CN103202775A - Double-layer cleansing lotion and preparation method thereof - Google Patents
Double-layer cleansing lotion and preparation method thereof Download PDFInfo
- Publication number
- CN103202775A CN103202775A CN2013100969862A CN201310096986A CN103202775A CN 103202775 A CN103202775 A CN 103202775A CN 2013100969862 A CN2013100969862 A CN 2013100969862A CN 201310096986 A CN201310096986 A CN 201310096986A CN 103202775 A CN103202775 A CN 103202775A
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- Prior art keywords
- oil
- water
- soluble
- wetting agent
- polyethylene glycol
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- 239000001540 sodium lactate Substances 0.000 claims description 2
- 235000011088 sodium lactate Nutrition 0.000 claims description 2
- 229940005581 sodium lactate Drugs 0.000 claims description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 2
- 235000011152 sodium sulphate Nutrition 0.000 claims description 2
- ZPNRBQVNNIDJHX-UHFFFAOYSA-M sodium;3-acetyl-6-methyl-2-oxopyran-4-olate Chemical compound [Na+].CC(=O)C1=C([O-])C=C(C)OC1=O ZPNRBQVNNIDJHX-UHFFFAOYSA-M 0.000 claims description 2
- 229940032094 squalane Drugs 0.000 claims description 2
- 229940099373 sudan iii Drugs 0.000 claims description 2
- 239000010677 tea tree oil Substances 0.000 claims description 2
- 229940111630 tea tree oil Drugs 0.000 claims description 2
- ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 claims description 2
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 claims description 2
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical compound CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 claims 1
- 238000004945 emulsification Methods 0.000 abstract description 4
- 239000000839 emulsion Substances 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 230000003020 moisturizing effect Effects 0.000 abstract 2
- 239000000047 product Substances 0.000 description 52
- 239000000126 substance Substances 0.000 description 31
- 239000010410 layer Substances 0.000 description 28
- 239000002537 cosmetic Substances 0.000 description 16
- 239000006071 cream Substances 0.000 description 10
- 238000004140 cleaning Methods 0.000 description 9
- 235000013336 milk Nutrition 0.000 description 9
- 239000008267 milk Substances 0.000 description 9
- 210000004080 milk Anatomy 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 8
- 229910052751 metal Inorganic materials 0.000 description 8
- 239000002184 metal Substances 0.000 description 8
- 230000002906 microbiologic effect Effects 0.000 description 8
- 230000001953 sensory effect Effects 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 239000003153 chemical reaction reagent Substances 0.000 description 7
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 6
- 229910052709 silver Inorganic materials 0.000 description 6
- 239000004332 silver Substances 0.000 description 6
- 230000001804 emulsifying effect Effects 0.000 description 3
- 210000000481 breast Anatomy 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 235000013373 food additive Nutrition 0.000 description 2
- 239000002778 food additive Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
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- 210000000697 sensory organ Anatomy 0.000 description 1
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- 239000004094 surface-active agent Substances 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a double-layer cleansing lotion and a preparation method thereof. The double-layer cleansing lotion comprises a water-phase layer and an oil-phase layer. The water-phase layer comprises water soluble preservatives, water soluble grease, inorganic salt electrolyte, moisturizing agent and water. The oil-phase layer comprises water-insoluble grease, oil soluble preservatives and oil soluble pigment. The preparation method includes: sequentially adding water soluble preservatives, water soluble grease, inorganic salt electrolyte and moisturizing agent into water, well mixing to obtain water-phase layer components, sequentially adding oil soluble preservatives and oil soluble pigment in water-insoluble grease, well mixing to obtain oil-phase layer components, and mixing the water-phase layer components and the oil-phase layer components to obtain the double-layer cleansing lotion. During use, the double-layer cleansing lotion can be emulsified by shaking to form emulsion, and instant deemulsification occurs to form double-layer structure with clearly-separated oil and water when the double-layer cleansing lotion stands still. The double-layer cleansing lotion is mild in cleansing, instant in emulsification, fast in deemulsification, clear in boundary and the like.
Description
Technical field
The invention belongs to the cosmetics technical field, be specifically related to a kind of bilayer makeup removing liquid for eye or lip makeup removing usefulness and preparation method thereof.
Background technology
The cosmetic cleaning product is converted to diversification of today along with the sectionalization in cosmetics market by original kind unification.Cleaning is the vital first step for the skin maintenance, and clean skin could absorb every nursing such as ensuing elite, emulsion, facial cream.The cosmetic cleaning product is invented out different products according to the research of human body different parts now, and wherein for the cleaning of eye and lip, numerous women more pay attention to.
