CN114642607A - Moisturizing, moisturizing and long-acting skin care double-bottle essence and preparation and use methods thereof - Google Patents

Moisturizing, moisturizing and long-acting skin care double-bottle essence and preparation and use methods thereof Download PDF

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Publication number
CN114642607A
CN114642607A CN202110460644.9A CN202110460644A CN114642607A CN 114642607 A CN114642607 A CN 114642607A CN 202110460644 A CN202110460644 A CN 202110460644A CN 114642607 A CN114642607 A CN 114642607A
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moisturizing
long
skin care
parts
essence
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潘璐
张若飞
童俊
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Shanghai Kangmei International Biochemical Co ltd
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Shanghai Kangmei International Biochemical Co ltd
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Priority to CN202110460644.9A priority Critical patent/CN114642607A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/88Two- or multipart kits
    • A61K2800/882Mixing prior to application

Abstract

The invention discloses a moisturizing, moisturizing and long-acting skin care essence in two bottles, which comprises two parts of oleogel and hydrogel; the oleogel stock contained the following ingredients: polypeptide, squalane, glycerol, thickener, emollient, vegetable oil, plant extract; the hydrogel raw material comprises the following components: water, dihydric alcohol, a humectant, a thickening agent, alkaline amino acid, a chelating agent, a skin conditioning agent, a protein hydrolysate composition and a surfactant. According to the invention, the skin care essence of the oil phase and the water phase is stored in the double bottles, so that the phenomena of layering, precipitation and inactivation caused by long-term storage of effective active ingredients in the oil in the water phase are effectively avoided; and the double-bottle essence composition prepared by selecting the specific raw materials has excellent long-acting moisturizing and moisture-keeping effects, and can ensure the beneficial effects and physicochemical properties of the product.

Description

Moisturizing, moisturizing and long-acting skin care double-bottle essence and preparation and use methods thereof
Technical Field
The invention relates to the field of skin care products, in particular to a double-bottle essence capable of moisturizing, preserving moisture and protecting skin for a long time, and a preparation method and a use method thereof.
Background
The skin is the first line of body defense for protecting people from external invasion, and the strength of the skin protection usually represents the contact strength of human body systems with external bacteria and pathogens. Therefore, the skin care product industry has been receiving more and more attention in recent years, has developed more and more rapidly, and has gradually developed into one of the fastest growing industries in the 21 st century.
The skin care product can perform certain guarantee, repair and maintenance functions on the skin of people. With the recent improvement of chemical synthesis and chemical technology, more and more synthetic chemicals or plant extracts are applied to skin care products, so as to improve the effects of moisturizing, whitening and the like of the skin care products. However, with the emergence of safety and quality events such as some public skin care products and cosmetics, people tend to pay more and more attention to the affinity and quality effects of skin care products. In the existing single skin care product, the components are more, and the phenomena of incompatibility, precipitation and even failure are easy to occur among the components, which greatly influences the functional effect of the skin care product, especially the phenomena that some skin care active ingredients are easy to fail in water, which not only influences the skin care effect, but also increases the cost of manufacturers and consumers, and causes unnecessary economic loss.
Therefore, a moisturizing, moisture-preserving and long-acting skin care essence composition is very meaningful work.
Disclosure of Invention
In order to solve the above problems, the present invention provides, in a first aspect, a moisturizing, long-lasting skin care essence comprising an oleogel and a hydrogel.
As a preferred scheme, the raw materials of the oil gel comprise the following parts by weight: 2-6 parts of polypeptide, 12-16 parts of squalane, 25-35 parts of glycerol, 0.01-0.03 part of thickening agent, 44-58 parts of emollient, 0.5-1.5 parts of vegetable oil and 0.05-0.2 part of plant extract.
As a preferable scheme, the raw materials of the hydrogel comprise the following parts by weight: 80-100 parts of water, 0.3-1.6 parts of dihydric alcohol, 0.2-2 parts of humectant, 0.1-1 part of thickener, 0.5-2 parts of basic amino acid, 0.2-0.6 part of chelating agent, 1-3 parts of skin conditioner, 0.1-1 part of hydrolyzed protein composition and 1-3 parts of surfactant.
