous to solid material all it is scattered it is homogeneous after start to cool；
(2), the oily gel composition weighed up, essence and flavoring agent are well mixed standby；
(3) 45 °C or so, are cooled to, sequentially adds functional component and preservative；
(4), mixed system obtained by step (3) is stirred continuously, step（2）Gained mixed system is slowly added into, then with suitable
Container is rinsed clean and washing lotion is poured into mixed system obtained by step (3) by amount deionized water；
(5), mixed system obtained by step (4) is stirred, stops stirring；
(6), mixture obtained by step (5) is sampled, micro- inspection is qualified, goes out sample.
The proportioning of the moisturizing elite of table 2（Parts by weight）
It is supplied to volunteer to be tried out the moisturizing elite of the embodiment of the present invention；Volunteer is to select 15 people at random, unlimited man
Female, common skin, application method are that full face use elite after face cleaning, and questionnaire is filled in after trying out.
It is subject's self-test assessment result below, data processed result is shown in Table 3：
The subject's self-test assessment result of table 3
Note：Metrics evaluation best result 5, numerical value is bigger to represent that Consumer acceptance is more high more likes, or represents that mildness is better.
Subject's self-test assessment design sketch is as shown in figure 1, it can be seen from subject feedback and above-mentioned test result, the present invention
The moisturizing elite being prepared is good using skin sense, salubrious moisturizing.
Claims (9)
1. a kind of moisturizing elite, it is characterised in that count in parts by weight, include following component：
Polyalcohol NMF 0.5-15 parts, thickener 0.01-5 parts, humectants and emollientses 1-16 parts, oily gel composition 0.01-10
Part, functional component 2-30 parts, essence and flavoring agent 0.001-1 parts, preservative 0.01-0.5 parts, surplus is deionized water.
2. moisturizing elite according to claim 1, it is characterised in that count in parts by weight, include following component：
Polyalcohol NMF 3-8 parts, thickener 1-2 parts, humectants and emollientses 5-10 parts, oily gel composition 0.5-3 parts, effect into
Divide 10-20 parts, essence and flavoring agent 0.01-0.3 parts, preservative 0.05-0.3 parts, surplus is deionized water.
3. moisturizing elite according to claim 1 or 2, it is characterised in that the oily gel composition, by weight percentage
Meter, includes following component：
Nonionic surfactant 2-30%；Grease 20-60%；Polyalcohol 20-40%；Water surplus.
4. moisturizing elite according to claim 3, it is characterised in that described nonionic surfactant is polyol type
Surfactant, preferably PEG-60 rilanit specials, PEG-20 iso stearic acid of glycerine ester, Natrulon H-10 isostearate
Or one or more of mixing in Natrulon H-10 dioleate；The polyalcohol is glycerine, 1,3 butylene glycol, 1,2- the third two
One or more of mixing, preferably glycerine or diglycerol in alcohol, 1,3-PD or diglycerol；The grease be artificial oil,
Mineral oil, silicone oil, hydrocarbon ils or plant origin oil in one or more of mixing, preferably glycerine three（Thylhexoic acid）Ester is pungent
One or more of mixing in acid/Triglyceride DDD.
5. moisturizing elite according to claim 3, it is characterised in that its particle diameter of the oily gel composition is through Malvern grain
Footpath instrument test is less than 200nm, viscosity 1000mpas-500000mpas, preferable particle size 100-150nm, and preferred viscosities are
150000mpas-250000mpas。
6. moisturizing elite according to claim 3, it is characterised in that the preparation method of the oily gel composition, including
Following steps：
（1）By nonionic surfactant, polyalcohol, water, low-grade fever dissolving is well mixed in proportion, is designated as A, wherein nonionic table
Face activating agent：Polyalcohol：Water=1 ~ 2:1~2：（0~4）, the low-grade fever is the temperature not higher than 45 °C；
（2）Under A stirring conditions, grease is slowly added into, is designated as B；
（3）Under B stirring conditions, it will be slowly added into after remaining polynary alcohol and water premix, stir evenly and produce.
7. moisturizing elite according to claim 1 or 2, it is characterised in that the polyalcohol NMF is glycerine, 1,3- fourths
Glycol, 1,2- propane diols, 1,3- propane diols, diglycerol, dipropylene glycol, 1,2- hexylene glycols or one kind or several in 1,2- pentanediols
The mixing of kind；The thickener is ammonium acryloyldime-thyltaurate/VP copolymers, acrylic acid（Ester）Class/C10-30 alkanols
Acrylate crosspolymers, hydroxyethyl cellulose, carbomer, polyacrylic acid, Scleroglucan, Sodium Polyacrylate graft starch,
Acrylic acid（Ester）It is one or more of mixed in analog copolymer sodium or PAA/sodium acryloyldimethyl taurate copolymers
Close；The humectants and emollientses are polyethylene glycol -32, PEG-8, glycine betaine, trehalose, double-PEG-18 methyl ethers diformazans
Base silane, saualane, water-soluble olive oil, entire leaf Queensland nut seed oil tocopherol, Butyrospermum parkii fruit fat, olive shell
Oil, phytosterol Tower rape oil glyceride type, white pond flower seed oil, glycerine three（Thylhexoic acid）Ester or cetanol thylhexoic acid
One or more of mixing in ester, preferably polyethylene glycol -32, PEG-8, trehalose or double-PEG-18 methyl ethers
One or more of mixing in dimethylsilane.