In that we see the makeup removing liquid (breast) of many lips and eye cleaning on the market, but most of products all are oil-in-water type (O/W), and have a significant effect for fat-soluble cosmetics for monolayer, these makeup removing liquid (breast) are difficult to simultaneously effectively cleaning water-based soils and oily dirt.
Summary of the invention
The objective of the invention is to provide in order to solve above-mentioned technical problem a kind of double-deck makeup removing liquid.
Two of purpose of the present invention is to provide the preparation method of above-mentioned a kind of double-deck makeup removing liquid.
Technical scheme of the present invention
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 1～10%
Water-soluble grease 5～15 %
Inorganic salt electrolyte 0.1～10%
Waterborne-type preservation 0.1～0.5%
Water-insoluble oils and fats 39.8～49.6%
Oil-soluble pigment 0.00001～0.01%
Oil-solvent preservative 0.1～0.5%
Surplus is water.
Wherein said wetting agent is polyalcohols wetting agent, hyaluronic acid wetting agent, lactic acid and sodium lactate wetting agent, pyrrolidone sodium carboxylate, ceramide type wetting agent, amide-type wetting agent, glucose esters wetting agent, collagen protein class wetting agent, chitin derivative or chitosan, is preferably the polyalcohols wetting agent;
Described polyalcohols wetting agent is 1,2 propylene glycol, 1,3 butanediol or glycerol;
Described water-soluble grease is water-soluble plant oils and fats, water-soluble silicon oils or water-soluble plant oils and fats and water-soluble silicon oils composition mixture;
Wherein the water-soluble plant oils and fats is Polyethylene Glycol (75) lanoline, Polyethylene Glycol (120) Jojoba ester, Polyethylene Glycol (7) Fructus Canarii albi grease, Polyethylene Glycol (7) Oleum Cocois glyceride, Polyethylene Glycol (30) Oleum Cocois glyceride, Polyethylene Glycol (80) Oleum Cocois glyceride, Polyethylene Glycol (200) hydrogenated palm acid glyceride, Polyethylene Glycol (10) olive oil glyceride, glycerol alcohol ether-8 hydroxy stearic acid ester, Polyethylene Glycol (26) glycerin ether, Polyethylene Glycol (7) glycerin ether, Polyethylene Glycol (16) macadimia nut glyceride, Polyethylene Glycol (10) Oleum helianthi glyceride, Polyethylene Glycol (80) Jojoba wax ester, Polyethylene Glycol (120) Jojoba wax ester, the water solublity castor oil hydrogenated, one or more mixture of forming in the water solublity Jojoba oil;
Water-soluble silicon oils is Polyethylene Glycol (8) polydimethylsiloxane, Polyethylene Glycol (10) polydimethylsiloxane, Polyethylene Glycol (12) polydimethylsiloxane, Polyethylene Glycol (17) polydimethylsiloxane, the mixture that one or more in the dimethiconol are formed;
Described inorganic salt electrolyte is one or more mixture of forming of sodium chloride, potassium chloride, magnesium sulfate, sodium sulfate;
Described waterborne-type preservation is the waterborne-type preservation of sodium hydroxy methyl glycinate, germall series, GLYDANT series or the serial class of triumphant pine;
The waterborne-type preservation of wherein said germall series is imidazolidinyl urea, two imidazolidinyl urea or iodo propinyl butyl meglumine acid fat;
The waterborne-type preservation of described triumphant pine series is 5-chloro-2-methyl-4-isothiazole-3-ketone or 2-methyl-4-isothiazole-3-ketone;
The waterborne-type preservation of described GLYDANT series is 1,3-dihydroxy 5,5-dimethyl hydantoin, 3-iodo-2-propynyl butyl carbamate or 1,3-dihydroxy 5, the mixture that 5-dimethyl hydantoin and 3-iodo-2-propynyl butyl carbamate are formed;
Described water-insoluble oils and fats is liquid fat, and described liquid fat is Vegetable oil lipoprotein, animal oil or synthetic ester oil;
Wherein said Vegetable oil lipoprotein is Oleum Ricini, olive oil, Oleum Arachidis hypogaeae semen, Oleum Cocois, Oleum Gossypii semen, almond oil, Apricot kernel oil, Petiolus Trachycarpi oil, palm-kernel oil, Oleum Glycines, Semen Tritici aestivi germ oil, Semen Maydis oil, Oleum Camelliae, Japan's Oleum Camelliae, Testa oryzae oil, American Avocado Tree oil, macadimia nut oil, candlenut oil, Jojoba oil, Oleum Hippophae, water Bulbus Allii meson oil, cameline oil, the Herba Passiflorae Caeruleae caul-fat, Flos Inulae oil, the Fructus Mangifera Indicae kernel oil, the Flos Rosae Multiflorae fruit oil, aloe, tea tree oil, Herba Medicaginis oil, the formed mixed vegetable oil of in the Oil of Spanish sage one or more;
Described animal oil is one or more the formed mixing animal oil in mink oil, shark liver oil, manhaden oil, Fructus Citri tangerinae sour jujube Channa argus oil, turtle oil, Adeps Serpentis, 10# low viscosity white oil, the wool oil;