As a preferable scheme, the mass ratio of the oil gel to the hydrogel is 1: 1 to 2.
In a preferred embodiment, the thickener is at least one of carbomer, xanthan gum, cetyl alcohol, stearyl alcohol and whale wax polyoxyethylene ether.
In a preferred embodiment, the polypeptide is at least one of palmitoyl tripeptide, pentapeptide-3, dipeptide-2, acetyl tetrapeptide, carnosine and surfactin sodium.
Preferably, the vegetable oil is at least one of olive oil, jojoba seed oil, shea butter, tea seed oil, and sweet almond oil.
In a preferred embodiment, the basic amino acid is at least one of arginine, histidine and lysine.
The second aspect of the invention provides a preparation method of the double-bottle essence for moisturizing, moisturizing and long-acting skin care, which comprises the following steps: (1) preparing oil gel: mixing and stirring squalane, glycerol and a thickening agent for 20-40 minutes until the mixture is uniformly stirred, then adding a small amount of an emollient, stirring vegetable oil for 20-40 minutes, uniformly mixing, then adding polypeptide and a plant extract, and stirring for 20-40 minutes; (2) preparing hydrogel: heating water, dihydric alcohol, a humectant, a thickening agent, alkaline amino acid, a chelating agent and a surfactant to 50-70 ℃, stirring for dissolving, cooling to 40 ℃, adding a skin conditioner and a hydrolyzed protein composition, stirring for 20-40 minutes, and uniformly dispersing; (3) and (4) bottling and assembling the obtained oil gel and the hydrogel to obtain the double-bottle essence.
The third aspect of the invention provides a use method of the double-bottle essence for moisturizing, moisturizing and long-acting skin care, which comprises the following steps: the oil gel and the hydrogel of the skin-care double-bottle essence are respectively stored in separate bottles, and when the skin-care double-bottle essence is used, the oil gel and the hydrogel emulsion are uniformly mixed according to a certain proportion, and the mixed emulsion is smeared on the skin.
Has the beneficial effects that:
1. according to the invention, the skin care essences of the oil phase and the water phase are stored in the double bottles, so that the phenomena of layering, precipitation and inactivation caused by long-term storage of effective active ingredients in the oil in the water phase are effectively avoided, the active ingredients in the two phases can be efficiently utilized, and the effect of prolonging the product is ensured.
2. According to the invention, by adding the specific polypeptide raw material, the emulsification effect of the oleogel phase in the skin-care double-bottle essence is effectively improved, the skin-care double-bottle essence has good uniform and thickening effects, the oil separation phenomenon can not occur in the long-time use process, and the excellent stability is maintained.
3. According to the invention, through the synergistic effect of the specific polypeptide raw materials and the raw materials in the hydrogel, the mixing compatibility effect of the hydrogel in the oil gel is effectively improved, so that the double-bottle essence can be quickly and effectively mixed in use to form uniform skin-care emulsion with good spreadability, and the use effect of the skin-care essence is enhanced.
Detailed Description
The disclosure may be understood more readily by reference to the following detailed description of preferred embodiments of the invention and the examples included therein. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In case of conflict, the present specification, including definitions, will control.
The term "prepared from …" as used herein is synonymous with "comprising". The terms "comprises," "comprising," "includes," "including," "has," "having," "contains," "containing," or any other variation thereof, as used herein, are intended to cover a non-exclusive inclusion. For example, a composition, process, method, article, or apparatus that comprises a list of elements is not necessarily limited to only those elements but may include other elements not expressly listed or inherent to such composition, process, method, article, or apparatus.
The conjunction "consisting of …" excludes any unspecified elements, steps or components. If used in a claim, the phrase is intended to claim as closed, meaning that it does not contain materials other than those described, except for the conventional impurities associated therewith. When the phrase "consisting of …" appears in a clause of the subject matter of the claims rather than immediately after the subject matter, it defines only the elements described in the clause; other elements are not excluded from the claims as a whole.