8. moisturizing elite according to claim 1 or 2, it is characterised in that the functional component is that antiallergic is releived class, whitening
It is at least a kind of in class, moisturizing class, the anti-ageing class of smoothing wrinkle or equilibrium oil lipid functional component；Antiallergic class functional component of releiving is
Dipotassium glycyrrhizinate, bisabolol, purslane extract, allantoin, cynara scolymus leaf extract, tuckahoe extracts, hamamelis carry
Take at least one of thing or camomile extract；The whitening class functional component is ursin, niacinamide, the extraction of fructus crataegi cuneatae fruit
At least one of thing, wineberry berry extract or Echinacea angustifolia extract；The moisturizing class functional component be hyaluronic acid,
At least one of dried tremella extract or glucan；The anti-ageing class functional component of smoothing wrinkle is adenosine, sugar Thallus Laminariae (Thallus Eckloniae) extract, palm
At least one of acyl oligopeptides, Matrixyl -4 or Argireline；The equilibrium oil lipid functional component is tartaric acid, Portugal
At least one of saccharic acid zinc or Folium Aloe extract.
9. the preparation method of the moisturizing elite according to claim any one of 1-8, it is characterised in that comprise the following steps：
(1), polyalcohol NMF, thickener, humectants and emollientses are added in deionized water, are heated to 50-60 °C of stirring or low
Fast homogeneous to solid material all it is scattered it is homogeneous after start to cool；
(2), oily gel composition, essence and flavoring agent are well mixed standby；
(3) 45 °C or so, are cooled to, sequentially adds functional component and preservative；
(4), mixed system obtained by step (3) is stirred continuously, step（2）Gained mixed system is slowly added into, then with suitable
Container is rinsed clean and washing lotion is poured into mixed system obtained by step (3) by amount deionized water；
(5), mixed system obtained by step (4) is stirred, stops stirring；
(6), mixture obtained by step (5) is sampled, micro- inspection is qualified, goes out sample.
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| CN108272693A (en) * | 2018-04-11 | 2018-07-13 | 广州赛莱拉干细胞科技股份有限公司 | Whitening spot-eliminating composition and preparation method thereof |
| CN109464302A (en) * | 2018-12-29 | 2019-03-15 | 上海家化联合股份有限公司 | Composition containing dipotassium glycyrrhizinate |
| CN109464314A (en) * | 2018-11-02 | 2019-03-15 | 蝶柔化妆品(浙江)有限公司 | Gold bullet moistens Face-protecting mask and preparation method thereof |
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| CN114366696A (en) * | 2022-01-07 | 2022-04-19 | 广州妮趣化妆品有限公司 | A nanometer emulsion of fructus Bruceae oil with antiaging effect, and its preparation method and application |
| CN114392198A (en) * | 2022-01-14 | 2022-04-26 | 广州暨大美塑生物科技有限公司 | Cosmetic composition and preparation method thereof |
| CN114642607A (en) * | 2021-04-27 | 2022-06-21 | 上海康美国际生化有限公司 | Moisturizing, moisturizing and long-acting skin care double-bottle essence and preparation and use methods thereof |
| CN116139040A (en) * | 2022-12-26 | 2023-05-23 | 科乐美(广州)生物科技有限公司 | Moisturizing composition, moisturizing essence and preparation method of moisturizing essence |
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| CN111012699A (en) * | 2020-01-08 | 2020-04-17 | 澳宝化妆品（惠州）有限公司 | Antioxidant oil-controlling emulsion containing fucoidan-kelp extract |
| CN111297712B (en) * | 2020-03-13 | 2022-09-06 | 上海新高姿化妆品有限公司 | Face cream composition and preparation method thereof |
| CN111297712A (en) * | 2020-03-13 | 2020-06-19 | 上海新高姿化妆品有限公司 | Face cream composition and preparation method thereof |
| CN111407714A (en) * | 2020-04-15 | 2020-07-14 | 东阿阿胶股份有限公司 | Anti-allergy, relieving and moisturizing lotion and preparation method thereof |
| CN111671670A (en) * | 2020-08-06 | 2020-09-18 | 江西沁华蔓医药科技有限公司 | Moisturizing essence toner |
| CN114642607A (en) * | 2021-04-27 | 2022-06-21 | 上海康美国际生化有限公司 | Moisturizing, moisturizing and long-acting skin care double-bottle essence and preparation and use methods thereof |
| CN113304094A (en) * | 2021-06-15 | 2021-08-27 | 罗上兵 | Freckle-removing and whitening essence and preparation method thereof |
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| CN116139040A (en) * | 2022-12-26 | 2023-05-23 | 科乐美(广州)生物科技有限公司 | Moisturizing composition, moisturizing essence and preparation method of moisturizing essence |
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