Described synthetic ester oil is polyoxyethylene-polyoxypropylene wool oil, squalane, polydimethylsiloxane, one or more the formed mixing synthetic ester oil in polymethyl-benzene base silica, ring-type methylsiloxane, sad capric acid triglyceride, the isopropyl palmitate;
Described oil-soluble pigment is synthetic dyestuff or natural pigment;
Wherein said synthetic dyestuff is one or more the formed mixture in permanent orange, sudan III, upright lock rubine B, setting sun Huang, Indian yellow 73, acid red 87, Food Red 14, solvent red 43, food indigo plant 2, Food Green 3, solvent green 3, the green GC of alizarin blue or green plain cyanine, solvent yellow 33, quinoline yellow, acid yellow 11, Citronin A, food indigo plant 1, indigo, lemon yellow pigment, light green pigment, 85% lemon yellow;
Described natural pigment is that β-phylloerythrin, carmine, CHLOROPHYLLINE potassium sodium copper, class carotene, anthraquinone pigment, Folium Perillae are red, one or more the formed mixture in the cashaw pigment, curcumin;
Described oil-solvent preservative is that trichlorine is to the oil-solvent preservative of hexichol, bronocot, hexachlorophene, dehydroacetic acid or dehydroacetic acid sodium salt, o-phenyl phenol, Buddhist nun's platinum lipid or the serial class of triumphant pine;
The oil-solvent preservative of wherein said Buddhist nun's platinum lipid is one or more the formed mixture in methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, nipalgin isopropyl ester, nipalgin isobutyl ester, the different methyl ester of nipalgin;
The oil-solvent preservative of the serial class of described triumphant pine is one or more the formed mixture in methyl-chloro-isothiazolone, methyl-isothiazolone, the biphenyl isothiazolone.
The preparation method of above-mentioned a kind of double-deck makeup removing liquid specifically comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
A kind of double-deck makeup removing liquid of above-mentioned gained is used for makeup removing, and instantaneous emulsifying is in use shaken in the particularly makeup removing of eye or lip, be applied in the makeup removing position after forming emulsification system, particularly eye or lip are clean with flushing with clean water then, namely finish the makeup removing to the makeup removing position.
Beneficial effect of the present invention
Double-deck makeup removing liquid of the present invention, can instantaneous emulsifying under the condition of in use shaking, form emulsification system, but fast hierarchical again after placing, the demarcation line is clear, and outward appearance is beautiful, owing to contain water-soluble grease, water-insoluble oils and fats and water simultaneously, therefore its cleaning capacity for liposoluble and water miscible dirt is all more remarkable, and the dirt on the skin is dispeled with obtaining optimum degree.And should the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard after testing of bilayer makeup removing liquid.
Further, double-deck makeup removing liquid of the present invention because employed surfactant is relatively gentleer, can not cause any stimulation to skin in cleaning course.
Further, therefore the preparation method of a kind of double-deck makeup removing liquid of the present invention because just each raw material simply mixes, has that preparation process is simple, convenience operation.
Specific implementation method
Below by specific embodiment the present invention is further set forth, but do not limit the present invention.
Among the present invention among each embodiment used water be industrial deionized water.
Embodiment 1
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 1%
Water-soluble grease 5%
Inorganic salt electrolyte 0.1%
Waterborne-type preservation 0.1%
Water-insoluble oils and fats 45.9%
Oil-soluble pigment 0.00001%
Oil-solvent preservative 0.1%
Water 47.79999%
Described wetting agent is 1,2 propylene glycol, the SILVER REAGENT product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described water-soluble grease is the water solublity castor oil hydrogenated, the technical grade product that BASF (China) chemical industry company limited is produced;
Described inorganic salt electrolyte is sodium chloride, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described waterborne-type preservation is two imidazolidinyl urea, the cosmetics industry level product that international special product (China) company limited of Ashland provides;
Described water-insoluble oils and fats is 10# low viscosity white oil, the technical grade product that Hangzhou Refinery provides;
Described oil-solvent preservative is Buddhist nun's platinum propyl ester, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described oil-soluble pigment is indigo, the technical grade product of sky, the Guangzhou safe pigment of sun company.