When an amount, concentration, or other value or parameter is expressed as a range, preferred range, or as a range of upper preferable values and lower preferable values, this is to be understood as specifically disclosing all ranges formed from any pair of any upper range limit or preferred value and any lower range limit or preferred value, regardless of whether ranges are separately disclosed. For example, when a range of "1 to 5" is disclosed, the described range should be interpreted to include the ranges "1 to 4", "1 to 3", "1 to 2 and 4 to 5", "1 to 3 and 5", and the like. When a range of values is described herein, unless otherwise stated, the range is intended to include the endpoints thereof and all integers and fractions within the range.
The singular forms "a", "an" and "the" include plural referents unless the context clearly dictates otherwise. "optional" or "any" means that the subsequently described event or events may or may not occur, and that the description includes instances where the event occurs and instances where it does not.
Approximating language, as used herein throughout the specification and claims, is intended to modify a quantity, such that the invention is not limited to the specific quantity, but includes portions that are literally received for modification without substantial change in the basic function to which the invention is related. Accordingly, the use of "about" to modify a numerical value means that the invention is not limited to the precise value. In some instances, the approximating language may correspond to the precision of an instrument for measuring the value. In the present description and claims, range limitations may be combined and/or interchanged, including all sub-ranges contained therein if not otherwise stated.
In addition, the indefinite articles "a" and "an" preceding an element or component of the invention are intended to have no limitation on the number (i.e., number of occurrences) of the element or component. Thus, "a" or "an" should be read to include one or at least one, and the singular form of an element or component also includes the plural unless the stated number clearly indicates that the singular form is intended.
In order to solve the above problems, the present invention provides, in a first aspect, a moisturizing, long-lasting skin care essence comprising an oleogel and a hydrogel.
In some preferred embodiments, the starting materials for the oleogel comprise the following parts by weight: 2-6 parts of polypeptide, 12-16 parts of squalane, 25-35 parts of glycerol, 0.01-0.03 part of thickening agent, 44-58 parts of emollient, 0.5-1.5 parts of vegetable oil and 0.05-0.2 part of plant extract.
In some preferred embodiments, the raw materials of the hydrogel comprise the following parts by weight: 80-100 parts of water, 0.3-1.6 parts of dihydric alcohol, 0.2-2 parts of humectant, 0.1-1 part of thickener, 0.5-2 parts of basic amino acid, 0.2-0.6 part of chelating agent, 1-3 parts of skin conditioner, 0.1-1 part of hydrolyzed protein composition and 1-3 parts of surfactant.
In some preferred embodiments, the mass ratio of the oleogel to the hydrogel is 1: 1 to 2.
In some preferred embodiments, the mass ratio of the oleogel to the hydrogel is 1: 1.5.
in some preferred embodiments, the thickener is at least one of carbomer, xanthan gum, cetyl alcohol, stearyl alcohol, whale wax polyoxyethylene ether.
In some preferred embodiments, the thickener in the oleogel is xanthan gum; the thickening agent in the hydrogel is carbomer.
In some preferred embodiments, the emollient is cyclopentadimethicone and diethylhexyl carbonate.
In some preferred embodiments, the emollient further comprises an alkane composition; the alkane composition comprises the following components in percentage by mass: 90% of C9-12 alkane and 10% of coconut oil alcohol-caprylate.
In some preferred embodiments, the polypeptide is at least one of palmitoyl tripeptide, pentapeptide-3, dipeptide-2, acetyl tetrapeptide, carnosine, and surfactin sodium.
In some preferred embodiments, the polypeptide is sodium surfactin.
In some preferred embodiments, the mass ratio of the sodium surfactin to the surfactant is 3-5: 2.
in some preferred embodiments, the mass ratio of the sodium surfactin to the surfactant is 4: 2.
the applicant finds that the addition of sodium surfactin in the skin care essence can effectively improve the dispersion and dissolution effects of active ingredients in the oil gel in the hydrogel, so that the double-bottle essence has good applicability, and particularly when the mass ratio of the oil gel to the hydrogel is 1: 1.5, and the mass ratio of the surfactin sodium to the surfactant is 4: 2, the oil-water mixed gel has the best compatibility effect. The applicant speculates that: the added amount of sodium surfactin can form molecular micelles in the aqueous phase by the cyclic peptide structure, and can form intermolecular hydrogen bonds between the molecular micelles by the amino acid hydrophilic group, forming a polymer in the aqueous phase by a very small number of molecules. Meanwhile, the added sodium surfactin can also act synergistically with the surfactant in the hydrogel, so that the minimum concentration limit of the surfactant in the aqueous solution to associate into micelles is reduced, and the compatibilization of the surfactant in the oil-water mixed gel is enhanced.