The preparation method of above-mentioned a kind of double-deck makeup removing liquid comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
The industry standard of liquid product owing to do not remove ornaments and formal dress at present, therefore with the bilayer makeup removing liquid of above-mentioned gained, the detection of sensory evaluation and physical and chemical index, microbiological indicator and content of beary metal is carried out in requirement according to QB/T1645-2004 cleansing milk (cream) cosmetic standard, and testing result sees Table 1, table 2;
Table 1, sanitary index
Table 2, sense organ, physical and chemical index
Result from table 1 and table 2 as can be seen, the requirement of the equal accord with Q B/T1645-2004 cleansing milk of the detection of sensory evaluation and physical and chemical index, microbiological indicator and content of beary metal (cream) cosmetic standard.
Embodiment 2
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 10%
Water-soluble grease 15%
Inorganic salt electrolyte 10%
Waterborne-type preservation 0.5%
Water-insoluble oils and fats 44.49%
Oil-soluble pigment 0.01%
Oil-solvent preservative 0.5%
Water 19.5%
Described wetting agent is 1,3 butanediol, the SILVER REAGENT product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described water-soluble grease is Polyethylene Glycol (12) polydimethylsiloxane, the Dowcorning(DOW CORNING) product produced of chemical company limited;
Described inorganic salt electrolyte is magnesium sulfate, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described waterborne-type preservation is 1,3-dihydroxy 5, the mixture (Liquid Glydant Plus) that 5-dimethyl hydantoin and 3-iodo-2-propynyl butyl carbamate are formed, the technical grade product that husky (China) company limited of dragon provides;
Described water-insoluble oils and fats is sad capric acid triglyceride, the technical grade product that BASF (China) chemical industry company limited is produced;
Described oil-solvent preservative is Buddhist nun's platinum propyl ester, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described oil-soluble pigment is indigo, the technical grade product of sky, the Guangzhou safe pigment of sun company.
The preparation method of above-mentioned a kind of double-deck makeup removing liquid comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
Above-mentioned bilayer makeup removing liquid is measured by it being carried out sensory evaluation, physical and chemical index test, microbiological indicator and content of beary metal, detects the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard.
Above-mentioned bilayer makeup removing liquid is measured by it being carried out sensory evaluation, physical and chemical index test, microbiological indicator and content of beary metal, detects the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard.
Embodiment 3
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 5%
Water-soluble grease 10%
Inorganic salt electrolyte 5%
Waterborne-type preservation 0.2%
Water-insoluble oils and fats 49.60%
Oil-soluble pigment 0.0001%
Oil-solvent preservative 0.2%
Water 29.9999%
Described wetting agent glycerol, the SILVER REAGENT product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described water-soluble grease water solublity Jojoba oil, the technical grade product that rich platinum chemical industry company limited is produced;
Described inorganic salt electrolyte is potassium chloride, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described waterborne-type preservation is two imidazolidinyl urea, the technical grade product that international special product (China) company limited of Ashland provides;
Described water-insoluble oils and fats is isopropyl palmitate, the technical grade product that BASF (China) chemical industry company limited is produced;
Described oil-solvent preservative is Buddhist nun's platinum propyl ester, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described oil-soluble pigment is indigo, the technical grade product of sky, the Guangzhou safe pigment of sun company;
The preparation method of above-mentioned a kind of double-deck makeup removing liquid comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
Above-mentioned bilayer makeup removing liquid is measured by it being carried out sensory evaluation, physical and chemical index test, microbiological indicator and content of beary metal, detects the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard.
Embodiment 4
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 8%
Water-soluble grease 8%
Inorganic salt electrolyte 0.3%
Waterborne-type preservation 0.15%
Water-insoluble oils and fats 41.7%
Oil-soluble pigment 0.00002%
Oil-solvent preservative 0.15%
Water 41.69998%
Described wetting agent is 1,2 propylene glycol, the SILVER REAGENT product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described water-soluble grease is Polyethylene Glycol (16) macadimia nut glyceride, the technical grade product that rich platinum chemical industry company limited is produced;
Described inorganic salt electrolyte is potassium chloride, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described waterborne-type preservation is sodium hydroxy methyl glycinate, the cosmetics industry level product that international special product (China) company limited of Ashland provides;
Described water-insoluble oils and fats is olive oil, the technical grade product that Lai Baokang (China) chemical industry company limited provides;
Described oil-solvent preservative is Buddhist nun's platinum isopropyl ester, the chemical pure product of Ke Laien (China) company limited;
Described oil-soluble pigment is lemon yellow pigment, the technical grade product of gentle inferior (Shanghai) food additive company.