In some preferred embodiments, the vegetable oil is at least one of olive oil, jojoba seed oil, shea butter, tea seed oil, sweet almond oil.
In some preferred embodiments, the vegetable oil is jojoba seed oil.
In some preferred embodiments, the plant extract is at least one of haematococcus pluvialis extract, turmeric root extract, withania japonica extract, centella asiatica extract, aloe vera extract.
In some preferred embodiments, the plant extract is haematococcus pluvialis extract.
In some preferred embodiments, the glycol is at least one of dipropylene glycol, 1, 2-ethylene glycol, and propylene glycol.
In some preferred embodiments, the humectant is at least one of tamarind seed polysaccharide, a glycerin-based composition, and glyceryl polyether-26.
In some preferred embodiments, the humectant is a tamarind seed polysaccharide and glycerin-based composition; the weight ratio of the tamarind seed polysaccharide to the glycerin-based composition is 1: 1.
in some preferred embodiments, the components of the glyceryl composition comprise the following mass percentages: 60% of glycerol, 35% of deionized water, 3% of glycerol acrylate copolymer and 2% of propylene glycol.
In some preferred embodiments, the basic amino acid is at least one of arginine, histidine, lysine.
In some preferred embodiments, the chelating agent is an acid alcohol composition; the acid-alcohol composition comprises the following components in percentage by mass: 1% of glycerol caprylate, 12% of caprylyl hydroximic acid and 87% of propylene glycol.
In some preferred embodiments, the skin conditioning agent is at least one of sodium hyaluronate, ceramide, niacinamide, tetrahydromethylpyrimidine carboxylic acid, a polysaccharide composition, an artemia extract.
In some preferred embodiments, the skin conditioning agent is a polysaccharide composition with an artemia extract.
In some preferred embodiments, the hydrolyzed protein composition is a hydrolyzed royal jelly protein composition.
In some preferred embodiments, the surfactant is at least one of sodium lauryl sulfate, cocamidopropyl betaine, polyoxyethylene lauryl ether, methylsilanol mannuronate.
In some preferred embodiments, the surfactant is methylsilanol mannuronate.
In some preferred embodiments, the weight ratio of the plant extract to the polypeptide is 2-3: 60 to 100.
In some preferred embodiments, the weight ratio of plant extract to polypeptide is 2: 80.
the second aspect of the invention provides a preparation method of the double-bottle essence for moisturizing, moisturizing and long-acting skin care, which comprises the following steps: (1) preparing oil gel: mixing and stirring squalane, glycerol and a thickening agent for 20-40 minutes until the mixture is uniformly stirred, then adding a small amount of an emollient, stirring vegetable oil for 20-40 minutes, uniformly mixing, then adding polypeptide and a plant extract, and stirring for 20-40 minutes; (2) preparing hydrogel: heating water, dihydric alcohol, a humectant, a thickening agent, alkaline amino acid, a chelating agent and a surfactant to 50-70 ℃, stirring for dissolving, cooling to 40 ℃, adding a skin conditioner and a hydrolyzed protein composition, stirring for 20-40 minutes, and uniformly dispersing; (3) and (4) bottling and assembling the obtained oil gel and the hydrogel to obtain the double-bottle essence.
The third aspect of the invention provides a use method of the double-bottle essence for moisturizing, moisturizing and long-acting skin care, which comprises the following steps: the oil gel and the hydrogel of the skin-care double-bottle essence are respectively stored in separate bottles, and when the skin-care double-bottle essence is used, the oil gel and the hydrogel emulsion are uniformly mixed according to a certain proportion, and the mixed emulsion is smeared on the skin.
Examples
The technical solution of the present invention is described in detail by the following examples, but the scope of the present invention is not limited to all of the examples. The starting materials of the present invention are all commercially available unless otherwise specified.
Example 1
Example 1 in a first aspect, a moisturizing, long-lasting skin care dual bottle essence is provided, comprising an oleogel and a hydrogel.