The preparation method of above-mentioned a kind of double-deck makeup removing liquid comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
Above-mentioned bilayer makeup removing liquid is measured by it being carried out sensory evaluation, physical and chemical index test, microbiological indicator and content of beary metal, detects the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard.
Embodiment 5
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 6%
Water-soluble grease 12%
Inorganic salt electrolyte 2%
Waterborne-type preservation 0.2%
Water-insoluble oils and fats 39.8%
Oil-soluble pigment 0.01%
Oil-solvent preservative 0.2%
Water 39.79%
Described wetting agent is 1,3 butanediol, the SILVER REAGENT product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described water-soluble grease is Polyethylene Glycol (7) Oleum Cocois glyceride, the CORUM(Cologne) product produced of chemical company limited;
Described inorganic salt electrolyte is magnesium sulfate, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described waterborne-type preservation is imidazolidinyl urea (Germall 115), the technical grade product that international special product (China) company limited of Ashland provides;
Described water-insoluble oils and fats is palm-kernel oil, the technical grade product that BASF (China) chemical industry company limited is produced;
Described oil-solvent preservative is bronocot, the chemical pure product of Ke Laien (China) chemical reagent company limited;
Described oil-soluble pigment is light green pigment, the technical grade product of gentle inferior (Shanghai) food additive company.
The preparation method of above-mentioned a kind of double-deck makeup removing liquid comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
Above-mentioned bilayer makeup removing liquid is measured by it being carried out sensory evaluation, physical and chemical index test, microbiological indicator and content of beary metal, detects the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard.
Embodiment 6
A kind of double-deck makeup removing liquid is calculated by mass percentage, and its raw material composition and content are as follows:
Wetting agent 3%
Water-soluble grease 6%
Inorganic salt electrolyte 3%
Waterborne-type preservation 0.3%
Water-insoluble oils and fats 43.7%
Oil-soluble pigment 0.0001%
Oil-solvent preservative 0.3%
Water 43.6999%.
Described wetting agent glycerol, the SILVER REAGENT product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described water-soluble grease dimethiconol, the technical grade product that the triumphant organosilicon of prestige (Shanghai) Co., Ltd. produces;
Described inorganic salt electrolyte is potassium chloride, the chemical pure product of Chemical Reagent Co., Ltd., Sinopharm Group;
Described waterborne-type preservation is the mixture (Germall Plus) that two imidazolidinyl urea and iodo propinyl butyl methylamine acid esters are formed, the technical grade product that international special product (China) company limited of Ashland provides;
Described water-insoluble oils and fats is Oleum Ricini, the technical grade product that BASF (China) chemical industry company limited is produced;
Described oil-solvent preservative is the mixture (LIQUAPAR OIL) that nipalgin isopropyl ester, nipalgin isobutyl ester are formed, the chemical pure product of international special product (China) company limited of Ashland;
Described oil-soluble pigment is 85% lemon yellow, the technical grade product of Shanghai base of a fruit section company limited.
The preparation method of above-mentioned a kind of double-deck makeup removing liquid comprises the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
Above-mentioned bilayer makeup removing liquid is measured by it being carried out sensory evaluation, physical and chemical index test, microbiological indicator and content of beary metal, detects the requirement of its every index accord with Q B/T1645-2004 cleansing milk (cream) cosmetic standard.
A kind of double-deck makeup removing liquid of above-mentioned gained is used for makeup removing, during particularly for eye or lip makeup removing, in use shake instantaneous emulsifying, form emulsification system, after be applied in the makeup removing position, particularly eye or lip, clean with flushing with clean water then, namely finish the makeup removing to the makeup removing position, especially its cleaning capacity to the liposoluble of eye or lip and water miscible dirt is more remarkable, and the dirt on the skin is dispeled with obtaining optimum degree, but fast hierarchical again after placing, the demarcation line is clear, and outward appearance is beautiful.
Foregoing only is the basic explanation of the present invention under conceiving, and according to any equivalent transformation that technical scheme of the present invention is done, all should belong to protection scope of the present invention.