The oil gel and the hydrogel are uniformly mixed when in use, and the mass ratio of the oil gel to the hydrogel is 1: 1.5.
the raw materials of the oil gel comprise the following components in parts by weight: 4 parts of surfactin sodium, 14.38 parts of squalane, 30 parts of glycerol, 0.02 part of xanthan gum, 11.5 parts of alkane composition, 9 parts of cyclopenta dimethyl siloxane, 30 parts of diethylhexyl carbonate, 1 part of jojoba seed oil and 0.1 part of haematococcus pluvialis extract.
The hydrogel comprises the following raw materials in parts by weight: 91.7 parts of deionized water, 0.5 part of dipropylene glycol, 1, 2-hexanediol, 0.5 part of a glyceryl composition, 0.5 part of lima bean seed polysaccharide, 0.5 part of carbomer, 1 part of arginine, 0.4 part of an acid alcohol composition, 1 part of a polysaccharide composition, 1 part of a artemia extract, 0.5 part of a hydrolyzed royal jelly protein composition and 2 parts of methylsilanol mannuronate.
In this example, sodium surfactin is a sodium surfactin product sold by bells corporation of japan.
In this example, the alkane composition is an alkane composition product (ingredients: 90% C9-12 alkane and 10% coconut oil alcohol-caprylate) sold by BIOSYNTHIS, France.
In this example, Cyclopentadimethylsiloxane CAS is 541-02-6; diethylhexylcarbonate CAS: 105-58-8.
In this example, the haematococcus pluvialis extract is a haematococcus pluvialis extract product produced and sold by Nanjing Sibaike.
In this example, the glycerin-based composition was a glycerin-based composition (components: glycerin 60%, deionized water 35%, glycerin acrylate copolymer 3%, propylene glycol 2%) sold by the company CosMol, korea.
In this example, the acid alcohol composition is sold by NAGO, Guangzhou (R) corporation as the acid alcohol composition (ingredients: 1% glyceryl caprylate, 12% caprylyl hydroxamic acid, 87% propylene glycol).
In this example, the polysaccharide composition was a polysaccharide composition product (component: water 33.5%, glucuronic acid 40%, mannose 15%, β -glucan 5%, lactobionic acid 5%, p-hydroxyacetophenone 0.5%, and hexylene glycol 1%) sold by Guangzhou Mianrun company.
In this example, the artemia extract was a product of artemia extract (water 97.366%, artemia extract 0.35%, phenoxyethanol 1%, potassium sorbate 0.134%, glucose 1%) sold by france vince.
In this example, the hydrolyzed royal jelly protein composition is a product of hydrolyzed royal jelly protein composition produced and sold by Nippon Kogyo Co.
In this example, methylsilanol mannuronate is a methylsilanol mannuronate product sold by Monago Essemei.
The second aspect of the present embodiment provides a preparation method of the above dual-bottle essence for moisturizing, moisturizing and long-acting skin care: (1) preparing oil gel: mixing squalane, glycerol and xanthan gum, stirring for 30 minutes until the mixture is uniformly stirred, then adding a small amount of cyclopentadimethylsiloxane, diethylhexyl carbonate, an alkane composition and jojoba seed oil, stirring for 30 minutes, uniformly mixing, adding surfactin sodium and haematococcus pluvialis extract, and stirring for 30 minutes; (2) preparing hydrogel: heating water, dipropylene glycol, 1, 2-hexanediol, tamarind seed polysaccharide, a glyceryl composition, carbomer, arginine, an acid-alcohol composition and methylsilanol mannuronate to 60 ℃, stirring for dissolving, cooling to 40 ℃, adding the polysaccharide composition, the artemia extract and the hydrolyzed royal jelly protein composition, stirring for 30 minutes, and uniformly dispersing; (3) and (4) bottling and assembling the obtained oil gel and the hydrogel to obtain the double-bottle essence.
Example 2
The embodiment of the present invention is different from embodiment 1 in that: the mass ratio of the oil gel to the hydrogel is 1: 1.
example 3
The embodiment of the present invention is different from embodiment 1 in that: 3 parts of sodium surfactin.
Comparative example 1
The embodiment of this comparative example is the same as example 1 except that: the mass ratio of the oil gel to the hydrogel is 1: 3.
comparative example 2
The embodiment of this comparative example is the same as example 1 except that: methylsilanol mannuronate is 0.5 part.
Comparative example 3
The embodiment of this comparative example is the same as example 1 except that: 0.5 part of sodium surfactin.
Comparative example 4
The embodiment of this comparative example is the same as example 1 except that: 0.05 part of haematococcus pluvialis extract.
Evaluation of Performance
1. Radical scavenging effect: (1) test samples: will implementThe two bottles of essences prepared in the examples and the comparative examples are uniformly mixed and stirred according to the corresponding proportion, and are mixed and diluted into a test solution with the mass fraction of 1 wt% by pure water; (2) the test method comprises the following steps: hydroxyl radical scavenging experiments: taking 0.5mL of absolute ethanol solution of o-diazaphenanthrene with the concentration of 0.75mmol/L into a test tube with a plug, respectively adding 2mL and 1mL of test solution of phosphate buffer solution with the pH value of 7.4 and the concentration of 0.2mol/L, fully and uniformly mixing, adding 0.5mL of FeSO with the concentration of 0.75mmol/L4·7H2O solution, mixed again and then added with 0.5mL of 0.01% (v/v) H2O2After being put in a constant-temperature water bath at 37 ℃ for 60min, the absorbance values of all groups of mixed solutions are respectively measured at 536nm and recorded As As, the absorbance values are measured by using distilled water instead of sample solution As a blank group and recorded As Ab, and the distilled water instead of H2O2And measuring the absorbance value An of the damage group, and calculating the hydroxyl radical clearance of the test sample according to the following formula: hydroxyl radical clearance (%) - (As-An)/(Ab-An)]100%, the test results are tabulated by taking the average of 5 tests, 5 specimens are tested per comparative example of example, and the average of the measured values is tabulated in Table 1.
2. Compatibility in mixed use: the method comprises the steps of uniformly mixing and stirring the double bottles of essence prepared in the examples and the comparative examples according to the corresponding proportion, placing the mixture for 24 hours in a clean environment, observing whether the mixed essence emulsion has a macroscopic obvious layering phenomenon, testing 100 samples in each example and comparative example, recording the layering of 5 samples which are less than or equal to A, recording the layering of 20 samples which are more than 5 samples which are less than or equal to B, and recording the layering of 20 samples which are more than 20 samples which are C, and recording the measured results in a table 1.
TABLE 1
Examples Free radical scavenging effect% Compatibility in Mixed applications
Example 1 83.5 A
Example 2 82.8 A
Example 3 82.1 A
Comparative example 1 52.4 C
Comparative example 2 65.1 B
Comparative example 3 58.8 C
Comparative example 4 32.4 B
Through the embodiments 1-3, the comparative examples 1-4 and the table 1, it can be known that the moisturizing, moisturizing and long-acting skin care double-bottle essence provided by the invention has good long-acting moisturizing effect, active ingredients in a skin care product are not easy to inactivate, layering and precipitation phenomena of the skin care product are effectively reduced, and the moisturizing, moisturizing and long-acting skin care double-bottle essence is suitable for being popularized in the field of skin care products and has a wide development prospect. Wherein, the example 1 obtains the best performance index under the factors of the best raw material proportion, the best preparation process and the like.
Finally, it should be understood that the above-described embodiments are merely preferred embodiments of the present invention, and not intended to limit the present invention, and any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (10)

1. The double-bottle essence capable of replenishing water, preserving moisture and protecting skin for a long time is characterized in that: including oleogels and hydrogels.
2. The moisturizing, moisturizing and long-acting skin care essence of claim 1, wherein the moisturizing, moisturizing and long-acting skin care essence comprises: the raw materials of the oil gel comprise the following components in parts by weight: 2-6 parts of polypeptide, 12-16 parts of squalane, 25-35 parts of glycerol, 0.01-0.03 part of thickening agent, 44-58 parts of emollient, 0.5-1.5 parts of vegetable oil and 0.05-0.2 part of plant extract.