Claims (8)
1. a double-deck makeup removing liquid is characterized in that by weight calculating, and its raw material composition and content are as follows:
Wetting agent 1～10%
Water-soluble grease 5～15 %
Inorganic salt electrolyte 0.1～10%
Waterborne-type preservation 0.1～0.5%
Water-insoluble oils and fats 39.8～49.6%
Oil-soluble pigment 0.00001～0.01%
Oil-solvent preservative 0.1～0.5%
Surplus is water;
Wherein said wetting agent is polyalcohols wetting agent, hyaluronic acid wetting agent, lactic acid or sodium lactate wetting agent, pyrrolidone sodium carboxylate, ceramide type wetting agent, amide-type wetting agent, glucose esters wetting agent, collagen protein class wetting agent, chitin derivative or chitosan;
Described polyalcohols wetting agent is 1,2 propylene glycol, 1,3 butanediol or glycerol;
Described water-soluble grease is water-soluble plant oils and fats, water-soluble silicon oils or water-soluble plant oils and fats and water-soluble silicon oils composition mixture;
Wherein the water-soluble plant oils and fats is Polyethylene Glycol (75) lanoline, Polyethylene Glycol (120) Jojoba ester, Polyethylene Glycol (7) Fructus Canarii albi grease, Polyethylene Glycol (7) Oleum Cocois glyceride, Polyethylene Glycol (30) Oleum Cocois glyceride, Polyethylene Glycol (80) Oleum Cocois glyceride, Polyethylene Glycol (200) hydrogenated palm acid glyceride, Polyethylene Glycol (10) olive oil glyceride, glycerol alcohol ether-8 hydroxy stearic acid ester, Polyethylene Glycol (26) glycerin ether, Polyethylene Glycol (7) glycerin ether, Polyethylene Glycol (16) macadimia nut glyceride, Polyethylene Glycol (10) Oleum helianthi glyceride, Polyethylene Glycol (80) Jojoba wax ester, Polyethylene Glycol (120) Jojoba wax ester, the water solublity castor oil hydrogenated, one or more mixture of forming in the water solublity Jojoba oil;
Water-soluble silicon oils is one or more mixture formed in Polyethylene Glycol (8) polydimethylsiloxane, Polyethylene Glycol (10) polydimethylsiloxane, Polyethylene Glycol (12) polydimethylsiloxane, Polyethylene Glycol (17) polydimethylsiloxane, the dimethiconol;
Described inorganic salt electrolyte is one or more mixture of forming of sodium chloride, potassium chloride, magnesium sulfate, sodium sulfate;
Described waterborne-type preservation is the waterborne-type preservation of sodium hydroxy methyl glycinate, germall series, GLYDANT series or the serial class of triumphant pine;
The waterborne-type preservation of wherein said germall series is the mixture of one or more compositions in imidazolidinyl urea, two imidazolidinyl urea, the iodo propinyl butyl meglumine acid fat;
The waterborne-type preservation of described triumphant pine series is 5-chloro-2-methyl-4-isothiazole-3-ketone or 2-methyl-4-isothiazole-3-ketone;
The waterborne-type preservation of described GLYDANT series is 1,3-dihydroxy 5,5-dimethyl hydantoin, 3-iodo-2-propynyl butyl carbamate or 1,3-dihydroxy 5, the mixture that 5-dimethyl hydantoin and 3-iodo-2-propynyl butyl carbamate are formed;
Described water-insoluble oils and fats is liquid fat, and described liquid fat is Vegetable oil lipoprotein, animal oil or synthetic ester oil;
Wherein said Vegetable oil lipoprotein is Oleum Ricini, olive oil, Oleum Arachidis hypogaeae semen, Oleum Cocois, Oleum Gossypii semen, almond oil, Apricot kernel oil, Petiolus Trachycarpi oil, palm-kernel oil, Oleum Glycines, Semen Tritici aestivi germ oil, Semen Maydis oil, Oleum Camelliae, Japan's Oleum Camelliae, Testa oryzae oil, American Avocado Tree oil, macadimia nut oil, candlenut oil, Jojoba oil, Oleum Hippophae, water Bulbus Allii meson oil, cameline oil, the Herba Passiflorae Caeruleae caul-fat, Flos Inulae oil, the Fructus Mangifera Indicae kernel oil, the Flos Rosae Multiflorae fruit oil, aloe, tea tree oil, Herba Medicaginis oil, the formed mixed vegetable oil of in the Oil of Spanish sage one or more;
Described animal oil is one or more the formed mixing animal oil in mink oil, shark liver oil, manhaden oil, Fructus Citri tangerinae sour jujube Channa argus oil, turtle oil, Adeps Serpentis, 10# low viscosity white oil, the wool oil;