3. The moisturizing, moisturizing and long-acting skin care essence of claim 1, wherein the moisturizing, moisturizing and long-acting skin care essence comprises: the hydrogel comprises the following raw materials in parts by weight: 80-100 parts of water, 0.3-1.6 parts of dihydric alcohol, 0.2-2 parts of humectant, 0.1-1 part of thickener, 0.5-2 parts of basic amino acid, 0.2-0.6 part of chelating agent, 1-3 parts of skin conditioner, 0.1-1 part of hydrolyzed protein composition and 1-3 parts of surfactant.
4. The moisturizing, moisturizing and long-acting skin care essence of claim 1, wherein the moisturizing, moisturizing and long-acting skin care essence comprises: the mass ratio of the oleogel to the hydrogel is 1: 1 to 2.
5. The moisturizing, moisturizing and long-acting skin care essence of claim 2 or 3, wherein the moisturizing, moisturizing and long-acting skin care essence comprises: the thickener is at least one of carbomer, xanthan gum, cetyl alcohol, stearyl alcohol and whale wax polyoxyethylene ether.
6. The moisturizing, moisturizing and long-acting skin care essence provided by claim 2, wherein the moisturizing, moisturizing and long-acting skin care essence comprises the following components in parts by weight: the polypeptide is at least one of palmitoyl tripeptide, pentapeptide-3, dipeptide-2, acetyl tetrapeptide, carnosine and surfactin sodium.
7. The moisturizing, moisturizing and long-acting skin care essence of claim 2, wherein the moisturizing, moisturizing and long-acting skin care essence comprises: the vegetable oil is at least one of olive oil, jojoba seed oil, shea butter, tea seed oil, and sweet almond oil.
8. The moisturizing, moisturizing and long-acting skin care essence of claim 3, wherein the moisturizing, moisturizing and long-acting skin care essence comprises: the basic amino acid is at least one of arginine, histidine and lysine.
9. The preparation method of the moisturizing, moisturizing and long-acting skin care essence according to any one of claims 1 to 8, characterized by comprising the following steps: (1) preparing oil gel: mixing and stirring squalane, glycerol and a thickening agent for 20-40 minutes until the mixture is uniformly stirred, then adding a small amount of an emollient, stirring vegetable oil for 20-40 minutes, uniformly mixing, then adding polypeptide and a plant extract, and stirring for 20-40 minutes; (2) preparing hydrogel: heating water, dihydric alcohol, a humectant, a thickening agent, alkaline amino acid, a chelating agent and a surfactant to 50-70 ℃, stirring for dissolving, cooling to 40 ℃, adding a skin conditioner and a hydrolyzed protein composition, stirring for 20-40 minutes, and uniformly dispersing; (3) and (4) bottling and assembling the obtained oil gel and the hydrogel to obtain the double-bottle essence.
10. The use method of the moisturizing, moisturizing and long-acting skin care double-bottle essence according to any one of claims 1 to 8 is characterized in that: the oil gel and the hydrogel of the skin-care double-bottle essence are respectively stored in separate bottles, and when the skin-care double-bottle essence is used, the oil gel and the hydrogel emulsion are uniformly mixed according to a certain proportion, and the mixed emulsion is smeared on the skin.
CN202110460644.9A 2021-04-27 2021-04-27 Moisturizing, moisturizing and long-acting skin care double-bottle essence and preparation and use methods thereof Pending CN114642607A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115212740A (en) * 2022-06-22 2022-10-21 汕头市奇伟实业有限公司 Emulsification method, double-tube type anti-wrinkle cream, preparation method and application of double-tube type anti-wrinkle cream in neck skin care products

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107693433A (en) * 2017-11-13 2018-02-16 广州市花安堂生物科技有限公司 A kind of moisturizing elite and preparation method thereof
CN110787093A (en) * 2019-10-12 2020-02-14 广州市百好博有限公司 Two-agent moisturizing essence and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107693433A (en) * 2017-11-13 2018-02-16 广州市花安堂生物科技有限公司 A kind of moisturizing elite and preparation method thereof
CN110787093A (en) * 2019-10-12 2020-02-14 广州市百好博有限公司 Two-agent moisturizing essence and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115212740A (en) * 2022-06-22 2022-10-21 汕头市奇伟实业有限公司 Emulsification method, double-tube type anti-wrinkle cream, preparation method and application of double-tube type anti-wrinkle cream in neck skin care products

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