Described synthetic ester oil is polyoxyethylene-polyoxypropylene wool oil, squalane, polydimethylsiloxane, one or more the formed mixing synthetic ester oil in polymethyl-benzene base silica, ring-type methylsiloxane, sad capric acid triglyceride, the isopropyl palmitate;
Described oil-soluble pigment is synthetic dyestuff or natural pigment;
Wherein said synthetic dyestuff is one or more the formed mixture in permanent orange, sudan III, upright lock rubine B, setting sun Huang, Indian yellow 73, acid red 87, Food Red 14, solvent red 43, food indigo plant 2, Food Green 3, solvent green 3, the green GC of alizarin blue or green plain cyanine, solvent yellow 33, quinoline yellow, acid yellow 11, Citronin A, food indigo plant 1, indigo, lemon yellow pigment, light green pigment, 85% lemon yellow;
Described natural pigment is that β-phylloerythrin, carmine, CHLOROPHYLLINE potassium sodium copper, class carotene, anthraquinone pigment, Folium Perillae are red, one or more the formed mixture in the cashaw pigment, curcumin;
Described oil-solvent preservative is that trichlorine is to the oil-solvent preservative of hexichol, bronocot, hexachlorophene, dehydroacetic acid or dehydroacetic acid sodium salt, o-phenyl phenol, Buddhist nun's platinum lipid or the serial class of triumphant pine;
The oil-solvent preservative of wherein said Buddhist nun's platinum lipid is one or more formed mixture of methyl hydroxybenzoate, ethyl hydroxybenzoate, propylparaben, nipalgin isopropyl ester, nipalgin isobutyl ester, the different methyl ester of nipalgin;
The oil-solvent preservative of the serial class of described triumphant pine is one or more the formed mixture in methyl-chloro-isothiazolone, methyl-isothiazolone, the biphenyl isothiazolone.
2. a kind of double-deck makeup removing liquid as claimed in claim 1 is characterized in that counting by weight percentage, and its raw material composition and content are as follows:
Wetting agent 1%
Water-soluble grease 5%
Inorganic salt electrolyte 0.1%
Waterborne-type preservation 0.1%
Water-insoluble oils and fats 45.9%
Oil-soluble pigment 0.00001%
Oil-solvent preservative 0.1%
Surplus is water;
Described wetting agent is 1,2 propylene glycol;
Described water-soluble grease is the water solublity castor oil hydrogenated;
Described inorganic salt electrolyte is sodium chloride;
Described waterborne-type preservation is two imidazolidinyl urea;
Described water-insoluble oils and fats is 10# low viscosity white oil;
Described oil-solvent preservative is Buddhist nun's platinum propyl ester;
Described oil-soluble pigment is indigo.
3. a kind of double-deck makeup removing liquid as claimed in claim 1 is characterized in that counting by weight percentage, and its raw material composition and content are as follows:
Wetting agent 10%
Water-soluble grease 15%
Inorganic salt electrolyte 10%
Waterborne-type preservation 0.5%
Water-insoluble oils and fats 44.49%
Oil-soluble pigment 0.01%
Oil-solvent preservative 0.5%
Surplus is water;
Described wetting agent is 1,3 butanediol;
Described water-soluble grease is Polyethylene Glycol (12) polydimethylsiloxane;
Described inorganic salt electrolyte is magnesium sulfate;
Described waterborne-type preservation is 1,3-dihydroxy 5, the mixture that 5-dimethyl hydantoin and 3-iodo-2-propynyl butyl carbamate are formed;
Described water-insoluble oils and fats is sad capric acid triglyceride;
Described oil-solvent preservative is Buddhist nun's platinum butyl ester;
Described oil-soluble pigment is indigo.
4. a kind of double-deck makeup removing liquid as claimed in claim 1 is characterized in that counting by weight percentage, and its raw material composition and content are as follows:
Wetting agent 5%
Water-soluble grease 10%
Inorganic salt electrolyte 5%
Waterborne-type preservation 0.2%
Water-insoluble oils and fats 49.60%
Oil-soluble pigment 0.0001%
Oil-solvent preservative 0.2%
Surplus is water;
Described wetting agent glycerol;
Described water-soluble grease is Jojoba oil;
Described inorganic salt electrolyte is potassium chloride;
Described waterborne-type preservation is two imidazolidinyl urea;
Described water-insoluble oils and fats is isopropyl palmitate;
Described oil-solvent preservative is Buddhist nun's platinum propyl ester;
Described oil-soluble pigment is indigo.
5. a kind of double-deck makeup removing liquid as claimed in claim 1 is characterized in that counting by weight percentage, and its raw material composition and content are as follows:
Wetting agent 8%
Water-soluble grease 8%
Inorganic salt electrolyte 0.3%
Waterborne-type preservation 0.15%
Water-insoluble oils and fats 41.7%
Oil-soluble pigment 0.00002%
Oil-solvent preservative 0.15%
Surplus is water;
Described wetting agent is 1,2 propylene glycol;
Described water-soluble grease is Polyethylene Glycol (16) macadimia nut glyceride;
Described inorganic salt electrolyte is potassium chloride;
Described waterborne-type preservation is sodium hydroxy methyl glycinate;
Described water-insoluble oils and fats is olive oil;
Described oil-solvent preservative is Buddhist nun's platinum isopropyl ester;
Described oil-soluble pigment is lemon yellow pigment.
6. a kind of double-deck makeup removing liquid as claimed in claim 1 is characterized in that counting by weight percentage, and its raw material composition and content are as follows:
Wetting agent 6%
Water-soluble grease 12%
Inorganic salt electrolyte 2%
Waterborne-type preservation 0.2%
Water-insoluble oils and fats 39.8%
Oil-soluble pigment 0.01%
Oil-solvent preservative 0.2%
Surplus is water;
Described wetting agent is 1,3 butanediol;
Described water-soluble grease is Polyethylene Glycol (7) Oleum Cocois glyceride;
Described inorganic salt electrolyte is magnesium sulfate;
Described waterborne-type preservation is imidazolidinyl urea;
Described water-insoluble oils and fats is palm-kernel oil;
Described oil-solvent preservative is bronocot;
Described oil-soluble pigment is light green pigment.
7. a kind of double-deck makeup removing liquid as claimed in claim 1 is characterized in that counting by weight percentage, and its raw material composition and content are as follows:
Wetting agent 3%
Water-soluble grease 6%
Inorganic salt electrolyte 3%
Waterborne-type preservation 0.3%
Water-insoluble oils and fats 43.7%
Oil-soluble pigment 0.0001%
Oil-solvent preservative 0.3%
Surplus is water
Described wetting agent glycerol;
Described water-soluble grease dimethiconol;
Described inorganic salt electrolyte is potassium chloride;
Described waterborne-type preservation is the mixture that two imidazolidinyl urea and iodo propinyl butyl methylamine acid esters are formed;
Described water-insoluble oils and fats is Oleum Ricini;
Described oil-solvent preservative is the mixture that nipalgin isopropyl ester, nipalgin isobutyl ester are formed;
Described oil-soluble pigment is 85% lemon yellow.
8. as the preparation method of the arbitrary described a kind of double-deck makeup removing liquid of claim 1 to 7, it is characterized in that specifically comprising the steps:
(1), respectively waterborne-type preservation, water-soluble grease, inorganic salt electrolyte, wetting agent are added to the water successively, stirring obtains the aqueous layer component;
(2), oil-solvent preservative, oil-soluble pigment are added in the water-insoluble oils and fats successively, stirring obtains the oil phase layer component;
(3), the aqueous layer component of step (1) gained is mixed with the oil phase layer component of step (2) gained namely get double-deck makeup removing liquid again.
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| CN103505381A (en) * | 2013-09-17 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Double-layer makeup removal emulsion and preparation method thereof |
| CN103908422A (en) * | 2014-03-26 | 2014-07-09 | 张金杰 | Mild and harmless cleansing water |
| CN104288027A (en) * | 2014-09-26 | 2015-01-21 | 天津天狮生物发展有限公司 | Eye and lip cleansing lotion and preparation method thereof |
| CN105581948A (en) * | 2016-03-05 | 2016-05-18 | 广州丹奇日用化工厂有限公司 | Skin surface lipid film repair type makeup removal paste and preparation method thereof |
| CN105596237A (en) * | 2016-01-20 | 2016-05-25 | 广州丹奇日用化工厂有限公司 | Skin surface lipid repair type makeup removing cream and preparation method thereof |
| CN105687039A (en) * | 2016-03-05 | 2016-06-22 | 广州丹奇日用化工厂有限公司 | Lavender makeup removing paste and preparation method thereof |
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| CN103505381A (en) * | 2013-09-17 | 2014-01-15 | 广州环亚化妆品科技有限公司 | Double-layer makeup removal emulsion and preparation method thereof |
| CN103908422A (en) * | 2014-03-26 | 2014-07-09 | 张金杰 | Mild and harmless cleansing water |
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